04-08-2023 дата публикации
Номер: CN116536532A
Принадлежит:
According to the system and method for preparing the metal germanium, hydrogen is adopted for directly reducing germanium tetrachloride to prepare the metal germanium, a corresponding tail gas comprehensive recovery and treatment system is matched, raw material recycling is achieved, the reaction is closed, new impurity elements are not introduced, and the product quality can be guaranteed. Meanwhile, internal circulation of elements is achieved, especially after the chlorine element and germanium tetrachloride are reduced, the chlorine element forms hydrogen chloride, the hydrogen chloride gas forms hydrochloric acid after being recycled, the hydrochloric acid is subjected to chlorination distillation, germanium tetrachloride is obtained, the problem of waste acid treatment in actual production is solved, and good economic and environment-friendly benefits are achieved. The method has the advantages of being short in technological process, high in raw material utilization rate, almost ...
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