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Небесная энциклопедия

Космические корабли и станции, автоматические КА и методы их проектирования, бортовые комплексы управления, системы и средства жизнеобеспечения, особенности технологии производства ракетно-космических систем

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Мониторинг СМИ

Мониторинг СМИ и социальных сетей. Сканирование интернета, новостных сайтов, специализированных контентных площадок на базе мессенджеров. Гибкие настройки фильтров и первоначальных источников.

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Форма поиска

Поддерживает ввод нескольких поисковых фраз (по одной на строку). При поиске обеспечивает поддержку морфологии русского и английского языка
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Применить Всего найдено 20837. Отображено 100.
12-01-2012 дата публикации

Effect pigments based on coated glass flakes

Номер: US20120010300A1
Принадлежит: Individual

The present invention relates to effect pigments based on thin glass flakes and to a method for the production of such pigments. The resulting pigment can be used in any application for which pearlescent pigments have been heretofore used such as, for example, in plastics, paints, inks, cosmetic formulations, coatings including solvent or waterborne automotive paint systems, powder coatings, inks and agriculture foils.

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26-01-2012 дата публикации

Nickel hydroxide electrode for rechargeable batteries

Номер: US20120018670A1
Принадлежит: PowerGenix Systems Inc

The nickel hydroxide particles for a nickel hydroxide electrode may be treated using an alkaline solution of a strong oxidizing agent such as sodium or potassium persulfate to modify the surface nickel hydroxide structure. The resulting modified surface structure has been found to impart various benefits to electrodes formed from the nickel hydroxide. It is believed that the oxidation of cobalt compounds at the surface of the nickel hydroxide particles results in a highly conductive cobalt compound that plays an important role in the high reliability, high stability and high capacity utilization of nickel electrodes as described herein.

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24-05-2012 дата публикации

Black composite particle, black resin composition, color filter substrate and liquid crystal display

Номер: US20120128898A1
Принадлежит: TORAY INDUSTRIES INC

Disclosed are black composite particles having a high light-shielding performance suitable as a black component such as a black matrix in a color filter. Further disclosed is a black resin composition from which a black matrix having a high light-shielding performance can be formed. The black composite particles are represented by the composition formula: TiNxOy.zX (wherein X is a metal atom such as silver; x is a number greater than 0 and less than 2; y is a number not less than 0 and less than 2; and z is a number greater than 0 and less than 10). The black resin composition comprises at least a light shielding agent, a resin, and a solvent and comprises the black composite particles as the light shielding agent.

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31-05-2012 дата публикации

Dispersion Liquid of Core-Shell Type Composite Oxide Fine Particles, Process for Producing the Dispersion Liquid, and Coating Composition Containing the Fine Particles

Номер: US20120132108A1
Принадлежит: JGC Catalysts and Chemicals Ltd

Core-shell type composite oxide fine particles are described in which the core particles are oxide fine particles or composite oxide fine particles that do not contain silicon and/or aluminum as main components, and the surface of the core particles is covered with a shell including a composite oxide that contains silicon and aluminum as main components, the shell containing silicon and aluminum in a weight ratio in terms of oxides, SiO 2 /Al 2 O 3 , in the range of 2.0 to 30.0. A dispersion liquid of the core-shell type composite oxide fine particles exhibits very high stability.

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12-07-2012 дата публикации

Cathode material for fuel cell, cathode for fuel cell including the same, method of manufacturing the cathode, and solid oxide fuel cell including the cathode

Номер: US20120178016A1

A cathode material for a fuel cell, the cathode material for a fuel cell including a lanthanide metal oxide having a perovskite crystal structure; and a bismuth metal oxide represented by Chemical Formula 1 below, Bi 2-x-y A x B y O 3 ,  Chemical Formula 1 wherein A and B are each a metal with a valence of 3, A and B are each independently at least one element selected from a rare earth element and a transition metal element, A and B are different from each other, and 0<x≦0.3 and 0<y≦0.3.

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01-11-2012 дата публикации

Titanium Oxide Spacing by SIP

Номер: US20120277346A1
Принадлежит: Behr Process Corp

A method of making a titanium oxide-containing coating composition comprises attaching an initiator to a pretreated titanium oxide to form an initiator/pretreated titanium oxide complex. The pretreated titanium oxide includes a plurality of pretreated titanium oxide particles which are titanium oxide particles that are pretreated with at least one metal oxide. The initiator/pretreated titanium oxide complex is contacted with a polymerizable unsaturated monomer such that a polymeric encapsulate forms on the initiator/pretreated titanium oxide particles to form polymeric encapsulated titanium oxide particles.

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08-11-2012 дата публикации

Spray Pyrolysis Synthesis of Mesoporous Positive Electrode Materials for High Energy Lithium-Ion Batteries

Номер: US20120282522A1
Принадлежит: Washington University in St Louis WUSTL

A lithium metal oxide positive electrode material useful in making lithium-ion batteries that is produced using spray pyrolysis. The material comprises a plurality of metal oxide secondary particles that comprise metal oxide primary particles, wherein the primary particles have a size that is in the range of about 1 nm to about 10 μm, and the secondary particles have a size that is in the range of about 10 nm to about 100 μm and are uniformly mesoporous.

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08-11-2012 дата публикации

Production process for composite oxide, positive-electrode active material for lithium-ion secondary battery and lithium-ion secondary battery

Номер: US20120282526A1
Принадлежит: Toyota Industries Corp

A composite oxide, whose major component is a lithium-manganese-system oxide including Li and tetravalent Mn at least and having a crystal structure that belongs to a layered rock-salt structure, is produced via the following: a raw-material mixture preparation step of preparing a raw-material mixture by mixing a metallic-compound raw material and a molten-salt raw material with each other, the metallic-compound raw material at least including one or more kinds of metallic compounds being selected from the group consisting of oxides, hydroxides and metallic salts that include one or more kinds of metallic elements in which Mn is essential, the molten-salt raw material including lithium hydroxide and lithium nitrate, and exhibiting a proportion of the lithium hydroxide with respect to the lithium nitrate (i.e., (Lithium Hydroxide)/(Lithium Nitrate)) that falls in a range of from 1 or more to 10 or less by molar ratio; a molten reaction step of reacting said raw-material mixture at a melting point of said molten-salt raw material or more by melting it: and a recovery step of recovering said composite oxide being generated from said raw-material mixture that has undergone the reaction.

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10-01-2013 дата публикации

Multiple inorganic compound structure and use thereof, and method of producing multiple inorganic compound structure

Номер: US20130011729A1
Автор: Shogo Esaki, Takeshi Yao
Принадлежит: Individual

In a multiple inorganic compound structure according to the present invention, elements included in a main crystalline phase and elements included in a sub inorganic compound are present in at least a first region and a second region, the first region and the second region each have an area of nano square meter order, the first region is adjacent to the second region, and the first region and the second region each include an element of an identical kind, which element of the identical kind present in the first region has a concentration different from that of the element of the identical kind present in the second region.

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17-01-2013 дата публикации

Positive electrode active material

Номер: US20130015410A1
Принадлежит: Hitachi Chemical Co Ltd, HITACHI LTD

A lithium ion secondary battery has a high cycle retention rate, and has its battery capacity increased. A positive electrode active material is used which includes a crystal phase having a structure formed by collecting a plurality of crystallites 101 , and powder particles containing amorphous phases 103 a and 103 b formed between the crystallites 101 . The amorphous phases 103 a and 103 b contain one or more kinds of metal oxides selected from the group consisting of vanadium oxide, iron oxide, manganese oxide, nickel oxide and cobalt oxide. The crystal phase and the amorphous phase 103 a and 103 b are capable of intercalation and deintercalation of lithium ions.

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04-04-2013 дата публикации

Microspheres and photoprotective personal care composition comprising same

Номер: US20130084318A1
Принадлежит: Conopco Inc

The invention relates to photoprotective cosmetic compositions comprising microspheres and a process to prepare them. In particular, the invention is especially effective in protecting the skin against visible solar radiation while ensuring a highly acceptable even skin tone and appearance. The present inventors have developed a microsphere with hollow interior and shell of a material having a specific optical property and specific thickness and coated with another material having a different specific optical property, a combination of which gives the microsphere surprising benefits both in terms of protection from the harmful sun rays while giving a pleasing skin appearance when these microspheres are incorporated in topical compositions.

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25-04-2013 дата публикации

Semiconductor nanocrystal-polymer composite, method of preparing the same, and composite film and optoelectronic device including the same

Номер: US20130099213A1
Принадлежит: SAMSUNG ELECTRONICS CO LTD

A semiconductor nanocrystal-polymer composite including a semiconductor nanocrystal, a polymer comprising a plurality of carboxylate anion groups (—COO − ) bindable to a surface of the semiconductor nanocrystal, and a metal cation bindable to a carboxylate anion group of the plurality of carboxylate anion groups.

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25-04-2013 дата публикации

Doped Nanoparticles and Methods of Making and Using Same

Номер: US20130101848A1

Doped nanoparticles, methods of making such nanoparticles, and uses of such nanoparticles. The nanoparticles exhibit a metal-insulator phase transition at a temperature of −200° C. to 350° C. The nanoparticles have a broad range of sizes and various morphologies. The nanoparticles can be used in coatings and in device structures.

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06-06-2013 дата публикации

Positive electrode materials for lithium ion batteries having a high specific discharge capacity and processes for the synthesis of these materials

Номер: US20130142944A1
Принадлежит: Envia Systems Inc

Positive electrode active materials are described that have a very high specific discharge capacity upon cycling at room temperature and at a moderate discharge rate. Some materials of interest have the formula Li 1+x Ni 60 Mn β Co γ O 2 , where x ranges from about 0.05 to about 0.25, α ranges from about 0.1 to about 0.4, β range's from about 0.4 to about 0.65, and γ ranges from about 0.05 to about 0.3. The materials can be coated with a metal fluoride to improve the performance of the materials especially upon cycling. Also, the coated materials can exhibit a very significant decrease in the irreversible capacity lose upon the first charge and discharge of the cell. Methods for producing these materials include, for example, a co-precipitation approach involving metal hydroxides and sol-gel approaches.

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11-07-2013 дата публикации

Cathode active material and lithium secondary battery comprising the same

Номер: US20130177816A1
Принадлежит: LG Chem Ltd

Disclosed is a cathode active material for secondary batteries comprising one or more compounds having a layered-crystal structure, represented by the following Formula 1, wherein a transition metal layer contains Li, in an amount lower than 20%, based on a total amount of a transition metal site, and a ratio of Ni positioned in a lithium layer, that is, a cation mixing ratio is 1% to 4.5%, based on a total amount of a lithium site in the lithium layer to stably support the layered-crystal structure: (1-s-t)[Li(Li a Mn (1-a-x-y) Ni x Co y )O 2 ]*s [Li 2 CO 3 ]*t[LiOH] (1), wherein 0<a<0.2; 0<x<0.9; 0<y<0.5; a+x+y<1; 0<s<0.03; and 0<t<0.03. The cathode active material exhibits long lifespan and superior stability at room temperature and high temperatures in spite of repeated charge and discharge at a high current.

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01-08-2013 дата публикации

Refractory metal ceramics and methods of making thereof

Номер: US20130196132A1
Принадлежит: US Department of Navy

A composition having nanoparticles of a refractory-metal carbide or refractory-metal nitride and a carbonaceous matrix. The composition is not in the form of a powder. A composition comprising a metal component and an organic component. The metal component is nanoparticles or particles of a refractory metal or a refractory-metal compound capable of decomposing into refractory metal nanoparticles. The organic component is an organic compound having a char yield of at least 60% by weight or a thermoset made from the organic compound. A method of combining particles of a refractory metal or a refractory-metal compound capable of reacting or decomposing into refractory-metal nanoparticles with an organic compound having a char yield of at least 60% by weight to form a precursor mixture.

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08-08-2013 дата публикации

Hybrid particles and associated methods

Номер: US20130200313A1
Принадлежит: Battelle Energy Alliance Llc

Hybrid particles that comprise a coating surrounding a chalcopyrite material, the coating comprising a metal, a semiconductive material, or a polymer; a core comprising a chalcopyrite material and a shell comprising a functionalized chalcopyrite material, the shell enveloping the core; or a reaction product of a chalcopyrite material and at least one of a reagent, heat, and radiation. Methods of forming the hybrid particles are also disclosed.

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15-08-2013 дата публикации

Particles, process for production thereof and use thereof

Номер: US20130209840A1
Принадлежит: BASF SE

Particles comprising a mixed oxide of the general formula (I) Li 1+a Ni b Co c Mn d O z   (I) in which the variables are each defined as follows: b is a number in the range from 0.25 to 0.45 c is a number in the range from 0.15 to 0.25 d =1− b−c, (1+a) is in the range from 1.05 to 1.20, 1.8+ a≦z ≦2.2+ a, the particles having been fully or partially coated with one or more fluorides; and also a process for producing inventive particles and use of inventive particles.

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22-08-2013 дата публикации

Layer-layer lithium rich complex metal oxides with high specific capacity and excellent cycling

Номер: US20130216900A1
Принадлежит: Envia Systems Inc

Lithium rich and manganese rich lithium metal oxides are described that provide for excellent performance in lithium-based batteries. The specific compositions can be engineered within a specified range of compositions to provide desired performance characteristics. Selected compositions can provide high values of specific capacity with a reasonably high average voltage. Compositions of particular interest can be represented by the formula, x Li 2 MnO 3 .(1−x) Li Ni u+Δ Mn u−Δ Co w A y O 2 . The compositions undergo significant first cycle irreversible changes, but the compositions cycle stably after the first cycle.

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29-08-2013 дата публикации

Lithium secondary battery positive electrode material for improving output characteristics and lithium secondary battery including the same

Номер: US20130221283A1
Принадлежит: LG Chem Ltd

Provided are a positive electrode active material for improving an output and a lithium secondary battery including the same. Particularly, graphite and conductive carbon which have shapes and sizes different from each other, may be simultaneously coated on a mixed positive electrode material of a 3-component system lithium-containing metal oxide having a layered structure and expressed as following Chemical Formula 1 and LiFePO 4 having an olivine structure as an conductive material to improve high resistance occurrence and conductivity reduction phenomenon of a 3-component system lithium metal oxide due to a difference between particle sizes and surface areas of the 3-component system lithium-containing metal oxide and LiFePO 4 olivine. Li 1+a Ni x Co y Mn 1-x-y O 2 , 0≦a<0.5, 0<x<1, 0<y<0.5   [Chemical formula 1]

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05-09-2013 дата публикации

Active material for nonaqueous electrolyte secondary battery, method for production of the active material, electrode for nonaqueous electrolyte secondary battery and nonaqueous electrolyte secondary battery

Номер: US20130230775A1
Автор: Daisuke Endo
Принадлежит: GS YUASA INTERNATIONAL LTD

There is provided an active material for a nonaqueous electrolyte secondary battery, including a lithium-transition metal composite oxide which has an α-NaFeO 2 -type crystal structure and of which the average composition is represented by the composition formula of Li 1+α Me 1−α O 2 (Me is a transition metal containing Co, Ni and Mn; and α> 0 ), wherein the lithium-transition metal composite oxide is a particle having a core and a coated part, the cobalt concentration of the coated part is higher than the cobalt concentration of the core, the manganese concentration of the coated part is lower than the manganese concentration of the core, and the ratio of cobalt present in the coated part is 3 to 10% in terms of a molar ratio based on the amount of the transition metal present in the core.

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19-09-2013 дата публикации

Lithium titanate particles and process for producing the lithium titante particles, MG-Containing lithium titanate particles and process for producing the MG-Containing lithium particles, negative electrode active substance particles for non-aqueous electrolyte secondary batteries, and non-aqeous electrolyte secondary battery

Номер: US20130244114A1
Принадлежит: Toda Kogyo Corp

According to the present invention, there are provided lithium titanate particles which exhibit an excellent initial discharge capacity and an enhanced high-efficiency discharge capacity retention rate as an active substance for non-aqueous electrolyte secondary batteries and a process for producing the lithium titanate particles, and Mg-containing lithium titanate particles. The present invention relates to lithium titanate particles with a spinel structure comprising TiO 2 in an amount of not more than 1.5%, Li 2 TiO 3 in an amount of not less than 1% and not more than 6%, and Li 4 Ti 5 O 12 in an amount of not less than 94% and not more than 99% as determined according to Rietveld analysis when indexed with Fd-3m by XRD, and having a specific surface area of 7 to 15 m 2 /g as measured by BET method, a process for producing lithium titanate particles comprising the steps of adding and mixing a water-soluble lithium solution into a water suspension of an oxide of titanium having a BET specific surface area of 40 to 400 m 2 /g and a primary particle diameter of 5 to 50 nm and subjecting the resulting mixed suspension to aging reaction at a temperature of 50 to 100° C.; subjecting the resulting reaction product to filtration, drying and pulverization; and subjecting the obtained dry particles to heat-calcination treatment at a temperature of 550 to 800° C., and Mg-containing lithium titanate particles having a composition represented by the formula: Li x Mg y Ti z O 4 wherein x, z>0; 0.01≦y≦0.20; 0.01≦y/z≦0.10; and 0.5≦(x+y)/z≦1.0, the Mg-containing lithium titanate particles having a BET specific surface area of 5 to 50 m 2 /g, a spinel single phase as a crystal structure, and a lattice constant (a) represented by a value of 0.050y+8.3595<a≦0.080y+8.3595 (Å).

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20-02-2014 дата публикации

Positive active material for rechargeable lithium battery, method for preparing same and rechargeable lithium battery including same

Номер: US20140050993A1
Автор: Jung-Joon Park
Принадлежит: Samsung SDI Co Ltd

A positive active material including a compound represented by Li 1+x M 1−k Me k O 2 . A surface part of a particle of the positive active material has a mole ratio [Me/M] (A) of element represented by Me to element represented by M in Li 1+x M 1−k Me k O 2 of 0.05≦A≦0.60; the entire particle has a mole ratio [Me/M] (B) of element represented by Me to element represented by M in Li 1+x M 1−k Me k O 2 of 0.003≦B≦0.012; and element represented by Me has a concentration difference of between two positions of less than or equal to about 0.02 wt % in an inner part of the particle. In Li 1+x M 1−k Me k O 2 , −0.2≦x≦0.2, 0<k≦0.05 M is one selected from Ni, Mn, Co, and a combination thereof, Me is one selected from Al, Mg, Ti, Zr, B, Ni, Mn, and a combination thereof, and M is not the same element as Me or does not include the same element as Me.

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27-02-2014 дата публикации

Composite anode active material, method of preparing the same, and lithium battery including the composite anode active material

Номер: US20140057172A1
Принадлежит: Samsung SDI Co Ltd

In an aspect, a composite anode active material including lithium titanium oxide particles; and a TiN, and TiN a method of preparing the composite anode active material, and a lithium battery including the composite anode active material is provided.

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02-01-2020 дата публикации

CERAMIC PARTICLE CARRYING MEDICAL TUBE AND/OR CUFF

Номер: US20200000684A1
Принадлежит:

It is an object of the present invention to provide a ceramic particle carrying medical tube and/or cuff excellent in cell adhesive property and the like. 1. A medical tube and/or cuff carrying a ceramic particle in at least a part thereof , whereinthe ceramic particle has a particle diameter within a range of 10 nm to 700 nm,the ceramic particle is a calcium phosphate sintered body particle, andthe ceramic particle contains no calcium carbonate.2. The medical tube and/or cuff according to claim 1 , wherein the ceramic particle is spherical.3. A medical tube and/or cuff carrying a ceramic particle in at least a part thereof claim 1 , whereinthe ceramic particle has a minor axis maximum diameter of 30 nm to 5 μm and a major axis of 75 nm to 10 μm, grows in a c axis direction, and has an aspect ratio of a crystal (c axis length/a axis length) of 1 to 30,the ceramic particle is a calcium phosphate sintered body particle, andthe ceramic particle contains no calcium carbonate.4. The medical tube and/or cuff according to claim 1 , wherein the ceramic particle is a hydroxyapatite sintered body particle.5. The medical tube and/or cuff according to claim 1 , wherein the ceramic particle contains no alkali metal elements.6. The medical tube and/or cuff according to claim 1 , wherein the ceramic particle contains carbonate apatite at least on a surface thereof.7. The medical tube and/or cuff according to claim 1 , wherein the ceramic particle satisfies the following property (A): (A) the medical tube and/or cuff shows a reduction in weight of 2% or less in a temperature range of 25° C. to 200° C. when sufficiently dried claim 1 , left to stand for 3 days or more under conditions of normal pressure claim 1 , a temperature of 25° C. claim 1 , and a humidity of 50% claim 1 , and then measured for the weight under conditions of a nitrogen stream and 10° C./min by using a thermogravimetric differential thermal analyzer (TG-DTA claim 1 , EXSTAR6000 manufactured by Seiko Instruments ...

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07-01-2021 дата публикации

Metal Oxide Nanoparticle-Based T1-T2 Dual-Mode Magnetic Resonance Imaging Contrast Agent

Номер: US20210000983A1
Принадлежит: INTRON BIOTECHNOLOGY, INC.

The present invention relates to a magnetic resonance imaging (MRI) contrast agent, particularly a metal oxide nanoparticle-based T1-T2 dual-mode MRI contrast agent that can be used not only as a T1 MRI contrast agent but also as a T2 MRI contrast agent, and a method for producing the same. The metal oxide nanoparticle-based T1-T2 dual-mode MRI contrast agent can provide more accurate and detailed information associated with disease than single MRI contrast agent by the beneficial contrast effects in both T1 imaging with high tissue resolution and T2 imaging with high feasibility on detection of a lesion. 1. (canceled)2. (canceled)3. (canceled)4. (canceled)5. (canceled)6. (canceled)7. (canceled)8. (canceled)9. (canceled)10. (canceled)11. (canceled)12. (canceled)13. (canceled)14. (canceled)15. (canceled)16. (canceled)17. (canceled)18. (canceled)19. (canceled)20. (canceled)21. (canceled)22. (canceled)23. (canceled)24. (canceled)25. A method for producing a T1-T2 dual-mode MRI contrast agent derived from nanoparticles that have a core of manganese oxide and a porous shell of manganese ion-doped iron oxide on the core , comprising the following steps:A) synthesizing manganese oxide nanoparticles under inert gas environment;B) forming an epitaxial layer of iron oxide on the surface of manganese oxide nanoparticles under inert gas environment;C) maintaining the formation of the layer of porous manganese ion-doped iron oxide under dry air environment to form multilayer nanoparticles having a porous shell adjacent to core structure; andD) coating multilayer nanoparticles with a biocompatible polymer.26. The method for producing a T1-T2 dual-mode MRI contrast agent according to claim 25 , wherein the manganese oxide nanoparticles are synthesized with at least one shape selected from the group consisting of octahedral and cross shapes.27. The method for producing a T1-T2 dual-mode MRI contrast agent according to claim 25 , wherein the biocompatible polymer is at least one ...

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07-01-2016 дата публикации

Flame Retardant Composite Particles

Номер: US20160002538A1
Принадлежит: Shayonano Singapore Pte Ltd.

The present invention relates to a method of producing a composite particle having a metal oxide core and a metal hydroxide outer shell, said method comprising the steps of: (a) thermally treating a metal hydroxide under conditions to produce a pure phase crystalline metal oxide; (b) hydrating said pure phase crystalline metal oxide to form said composite particle. (c) hydrating said pure phase crystalline metal oxide under conditions to form a metal oxide inner core and a metal hydroxide outer shell. 18-. (canceled)9. A method of producing a composite particle having a metal oxide inner core encapsulated by a metal hydroxide outer shell comprising the steps of:(a) irradiating a metal hydroxide particle under conditions to increase the porosity of said metal hydroxide particle to yield a porous metal hydroxide;(b) thermally treating said porous metal hydroxide particle under conditions to yield a pure phase crystalline metal oxide;(c) hydrating said pure phase crystalline metal oxide under conditions to form a metal oxide inner core and a metal hydroxide outer shell.10. The method of claim 9 , wherein said step of irradiating comprises use of microwaves of frequencies of 300 MHz to 300 GHz.11. The method of claim 9 , wherein said thermal treatment step (b) comprises thermal annealing.12. The method of claim 11 , wherein said annealing step comprises subjecting said metal hydroxide particle to a temperature selected from 200° C. to 800° C.13. The method of claim 12 , wherein said annealing step is performed under atmospheric pressure.14. The method of claim 13 , wherein the annealing step is undertaken for a duration selected from 1 hour to 16 hours.15. The method of claim 9 , wherein said metal hydroxide particle is formed of a metal selected from the group consisting of: Al claim 9 , Be claim 9 , Mg claim 9 , Ca claim 9 , Sr claim 9 , Ba claim 9 , Ra claim 9 , Sc claim 9 , Ti claim 9 , V claim 9 , Cr claim 9 , Mn claim 9 , Fe claim 9 , Co claim 9 , Ni claim 9 , Cu ...

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05-01-2017 дата публикации

Tellurium compound nanoparticles, composite nanoparticles, and production methods therefor

Номер: US20170002265A1
Принадлежит: Nagoya University NUC, Nichia Corp

Tellurium compound nanoparticles, including: an element M 1 where M 1 is at least one element selected from Cu, Ag, and Au; an element M 2 where M 2 is at least one element selected from B, Al, Ga, and In; Te; and optionally an element M 3 where M 3 is at least one element selected from Zn, Cd, and Hg; wherein a crystal structure of the tellurium compound nanoparticles is a hexagonal system, the tellurium compound nanoparticles are of a rod shape and have an average short-axis length of 5.5 nm or less, and when irradiated with light at a wavelength in a range of 350 nm to 1,000 nm, the tellurium compound nanoparticles emit photoluminescence having a wavelength longer than the wavelength of the irradiation light.

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02-01-2020 дата публикации

Heat storage particle, composition for thermostatic device, and thermostatic device

Номер: US20200002590A1
Принадлежит: Murata Manufacturing Co Ltd

A heat storage particle that includes a ceramic particle containing a vanadium oxide as a main component thereof, and a metal film covering the ceramic particle.

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01-01-2015 дата публикации

Rare earth metal compounds, methods of making, and methods of using the same

Номер: US20150004086A1
Принадлежит: Spectrum Pharmaceuticals Inc

Rare earth metal compounds, particularly lanthanum, cerium, and yttrium, are formed as porous particles and are effective in binding metals, metal ions, and phosphate. A method of making the particles and a method of using the particles is disclosed. The particles may be used in the gastrointestinal tract or the bloodstream to remove phosphate or to treat hyperphosphatemia in mammals. The particles may also be used to remove metals from fluids such as water.

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04-01-2018 дата публикации

Cathode material of lithium cobalt oxide for a lithium ion secondary battery and preparation methods and applications thereof

Номер: US20180006302A1

The invention relates to a cathode material of lithium cobalt oxide for a lithium ion secondary battery and preparation methods and applications thereof. A cathode material comprises a core material and a coating layer, wherein the core material is Li x Co (1−y) A y O (2+z) , wherein 1.0≦x≦1.11, 0≦y≦0.02, −0.2<z<0.2, and A is one or two or more selected from the group consisting of Al, Mg, Y, Zr and Ti, wherein the coating layer is Li a M b B c O d , wherein M is a lithium ion active metal element and one or two or more selected from the group consisting of Co, Ni, Mn and Mo, and B is an inactive element, and one or two or more selected from the group consisting of Al, Mg, Ti, Zr and Y, and 0.95<b+c<2.5, and the molar ratio of Li to the active metal element M is 0<a/b<1. The battery prepared by the cathode material has advantages of high capacity, high compacted density and excellent cycling stability etc., under high voltage.

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07-01-2021 дата публикации

Method for Preparing Positive Electrode Active Material for Secondary Battery

Номер: US20210005878A1
Принадлежит: LG Chem Ltd

A method for preparing a positive electrode active material for a secondary battery includes the steps of: providing a positive electrode active material precursor including a core portion and a shell portion, wherein the core portion contains nickel (Ni), cobalt (Co), and manganese (Mn), and the shell portion contains cobalt (Co) and surrounds the core portion; and forming a lithium composite transition metal oxide in a single particle form by mixing the positive electrode active material precursor with a lithium raw material to obtain a mixture, and firing the mixture at a temperature of 970° C. or more.

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09-01-2020 дата публикации

IMPLANT COMPRISING A CALCIUM SALT-CONTAINING COMPOSITE POWDER HAVING MICROSTRUCTURED PARTICLES

Номер: US20200009297A1
Принадлежит:

Implant comprising composite powder with microstructured particles, obtained by a process in which large particles are bonded to small particles, wherein 2. The method according to claim 1 , characterized in that the particles of the composite powder have a particle size dof less than 350 μm.3. The method according to claim 1 , characterized in that the particles of the composite powder have an average particle size dwithin the range from 20 μm to less than 150 μm.4. The method according to claim 1 , characterized in that the particles of the composite powder have a d/dratio of less than 100% and/or that the calcium salt has an aspect ratio of less than 5 and/or that the calcium salt comprises spherical calcium carbonate and/or that the calcium salt comprises calcium phosphate.5. The method according to claim 1 , characterized in that the large particles comprise at least one thermoplastic polymer.6. The method according to claim 1 , characterized in that the large particles comprise at least one absorbable polymer.7. The method according to claim 6 , characterized in that the absorbable polymer has an inherent viscosity claim 6 , measured in chloroform at 25° C. claim 6 , 0.1% polymer concentration claim 6 , within the range from 0.3 dl/g to 8.0 dl/g.8. The method implant according to claim 1 , characterized in that the large particles comprise poly-D claim 1 , poly-L and/or poly-D claim 1 ,L-lactic acid.9. The method according to claim 1 , characterized in that the large particles comprise at least one absorbable polyester having a number average molecular weight in the range from 500 g/mol to 1 claim 1 ,000 claim 1 ,000 g/mol.10. The method according to claim 1 , characterized in that the large particles comprise at least one polyamide.11. The method according to claim 1 , characterized in that the large particles comprise at least one polyurethane.12. The method according to claim 1 , characterized in that the percentage by weight of the calcium salt particle ...

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09-01-2020 дата публикации

METHOD FOR PRODUCING LANTHANUM HEXABORIDE-CONTAINING COMPOSITE PARTICLES AND METHOD FOR PRODUCING FORMED PRODUCT

Номер: US20200010684A1
Принадлежит: AGC Inc.

To provide a method for producing lanthanum hexaboride-containing composite particles which are capable of forming a formed product having sufficiently high transparency and which are excellent in weather resistance, by a simple operation without calcination treatment at high temperature, and a method for producing a formed product using it. 1. A method for producing lanthanum hexaboride-containing composite particles , which comprises:reacting at least one silica precursor selected from the group consisting of a tetraalkoxysilane, its hydrolysate and its condensate, in the presence of lanthanum hexaboride particles, a base having a boiling point of at most 200° C., water and an organic solvent to obtain a first reaction mixture, andreacting the first reaction mixture with at least one silicon compound selected from the group consisting of an amino-modified silicone, an alkylsilane and an aminosilane, or with the silicon compound and the silica precursor, to obtain a second reaction mixture containing lanthanum hexaboride-containing composite particles.2. The production method according to claim 1 , wherein after the second reaction mixture is obtained claim 1 , the second reaction mixture is dried to recover the lanthanum hexaboride-containing composite particles.3. The production method according to claim 2 , wherein the second reaction mixture is a dispersion having the lanthanum hexaboride-containing composite particles dispersed in an organic solvent claim 2 , and the second reaction mixture is subjected to centrifugal separation claim 2 , the supernatant is removed and the sediment is recovered claim 2 , and the sediment is dried.4. The production method according to claim 1 , wherein the first reaction mixture contains the silica precursor which remains unreacted.5. The production method according to claim 1 , wherein the reaction of the silica precursor to obtain the first reaction mixture is carried out in the further presence of zirconium oxide particles.6 ...

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11-01-2018 дата публикации

Ferrite particle having outer shell structure

Номер: US20180011414A1
Автор: Koji Aga, Takao Sugiura
Принадлежит: Powdertech Co Ltd

An object of the present invention is to provide a ferrite particle having a low apparent density, filling a specified volume with a low weight with various properties maintained in a controllable state, a ferrite carrier core material composed of the ferrite particle, and a ferrite carrier using the ferrite core material and an electrophotographic developer. To achieve the object, the ferrite particle having the outer shell structure containing the Ti oxide for the ferrite carrier core material, and the ferrite carrier using the ferrite particle as the ferrite carrier core material and the electrophotographic developer are employed.

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09-01-2020 дата публикации

COMPOSITE NANOPARTICLE COMPOSITIONS AND ASSEMBLIES

Номер: US20200013939A1
Принадлежит:

Composite nanoparticle compositions and associated nanoparticle assemblies are described herein which, in some embodiments, exhibit enhancements to one or more thermoelectric properties including increases in electrical conductivity and/or Seebeck coefficient and/or decreases in thermal conductivity. In one aspect, a composite nanoparticle composition comprises a semiconductor nanoparticle including a front face and a back face and sidewalls extending between the front and back faces. Metallic nanoparticles are bonded to at least one of the sidewalls establishing a metal-semiconductor junction. 1. A composite nanoparticle composition comprising:a semiconductor nanoparticle including a front face and a back face and sidewalls extending between the front and back faces; andmetallic nanoparticles bonded to at least one of the sidewalls establishing a metal-semiconductor junction.2. The composite nanoparticle of claim 1 , wherein the metallic nanoparticles are bonded to a plurality of the sidewalls establishing multiple metal-semiconductor junctions.3. The composite nanoparticle of claim 1 , wherein a Schottky barrier is established at the metal-semiconductor junction.4. The composite nanoparticle of claim 3 , wherein the Schottky barrier has a height of at least 100 meV.5. The composite nanoparticle of claim 1 , wherein the semiconductor nanoparticles is a chalcogenide.6. The composite nanoparticle of claim 5 , wherein the metallic nanoparticles are formed of one or more transition metals.7. The composite nanoparticle of claim 6 , wherein the one or more transition metals are selected from Groups IVA-VIIIA and Group IB of the Periodic Table.8. The composite nanoparticle of claim 6 , wherein the one or more transition metals are a noble metal.9. The composite nanoparticle of claim 1 , wherein the semiconductor nanoparticle is a platelet.10. The composite nanoparticle of further comprising an interfacial transition region between the semiconductor nanoparticle and ...

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19-01-2017 дата публикации

Preparation method of fluorine-doped lamellar black titanium dioxide nano material

Номер: US20170014811A1
Принадлежит: NORTH CHINA ELECTRIC POWER UNIVERSITY

The method for preparing fluorine-doped lamellar black TiO 2 nanomaterials includes mixing a solution of tetra-n-butyl titanate, n-propanol and hydrofluoric acid together, and then stir the solutions for a period of time. The solution is transferred into an autoclave and reacts at a certain temperature for a period of time. The sample obtained by the reaction is washed and dried. Then, the sample is heated in a protective atmosphere for a period of time so as to produce the fluorine-doped lamellar black TiO 2 nanomaterials. This fluorine-doped lamellar black TiO 2 owns superior optical absorption and electron transport performances.

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15-01-2015 дата публикации

Carbon material for lithium ion secondary battery, negative electrode material for lithium ion secondary battery, and lithium ion secondary battery

Номер: US20150017539A1
Принадлежит: Sumitomo Bakelite Co Ltd

A carbon material for lithium ion secondary batteries of the invention contains amorphous carbon and graphite. The amorphous carbon is deposited on a surface of the graphite, the amorphous carbon content is 55% by weight to 99% by weight, and the graphite content is 1% by weight to 45% by weight.

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19-01-2017 дата публикации

Process of manufacture of particles with a natural calcium carbonate and ethylene acrylic acid salts base, suspensions and dry pigments obtained, their uses

Номер: US20170015859A1
Принадлежит: Omya International AG

The present invention consists of a process of preparation of at least one mineral matter and/or of at least one pigment, including a calcium carbonate made at once partially organophilic and partially hydrophilic, in which the carbonate is blended and/or ground and/or concentrated in an aqueous medium, in the presence of at least one salt of ethylene acrylic acid, one dispersing agent and/or one grinding aid agent, which is introduced before and/or during this treatment stage. Another object of the invention lies in the aqueous dispersions and suspensions of calcium carbonate thus obtained. They may be dried and the dry pigments obtained also constitute an object of the invention. Use of these aqueous dispersions and these dry pigments in the field of plastic, paints and paper constitutes another object of the invention.

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18-01-2018 дата публикации

Production of Alkali Sulfide Cathode Material and Methods for Processing Hydrogen Sulfide

Номер: US20180016144A1
Принадлежит:

Disclosed herein are methods of producing metal sulfide materials, including cathode materials. In some embodiments, the metal sulfide material comprises a secondary cluster of metal sulfide nanoparticles surrounded by a carbon layer. The carbon layer may be created by carbonizing one or more polymer layers disposed about the secondary cluster. The carbonized layer may aid in optimizing performance of the cathode material. Also disclosed herein are methods, processes, devices, and systems for removing hydrogen sulfide from a waste stream. In some embodiments, the waste stream containing hydrogen sulfide is a gas. The waste stream can be combined with a solvent containing a metal-catalyst complex, and the reaction of hydrogen sulfide with the metal results in production of a hydrogen gas and a solid comprising metal sulfide. 1. A method of converting a hydrogen sulfide gas to a metal sulfide material , the method comprising:combing an alkalai metal and an alcohol to create a metal alkoxide;creating an anhydrous solution comprising the metal alkoxide;flowing a gas through the solution, the gas comprising hydrogen sulfide;allowing the hydrogen sulfide gas to react with the metal to form a solid metal sulfide particle, hydrogen gas, and regenerate the alcohol; andprecipitating the solid metal sulfide and capturing the hydrogen gas; andseparating the solid metal sulfide precipitate from the alcohol.2. The method of claim 1 , wherein the solution further comprises a polymer and a solvent.3. The method of claim 2 , wherein heating of the precipitate creates a secondary cluster of polymer-coated metal sulfide particles.4. The method of claim 3 , wherein the polymer-coated particles are coated with a layer of carbon.5. The method of claim 2 , wherein the polymer is selected from polyvinylpyrrolidone (PVP claim 2 , [CHNO]n) claim 2 , poly(2-ethyl-2-oxazoline) (PEOZ claim 2 , [CHNO]n) claim 2 , and polyacrylonitrile (PAN claim 2 , [CHN]n) and the solvent is selected from ...

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18-01-2018 дата публикации

NEAR-INFRARED ABSORBING FINE PARTICLE DISPERSION LIQUID AND METHOD FOR PRODUCING THE SAME

Номер: US20180016451A1
Принадлежит: SUMITOMO METAL MINING CO., LTD.

A near infrared absorbing fine particle dispersion liquid, which can be applied to offset printing, including: a solvent of one or more kinds selected from vegetable oils and vegetable oil-derived compounds; near infrared ray-absorbing fine particles of one or more kinds selected from composite tungsten oxide expressed by MxWyOz or tungsten oxide having a Magneli phase expressed by a general formula WyOz; a solvent of one or more kinds selected from alcohols, ethers, esters, ketones, aromatic hydrocarbons and glycol ethers and having a boiling point of 180° C. or less, wherein a content of the solvent of one or more kinds selected from alcohols, ethers, esters, ketones, aromatic hydrocarbons and glycol ethers is 5 mass % or less. 1. A near infrared absorbing fine particle dispersion liquid , comprising:a solvent of one or more kinds selected from vegetable oils and vegetable oil-derived compounds;{'sub': y', 'z, 'near infrared absorbing fine particles of one or more kinds selected from composite tungsten oxide expressed by MxWyOz (M is H, He, alkali metal, alkaline earth metal, rare earth element, Mg, Zr, Cr, Mn, Fe, Ru, Co, Rh, Ir, Ni, Pd, Pt, Cu, Ag, Au, Zn, Cd, Al, Ga, In, Tl, Si, Ge, Sn, Pb, Sb, B, F, P, S, Se, Br, Te, Ti, Nb, V, Mo, Ta, Re, Be, Hf, Os, Bi, and I, W is tungsten, and O is oxygen, satisfying 0.001≦x/y≦1, 2.2≦z/y≦3.0), or a tungsten oxide having a Magneli phase expressed by a general formula WO(W is tungsten, O is oxygen, satisfying 2.45≦z/y≦2.999), and'}a solvent of one or more kinds selected from alcohols, ethers, esters, ketones, aromatic hydrocarbons, and glycol ethers and having a boiling point of 180° C. or less,wherein a content of the solvent of one or more kinds selected from alcohols, ethers, esters, ketones, aromatic hydrocarbons and glycol ethers is 5 mass % or less.2. The near infrared absorbing fine particle dispersion liquid according to claim 1 , wherein the near infrared absorbing fine particle dispersion liquid further contains a ...

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21-01-2021 дата публикации

METHODS FOR PREPARING PARTICLE PRECURSOR AND CATHODE ACTIVE PARTICLES, AND PARTICLE PRECURSOR PREPARED THEREBY

Номер: US20210017040A1
Принадлежит:

The invention relates to a method for preparing transitional-metal particles (cathode particle precursor) under a co-precipitation reaction. In this method, by feeding different types of anion compositions and/or cation compositions, and adjusting the pH to match with the species, precipitated particles are deposited to form a slurry, colleting the slurry, treating with water, and drying to get a cathode particle precursor. Mixing the cathode particle precursor with a lithium source and calcining to yield core-shell structured cathode active particles. Such cathode active particle can be used to prepare cathode of lithium-ion battery. 1. A method for preparing a particle precursor , comprising the following steps:{'sub': 1', '2', '1', '2, 'feeding stream (b) into a reactor for providing precipitating anions, feeding stream (a) for providing transitional-metal cations, whereby the precipitating anions and the transitional-metal cations reacting to form a precipitated particle slurry; the stream (b) comprises at least a first anion composition Band a second anion composition B, the first anion composition Bis switched to the second anion composition Bat a first switching time between the time the co-precipitation starts and the time the reaction ends, the stream (a) comprises at least one cation composition; and'}filtering, and drying the precipitated particle slurry to yield the particle precursor.2. The method of claim 1 , wherein the particle precursor has a formula of (NiMnCoMe)(CO)(OH) claim 1 , where x+y+z≥0.9 claim 1 , z≤0.2 claim 1 , 0≤a≤1 claim 1 , “Me” is at least one additional metal element selected from the group consisting of Mg claim 1 , Ca claim 1 , Zr claim 1 , Ti claim 1 , V claim 1 , Cr claim 1 , Fe claim 1 , Cu and Al.3. The method of claim 1 , wherein the stream (b) comprises anions whose concentration is 0.001-14 mol anion/L; and/or the stream (a) comprises cations whose concentration is 0.001-6 mol cation/L.4. The method of claim 1 , wherein the ...

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21-01-2021 дата публикации

COMPOSITE PARTICLES AND METHOD FOR PRODUCING COMPOSITE PARTICLES

Номер: US20210017391A1
Принадлежит:

Provided are: composite particles having excellent oxidation resistance; and a method for producing composite particles. The composite particles are obtained by forming a composite of TiN and at least one of Al, Cr, and Nb. In the method for producing composite particles, a titanium powder and a powder of at least one of Al, Cr, and Nb are used as raw material powders and composite particles are produced using a gas phase method. 1. Composite particles in which TiN is combined with at least one of Al , Cr and Nb.2. The composite particles according to claim 1 , wherein when the TiN is combined with the Al claim 1 , a content of the Al is 0.1 to 20 mass %.3. The composite particles according to claim 1 , wherein when the TiN is combined with the Cr claim 1 , a content of the Cr is 0.1 to 20 mass %.4. The composite particles according to claim 1 , wherein when the TiN is combined with the Nb claim 1 , a content of the Nb is 0.1 to 20 mass %.5. A method of producing composite particles in which TiN is combined with at least one of Al claim 1 , Cr and Nb claim 1 , wherein the composite particles are produced using powder of titanium and powder of at least one of Al claim 1 , Cr and Nb as feedstock by means of a gas-phase process.6. The method of producing composite particles according to claim 5 , wherein the gas-phase process is a thermal plasma process claim 5 , a flame process claim 5 , an arc plasma process claim 5 , a microwave heating process or a pulsed wire process.7. The method of producing composite particles according to claim 6 , wherein the thermal plasma process involves a step of supplying carrier gas having the feedstock dispersed therein to a thermal plasma flame and a step of supplying cooling gas to a terminating portion of the thermal plasma flame to thereby produce the composite particles.8. The method of producing composite particles according to claim 7 , wherein the thermal plasma flame is derived from at least one of argon gas and nitrogen gas. ...

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21-01-2021 дата публикации

FILLER FOR RESINOUS COMPOSITION, FILLER-CONTAINING SLURRY COMPOSITION AND FILLER-CONTAINING RESINOUS COMPOSITION AS WELL AS PRODUCTION PROCESS FOR FILLER FOR RESINOUS COMPOSITION

Номер: US20210017392A1
Принадлежит: ADMATECHS CO., LTD.

A filler for resinous composition is contained and used in resinous composition constituting electronic packaging material for electronic device, and includes: a filler ingredient including a crystalline siliceous material with a crystal structure made of at least one member selected from the group consisting of type FAU, type FER, type LTA, type MFI and type CHA, and/or type MWW, wherein: the filler ingredient is free of any activity when evaluated by an “NH3-TPD” method; and includes the crystalline siliceous material in an amount falling in a range allowing the filler ingredient to exhibit a negative thermal expansion coefficient. The filler ingredient may further be free of a surface in which silver, copper, zinc, mercury, tin, lead, bismuth, cadmium, chromium, cobalt and nickel are exposed. 1. A filler for resinous composition , the filler contained and used in resinous composition constituting electronic packaging material for electronic device , the filler comprising:a filler ingredient including a crystalline siliceous material with a crystal structure made of at least one member selected from the group consisting of type FAU, type FER, type LTA, type MFI, type CHA, and type MWW, wherein:the filler ingredient does not have any activity when evaluated by an NH3-TPD method;the filler ingredient includes the crystalline siliceous material in an amount falling in a range allowing the filler ingredient to exhibit a negative thermal expansion coefficient;the crystalline siliceous material includes an alkali metal in a content of 0.1% by mass or less; andwhen the crystalline siliceous material is immersed in water conditioned at 120° C. and under two atm for 24 hours, an amount of each of Li, Na and K extracted in the water is five ppm or less.2. A filler for resinous composition , the filler contained and used in resinous composition , the filler comprising:a filler ingredient including a crystalline siliceous material with a crystal structure made of at least one ...

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18-01-2018 дата публикации

POSITIVE ELECTRODE ACTIVE MATERIAL FOR SECONDARY BATTERY AND SECONDARY BATTERY INCLUDING THE SAME

Номер: US20180019504A1
Принадлежит: LG CHEM, LTD.

Provided are a positive electrode active material for a secondary battery, in which, since the positive electrode active material includes a lithium-metal oxide having high-temperature stability and a metal oxide on a surface of a particle and a surface side in the particle, there is no concern about gas generation, because the occurrence of cracks on the surface of the active material is prevented during charge and discharge, and high-temperature storage stability and life characteristics may be improved when the positive electrode active material is used in the battery, and a secondary battery including the same. 1. A positive electrode active material for a secondary battery , the positive electrode active material comprising:a core including a lithium cobalt oxide; anda lithium-metal oxide and a metal oxide, which include at least one metal selected from the group consisting of aluminum (Al), magnesium (Mg), tungsten (W), molybdenum (Mo), zirconium (Zr), titanium (Ti), tantalum (Ta), iron (Fe), vanadium (V), chromium (Cr), barium (Ba), calcium (Ca), and niobium (Nb), on a surface of the core,wherein the lithium-metal oxide is a heat fused material of the lithium cobalt oxide and the metal oxide.2. The positive electrode active material for a secondary battery of claim 1 , further comprising the lithium-metal oxide and the metal oxide in a region corresponding to a distance from the surface of the core of 0% or more to less than 100% of a total distance from the surface of the core to a center thereof.3. The positive electrode active material for a secondary battery of claim 1 , wherein the lithium-metal oxide and the metal oxide comprise at least one metal selected from the group consisting of Al claim 1 , Mg claim 1 , and Ti.4. The positive electrode active material for a secondary battery of claim 1 , wherein the lithium-metal oxide and the metal oxide comprise Al.5. The positive electrode active material for a secondary battery of claim 1 , wherein the core ...

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16-01-2020 дата публикации

Method for manufacturing positive active material, and positive active material and lithium secondary battery using same

Номер: US20200020934A1

A method for preparing a positive electrode active material, a positive electrode active material prepared using the same, and a lithium secondary battery, and in particular, to a method for preparing a positive electrode active material comprising the steps of (a) preparing a coating composition including a precursor of metal-phosphorous-oxynitride; (b) forming a precursor layer on a positive electrode active material with the coating composition of (a) using a solution process; and (c) forming a metal-phosphorous-oxynitride protective layer on the positive electrode active material by heat treating the positive electrode active material having the precursor layer formed thereon. The method for preparing a positive electrode active material uses a solution process, which is advantageous in terms of simplifying the whole process and reducing costs, and high capacity, high stabilization and long lifetime are obtained as well by the formed protective layer having excellent properties.

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26-01-2017 дата публикации

Separation of terbium(iii,iv) oxide

Номер: US20170022071A1

Various embodiments relate to separation of terbium(III,IV) oxide. In various embodiments, present invention provides a method of separating terbium(III,IV) oxide from a composition. The method can include contacting a composition including terbium(III,IV) oxide and one or more other trivalent rare earth oxides with a liquid including acetic acid to form a mixture. The contacting can be effective to dissolve at least some of the one or more other trivalent rare earth oxides into the liquid. The method can include separating undissolved terbium(III,IV) oxide from the mixture, to provide separated terbium(III,IV) oxide.

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10-02-2022 дата публикации

NANOSTRUCTURED SILICON CARBONACEOUS COMPOSITE MATERIAL AND METHODS FOR PRODUCING THE SAME

Номер: US20220041454A1
Принадлежит:

Described herein is a nanostructured silicon carbonaceous composite material and methods for producing the same. The methods include formation of a metal organic framework/silica (MOF/SiO) intermediate material and conversion of the MOF/SiOintermediate material to the nanostructured silicon carbonaceous composite material. Relatively inexpensive and/or recycled materials can be used as precursors in manufacturing the nanostructured silicon carbon composition material, which can be used in various applications, including as silicon anode material in a lithium-ion battery. 1. A method for making a nano-crystalline metal organic framework/silica intermediate material , the method comprisingcontacting a metal-silica precursor with an organic ligand in water to form an aqueous mixture, andheating the aqueous mixture at a temperature ranging from about 25° C. to 300° C. thereby forming the nano-crystalline metal organic framework/silica intermediate material.2. The method of claim 1 , wherein the metal-silica precursor comprises a metal oxide confined in silica or a metal silicate.3. The method of claim 2 , wherein the metal oxide confined in silica is synthetic metal oxide.4. The method of claim 2 , wherein the metal silicate is mineral metal silicate.5. The method of claim 4 , wherein the mineral metal silicate comprises halloysite or kaolinite.6. The method of claim 4 , wherein the mineral metal silicate comprises asbestos claim 4 , fly ash or bottom ash.7. The method of claim 1 , wherein the organic ligand comprises PET derived from a plastic bottle claim 1 , preferably a recycled plastic bottle.8. The method of claim 1 , wherein the metal-silica precursor and organic ligand are also contacted with organic solvent.9. The method of claim 8 , wherein the organic solvent comprises methanol claim 8 , ethanol claim 8 , tetrahydrofuran claim 8 , N claim 8 ,N-dimethylformamide claim 8 , N claim 8 ,N-dimethylacetamide claim 8 , acetonitrile claim 8 , acetone.10. The method of ...

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10-02-2022 дата публикации

MODIFIED ZIRCONIUM PHOSPHATE TUNGSTATE, NEGATIVE THERMAL EXPANSION FILLER AND POLYMER COMPOSITION

Номер: US20220041841A1
Принадлежит: Nippon Chemical Industrial Co., Ltd.

There is provided a modified zirconium phosphate tungstate which effectively suppresses the elution of phosphorus ions even when it contacts with water, can develop the performance excellent as a negative thermal expansion material, and can be dispersed in a polymer compound such as a resin, and use of which enables a low-thermal expansive material containing a negative thermal expansion filler to be well produced. The surface of a zirconium phosphate tungstate particle is coated with an inorganic compound containing one or two or more elements (M) selected from Zn, Si, Al, Ba, Ca, Mg, Ti, V, Sn, Co, Fe and Zr. The BET specific surface area of the zirconium phosphate tungstate particle is preferably 0.1 m/g to 50 m/g. 1. A modified zirconium phosphate tungstate , wherein a surface of a zirconium phosphate tungstate particle is coated with an inorganic compound containing one or two or more elements (M) selected from Zn , Si , Al , Ba , Ca , Mg , Ti , V , Sn , Co , Fe and Zr ,wherein an amount of phosphorus ions eluted when 1 g of the modified zirconium phosphate tungstate is heated in 70 mL of water at 85° C. for 1 hour, then cooled to 25° C. and allowed to stand for 24 hours is 100 μg or smaller per g of the modified zirconium phosphate tungstate.2. The modified zirconium phosphate tungstate according to claim 1 , wherein the particle has a BET specific surface area of 0.1 m/g to 50 m/g.3. The modified zirconium phosphate tungstate according to claim 1 , wherein the particle has an average particle diameter of 0.02 μm to 50 μm.4. The modified zirconium phosphate tungstate according to claim 1 , wherein the particle further comprises a sub-component element.5. The modified zirconium phosphate tungstate according to claim 1 , wherein a coating amount of the inorganic compound in terms of the element (M) contained in the inorganic compound with respect to the particle is 0.1% by mass to 10% by mass.6. (canceled)7. The modified zirconium phosphate tungstate according ...

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10-02-2022 дата публикации

CATHODE ACTIVE MATERIAL, METHOD FOR PREPARING SAME, AND LITHIUM SECONDARY BATTERY COMPRISING SAME

Номер: US20220045317A1
Принадлежит:

A positive active material, a manufacturing method thereof, and a lithium secondary battery including the same are disclosed, and a positive active material including lithium metal oxide particles in a secondary particle form including primary particles, wherein the secondary particle surface includes planar primary particles with a narrow angle of 70 to 90° from among angles between a c axis of the primary particles and a straight line connecting a virtual point of a center of the primary particle and a center point of the secondary particle may be provided. 1. A positive active material including lithium metal oxide particles in a secondary particle form including primary particles ,wherein the secondary particle surface includes planar primary particles with a narrow angle of 60 to 90° from among angles between a c axis of the primary particles and a straight line connecting a virtual point of a center of the primary particle and a center point of the secondary particle.2. The positive active material of claim 1 , whereinwith respect to the area of 100 area % formed by a circle of 50% reference of a radius of the secondary particles at the center point of the secondary particle,an area occupied by the planar primary particles is equal to or greater than 20 area %.3. The positive active material of claim 2 , whereinwith respect to the area 100 area % formed by a circle of 50% reference of a radius of the secondary particles at the center point of the secondary particle,an average length of the planar primary particles existing in the area is 750 nm to 1.25 μm.4. The positive active material of claim 1 , whereinan inside of the secondary particle includes acicular primary particles with a narrow angle of equal to or greater than 0° and less than 70° from among angles between a c axis of the primary particles and a straight line connecting a virtual point of a center of the primary particle and a center point of the secondary particle.5. The positive active material ...

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01-02-2018 дата публикации

MICRON-SCALE CERIUM OXIDE PARTICLE HAVING MULTI-CORE SINGLE-SHELL STRUCTURE AND PREPARATION METHOD THEREFOR

Номер: US20180029012A1
Принадлежит:

The present invention involves micron-scale cerium oxide particles having a multi-cores single-shell structure, comprising: a cerium oxide shell, the shell being composed of crystalline and/or amorphous nano-scale cerium oxide particles; and a plurality of nano-scale cerium oxide grain cores aggregates located in the interior of the shell. Also involved is a preparation method for the micron-scale cerium oxide particle having a multi-cores single-shell structure. A supported catalyst with the micron-scale cerium oxide particles according to the invention as the support have good hydrothermal stability and good sulfur resistance, and the active components of the supported catalyst are not easily embedded, and the supported catalyst has a great application prospect in the field of catalytic oxidation of exhaust emissions such as CO, NO or volatile organic compounds. 1. A micro-scale cerium oxide particle having multi-cores single-shell structure , characterized in that the micro-scale cerium oxide particle comprises: a cerium oxide shell , the shell being composed of crystalline and/or amorphous nano-scale cerium oxide particles; and a plurality of nano-scale cerium oxide grain cores aggregates located in the interior of the shell.2. The micro-scale cerium oxide particle having multi-cores single-shell structure according to claim 1 , characterized in that the micro-scale cerium oxide particles are spherical or sphere-like particles claim 1 , having an average particle size of 0.5 μm to 50 μm claim 1 , and a BET specific surface area of 50 to 200 m/g; the mass of the plurality of nano-scale cerium oxide grain cores aggregates in the interior of the shell is from 85 to 99% based on the total mass of the micro-scale cerium oxide particles claim 1 , and the mass of the cerium oxide shell is from 1 to 15% based on the total mass of the micro-scale cerium oxide particles; the cerium oxide shell has a thickness ranging from 10 to 200 nm; the nano-scale cerium oxide grains ...

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23-01-2020 дата публикации

POSITIVE ELECTRODE ACTIVE MATERIAL CONTAINING SOLID SOLUTION ACTIVE MATERIAL, POSITIVE ELECTRODE CONTAINING THE POSITIVE ELECTRODE ACTIVE MATERIAL, AND NON-AQUEOUS ELECTROLYTE SECONDARY BATTERY USING THE POSITIVE ELECTRODE

Номер: US20200028162A1
Принадлежит:

A method for producing a positive electrode active material includes coating a surface of a solid solution active material represented by formula (1): Li[NiMnCo[Li]]O, wherein X represents at least one selected from Ti, Zr and Nb, 0≤e≤0.5, a+b++c+d+e=1.5, 0.1≤d≤0.4, and 1.1≤[a+b+c+e]≤1.4, and z represents the number of oxygen atoms satisfying an atomic valence, with alumina; and preparing the solid solution active material. The preparing comprises mixing an organic acid salt of a transition metal having a melting point of 100° C. to 350° C., melting the mixture obtained in the first step at 100° C. to 350° C., subjecting the molten substance to pyrolysis at a temperature equal to higher than the melting point and calcining the pyrolysate obtained. 1. A method for producing a positive electrode active material for a non-aqueous electrolyte secondary battery , comprising: {'br': None, 'sub': 1.5', '0.40', '0.60', '0.40', '0.1', 'z, 'Li[NiMnCo[Li]]O\u2003\u2003(1)'}, 'coating a surface of a solid solution active material represented by the composition formula (1)wherein X represents at least one selected from Ti, Zr and Nb, 0≤e≤0.5, a+b++c+d+e=1.5, 0.1≤d≤0.4, and 1.1≤[a+b+c+e]≤1.4, and z represents the number of oxygen atoms satisfying an atomic valence, with alumina; and a first step of mixing an organic acid salt of a transition metal having a melting point of 100° C. to 350° C.;', 'a second step of melting the mixture obtained in the first step at 100° C. to 350° C.;', 'a third step of subjecting the molten substance obtained in the second step to pyrolysis at a temperature equal to higher than the melting point; and', 'a fourth step of calcining the pyrolysate obtained in the third step., 'preparing the solid solution active material, wherein the preparing comprises2. The method according to claim 1 , wherein a citrate of at least one of Ti claim 1 , Zr and Nb is further mixed in the first step.3. The method according to claim 1 , wherein an organic acid salt of an ...

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28-01-2021 дата публикации

Method of producing magnetic powder and method of producing magnetic recording medium

Номер: US20210027807A1
Принадлежит: Sony Corp

[Solving Means] A method of producing a magnetic powder includes: coating a surface of each of silica-coated precursor particles with at least one type of coating agent of a metal chloride or a sulfate; and firing the precursor particles coated with the coating agent.

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28-01-2021 дата публикации

Negative electrode active material for non-aqueous electrolyte secondary battery, non-aqueous electrolyte secondary battery, and method for producing negative electrode material for non-aqueous electrolyte secondary battery

Номер: US20210028447A1
Принадлежит: Shin Etsu Chemical Co Ltd

A negative electrode active material for a non-aqueous electrolyte secondary battery, containing a negative electrode active material particle, wherein the negative electrode active material particle includes a silicon compound particle containing a silicon compound (SiOx: 0.5≤x≤1.6), the silicon compound particle contains a Li compound, at least a part of the silicon compound particle is coated with a carbon material, and an O-component fragment and a CH-component fragment are detected from the negative electrode active material particle in a measurement by TOF-SIMS, and a ratio of a peak intensity A of the O-component fragment to a peak intensity B of the CH-component fragment is 0.5≤A/B≤100. This provides a negative electrode active material for a non-aqueous electrolyte secondary battery capable of increasing battery capacity and improving the cycle characteristics and battery initial efficiency.

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28-01-2021 дата публикации

One-Pot Synthesis for LiNbO3 Coated Spinel

Номер: US20210028448A1
Принадлежит:

Provided is an improved method for forming a coated lithium ion cathode materials specifically for use in a battery. The method comprises forming a first solution comprising a digestible feedstock of a first metal suitable for formation of a cathode oxide precursor and a multi-carboxylic acid. The digestible feedstock is digested to form a first metal salt in solution wherein the first metal salt precipitates as a salt of deprotonated multi-carboxylic acid thereby forming an oxide precursor and a coating metal is added to the oxide precursor. The oxide precursor is heated to form the coated lithium ion cathode material. 1. A method of forming a coated lithium ion cathode material comprising:forming a first solution comprising a digestible feedstock of a first metal suitable for formation of a cathode oxide precursor and a multi-carboxylic acid;digesting said digestible feedstock to form a first metal salt in solution wherein said first metal salt precipitates as a salt of deprotonated said multi-carboxylic acid thereby forming an oxide precursor;adding a coating metal precursor salt after said digestion;heating said oxide precursor to form said lithium ion cathode material with an oxide of said coating metal precursor salt as a coating on said lithium ion cathode material.2. The method of forming a coated lithium ion cathode material of wherein said coating metal precursor salt comprises niobium.3. The method of forming a coated lithium ion cathode material of wherein said oxide of said coating metal precursor salt is lithium niobate.4. The method of forming a coated lithium ion cathode material of wherein said coating metal precursor salt comprises a multi-carbonate salt.5. The method of forming a coated lithium ion cathode material of wherein said multi-carbonate is an oxalate.6. The method of forming a coated lithium ion cathode material of wherein said coating comprises at least 95 wt % said coating metal.7. The method of forming a coated lithium ion cathode ...

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04-02-2021 дата публикации

HYBRID STRUCTURE USING GRAPHENE-CARBON NANOTUBE AND PEROVSKITE SOLAR CELL USING THE SAME

Номер: US20210032108A1

Disclosed are a hybrid structure using a graphene-carbon nanotube and a perovskite solar cell using the same. The hybrid structure includes a graphene-carbon nanotube formed by laminating a second graphene coated with a polymer on an upper surface of a first graphene coated with a carbon nanotube. The perovskite solar cell includes: a substrate; a first electrode formed on the substrate and including a fluorine doped thin oxide (FTO); an electron transfer layer formed on the first electrode and including a compact-titanium oxide (c-TiO); a mesoporous-titanium oxide (m-TiO) formed on the electron transfer layer; a perovskite layer formed on the m-TiOand including a perovskite compound; and a graphene-carbon nanotube hybrid structure formed on the perovskite layer. 1. A hybrid structure comprising a graphene-carbon nanotube formed by laminating a second graphene coated with a polymer layer on an upper surface of a first graphene coated with a carbon nanotube layer ,wherein the first graphene has a first surface and an opposite second surface,the carbon nanotube layer has a first surface and an opposite second surface, and is coated on the second surface of the first graphene,the second graphene has a first surface and an opposite second surface, and is laminated on a surface of the carbon nanotube layer opposite the first graphene, andthe polymer layer has a first surface and an opposite second surface, and is coated on the second graphene on a surface of the second graphene opposite the carbon nanotube layer.2. The hybrid structure of claim 1 , wherein polymer in the polymer layer is at least one selected from the group consisting of poly(methyl methacrylate) (PMMA) claim 1 , poly(bisphenol A carbonate) (PC) claim 1 , polyvinylidenefluoride-hexafluoropropylene (PVDF-HFP) claim 1 , polyethylene oxide (PEO) claim 1 , polyacrylonitrile (PAN) claim 1 , and polyvinylalcohol (PVA).3. A preparation method of the hybrid structure according to claim 1 , comprising the steps:( ...

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01-02-2018 дата публикации

SURFACE-MODIFIED IRON-BASED OXIDE MAGNETIC PARTICLE POWDER, AND METHOD FOR PRODUCING SAME

Номер: US20180033528A1
Принадлежит:

A surface-modified iron-based oxide magnetic particle powder has good solid-liquid separation property in the production process, has good dispersibility in a coating material for forming a coating-type magnetic recording medium, has good orientation property, and has a small elution amount of a water-soluble alkali metal, and to provide a method for producing the surface-modified iron-based oxide magnetic particle powder. The surface-modified iron-based oxide magnetic particle powder can be obtained by neutralizing a solution containing dissolved therein a trivalent iron ion and an ion of the metal, by which the part of Fe sites is to be substituted, with an alkali aqueous solution, so as to provide a precursor, coating a silicon oxide on the precursor, heating the precursor to provide e-type iron-based oxide magnetic powder, and adhering a hydroxide or a hydrous oxide of one kind or two kinds of Al and Y thereto. 1. A surface-modified iron-based oxide magnetic particle powder comprising iron-based oxide magnetic particle powder containing ε-FeOor ε-FeO , a part of Fe sites of which is substituted by another metal element , having an average particle diameter measured with a transmission electron microscope of 5 nm or more and 30 nm or less , having adhered to a surface thereof a hydroxide or a hydrous oxide of a metal element S forming a precipitate of a hydroxide in an aqueous solution having pH of 7 or more and 12 or less.2. The surface-modified iron-based oxide magnetic particle powder according to claim 1 , wherein the metal element S is one kind or two kinds of Al and Y.3. The surface-modified iron-based oxide magnetic particle powder according to claim 1 , wherein the surface-modified iron-based oxide magnetic particle powder has a molar ratio SIM of 0.02 or more and 0.10 or less claim 1 , wherein M represents a sum of Fe and the substituting metal element contained therein.4. The surface-modified iron-based oxide magnetic particle powder according to claim ...

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04-02-2021 дата публикации

COMPOSITE PARTICLES HAVING COATED AGGREGATES WITH LOW STRUCTURE CARBON BLACK CORES, COATINGS AND INKS WITH HIGH RESISTIVITY AND OPTICAL DENSITY, DEVICES MADE THEREWITH, AND METHODS FOR MAKING SAME

Номер: US20210032475A1
Принадлежит:

Composite particles that super-aggregates of coated aggregates having low structure carbon black cores and metal/metalloid oxide mantles are described. Coatings containing filler-polymer compositions which have the composite particles as filler, such as curable coatings and cured coatings or films formed therefrom containing the filler-polymer compositions, with combinations of high resistivity, good optical density properties, good thermal stability, high dielectric constant, and good processability, along with their use in black matrices, black column spacers, light shielding elements in LCDs and other display devices, also are described. Inks containing the composite particle are described. Devices having these compositions, components and/or elements, and methods of preparing and making these various materials and products are described. 122-. (canceled)23. A method of making carbon black-metal/metalloid oxide composite particles , comprising:forming a stream of combustion gases by reacting a preheated air stream with a fuel;introducing first feedstock into the stream of combustion gases at a predetermined number of points arranged in a first ring pattern that is defined around the stream of combustion gases to form a reaction stream and start pyrolysis of the first feedstock in the reaction stream, wherein the first feedstock comprises carbon black-yielding feedstock;introducing an auxiliary hydrocarbon into the stream of combustion gases at a predetermined number of points arranged in a second ring pattern that is defined around the stream of combustion gases, wherein the first and second ring patterns may be located at a same location or different locations;additionally introducing into at least one of the stream of combustion gases or the reaction stream or any combinations thereof at least one substance containing at least one Group IA element or Group IIA element or any combinations thereof;allowing carbon black aggregates to form in the reaction stream, ...

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17-02-2022 дата публикации

Synthesis of graphitic shells on silicon nanoparticles

Номер: US20220052323A1
Принадлежит: UNIVERSITY OF CALIFORNIA

Discussed herein are methods for making an anode material comprising silicon nanoparticles and a graphite carbon coating thereon. The method can include providing silicon nanoparticles, applying an amorphous carbon coating thereon to create an amorphous carbon shell on the silicon nanoparticles at a first temperature, and converting the amorphous carbon shell to a graphite carbon shell at a second temperature higher than the first temperature. The method can optionally include producing silicon nanoparticles by providing an argon-silane mixture, exposing the argon-silane mixture to a non-thermal plasma to convert the silane mixture to amorphous clusters, and passing the amorphous clusters through a furnace at a first temperature so as to agglomerate them to silicon nanoparticles.

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17-02-2022 дата публикации

Positive electrode active material, positive electrode plate, lithium-ion secondary battery, and apparatus

Номер: US20220052338A1
Автор: Na LIU, Qifeng Li, Qilan ZHANG
Принадлежит: Contemporary Amperex Technology Co Ltd

The present application discloses a positive electrode active material, a positive electrode plate, a lithium-ion secondary battery, and an apparatus. The positive electrode active material satisfies a chemical formula Li 1+x (Ni a Co b Mn c ) 1−d M d O 2−y A y , wherein M is one or more selected from Zr, Sr, B, Ti, Mg, Sn and Al, A is one or more selected from S, N, F, Cl, Br and I, −0.01≤x≤0.2, 0.12≤b/c≤0.9, 0.002≤b×c/a 2 ≤0.23, a+b+c=1, 0≤d≤0.1, and 0≤y≤0.2; and an interval particle size distribution curve of the positive electrode active material has a full width at half maximum D FW of from 4 μm to 8 μm. The positive electrode active material provided in the present application has relatively low cobalt content and relatively high cycle life and capacity performance.

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11-02-2016 дата публикации

Titanium compound-containing core-shell powder and method of making the same, and titanium compound-containing sintered body

Номер: US20160039721A1
Автор: Masayuki Fujimoto
Принадлежит: Yageo Corp

A titanium compound-containing core-shell powder includes a plurality of core-shell particles, each of which includes a core body and a shell layer encapsulating said core body. The core body is electrically conductive. The shell layer includes a crystal that is selected from titanate oxides having a perovskite structure and titanate oxides having a spinel structure. The core body and the shell layer are chemically bonded to each other.

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31-01-2019 дата публикации

POSITIVE ELECTRODE ACTIVE MATERIAL FOR NONAQUEOUS ELECTROLYTE SECONDARY BATTERIES, METHOD FOR PRODUCING SAME, POSITIVE ELECTRODE MIXTURE PASTE FOR NONAQUEOUS ELECTROLYTE SECONDARY BATTERIES, AND NONAQUEOUS ELECTROLYTE SECONDARY BATTERY

Номер: US20190036112A1
Принадлежит: SUMITOMO METAL MINING CO., LTD.

A positive electrode active material for nonaqueous electrolyte secondary batteries and production method thereof that are able to improve the stability of positive electrode mixture material pastes used to produce nonaqueous electrolyte secondary batteries, as well as to improve the output characteristics and charge/discharge cycle characteristics of secondary batteries. A method for producing a positive electrode active material for nonaqueous electrolyte secondary batteries includes mixing a fired powder formed of a lithium-metal composite oxide having a layered crystal structure, a first compound which is at least one selected from a group consisting of a lithium-free oxide, a hydrate of the oxide, and a lithium-free inorganic acid salt, and water and drying a mixture resulting from the mixing. The fired powder includes secondary particles formed by agglomeration of primary particles. The first compound reacts with lithium ions in the presence of water to form a second compound including lithium. 1. A method for producing a positive electrode active material for nonaqueous electrolyte secondary batteries , the method comprising:mixing a fired powder formed of a lithium-metal composite oxide having a layered crystal structure, a first compound which is at least one selected from a group consisting of a lithium-free oxide, a hydrate of the oxide, and a lithium-free inorganic acid salt, and water; anddrying a mixture resulting from the mixing, wherein{'sub': s', '1-x-y-z', 'x', 'y', 'z', '2+α, 'the fired powder comprises secondary particles represented by a general formula (1) LiNiCoMnMO where 0.05≤x≤0.35; 0≤y≤0.35; 0≤z≤0.10; 1.00 Подробнее

12-02-2015 дата публикации

Abrasive particles having a unique morphology

Номер: US20150040486A1
Принадлежит: Diamond Innovations Inc

An abrasive particle having an irregular surface, wherein the surface roughness of the particle is less than about 0.95. A method for producing abrasive particles having a unique surface morphology including providing a plurality of abrasive particles; providing a plurality of metal particles; mixing the abrasive particles and the metal particles to form a mixture; compressing the mixture to form a compressed mixture; heating the compressed mixture; and recovering modified abrasive particles.

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09-02-2017 дата публикации

COMPOSITE PIGMENTS

Номер: US20170037250A1
Автор: Li Yaping, Zhang Zhenzhong
Принадлежит:

Composite pigments are provided which comprise a mineral pigment (such as kaolin clay, titanium dioxide, talc, mica or a mixture of two or more of these mineral pigments) and calcium carbonate precipitated in-situ on the surfaces of the particles of the mineral pigment. 1. A high brightness composite pigment which comprises a mineral pigment and in-situ precipitated calcium carbonate and which is produced by a plurality of carbonation cycles to precipitate calcium carbonate on surfaces of particles of the mineral pigment ,wherein the composite pigment has a substantially reduced amount of particles of less than 0.2 microns compared to the starting mineral pigment and an equivalent amount of particles of 1-2 microns compared to the starting mineral pigment.2. A composite pigment as defined by wherein the mineral pigment is kaolin clay claim 1 , titanium dioxide claim 1 , talc claim 1 , mica or a mixture of two or more of these mineral pigments.3. A composite pigment as defined by wherein the mineral pigment is kaolin clay.4. A composite pigment as defined by wherein the kaolin clay is hydrous kaolin clay.5. A composite pigment as defined by wherein the kaolin clay is delaminated kaolin clay.6. A composite pigment as defined by wherein the kaolin clay is calcined kaolin clay.7. A composite pigment as defined by wherein the kaolin clay is a mixture of hydrous kaolin clay and calcined kaolin clay.8. A composite pigment as defined by wherein the amount of calcium carbonate precipitated on the surfaces of the mineral pigment is from about 5.0 to about 90.0 weight percent based on the weight of the dry composite pigment.9. A composite pigment as defined by wherein the amount of calcium carbonate precipitated on the surfaces of the mineral pigment is from about 10.0 to about 60.0 weight percent based on the weight of the dry composite pigment.10. A composite pigment as defined by wherein the amount of calcium carbonate precipitated on the surfaces of the mineral pigment is ...

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09-02-2017 дата публикации

ABRASIVE GRAIN ON THE BASIS OF ELECTROFUSED ALUMINUM OXIDE WITH A SURFACE COATING COMPRISING TITANIUM OXIDE AND/OR CARBON

Номер: US20170037289A1
Автор: FUCHS Thomas

The present invention relates to an abrasive grain on the basis of electrofused aluminum oxide with a surface coating comprising titanium oxide and/or carbon, wherein compounds formed of titanium oxide and/or carbon particles at the abrasive grain surface by means of a temperature treatment are tightly connected to the abrasive grain surface without an additional binding agent. 1. An abrasive grain on the basis of electrofused aluminum oxide with a surface coating comprising titanium oxide and/or carbon , wherein compounds formed of titanium oxide and/or carbon particles at the abrasive grain surface by a temperature treatment are tightly connected to the abrasive grain surface ,characterized in thata direct tight bond without an additional binding agent is formed between the abrasive grain surface and the titanium oxide and/or carbon compounds comprising an average particle size of between 0.01 μm and 10 μm.2. The abrasive grain according to claim 1 ,characterized in thatthe titanium oxide and/or carbon compounds tightly connected on the surface have an average particle size in the range of between 1 μm and 10 μm.3. The abrasive grain according to claim 1 ,characterized in thatthe percentage by weight of the surface coating is between 0.01 and 5% by weight, based on the weight of the untreated abrasive grain.4. The abrasive grain according to claim 1 ,characterized in thatthe surface coating has a layer thickness of less than 10 μm.5. The abrasive grain according to claim 1 ,characterized in thatthe titanium oxide and/or carbon particles are sintered onto the abrasive grain surface at a temperature of more than 800° C.6. The abrasive grain according to claim 1 ,characterized in that{'sub': 2', '2, 'the ratio of TiOto carbon is between 10:1 and 1:10 prior to the sintering when using mixtures of TiOand Carbon.'}7. A method for making an abrasive grain on basis of electrofused aluminum oxide with a surface coating comprising titanium oxide and/or carbon claim 1 , ...

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04-02-2021 дата публикации

POSITIVE ELECTRODE ACTIVE MATERIAL FOR NONAQUEOUS ELECTROLYTE SECONDARY BATTERIES, AND PRODUCTION METHOD THEREOF

Номер: US20210036309A1
Принадлежит:

A method for producing a positive electrode active material for nonaqueous electrolyte secondary batteries, includes: a mixing step of adding a W compound powder having a solubility A adjusted to 2.0 g/L or less to a Li-metal composite oxide powder and stirring in water washing of the composite oxide powder, the solubility A being determined by stirring the W compound in water having a pH of 12.5 at 25° C. for 20 minutes, the composite oxide powder being represented by the formula: LiNiCoMOand composed of primary and secondary particles, followed by solid-liquid separation, to thereby obtain a tungsten-containing mixture with the tungsten compound dispersed in the composite oxide powder; and a heat-treating step of heat-treating the mixture to uniformly disperse W on the surface of primary particles and thereby form a compound containing W and Li from the W and Li in the mixture, on the surface of primary particles. 1. A method for producing a positive electrode active material for nonaqueous electrolyte secondary batteries , comprising:{'sub': c', '1-x-y', 'x', 'y', '2, 'a mixing step of adding a tungsten compound powder having a solubility A adjusted to 2.0 g/L or less to a lithium-metal composite oxide powder and stirring them in water washing of the lithium-metal composite oxide powder, the solubility A being determined by stirring the tungsten compound in water having a pH of 12.5 at 25° C. for 20 minutes, the lithium-metal composite oxide powder being represented by a general formula: LiNiCoMO(where 0≤x≤0.35, 0≤y≤0.35, and 0.97≤c≤1.25 are satisfied, and M is at least one element selected from Mn, V, Mg, Mo, Nb, Ti and Al) and being composed of primary particles and secondary particles formed by aggregation of the primary particles, followed by solid-liquid separation, to thereby obtain a tungsten-containing mixture with the tungsten compound dispersed in the lithium-metal composite oxide powder; and'}a heat-treating step of heat-treating the tungsten- ...

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24-02-2022 дата публикации

CARBON-COATED PARTICLES

Номер: US20220056241A1
Принадлежит:

Core particles produced in situ or introduced as preformed core particles are coated with a layer of carbon. Non-carbon as well as some carbon-based core materials can be utilized. The resulting carbon coated particles can find applications in rubber products, for instance as reinforcement for tire components. 148-. (canceled)49. A rubber composition or a rubber article comprising carbon-coated particles , wherein the carbon coated particles comprise a non-carbon core , a reclaimed pyrolysis carbon core , or a plasma CB core coated by a carbon layer.50. The rubber composition or the rubber article of claim 49 , wherein the non-carbon core is formed from a material selected from the group consisting of precipitated silica claim 49 , fumed silica claim 49 , surface modified silica and any combination thereof.51. The rubber composition or the rubber article of claim 49 , wherein the non-carbon core is formed from nanoparticles of clay claim 49 , rice husk silica claim 49 , calcium carbonate and any combination thereof.52. The rubber composition or the rubber article of claim 49 , wherein the carbon layer is from about 0.5 nm to about 20 nm thick.53. The rubber composition or the rubber article of claim 49 , wherein the carbon layer is amorphous carbon.54. The rubber composition or the rubber article of claim 49 , wherein the non-carbon core claim 49 , the reclaimed pyrolysis carbon core claim 49 , or the plasma CB core has aciniform microstructure.55. The rubber composition or the rubber article of claim 49 , wherein the carbon-coated particles have a STSA within the range of from about 5 to about 275 m/g; and a COAN within the range of from about 40 to about 150 cc/100 g.56. The rubber composition or the rubber article of claim 49 , wherein the carbon-coated particles have a STSA within the range of from about 30 to about 250 m/g; and a COAN within the range of from about 55 to about 110 cc/100 g.57. The rubber composition or the rubber article of claim 49 , wherein ...

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24-02-2022 дата публикации

Method for Producing Solid Particles, Solid Particles, and the Use Thereof

Номер: US20220056276A1
Принадлежит:

The invention relates to a method for producing solid particles from an inorganic solid containing at least one alkali metal and/or alkaline earth metal, comprising at least the following steps: 115-. (canceled)16. A method for producing solid particles from an inorganic solid containing at least one alkali metal and/or alkaline earth metal , comprising at least the following steps:a) providing the inorganic solid containing at least one alkali metal and/or alkaline earth metal;b) extracting the at least one alkali metal and/or alkaline earth metal from the inorganic solid containing alkali metal and/or alkaline earth metal to obtain an extract containing the alkali metal and/or alkaline earth metal and an alkali metal-depleted and/or alkaline earth metal-depleted residue;c) separating the extract from the residue;d) processing the residue to obtain the solid particles, wherein at least one processing step is selected from a group comprising transporting, filling, packaging, washing, drying, adjusting the pH value, separating according to a mean grain size and/or mass and/or density, adjusting a mean grain size, magnetic separating, calcining, thermal rounding and surface coating.17. The method according to claim 16 , wherein the residue is a lithium-depleted and/or magnesium-depleted residue claim 16 , the residue comprising less than 7 mass % of the extracted alkali metal and/or alkaline earth metal.18. The method according to claim 16 , wherein the residue is a lithium-depleted and/or magnesium-depleted residue claim 16 , the residue comprising less than 1.5 mass % of the extracted alkali metal and/or alkaline earth metal.19. The method according to claim 16 , wherein step d) comprises at least two of the processing steps mentioned.20. The method according to claim 19 , wherein the processing steps take place separately from one another in space and/or time.21. The method according to claim 16 , wherein the solid particles have a whiteness determined according to ...

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08-02-2018 дата публикации

Lithium complex oxide for lithium secondary battery positive active material and method of preparing the same

Номер: US20180040889A1
Принадлежит: Ecopro BM Co Ltd

Disclosed is a lithium complex oxide and method of manufacturing the same, more particularly, a lithium complex oxide effective in improving the characteristics of capacity, resistance, and lifetime with reduced residual lithium and with different interplanar distances of crystalline structure between a primary particle locating in an internal part of secondary particle and a primary particle locating on the surface part of the secondary particle, and a method of preparing the same.

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07-02-2019 дата публикации

MULTILAYERED GRAPHENE DISPERSION, BLACKENING AGENT FOR THERMOPHYSICAL PROPERTY MEASUREMENT, AND MOLD RELEASE AGENT/LUBRICANT FOR POWDER SINTERING

Номер: US20190039906A1
Автор: YANAGI Shohan

The present invention provides a multilayered graphene dispersion capable of instantaneously forming a thin uniform coating film containing multilayered graphene on the surface of a sample, a blackening agent for thermophysical property measurement excellent in a blackening effect, and a mold release agent/lubricant for powder sintering excellent in releasing and lubrication effects. The multilayered graphene dispersion of the present invention is characterized in that multilayered graphene is dispersed in a liquid phase containing an organic solvent and a liquefied gas. The blackening agent for thermophysical property measurement of the present invention is a blackening agent for forming a blackened film on the surface of a sample for thermophysical property measurement, and contains the multilayered graphene dispersion. The mold release agent/lubricant for powder sintering of the present invention is a mold release agent/lubricant for forming a separation layer between a sintering mold and a sintered body in powder sintering, and contains the multilayered graphene dispersion. 1. A multilayered graphene dispersion wherein multilayered graphene is dispersed in a liquid phase containing an organic solvent and a liquefied gas.2. The multilayered graphene dispersion according to claim 1 , wherein the multilayered graphene has a carbon purity of 90 mass % or more and a thickness of 1 nm to 10 nm.3. The multilayered graphene dispersion according to claim 1 , wherein the multilayered graphene has an average particle diameter of 1 μm to 10 μm.4. The multilayered graphene dispersion according to claim 1 , wherein the organic solvent contains a quick-drying solvent.5. The multilayered graphene dispersion according to claim 1 , comprising an organic polymer which is a dispersant of the multilayered graphene.6. The multilayered graphene dispersion according to claim 1 , wherein the multilayered graphene contains graphene oxide.7. A blackening agent for thermophysical property ...

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07-02-2019 дата публикации

Melted magnesium aluminate grain rich in magnesium

Номер: US20190039956A1
Автор: Stéphane RAFFY

A fused grain is essentially composed of a matrix of a magnesium aluminum oxide of MgAl2O4 spinel structure and/or of the MgO—MgAl2O4 eutectic structure, and of inclusions essentially composed of magnesium oxide. The grain has the following overall chemical composition, as percentages by weight, expressed in the form of oxides: more than 5.0% and less than 19.9% of Al2O3, Al2O3 and MgO together represent more than 95.0% of the weight of the grain. The cumulative content of CaO and of ZrO2 is less than 4000 ppm, by weight.

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06-02-2020 дата публикации

BORON NITRIDE AGGREGATED GRAIN, METHOD FOR PRODUCING SAME, AND THERMALLY CONDUCTIVE RESIN COMPOSITION USING SAME

Номер: US20200040245A1
Принадлежит:

A boron nitride powder includes boron nitride aggregated grains that are formed by aggregation of scaly hexagonal boron nitride primary particles, the boron nitride powder having the following characteristic properties (A) to (C): (A) the primary particles of the scaly hexagonal boron nitride have an average long side length of 1.5 μm or more and 3.5 μm or less and a standard deviation of 1.2 μm or less; (B) the boron nitride aggregated grains have a grain strength of 8.0 MPa or more at a cumulative breakdown rate of 63.2% and a grain strength of 4.5 MPa or more at a cumulative breakdown rate of 20.0%; and (C) the boron nitride powder has an average particle diameter of 20 μm or more and 100 μm or less. Also provided are a method for producing the same and a thermally conductive resin composition including the same. 1. A boron nitride powder comprising boron nitride aggregated grains that are formed by aggregation of scaly hexagonal boron nitride primary particles , the boron nitride powder having the following characteristics (A) to (C):(A) the primary particles of the scaly hexagonal boron nitride have an average long side length of 1.5 μm or more and 3.5 μm or less and a standard deviation of 1.2 μm or less;(B) the boron nitride aggregated grains have a grain strength of 8.0 MPa or more at a cumulative breakdown rate of 63.2% and a grain strength of 4.5 MPa or more at a cumulative breakdown rate of 20.0%; and(C) the boron nitride powder has an average particle diameter of 20 μm or more and 100 μm or less.2. The boron nitride powder according to claim 1 , wherein the average particle diameter of the boron nitride powder (C) is 30 μm or more and 80 μm or less.3. The boron nitride powder according to claim 1 , prepared by a method for producing a boron nitride powder characterized by the steps of:(a) pressure-nitridating and calcining a boron carbide having an average particle diameter of 6 μm or more and 55 μm or less and a carbon content of 18% or more and 21% or ...

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01-05-2014 дата публикации

Treated inorganic pigments having reduced photoactivity and improved anti-microbial properties and their use in polymer compositions

Номер: US20140121314A1
Автор: Charles David Musick
Принадлежит: EI Du Pont de Nemours and Co

The disclosure provides a polymer composition comprising a treated inorganic particle having improved photostability and improved anti-microbial properties, wherein the treated inorganic particle comprises: a inorganic core particle; a first treatment of a silicon compound, wherein the silicon compound is added in a single step; and a second treatment comprising a co-precipitated zinc oxide and alumina.

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07-02-2019 дата публикации

Topological quantum framework, composite anode active material, anode, lithium battery, semiconductor, and device comprising the topological quantum framework, and method of preparing the topological quantum framework

Номер: US20190044130A1
Принадлежит: SAMSUNG ELECTRONICS CO LTD

A topological quantum framework includes a plurality of one-dimensional nanostructures disposed in different directions and connected to each other, wherein a one-dimensional nanostructure of the plurality of one-dimensional nanostructures includes a first composition including a metal capable of incorporating and deincorporating lithium, and wherein the topological quantum framework is porous.

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06-02-2020 дата публикации

Core-shell composite particles for anode materials of lithium ion batteries

Номер: US20200044241A1
Принадлежит: Wacker Chemie AG

The invention relates to core-shell composite particles, the core being a porous, carbon-based matrix containing silicon particles and the shell being non-porous and being obtainable by the carbonization of one or more carbon precursors, the silicon particles having average particle sizes of 1 to 15 μm.

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06-02-2020 дата публикации

Oxide mixture and complex oxide coatings for cathode materials

Номер: US20200044242A1
Принадлежит: Apple Inc, UChicago Argonne LLC

Cathode active materials are provided. The cathode active material can include a plurality of cathode active compound particles. A coating is disposed over each of the cathode active compound particles. The coating can include at least one of ZrO2, La2O3, a mixture of Al2O3 and ZrO2 or a mixture of Al2O3 and La2O3. The battery cells that include the cathode active material are also provided.

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18-02-2016 дата публикации

Method for the use of slurries in spray pyrolysis for the production of non-hollow, porous particles

Номер: US20160049652A1

A process for preparing a metal oxide-containing powder that comprises conducting spray pyrolysis that comprises aerosolizing a slurry that comprises solidphase particles in a liquid that comprises at least one precursor compound, which comprises one or more metallic elements of at least one metal oxide, to form droplets of said slurry, and calcining the droplets to at least partially decompose the at least one precursor compound and form the metal oxide-containing powder having a non-hollow morphology.

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19-02-2015 дата публикации

Metal complex of fluorinated tin oxide and titanium oxide and preparation method thereof

Номер: US20150051069A1
Принадлежит: Korea Institute of Energy Research KIER

Disclosed is a metal complex including: a tin oxide; titanium oxide nanorods in a rutile phase formed on the tin oxide; and titanium oxide nanoparticles in an anatase phase formed on the titanium oxide nanorods in a rutile phase, and a preparation method thereof, and can be used as a catalyst support in various forms.

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03-03-2022 дата публикации

Titanium oxide powder and method for manufacturing same

Номер: US20220064016A1
Принадлежит: Tayca Corp

In producing titanium oxide containing rutile-type crystals by adding hydrochloric acid to an aqueous dispersion of an alkali metal titanate, sulfurous acid, disulfurous acid, sulfuric acid or a salt thereof is added. Thus, there is provided a titanium oxide powder which is doped with bivalent sulfur atoms (S 2− ) and in which a ratio (I A /I R ) of a peak intensity (I A ) of anatase-type crystals to a peak intensity (I R ) of rutile-type crystals as measured by X-ray diffractometry is 0.1 or less. Moreover, a cosmetic is provided by dispersing the titanium oxide powder in a dispersion medium. Thus, bluish color derived from Rayleigh scattering is negated, providing a dispersion, particularly a cosmetic, with excellent transparency and color tone.

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14-02-2019 дата публикации

Fibrous Structured Amorphous Silica Including Precipitated Calcium Carbonate and Compositions of Matter Made Therewith

Номер: US20190048197A1
Автор: MATHUR Vijay K.
Принадлежит: PACIFIC NANO PRODUCTS, INC.

A nano-composite structure. A synthetic nano-composite is described having a first component including a fibrous structured amorphous silica structure, and a second component including a precipitated calcium carbonate structure developed by pressure carbonation. The nano-composite may be useful for fillers in paints and coatings. Also, the nano-composite may be useful in coatings used in the manufacture of paper products. 1. A coating composition for coating paper , paperboard , or label stock , said coating composition comprising a water slurry including(a) a nano-composite material, said nano-composite material comprising an amorphous silica component, said amorphous silica component provided in three-dimensional haystack or globular configuration that presents a structure having interstitial spaces between amorphous silica structures with inner layers and outer layers with irregular interlacing amorphous silica structures or filaments which are fixed in relation to each other, and a crystalline calcium carbonate component, said crystalline calcium carbonate component comprising nano aragonite needle structures, said nano aragonite needle structures arising from said amorphous silica component, said nano-composite material having a major axis of length L in the range from 10 microns to 40 microns and a surface area of from 40 meters squared per gram to 200 meters squared per gram;(b) clay; and(c) wherein said coating composition, after mixing, passes through a screen of selected size.2. The coating composition as set forth in wherein said nano aragonite needle structures comprise aragonite crystals having a length of from 1 micron to 10 microns.3. The coating composition as set forth in claim 2 , wherein said nano aragonite crystals have a length of from 3 microns to 5 microns.4. The coating composition as set forth in claim 1 , wherein said nano aragonite needle structures comprise aragonite crystals having a diameter of from 100 nm to 200 nm.5. The coating ...

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14-02-2019 дата публикации

Additive for incorporating ultraviolet radiation protection into a polymer

Номер: US20190048198A1
Принадлежит: Sweet Living Group LLC

An additive for incorporating ultraviolet radiation protection into a synthetic polymer with the additive and the synthetic polymer for forming a synthetic material is disclosed which has a quantity of zinc oxide particles modified with a layer of a reactive group that forms a bond with a synthetic polymer having C—H bonds. A product for incorporating ultraviolet radiation protection into a synthetic polymer prior to forming a synthetic material has a quantity of a synthetic polymer and a quantity of zinc oxide particles modified with a layer of a reactive group that forms a bond with the quantity of the synthetic polymer.

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25-02-2021 дата публикации

Semiconductor nanoparticles and core/shell semiconductor nanoparticles

Номер: US20210054273A1
Принадлежит: Shoei Chemical Inc

An object of the present invention is to provide semiconductor nanoparticles having high quantum efficiency (QY) and a narrow full width at half maximum (FWHM). Semiconductor nanoparticles according to an embodiment of the present invention are semiconductor nanoparticles including at least, In, P, Zn and S, wherein the semiconductor nanoparticles include the components other than In in the following ranges: 0.50 to 0.95 for P, 0.30 to 1.00 for Zn, 0.10 to 0.50 for S, and 0 to 0.30 for halogen, in terms of molar ratio with respect to In.

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13-02-2020 дата публикации

BURNERS FOR CONVERSION OF METHANE TO OLEFINS, AROMATICS, AND NANOPARTICLES

Номер: US20200049346A1
Принадлежит:

Embodiments of the present disclosure describe burner () configurations used in an industrial process to convert methane to olefins, aromatics, and nanoparticles/nanomaterials. Both a vitiated coflow burner and piloted turbulent burner with inhomogeneous inlets are disclosed. 1. A method of controlling secondary reactions of a burner of combustion products using injected methane , the method comprising:establishing a jet flame in coaxial flow of hot combustion products from a premixed vitiated coflow of gas passing through a porous plate or catalytic monolith, said jet flame established by gas exiting from a central tube;providing a tube positioner to translate the tip of the central tube to an offset height relative to the porous plate or catalytic monolith; andcontrolling the tube positioner to vary the offset height of the central tube tip in a dynamic manner based on chemical inputs, with said controlling resulting in different secondary reactions of combustion products from the burner.2. The method of claim 1 , wherein the central tube is a blunt-tipped tube and the gas exiting the central tube is methane.3. The method of claim 1 , wherein the coflow gas is a combination of methane and oxygen.4. The method of claim 1 , wherein offset height of the central tube tip is controlled to provide both a methane/oxygen combustion process and subsequent pyrolysis of methane to form olefins claim 1 , aromatics or nanoparticles.5. A method of controlling secondary reactions of a burner of combustion products using injected methane claim 1 , the method comprising:establishing a jet flame in coaxial flow of hot combustion products from gas passing through a porous plate or catalytic monolith, with said jet flame established by a piloted turbulent burner with inhomogeneous inlets and defining three concentric tubes;providing a tube positioner to translate an innermost one of the three concentric tubs to different positions relative to an intermediate tube; andcontrolling the ...

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14-02-2019 дата публикации

POSITIVE ACTIVE MATERIAL, POSITIVE ELECTRODE AND LITHIUM BATTERY INCLUDING THE POSITIVE ACTIVE MATERIAL, AND METHOD OF MANUFACTURING THE POSITIVE ACTIVE MATERIAL

Номер: US20190051895A1
Принадлежит:

A positive active material, a method of preparing the positive active material, a positive electrode including the positive active material, and a lithium battery including the positive active material are disclosed. The positive active material includes a core including a lithium metal composite oxide and a coating layer formed on the core. The coating layer includes at least one of lithium fluoride (LiF) and lithium phosphate (LiPO). In this regard, the coating layer may improve the stability of the positive active material, and accordingly, the lifespan properties of a lithium battery including the positive active material may be improved. 1. A method of preparing a positive active material , the method comprising:providing a core that comprises a lithium metal composite oxide comprising free lithium; and{'sub': 3', '4, 'coating a surface of the core with at least one of a fluoride compound and a phosphate compound to form a coating layer comprising at least one of LiF and LiPO.'}2. The method of claim 1 , wherein LiF is a resultant product of a reaction between the free lithium and the fluoride compound and LiPOis a resultant product of a reaction between the free lithium and the phosphate compound.3. The method of claim 1 , wherein the fluoride compound is selected from NHF claim 1 , NHHF claim 1 , NHPF claim 1 , AlF claim 1 , MgF claim 1 , CaF claim 1 , MnF claim 1 , FeF claim 1 , CoF claim 1 , CoF claim 1 , NiF claim 1 , TiF claim 1 , CuF claim 1 , and ZnF claim 1 , or a combination thereof claim 1 , and the phosphate compound is selected from NHHPO claim 1 , (NH)HPO claim 1 , PO claim 1 , PO claim 1 , HPO claim 1 , MgHPO claim 1 , Mg(PO) claim 1 , Mg(HPO) claim 1 , NHMgPO claim 1 , AlPO claim 1 , FePO claim 1 , and Zn(PO) claim 1 , or a combination thereof.4. The method of claim 1 , further comprising claim 1 , after forming the coating layer claim 1 , heat-treating the core on which the coating layer is formed. Any and all applications for which a foreign ...

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10-03-2022 дата публикации

METHOD FOR MANUFACTURING SECONDARY BATTERY AND SECONDARY BATTERY

Номер: US20220073367A1
Принадлежит:

The present invention relates to a method for manufacturing a secondary battery and a secondary battery. A method for manufacturing a positive electrode active material with high charge and discharge capacity is provided. A method for manufacturing a positive electrode active material with high charging and discharging voltages is provided. A method for manufacturing a positive electrode active material with little deterioration is provided. The positive electrode active material is manufactured through a step of forming a composite oxide that contains lithium, nickel, manganese, cobalt, and oxygen; and a step of mixing the composite oxide and a calcium compound, and then heating the mixture at a temperature higher than or equal to 500° C. and lower than or equal to 1100° C. for 2 hours to 20 hours. By the heating, calcium is distributed at a preferred concentration in a surface portion of the positive electrode active material. 1. A method for manufacturing a secondary battery , comprising:forming a composite oxide comprising lithium, nickel, manganese, cobalt, and oxygen; andmixing the composite oxide and a calcium compound, and then performing heating at a temperature higher than or equal to 500° C. and lower than or equal to 1100° C. for a time longer than or equal to 2 hours and shorter than or equal to 20 hours.2. The method for manufacturing a secondary battery claim 1 , according to claim 1 ,wherein the calcium compound is calcium carbonate or calcium fluoride.3. The method for manufacturing a secondary battery claim 1 , according to claim 1 ,wherein when a sum of the number of atoms of the nickel, the manganese, and the cobalt included in the composite oxide is 100, the number of atoms of the nickel is greater than or equal to 50.4. A secondary battery comprising a positive electrode claim 1 ,wherein the positive electrode comprises a positive electrode active material,wherein the positive electrode active material comprises lithium, nickel, manganese, ...

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21-02-2019 дата публикации

AMORPHOUS AND POROUS ALKALI METAL CHALCOGENIDES FOR REMEDIATION APPLICATIONS

Номер: US20190055136A1
Принадлежит:

Amorphous metal chalcogenides having the formula ASnSbQare provided. In the chalcogenides, A is an alkali metal element, such as K or Cs, and Q is S or Se. The value of x can be in the range from 0.8 to 1. Porous chalcogenide materials made from the amorphous chalcogenides are also provided. These porous materials comprise metal chalcogenides having the formula (AB)SnSbQ, wherein x is in the range from 0.8 to 1, A and B are two different alkali metal elements, and Q is S or Se. 1. An amorphous metal chalcogenide having the formula ASnSbQ , wherein x is in the range from 0.8 to 1 , A is an alkali metal element , and Q is S or Se.2. The amorphous metal chalcogenide of claim 1 , wherein Q is S.3. The amorphous metal chalcogenide of claim 1 , wherein A is K or Cs.4. The amorphous metal chalcogenide of claim 1 , wherein the metal chalcogenide has the formula KSnSbS claim 1 , CsSnSbS claim 1 , or KSnSbSe.5. A porous material comprising a chalcogenide having the formula AMM′Q claim 1 , where A is an alkali metal element or a mixture of two or more alkali metal elements; M and M′ are main group metal elements or elements from groups 14 or 15 of the periodic table of the elements; Q is S claim 1 , Se or Te; x′ claim 1 , y claim 1 , and z are independently selected from values in the range from 0 to 10 claim 1 , and m is in the range from 1 to 20 claim 1 , wherein the material includes pores having pore sizes in the range from 200 nm to 10 μm.6. The porous material of claim 5 , wherein the material includes pores having sizes of at least 10 μm.7. The porous material of claim 5 , wherein the material includes pores having sizes of at least 100 μm.8. The porous material of claim 5 , wherein M is Sn and M′ is Sb.9. The material of claim 5 , wherein the chalcogenide has the formula (AB)SnSbQ claim 5 , wherein x is in the range from 0.8 to 1 claim 5 , A and B are two different alkali metal elements claim 5 , and Q is S or Se.10. The material of claim 9 , wherein Q is S.11. The ...

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04-03-2021 дата публикации

TITANIUM OXIDE POWDER, AND DISPERSION LIQUID AND COSMETIC USING SAID POWDER

Номер: US20210061669A1
Принадлежит: Sumitomo Osaka Cement Co., Ltd.

The titanium oxide powder of the present invention is a titanium oxide powder which has a BET specific surface area of 5 m/g or more and 15 m/g or less, and contains octahedral-shaped particles, wherein each octahedral-shaped particle thereof has line segments each of which connects two apexes which face each other and has a maximum value of the line segments, an average value of the maximum values is 300 nm or higher and 1000 nm or lower, and a value (D90/D10) is 1 or higher and 3 or lower, wherein the value is obtained by dividing a value (D90), which corresponds to 90% in a cumulative number percentage of the maximum values of line segments each of which connects two apexes which face each other, by a value (D10) which corresponds to 10% in the cumulative number percentage. 1. A titanium oxide powder , which has a BET specific surface area of 5 m/g or more and 15 m/g or less , and contains octahedral-shaped particles , whereineach octahedral-shaped particle thereof has line segments each of which connects two apexes which face each other and has a maximum value of the line segments,an average value of the maximum values is 300 nm or higher and 1,000 nm or lower, anda value (D90/D10) is 1 or higher and 3 or lower, wherein the value is obtained by dividing a value (D90), which corresponds to 90% in a cumulative number percentage of the maximum values of line segments each of which connects two apexes which face each other, by a value (D10) which corresponds to 10% in the cumulative number percentage.2. The titanium oxide powder according to claim 1 ,wherein a value (average value of the maximum values/BET-converted average particle diameter), which is obtained by dividing the average value of the maximum values of the line segments by an average particle diameter converted from the BET specific surface area, is 0.5 or higher and 2.5 or lower.3. The titanium oxide powder according to claim 1 ,wherein a content of the octahedral-shaped particles in the titanium oxide ...

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20-02-2020 дата публикации

METHODS FOR MODIFYING SILICON PARTICLES

Номер: US20200055737A1
Принадлежит:

The invention relates to methods for producing non-aggregated, modified silicon particles by treating non-aggregated silicon particles which have volume-weighted particle size distributions with diameter percentiles dof 1.0 μm to 10.0 μm at 80° C. to 900° C. with an oxygen-containing gas. 1. A method for producing nonaggregated , modified silicon particles , comprising:{'sub': '50', 'treating nonaggregated silicon particles having volume-weighted particle size distributions having diameter percentiles dof 3.0 μm to 7.0 μm with an oxygen-containing gas at 80° C. to 900° C., with the proviso that the oxygen content of the nonaggregated, modified silicon particles is 0.05% to 0.6% by weight greater than the oxygen content of the nonaggregated silicon particles used as reactant in each case based on the total weight of the silicon particles.'}2. The method for producing nonaggregated claim 1 , modified silicon particles of claim 1 , wherein the oxygen-containing gas contains 1 to 100 vol % claim 1 , in particular ≥5 vol % claim 1 , of oxygen based on the total volume of the oxygen-containing gas.3. The method for producing nonaggregated claim 2 , modified silicon particles of claim 2 , wherein the treatment with an oxygen-containing gas is carried out at 400° C. to 800° C.4. The method for producing nonaggregated claim 2 , modified silicon particles of claim 2 , wherein the treatment with an oxygen-containing gas is carried out at 80° C. to 400° C.5. The method for producing nonaggregated claim 1 , modified silicon particles of claim 1 , wherein the nonaggregated silicon particles used as reactant contain ≤2.0% by weight of oxygen based on the total weight of the nonaggregated silicon particles used as reactant.6. The method for producing nonaggregated claim 1 , modified silicon particles of claim 1 , wherein the nonaggregated claim 1 , modified silicon particles contain 0.1% to 3.0% by weight of oxygen based on the total weight of the nonaggregated claim 1 , modified ...

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02-03-2017 дата публикации

Paper, Paperboard, Or Label Stock Coated With Fibrous Structured Amorphous Silica Including Precipitated Calcium Carbonate

Номер: US20170058458A1
Автор: MATHUR Vijay K.
Принадлежит: PACIFIC NANO PRODUCTS, INC.

Paper, paperboard, or label stock coated with a synthetic nano-composite coating. A synthetic nano-composite coating includes a first component including a fibrous structured amorphous silica structure, and a second component including a precipitated calcium carbonate structure developed by pressure carbonation. 1. A coated , calendared , paperboard , comprising:(a) one or more layers of kraft pulp; (1) a nano-composite material, said nano-composite material comprising a fibrous amorphous silica component, said fibrous amorphous silica component provided in three-dimensional haystack or globular configuration that presents a fibrous structure having interstitial spaces between amorphous silica fibers with inner layers and outer layers with irregular interlacing amorphous silica fibers or filaments which are fixed in relation to each other, and a crystalline calcium carbonate component, said crystalline calcium carbonate component comprising aragonite needle structures, said aragonite needle structures arising from said fibrous amorphous silica component, said nano-composite material having a major axis of length L in the range from about 10 microns to about 40 microns and a surface area of from about 40 meters squared per gram to about 200 meters squared per gram;', '(2) clay;', '(3) one or more binders, said one or more binders including a selected latex, and/or including a selected protein., '(b) a base coating, said base coating comprising a coating composition including'}2. The coated claim 1 , calendared paperboard as set forth in claim 1 , further comprising a top coating claim 1 , wherein said top coating comprises:(1) a nano-composite material, said nano-composite material comprising a fibrous amorphous silica component, said fibrous amorphous silica component provided in three-dimensional haystack or globular configuration that presents a fibrous structure having interstitial spaces between amorphous silica fibers with inner layers and outer layers with ...

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20-02-2020 дата публикации

HOLLOW STRUCTURE PARTICLES, METHOD FOR PRODUCING SAME AND WHITE INK

Номер: US20200056060A1
Принадлежит:

Hollow structure particles which contain titanium oxide and silica, in which the crystal type of the titanium oxide is rutile type; a method for producing the hollow structure particles; a white ink which contains these hollow structure particles as a coloring agent; use of the white ink in inkjet recording; and an inkjet recording method which uses the white ink. 1. A hollow structure particle comprising titanium oxide and silica , wherein the crystal form of the titanium oxide is rutile.2. The hollow structure particle according to claim 1 , wherein a primary particle diameter B is 10 nm to 1 claim 1 ,000 nm.3. The hollow structure particle according to claim 1 , wherein a ratio of inner diameter A of a hollow structure to the primary particle diameter B claim 1 , A/B claim 1 , is 0.3 to 0.95.4. The hollow structure particle according to claim 1 , further comprising an element other than titanium oxide and silica.5. A method of producing a hollow structure particle claim 1 , comprising:forming a shell containing a titanium oxide precursor on a surface of a template particle, which becomes a core, to obtain a first core/shell particle;applying a silica precursor to a surface of the first core/shell particle to obtain a second core/shell particle;removing the template particle from the second core/shell particle to obtain a shell particle; and{'claim-ref': {'@idref': 'CLM-00001', 'claim 1'}, 'firing the shell particle to obtain the hollow structure particle according to .'}6. A method of producing a hollow structure particle claim 1 , comprising:forming a shell containing a titanium oxide precursor on a surface of a template particle which becomes a core, to obtain a first core/shell particle,applying a silica precursor to the surface of the first core/shell particle to obtain a second core/shell particle, and{'claim-ref': {'@idref': 'CLM-00001', 'claim 1'}, 'firing the second core/shell particle to remove the template particle to obtain the hollow structure ...

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01-03-2018 дата публикации

Coated positive electrode materials for lithium ion batteries

Номер: US20180062170A1
Принадлежит: Zenlabs Energy Inc

High specific capacity lithium rich lithium metal oxide materials are coated with inorganic compositions, such as metal fluorides, to improve the performance of the materials as a positive electrode active material. The resulting coated material can exhibit an increased specific capacity, and the material can also exhibit improved cycling. The materials can be formed while maintaining a desired relatively high average voltage such that the materials are suitable for the formation of commercial batteries. Suitable processes are described for the synthesis of the desired coated compositions that can be adapted for commercial production.

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04-03-2021 дата публикации

MAGNETIC PARTICLES, METHODS OF MAKING, AND USES THEREOF

Номер: US20210065943A1
Автор: CHEN Yajie, Zhang Li
Принадлежит:

In an aspect, a composition comprises a plurality of magnetic particles. The magnetic particles each independently comprise a nickel ferrite core having the formula NiMPeO, wherein M is at least one of Zn, Mg, Co, Cu, Al, Mn, or Cr; x is 0 to 0.95, and y=−0.5 to 0.5; and an iron nickel shell at least partially surrounding the core, wherein the iron nickel shell comprises iron, nickel, and optionally M. In another aspect, a method of forming the magnetic particles comprises heat treating a plurality of nickel ferrite particles in a hydrogen atmosphere to form the plurality of magnetic particles having the iron nickel shell on the nickel ferrite core. In yet another aspect, a composite can comprise the magnetic particles and a polymer. 1. A composition , comprising: [{'sub': 1−x', 'x', '2+y', '4, 'a nickel ferrite core having the formula NiMFeO, wherein M is at least one of Zn, Mg, Co, Cu, Al, Mn, or Cr; x is 0 to 0.95, and y=−0.5 to 0.5; and'}, 'an iron nickel shell at least partially surrounding the core, wherein the iron nickel shell comprises iron, nickel, and optionally M., 'a plurality of magnetic particles, wherein the magnetic particles each independently comprise'}2. The composition of claim 1 , wherein M comprises at least one of Zn or Co.3. The composition of claim 1 , wherein the nickel ferrite core has an average grain size of 5 to 100 nanometers.4. The composition of claim 1 , wherein x is 0.05 to 0.95.5. The composition of claim 1 , wherein M comprises at least one of Co or Zn.6. The composition of claim 1 , wherein the shell is free of oxygen.7. The composition of claim 1 , wherein the plurality of magnetic particles comprises at least one of irregularly-shaped particles claim 1 , spherical particles claim 1 , oval particles claim 1 , rod-shaped particles claim 1 , flakes claim 1 , or fibers.8. The composition of claim 1 , wherein the plurality of magnetic particles has a median D50 particle size of 0.5 to 800 micrometers.9. The composition of claim 1 ...

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27-02-2020 дата публикации

METHOD OF MANUFACTURING SEMICONDUCTOR MATERIAL FROM MAYENITE

Номер: US20200062606A1
Принадлежит:

A method of preparation of semiconductor material. The method includes: adding an organic substance containing a benzene ring and dodecacalcium hepta-aluminate (12CaO.7AlOor C12A7) to a test tube, and sealing the test tube; heating the test tube to a temperature of 200-300° C., and holding the temperature for 1 to 3 hours; and continuously heating the test tube to a temperature of 900-1300° C., and holding the temperature for 10-120 hours. 1. A method , comprising:(1) adding an organic substance containing a benzene ring and dodecacalcium hepta-aluminate (C12A7) to a test tube, and sealing the test tube;(2) heating the test tube to a temperature of 200-300° C., and holding the temperature for 1 to 3 hours; and(3) continuously heating the test tube to a temperature of 900-1300° C., and holding the temperature for 10-120 hours.2. The method of claim 1 , wherein the dodecacalcium hepta-aluminate is a monocrystalline or polycrystalline material.3. The method of claim 2 , wherein the polycrystalline material of the dodecacalcium hepta-aluminate is prepared as follows:weighing calcium nitrate tetrahydrate and aluminum nitrate nonahydrate according to a stoichiometric ratio thereof of 12 to 14; weighing urea which is three times a total stoichiometry of the calcium nitrate tetrahydrate and the aluminum nitrate nonahydrate, mixing and stirring the calcium nitrate tetrahydrate, the aluminum nitrate nonahydrate, and the urea with deionized water, to form a transparent solution;transferring the transparent solution to a corundum crucible, heating a muffle furnace to 500° C., calcining the corundum crucible in the muffle furnace for 2 hours, and cooling the muffle furnace, to yield polycrystalline C12A7 powders; andpressing the polycrystalline C12A7 powders into a tablet having a thickness of 0.5-0.8 mm under a pressure of 100-200 megapascal.4. The method of claim 2 , wherein the monocrystalline material of the dodecacalcium hepta-aluminate is prepared using a floating zone (FZ ...

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11-03-2021 дата публикации

A Method for Manufacturing a Nanoparticle Material and a Fluoride Ion Battery

Номер: US20210070626A1
Принадлежит: Ambercon Technology (UK) Ltd

A method is provided for manufacturing a nanoparticle material having an ionic conductivity as a battery material for Fluoride ion Batteries, thus, being capable for overcoming high resistances at the surfaces, grain-boundaries of nanoparticles or compartments of the nanoparticles by a material treatment selected from: (i) a ball-mill procedure under aerosol and/or vapour-pressure atmosphere, (ii) excess-synthesis, (iii) ball-milling with surface stabilizing and conductivity enhancing solid or/and gel/liquid additives or (iv) functionalizing the material to obtain functionalized nanoparticles (GSNP) comprising a dispersion of graphene, nanotubes and/or a further additive selected from carbon-black, graphite, Si and/or CF, Herein, fluorides (EmF), fluorides composites (Em1Em2. . . F) are synthesized, wherein a first metal, metalloid or non-metal Em or Em1 and a second metal, metalloid or non-metal Em2 are dissimilarly selected from various elements in a manner that a battery material having an increased ionic conductivity is obtained. 1. A method for manufacturing a nanoparticle material having an ionic conductivity as a battery material for a Fluoride Ion Battery , the method comprising the step of providing a fluoride compound , the fluoride compound comprising fluorine and at least one metal , metalloid or non-metal ,wherein the fluoride compound is subjected to an aerosol and/or vapour-pressure atmosphere and treated in a ball-mill procedure; and/orwherein the fluoride compound is synthesized by applying an excess synthesis, wherein the excess synthesis comprises a chemical reaction using a stoichiometric overplus of a fluoride precursor and/or wherein the fluoride compound is synthesized by applying at least one surface-stabilizing and conductivity-enhancing solid or/and gel/liquid additive,whereby the battery material having an increased ionic conductivity is obtained.2. The method of claim 1 , wherein a fluoride compound of formula EmF claim 1 , wherein ...

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17-03-2022 дата публикации

METHOD FOR FORMING A COMPOSITE HAVING SEMICONDUCTOR STRUCTURES INCLUDING A NANOCRYSTALLINE CORE AND SHELL EMBEDDED IN A MATRIX

Номер: US20220085254A1
Принадлежит:

Semiconductor structures having a nanocrystalline core and corresponding nanocrystalline shell and insulator coating, wherein the semiconductor structure includes an anisotropic nanocrystalline core composed of a first semiconductor material, and an anisotropic nanocrystalline shell composed of a second, different, semiconductor material surrounding the anisotropic nanocrystalline core. The anisotropic nanocrystalline core and the anisotropic nanocrystalline shell form a quantum dot. An insulator layer encapsulates the nanocrystalline shell and anisotropic nanocrystalline core. 1. A lighting apparatus , comprising:a light emitting diode; anda composite coating the light emitting diode, the composite comprising a matrix material; and a quantum dot comprising a nanocrystalline core comprising a first semiconductor material and a nanocrystalline shell comprising a second, different, semiconductor material at least partially surrounding the nanocrystalline core, the quantum dot having a photoluminescence quantum yield (PLQY) of at least 90%; and', 'an insulator layer encapsulating the quantum dot., 'a plurality of semiconductor structures embedded in the matrix material, each semiconductor structure comprising2. The lighting apparatus of claim 1 , wherein emission from each quantum dot is mostly claim 1 , or entirely claim 1 , from the nanocrystalline core.3. The lighting apparatus of claim 2 , wherein emission from the nanocrystalline core is at least approximately 75% of the total emission from the quantum dot.4. The lighting apparatus of claim 1 , wherein an absorption spectrum and an emission spectrum of each quantum dot are essentially non-overlapping.5. The lighting apparatus of claim 1 , wherein an absorbance ratio of each quantum dot for absorbance at 400 nanometers versus absorbance at an exciton peak for the quantum dot is approximately in the range of 5-35.6. The lighting apparatus of claim 1 , wherein each quantum dot is a down-converting quantum dot.7. The ...

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28-02-2019 дата публикации

Dielectric powder and multilayer ceramic electronic component using the same

Номер: US20190066920A1
Принадлежит: Samsung Electro Mechanics Co Ltd

A multilayer ceramic electronic component includes: a body part including dielectric layers and internal electrodes disposed to face each other with respective dielectric layers interposed therebetween; and external electrodes disposed on an outer surface of the body part and electrically connected to the internal electrodes. The dielectric layer includes grains including: a semiconductive or conductive grain core region containing a base material represented by ABO 3 , where A is at least one of Ba, Sr, and Ca, and B is at least one of Ti, Zr, and Hf, and a doping material including a rare earth element; and an insulating grain shell region enclosing the grain core region.

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08-03-2018 дата публикации

LITHIUM-IRON-MANGANESE-BASED COMPOSITE OXIDE AND LITHIUM-ION SECONDARY BATTERY USING SAME

Номер: US20180069236A1
Принадлежит:

There is provided a lithium-iron-manganese-based composite oxide capable of providing a lithium-ion secondary battery which has a high capacity retention rate in charge/discharge cycles and in which the generation of a gas caused by charge/discharge cycles is suppressed. A lithium-iron-manganese-based composite oxide having a layered rock-salt structure, wherein at least a part of the surface of a lithium-iron-manganese-based composite oxide represented by the following formula is coated with an oxide of at least one metal selected from the group consisting of La, Pr, Nd, Sm and Eu: 1. A lithium-iron-manganese-based composite oxide having a layered rock-salt structure , wherein at least a part of a surface of a lithium-iron-manganese-based composite oxide represented by the following formula (1) is coated with an oxide of at least one metal selected from the group consisting of La , Pr , Nd , Sm and Eu:{'br': None, 'sub': x', '(y-p)', 'p', '(z-q)', 'q', '(2-δ), 'sup': 1', '2, 'LiMMnMFeO'}{'sup': 1', '2, 'wherein 1.05≦x≦1.32, 0.33≦y≦0.63, 0.06≦z≦0.50, 0<≦p≦0.63, 0.06≦q≦0.50, 0≦δ≦0.80, y≧p, and z≧q; Mis at least one element selected from Ti and Zr; and Mis at least one element selected from the group consisting of Co, Ni and Mn.'}2. The lithium-iron-manganese-based composite oxide according to claim 1 , wherein at least a part of a surface of the lithium-iron-manganese-based composite oxide is coated with a mixture of an oxide of at least one metal selected from the group consisting of La claim 1 , Pr claim 1 , Nd claim 1 , Sm and Eu and an oxide of at least one metal selected from the group consisting of Ge claim 1 , Mo claim 1 , Zr claim 1 , Al and V.3. A lithium-iron-manganese-based composite oxide having a layered rock-salt structure claim 1 , wherein at least a part of a surface of a lithium-iron-manganese-based composite oxide represented by the following formula (1) is coated with a composite oxide of at least one metal selected from the group consisting of La ...

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28-02-2019 дата публикации

POSITIVE ELECTRODE ACTIVE MATERIAL AND ALKALINE BATTERY

Номер: US20190067687A1
Принадлежит:

An objective of the present invention is to provide a positive electrode active material that can inhibit the capacity changes associated with temperature variations, and an alkaline battery that contains this positive electrode active material. Aluminum and ytterbium are at least partially solid-dissolved in nickel hydroxide in the nickel composite hydroxide present in the positive electrode active material of the present invention. 1. A positive electrode active material containing a nickel composite hydroxide in which aluminum and ytterbium are at least partially solid-dissolved in nickel hydroxide.2. The positive electrode active material according to claim 1 , wherein the nickel composite hydroxide is represented by the following formula (I):{'br': None, 'sub': a', 'b', 'c', 'd, 'NiAlYb(OH)\u2003\u2003(I)'} a+b+c=1.00,', '0.70≤a<1.00,', '0 Подробнее

28-02-2019 дата публикации

CATHODE ACTIVE MATERIAL, METHOD FOR MANUFACTURING SAME, AND LITHIUM SECONDARY BATTERY COMPRISING SAME

Номер: US20190067694A1

A method for manufacturing a positive active material is provided. The method includes forming a positive active material precursor including nickel, mixing and firing the positive active material precursor and lithium salt to form a preliminary positive active material particle, forming a coating material including fluorine on the preliminary positive active material particle by dry-mixing the preliminary positive active material particle with a coating source including fluorine, and manufacturing a positive active material particle by thermally treating the preliminary positive active material particle on which the coating material is formed. 1. A method for manufacturing a positive active material , the method comprising:forming a positive active material precursor including nickel;mixing and firing the positive active material precursor and lithium salt to form a preliminary positive active material particle;forming a coating material including fluorine on the preliminary positive active material particle by dry-mixing the preliminary positive active material particle with a coating source including fluorine; andmanufacturing a positive active material particle by thermally treating the preliminary positive active material particle on which the coating material is formed.2. The method of claim 1 , wherein the preliminary positive active material particle is dry-mixed with the coating source such that surface residual lithium of the preliminary positive active material particle is reduced.3. The method of claim 1 , wherein the amount of surface residual lithium of the positive active material particle is less than the amount of surface residual lithium of the preliminary positive active material particle dry-mixed with the coating source.4. The method of claim 1 , wherein the coating material reacts with surface residual lithium of the preliminary positive active material particle by the thermal treating of the preliminary positive active material particle to ...

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27-02-2020 дата публикации

Magnetic recording medium

Номер: US20200066302A1
Принадлежит: Sony Corp

Provided is a magnetic recording medium including: a recording layer containing a powder of particles containing ε iron oxide, in which a ratio ((Hc(50)/Hc(25))×100) of a coercive force Hc(50) measured in a thickness direction of the magnetic recording medium at 50° C. and a coercive force Hc(25) measured in the thickness direction of the magnetic recording medium at 25° C. is 95% or greater, the coercive force Hc(25) is 200 kA/m or greater, and a squareness ratio measured in a transport direction of the magnetic recording medium is 30% or less.

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