15-09-2022 дата публикации
Номер: US20220289672A1
The present invention relates to a hydrated crystalline form of 2-acrylamido-2-methylpropane sulfonic acid having a 2-theta powder X-ray diffraction diagram comprising peaks at 10.58°, 11.2°, 12.65°, 13.66°, 16.28°, 18.45°, 20°, 20.4°, 22.5°, 25.5°, 25.88°, 26.47°, 28.52°, 30.28°, 30.8°, 34.09°, 38.19°, 40.69°, 41.82°, 43.74°, 46.04° degrees (+/−0.1°). 1. A (co)polymer of 2-acrylamido-2-methylpropanesulfonic acid , in its acidic and/or salified form ,wherein at least a portion of the 2-acrylamido-2-methylpropanesulfonic acid is in hydrated crystalline form and has a powder X-ray diffraction pattern including peaks at 10.58°, 11.2°, 12.65°, 13.66°, 16.28°, 18.45°, 20°, 20.4°, 22.5°, 25.5°, 25.88°, 26.47°, 28.52°, 30.28°, 30.8°, 34.09°, 38.19°, 40.69°, 41.82°, 43.74°, and 46.04° degrees 2-theta, all peak values being +/−0.1°.2. The (co)polymer according to claim 1 , wherein the (co)polymer comprises one or more additional monomers selected from the group consisting of non-ionic monomers claim 1 , cationic monomers claim 1 , zwitterionic monomers claim 1 , anionic monomers distinct from 2-acrylamido-2-methylpropanesulfonic acid being in hydrated crystalline form and having a powder X-ray diffraction pattern including peaks at 10.58° claim 1 , 11.2° claim 1 , 12.65° claim 1 , 13.66° claim 1 , 16.28° claim 1 , 18.45° claim 1 , 20° claim 1 , 20.4° claim 1 , 22.5° claim 1 , 25.5° claim 1 , 25.88° claim 1 , 26.47° claim 1 , 28.52° claim 1 , 30.28° claim 1 , 30.8° claim 1 , 34.09° claim 1 , 38.19° claim 1 , 40.69° claim 1 , 41.82° claim 1 , 43.74° claim 1 , and 46.04° degrees 2-theta claim 1 , all peak values being +/−0.1° claim 1 , and mixtures thereof.3. The (co)polymer according to claim 1 , wherein the (co)polymer is a copolymer of the hydrated crystalline form of 2-acrylamido-2-methylpropanesulfonic acid and at least one non-ionic monomer.4. The (co)polymer according to claim 1 , wherein the (co)polymer is a copolymer of the hydrated crystalline form of 2-acrylamido-2- ...
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