07-01-2021 дата публикации
Номер: US20210002177A1
Принадлежит:
A ceramic material, including: BaWO-xMCO-yBaO-zBO-wSiO, where x=0-0.2 mole, y=0-0.05 mole, z=0-0.2 mole, w=0-0.1 mole, M represents an alkali metal ion selected from Li, K, Na, and x, y, z, and w are not zero at the same time. 1. A ceramic material , comprising: BaWO-xMCO-yBaO-zBO-wSiO , wherein x=0-0.2 mole , y=0-0.05 mole , z=0-0.2 mole , w=0-0.1 mole , M represents an alkali metal ion selected from Li , K , Na , and x , y , z , and w are not zero at the same time.2. A method , comprising:{'sub': 3', '3', '2', '3', '2', '3', '2', '4', '2', '3', '2', '3', '2, 'sup': +', '+', '+, '1) weighing and mixing BaCO, WO, MCO, BOand SiObased on a chemical formula BaWO-xMCO-yBaO-zBO-wSiO, wherein x=0-0.2 mole, y=0-0.05 mole, z=0-0.2 mole, w=0-0.1 mole, M represents an alkali metal ion selected from Li, K, Na, and x, y, z, and w are not zero at the same time, to yield a first powder;'}2) mixing the first powder obtained in 1), zirconia balls, and deionized water according to a mass ratio of 1:5:1-2, ball-milling for 4-7 h, drying at 80-120° C., sieving with a 40-60 mesh sieve, calcining in air atmosphere at 700-900° C. for 2-4 h, to yield a second powder;3) mixing the second powder obtained in 2), zirconia balls, and deionized water according to a mass ratio of 1:5:1-2, ball-milling for 3-6 h, drying, to yield a third powder, and adding a binder to the third powder; and4) compression molding a resulting product obtained in 3) under a pressure of 20 megapascal, drying at 400-500° C. and sintering at 850° C.-900° C. for 0.5-2 h.3. The method of claim 2 , wherein the binder is an acrylic solution. Pursuant to 35 U.S.C. § 119 and the Paris Convention Treaty, this application claims foreign priority to Chinese Patent Application No. 201910603226.3 filed Jul. 5, 2019, the contents of which, including any intervening amendments thereto, are incorporated herein by reference. Inquiries from the public to applicants or assignees concerning this document or the related applications ...
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