Металлические соединения каликсаренов, содержащие их моющие составы и их применение в составах смазочных масел

Настоящее изобретение относится к продукту для применения в моющих составах, содержащему смесь металлических соединений каликсарена, не содержащего серы и диспергируемого в масле, которые могут быть частично представлены в виде соли, или быть нейтральными, или основными, или сверхосновными. Указанный каликсарен имеет общую формулу (I)в которой a) R, R, Rи Rнезависимо выбраны из водорода или линейного или разветвленного алкила с числом атомов углерода от 6 до 18; b) Rи Rпредставляют атомы водорода; c) n - число звеньев каликсаренового кольца, которое составляет 5, 6, 8; при этом по меньшей мере в одном из n звеньев каликсаренового кольца по меньшей мере один из заместителей R, R, Rи Rсодержит по меньшей мере одну кислотную группу карбонового типа, доступную для реакции с металлическим основанием, в котором металл выбран из щелочных металлов и щелочноземельных металлов, при условии, что указанная кислотная группа карбонового типа не содержится в звене каликсаренового кольца, относящегося ...

СПОСОБ И УСТРОЙСТВО ДЛЯ ПРИГОТОВЛЕНИЯ ЦИЛИНДРОВОГО МАСЛА

Изобретение относится к смазке машин и двигателей. Способ получения цилиндрового масла, согласно которому обеспечивают свежее системное масло, обеспечивают свежее цилиндровое масло и смешивают свежее системное масло со свежим цилиндровым маслом, причем свежее системное масло имеет более низкое значение общего щелочного числа (TBN), чем свежее цилиндровое масло, и причем цилиндровое масло и свежее цилиндровое масло являются проточными цилиндровыми маслами для использования в крейцкопфных дизельных двигателях и содержат щелочные присадки. Рассмотрен способ эксплуатации двигателя внутреннего сгорания, согласно которому: подготавливают цилиндровое масло в соответствии с любым способом приготовления цилиндрового масла, описанным в данном документе, и применяют цилиндровое масло в двигателе внутреннего сгорания. Рассмотрено также устройство для приготовления цилиндрового масла, содержащее смешивающее средство для смешивания использованного масла и свежего цилиндрового масла, характеризующееся ...

СПОСОБ И УСТРОЙСТВО ДЛЯ ПОЛУЧЕНИЯ МОЧЕВИНОВОЙ КОНСИСТЕНТНОЙ СМАЗКИ

Изобретение относится к способу получения мочевиновой консистентной смазки, который осуществляют в устройстве, использующем экструдер и содержащем несколько реакционных зон, смонтированных в ряд и связанных по текучей среде. При этом устройство включает в себя: (а) первую зону подачи; (b) вторую зону подачи; (с) первую зону реакции-смешивания и (d) зону охлаждения-смешивания, причем указанные зоны расположены в устройстве в порядке (а), (b), (с), (d), и способ включает введение первого исходного компонента в первую зону подачи (а); введение второго исходного компонента во вторую зону подачи (b); реакцию первого и второго компонентов в первой зоне реакции-смешивания (с) и охлаждение и смешивание продукта первой зоны реакции-смешивания в зоне охлаждения-смешивания (d) с получением мочевиновой консистентной смазки. Также изобретение относится к устройству для осуществления данного способа. Настоящее изобретение обладает такими преимуществами, как технологическая стабильность, обладает трансформируемостью ...

Способ получения пластичной кальциевой смазки

Изобретение относится к области нефтехимии, в частности к способам получения пластичных смазок - жировых солидолов, содержащих в качестве загустителей - кальциевые соли высших жирных кислот и находящих широкое применение в качестве антифрикционных смазок массового назначения (для узлов трения автомобилей, тракторов и других механизмов). В качестве исходного сырья для получения смазки используют минеральные масла различных марок и глицерин-сырец - отход производства биодизеля, содержащий в своем составе глицерин, метиловые эфиры жирных кислот и их калиевые соли жирных кислот. Смазку получают путем обработки хлористым кальцием смеси глицерина-сырца с минеральным маслом в безводной среде при 60-100°С в течение 4-6 ч, и последующим отделением от жидкого глицеринового слоя полученной вязко-пластичной массы, представляющей собой пластичную кальциевую смазку. Технический результат: упрощение процесса при использовании дешевого сырья, а также утилизация основного побочного продукта производства ...

Состав и способ приготовления смазочно-охлаждающей жидкости

Изобретение относится к машиностроению (металлообработке), в частности к составу и способу приготовления масляной СОЖ (смазочно-охлаждающей жидкости). Описан состав и способ приготовления масляной смазочно-охлаждающей жидкости. В качестве масляной основы используется индустриальное масло, а в качестве присадки - технический мел в количестве 25% от общего объема жидкости. СОЖ готовят в герметичной рабочей камере путем диспергирования при возбуждении ультразвуковых колебаний по направлению снизу вверх, при избыточном гидростатическом давлении в камере 0,25 МПа. Технический результат: позволяет повысить качество обрабатываемой поверхности отверстия и снизить себестоимость обрабатываемых деталей. 2 н.п. ф-лы, 3 ил.

КОМПОЗИЦИЯ ГИДРОКСИДА ЛИТИЯ, СПОСОБ ПОЛУЧЕНИЯ КОМПОЗИЦИИ ГИДРОКСИДА ЛИТИЯ И СПОСОБ ИСПОЛЬЗОВАНИЯ КОМПОЗИЦИИ ГИДРОКСИДА ЛИТИЯ

Изобретение относится к стабильной композиции гидроксида лития, содержащей гидроксид лития, базовое масло и соль жирной кислоты, используемой для получения консистентной смазки, полученная по способу, который включает контактирование компонента гидроксида лития, базового масла и компонента жирной кислоты, где компонент жирной кислоты добавлен в количестве от 3 до 10 мас.% в расчете на общую массу композиции гидроксида лития. Также настоящее изобретение относится к способу получения композиции гидроксида лития, к способу использования композиции гидроксида лития для получения концентрата мыла и к способу использования композиции гидроксида лития для получения консистентной смазки. 4 н. и 9 з.п. ф-лы, 4 пр., 1 табл.

СПОСОБ ПОЛУЧЕНИЯ СМАЗКИ НА ОСНОВЕ КОМПЛЕКСА СУЛЬФОНАТА КАЛЬЦИЯ

Настоящее изобретение относится к однофазному способу приготовления смазки на основе комплекса сульфоната кальция. В частности, изобретение относится к однофазному способу приготовления смазки на основе комплекса сульфоната кальция в отсутствие борной кислоты, включающему осуществление по меньшей мере одной стадии под давлением по меньшей мере 400 кПа и при температуре по меньшей мере 130°С. 18 з.п. ф-лы, 12 табл., 6 пр.

СПОСОБ ПОЛУЧЕНИЯ БИОРАЗЛАГАЕМОЙ НИЗКОТЕМПЕРАТУРНОЙ ПЛАСТИЧНОЙ СМАЗКИ

Изобретение относится к области смазочных материалов и, более конкретно, к биоразлагаемым пластичным смазкам, применяемым в узлах трения различных машин или механизмов, эксплуатируемых в условиях низких температур. Предложен новый способ получения биоразлагаемой низкотемпературной пластичной смазки на основе триэтилцитрата и загустителя - дисперсии аморфной наноцеллюлозы в водной среде. В качестве загустителя на основе целлюлозы используют дисперсию, последовательно промывают ее для удаления воды сначала ацетоном, а затем - триэтилцитратом, осуществляют вакуумную очистку от остаточных ацетона и воды, разбавляют триэтилцитратом до необходимой консистенции смазки и перемешивают при следующем соотношении компонентов, мас.%: целлюлоза - 1-15, триэтилцитрат - остальное. Согласно предлагаемому изобретению в качестве базового масла используют триэтилцитрат, а в качестве загустителя - дисперсию целлюлозы. Технический результат, расширение температурного диапазона применения биоразлагаемой смазки ...

УЛУЧШЕННЫЕ ИЗОЛИРУЮЩИЕ ТЕКУЧИЕ СРЕДЫ НА ВОДНОЙ ОСНОВЕ И СПОСОБЫ, СВЯЗАННЫЕ С НИМИ

... 1. Изолирующая текучая среда на водной основе, которая включает водную основу текучей среды, органическую жидкость, смешивающуюся с водой, и синтетический полимер. ! 2. Изолирующая текучая среда на водной основе по п. 1, в которой синтетический полимер сшивают. ! 3. Изолирующая текучая среда на водной основе по п. 1, в которой изолирующая текучая среда на водной основе далее включает добавку, выбранную из группы, содержащей: ингибиторы коррозии, модификаторы pH, биоциды, стеклянную дробь, полые сферы, полые микросферы, модификаторы реологии, буферы, ингибиторы гидратообразования, деэмульгаторы, индикаторы, дополнительные утяжелители, загустители, поверхностно-активные вещества и их комбинации. ! 4. Изолирующая текучая среда на водной основе по п. 1, в которой изолирующая текучая среда на водной основе включает солевой раствор, выбранный из группы содержащий: NaCl, NaBr, КCl, CaCl2, CaBr2, ZrBr2, карбонат натрия, формиат натрия, формиат калия, формиат цезия, и комбинации и производные этих ...

СПОСОБ ПОЛУЧЕНИЯ СМАЗЫВАЮЩЕГО МАТЕРИАЛА

Изобретение относится к нефтеперерабатывающей промышленности, в частности к способу получения смазочных материалов, а именно смазочно-охлаждающих технологических сред, с высоким индексом вязкости и может найти широкое применение в качестве базовых смазочных сред при производстве гидравлических, амортизационных, формовочных, смазочно-охлаждающих жидкостей, а также масел на основе нефтяного сырья в машиностроительной, металлургической, строительной отраслях промышленности. Способ включает одну стадию смешивания в поточном статическом смесителе нефтяных компонентов, полученных в процессе первичной переработки нефти. Смешивание осуществляют при температуре не менее 45°C, но не более 120°C, а в качестве нефтяных компонентов используют фракции остаточного дистиллята и тяжелого дизельного дистиллята при следующем соотношении компонентов в мас.%: остаточный дистиллят - 20-90, тяжелый дизельный дистиллят - 10-80. Технический результат - упрощение способа производства смазывающего материала, повышение ...

СПОСОБ ПОЛУЧЕНИЯ РАЗВЕТВЛЕННОГО УГЛЕВОДОРОДНОГО КОМПОНЕНТА

... 1. Базовое масло, отличающееся тем, что базовое масло содержит разветвленные углеводороды, имеющие число атомов углерода по меньшей мере С18, оно содержит по меньшей мере 90% по весу насыщенных углеводородов, не более чем 15% по весу мононафтенов, и не более чем 1% по весу конденсированных динафтенов и полинафтенов, с индексом вязкости более чем 120, с базовым маслом биологического происхождения, и по меньшей мере 60% по весу насыщенных углеводородов, имеющих не более чем 5 атомов углерода. ! 2. Базовое масло по п.1, отличающееся тем, что базовое масло включает по меньшей мере 95% по весу насыщенных углеводородов, и по меньшей мере 75% по весу насыщенных углеводородов, имеющих не более чем 3 атома углерода. ! 3. Базовое масло по п.2, отличающееся тем, что оно включает по меньшей мере 97% по весу насыщенных углеводородов. ! 4. Базовое масло по любому из пп.1-3, отличающееся тем, что индекс вязкости базового масла составляет по меньшей мере 130. ! 5. Базовое масло по п.1, отличающееся тем ...

СПОСОБ ПОЛУЧЕНИЯ СМАЗКИ НА ОСНОВЕ КОМПЛЕКСА СУЛЬФОНАТА КАЛЬЦИЯ

Металлические соединения каликсаренов, содержащие их моющие составы и их применение в составах смазочных масел

СПОСОБ И УСТРОЙСТВО ДЛЯ ПРИГОТОВЛЕНИЯ ЦИЛИНДРОВОГО МАСЛА

Protecting cold-drawn metal pipes against corrosion - by using lubricating substance which is then converted on pipes into permanent coating

Metal pipes are cold-drawn using substance (I) with lubricating properties which is then converted on the pipes into a permanent coating. Pipe is of Cu. (I) has viscosity such that amt. remains on pipe wall on drawing which, after conversion into coating, forms film 5-200 microns thick. (I) has viscosity 100-600 mPa.s. (I) is oligomer formed by polymerisation, polycondensation, or polyaddn. ADVANTAGE - Coating prevents pinhole corrosion and loss of heavy metal ions which could contaminate drinking, service, and ground water and soil; service life of pipes is increased; method avoids expense of cleaning used lubricant from pipe, checking for its absence, and disposing of used lubricant; wider range of plastics coatings can be used ...

Zusammensetzungen aus alpha-beta-ungesättigten Dicarbonsäureestern und olefinisch ungesättigten Verbindungen, geeignet für die Verwendung als Schmiermittel und Schmiermittelzusätze und Verfahren zur Herstellung dieser Zusammensetzungen

VERFAHREN ZUR HERSTELLUNG VON BASISSCHMIEROELEN UND SO ERHALTENE BASISSCHMIEROELE.

FILM AUF BASIS VON AMORPHEM KOHLENWASSERSTOFF UND GLEITELEMENT UND GLEITSYSTEM MIT DEM FILM

Eine reibungsarme Beschichtung 5 enthält: eine aliphatische Kohlenwasserstoffgruppe, die in einem Infrarot-Absorptionsspektrum einen Peak im Bereich von 2900 cm–1 bis 3000 cm–1 zeigt; eine Carbonylgruppe, die in einem Infrarot-Absorptionsspektrum einen Peak im Bereich von 1650 cm–1 bis 1800 cm–1 zeigt; eine aromatische Komponente (C7H7 +), die in einem durch TOF-SIMS erhaltenen Positivionenspektrum einen Peak bei einer Masse von 91,1 zeigt; und eine auf einem kondensierten Ring basierende Komponente (C9H7 +), die in dem durch TOF-SIMS erhaltenen Positivionenspektrum einen Peak bei einer Masse von 115,2 zeigt.

VERFAHREN ZUR KONTINUIERLICHEN HERSTELLUNG VON SEIFENSCHMIERFETTEN

HERSTELLUNGSVERFAHREN VON SCHMIERÖLEN MIT ROSTSCHUTZEIGENSCHAFTEN

Zip fastener lubricant

The fastener is pref. of plastic. The lubricant is a mixture of a chlorinated hydrocarbon such as perchloroethylene and an impregnating drying agent. The proportion of chlorinated hydrocarbon: impregnating agent is 3:1 at 50-60 degrees C. The substance is applied with an oil can or preferably with the sliding clasp to the part of the fastener above or below the claps. The substance will not stain the clothing to which the fastener is sewn.

Roentgenapparat

Schmierfette umfassend Metallseifen und Metallkomplexseifen auf Basis von R-10-Hydroxyoctadecansäure

Gegenstand der Erfindung sind Schmierfette auf Basis von Alkali- und/oder Erdalkali-Metallseifen und Metallkomplexseifen auf Basis von R-10-Hydroxyoctadecansäure und deren Verwendung.

VERFAHREN ZUM AUFBRINGEN VON TRENN- ODER SCHMIERMITTELN AUF DIE OBERFLAECHEN DER WERKZEUGE UND DER BEI DER SPANLOSEN FORMGEBUNG ZU VERARBEITENDEN WERKSTUECKE

Slide member

Improved lubrication product

A lubricant particularly for use to penetrate between closely fitting parts such as those of newly assembled engines, spring leaves, &c. consists of a lubricating oil of the paraffin, olefine or naphthene series in which is colloidally dispersed a polymerized product of the oil such as the asphaltic residues obtained in distilling the oils, the dispersion being diluted with a volatile solvent such as petroleum or coal tar naphtha. An antioxidant such as aniline, and an animal grease of polar character such as degras may be added.

MONITORING OF CHEMICAL ADDITIVES

INCREASING THE VISCOSITY INDEX OF LUBRICATING OIL FEEDSTOCKS BY ELECTROCHEMICAL REDUCTION

... 1382823 Electrolytic reduction EXXON RESEARCH & ENG CO 25 Feb 1972 [26 Feb 1971] 5557/71 Heading C7B The viscosity index of at least part of a lubricating oil feedstock comprising reducible compounds, e.g. naphthalene, is increased by reducing the compounds in an electrolytic cell having anode and cathode with an electrolytic system (solvent and electrolyte) comprising chemically bound hydrogen in which electrons from the cathode are accepted and solvated during passage of electric current. The solvent may be liquid ammonia or alkylamine (e.g. butyl- or ethylamine) or alkyl (e.g. tetrabutyl) ammonium chloride; the electrolyte may be an alkali metal salt e.g. LiCl, NaCl, LiOH or NaOH at least partly soluble in the solvent. The chemically bound hydrogen may be replaced during or after passage of the current by protonation, e.g. at an inert porous anode to which hydrogen is supplied, or outside the cell during recirculation of the system, the protonation agent being HCl or NH 4 Cl for LiCl ...

Improvements in or relating to the Preparation of Lubricants.

... 15,463. Blichfeldt, S. H. June 27. Lubricants for machinery.-A lubricant consists of an emulsion of relativelv insoluble liquids, one of which has comparatively low internal friction, the diameter of the suspended particles being 0À001 mm. or less. Emulsions of oil or fat in water, in aqueous solutions as of soap, or, where evaporation may be rapid, in glycerine or an aqueous solution of glycerine, are typical. Suitable emulsifying-apparatus is described in Specifications 7498/12, 23,653/13, 25,265/13, and 18,048/14, [all in Class 81 (i), Disinfecting &c.].

Method for producing lubricant additive (variants)

The invention relates to petroleum chemistry, more specifically to sulfur-containing molybdenum compounds and to the use thereof in the form of lubricant additives which decrease friction coefficient. In the first variant, molybdenum trisulfide nanoparticles and the derivatives thereof are produced from thio-molybdenum acid salts of the general formula M2MoS4-x Ox, wherein M=NH4, Na, x=0-3 in the presence of two modifiers, one of them being embodied in the form of tetra-alkyl-ammonium salts or a mixture of salt of the general formula R<1>R<2>R<3>R<4>NX, wherein R<1>R<2>R<3> and R<4> equal or different are selected from a group containing C1-C16 alkyl, X=Cl, Br, the second modifier being embodied in the form of a succinimide of the general formula Formula wherein R<5>= straight or branched-chain alkyl or oligoalkylene whose molar mass ranges from 140 to about 1000, R<6> is selected from a group comprising H, -C(=O)NH2, -(CH2CH2 NH)nCH3, n=1-4. The process is carried out by means of a thermal ...

Improvements in or relating to Preparation of Lubricants.

... 17,411. Blichfeldt, S. H. July 22. Lubricants for machinery.-A lubricant consists of such an emulsion of 5 to 25 per cent of water or watery solution in 95 to 75 per cent of oil or fat that the aqueous particles have a diameter of 0À001 mm. or less. In an example, 15 parts of a 10 per cent solution of soap are emulsified in 85 parts of engine oil. Suitable emulsifiers are described in Specifications 7498/12, 23,653/13, 25,265/13, and 18,048/14, [all in Class 81 (i), Disinfecting &c.].

MANUFACTURING ANTI-FRICTION MATERIALS

Enhancing the performance and/or durability of certain friction materials

A slide member for a slide bearing

A slide member 3 comprising a base member 1 and an overlay 22 provided on a slide receiving surface 7 of the base member wherein the overlay is formed by attaching a mixed solid lubricant 2C to the slide receiving surface of the base member. The mixed solid lubricant is made by mixing at least two kinds of solid lubricants which are; a large amount of hydrogen containing solid lubricant 2A which contains a large amount of hydrogen, and a small amount of hydrogen containing solid lubricant 2B which contains a smaller amount of hydrogen. A lubricant absence region (4, figure 4) may be provided where the overlay is absent on the slide receiving surface of the base member after sliding. An oxidized portion (5) may be provided where the base member is oxidized toward the inside of the base member from the lubricant absence region.

Process for improving lubricating qualities of lower quality base oil

Dielectric fluids and processes for making same

Methods for preparing and utilizing non-alkali metal quinolinolates and preparations obtained therein

Quinolinol esters are added to lubricating oils containing compounds of metals other than alkali metals to bind the metals as quinolinates. The preferred esters are those of 2-ethyl hexoic, myristic, palmitic, stearic and other higher fatty acids which are not subject to oxidation. The amount of ester added is normally in the range 0.02-0.2% by weight of the oil. The esters may also be added to coating compositions to combine with compounds of metals other than alkali metals to form a coating composition which is mildew-proof. In an example, aquinolinol ester is added to a wire-coating composition containing linseed oil, zinc oxide and rubber.ALSO:A quinolate (oxinate) of a metal other than an alkali metal is prepared by reacting an ester of a hydroxyquinoline in the absence of water with a compound of a metal other than an alkali metal. The reaction may be carried out in solution in an organic solvent at elevated temperature. The esters used as starting materials are prepared by conventional ...

Drawable coatings for forming metal containers and can-forming process.

A drawable precoating composition for a metal substrate for forming containers, e.g. from precoated metal sheet by a multiple drawing process, comprises a basic coating material which will adhere to a metal substrate and 3-10% by wt. of an incompatible lubricant having a specific gravity lower than that of the uncured precoating so that upon curing of the coating it forms a concentration gradient having its greatest concentration near the surface of the coating and furthest from the metal substrate. The lubricant facilitates forming of the coated metal substrate without loss of adhesion of the coating.

METAL WORKING FLUID

PREPARATION OF LITHIUM SOAP THICKENED GREASES

Preparation of suspensions of water-soluble solids in oleaginous media

A method of preparing a suspension of a water-soluble solid in an oily medium is to form a water-in-oil emulsion of the aqueous solution of the solid with oleaginous liquid using a vegetable wax as an emulsifying agent and thereafter dehydrating the emulsion. The oleaginous liquid may be a mineral oil (e.g. a lubricating oil, a residue, a fuel oil or kerosine), castor oil, a diester, a polyglycol, a polyether or a silicon-containing synthetic oil. It may be also thickened to form a lubricating grease. Solids which are suspended in the media include alkali metal and ammonium nitrites, carbonates, bicarbonates, sulphites, borates, chlorates, perchlorates, hypochlorites, silicates, phosphates, salicylates, citrates, tannates, lactates, tartrates, oxalates, phthalates, acetates, iodates, arsenites, chromates, molybdates and tungstates; amine nitrites, phosphates and iodates; hydroxy fatty acids, polycarboxylic acids, hydroxy polycarboxylic acids, sodium benzoate, amides and amino acids. Waxes ...

Process of making an improved carboxylic acid salt complex thickened lubricant

A process for the production of a substantially anhydrous lubricating composition comprising a mixture of metal salts of acetic acid and a C7 to C10 monocarboxylic acid, and lubricating oil, consists in heating the mixture to 250-350 DEG F., maintaining the proportion by weight of the said metal salts in the range of 20-50%, homogenizing in the range 80-150 DEG F. with the rate of shear in the range 100,000 to 500,000 reciprocal seconds, diluting with further amounts of lubricating oil, thus giving a concentration of 4-10 wt. per cent of metal salts and homogenizing in the range 80-150 DEG F., with the rate of shear in the range 100,000 to 750,000 reciprocal seconds, to give a fluid product of viscosity 80-200 S.S.U. at 210 DEG F. and said to be of improved stability. The lubricating oil has an initial viscosity in the range 55-100 S.S.U. at 210 DEG F. and a V.I. of 40-100; the molecular ratio of acetic to C7-C12 acid is in the range of 10 : 1 to 25 : 1. It is preferred to form the said ...

Facile synthesis of graphene, graphene derivativesand abrasive nanoparticles and their various uses , including as tribolofically-beneficial lubricantadditives

Calcium hydroxyapatite based calcium sulfonate grease compositions and method of manufacture

Facile synthesis of graphene, graphene derivativesand abrasive nanoparticles and their various uses , including as tribolofically-beneficial lubricantadditives

Calcium hydroxyapatite based calcium sulfonate grease compositions and method of manufacture

Nanostructure of a revitalizing agent and method for producing a stable form of a nanostructure of arevitalizing agent

Lubricating composition and method for the preparation thereof

Calcium carbonate based calcium sulfonate grease compositions and method of manufacture

Method for reducing the viscosity of viscous fluids.

Lubricating composition and method for the preparation thereof

Calcium carbonate based calcium sulfonate grease compositions and method of manufacture

Calcium hydroxyapatite based calcium sulfonate grease compositions and method of manufacture

Nanostructure of a revitalizing agent and method for producing a stable form of a nanostructure of arevitalizing agent

Facile synthesis of graphene, graphene derivativesand abrasive nanoparticles and their various uses , including as tribolofically-beneficial lubricantadditives

Lubricating composition and method for the preparation thereof

Nanostructure of a revitalizing agent and method for producing a stable form of a nanostructure of arevitalizing agent

Calcium carbonate based calcium sulfonate grease compositions and method of manufacture

SCHMIERMITTEL FUR ZAHNARZTLICHE HANDSTUCKE

THREAD CONNECTING PIECE FOR STEEL TUBES AND PROCEDURE FOR ITS SURFACE TREATMENT

VERFAHREN ZUR VERBESSERUNG DER SCHMIEREIGEN- SCHAFTEN VON MOLYBDAENSULFID

POLYOXYALKYLENPHOSPHONATE AND IMPROVING SYNTHESIS PROCEDURE FOR IT

COMPOSITIONS FROM OUTER ONES DICARBONIC ACID ESTERS AND OLEFINISCH INSATIATED CONNECTIONS, SUITABLY FOR THE USE AS LUBRICANTS AND LUBRICANT ADDITIVES AND PROCEDURE FOR THE PRODUCTION OF THESE COMPOSITIONS

CHROMATIERTES METALLBLECH MIT HOHER KORROSIONSBESTÄNDIGKEIT, DAS EINE VERBESSERTE GLEITFÄHIGKEIT UND ELEKTRISCHE LEITFÄHIGKEIT AUFWEIST

MIXED METAL HYDROXIDES FOR THICKENING WATER OR HYDROPHILIC LIQUIDS.

PROCEDURE FUER THE PRODUCTION OF STABLE OELIGEN COMPOSITIONS.

LUBRICANT FUR ZAHNARZTLICHE HAND STUCCO

LIQUID ALKYLATING DIPHENYLAMINANTIOXIDANT

DETERMINATION OF METAL SOURCE USED IN OIL

Oil-soluble molybdenum derivatives dervied from hydroxyethyl-substituted mannich bases

Process for preparing a complex calcium sulphonate grease

The present invention relates to a process for preparing a complex calcium sulphonate grease in one step. More particularly, the invention relates to a process for preparing a complex calcium sulphonate grease in one step, in the absence of boric acid and comprising the implementation of at least one stage under pressure.

Composition and method of manufacturing calcium magnesium sulfonate greases without a conventional non-aqueous converting agent

An overbased calcium magnesium sulfonate grease composition and method of making such grease without using any conventional non-aqueous converting agents, such as hexylene glycol, as a pre-conversion ingredient. The addition of magnesium sulfonate as an ingredient prior to conversion appears to act as a new, non-conventional converting agent, resulting in greases with improved thickener yield and excellent dropping point.

SCREW JOINT FOR STEEL PIPE

A screw joint for steel pipe, comprising pin (1) provided with a contact surface, which has screw portion (3) or (4) and nonthreaded metal contact portion (8), and box (2), wherein a lubricant coating exhibiting self-repair capability through liquid lubrication and having its surface tackiness restricted is formed on the contact surface of at least one of the pin and box so as to attain an enhancement of seizure resistance. This lubricant coating is either (1) a lubricant coating comprising a lubricant layer in liquid form at 0 to 40.ordm.C and, superimposed thereon, a lubricant layer in solid form at 40.ordm.C or (2) a lubricant coating in solid or semisolid form at 40.ordm.C comprising a mixture of lubricant oil in liquid form at 0 to 40.ordm.C and wax in solid form at 40.ordm.C (preferably a mixture obtained by liquefying the wax after mixing in advance and effecting mutual dissolution of the lubricant oil and wax).

PERFLUOROPOLYETHER ADDITIVES

Compounds formed of (per)fluoropolyether chains and end groups having a pyridine structure, with structural formula: T1-CW1-O-R f-CW2-T2(I) wherein T1, T2, equal to or different from each other, have the following meanings: - F, CF3, C2F5, (C2F4)C1: - CH2-B-Y, CH (CF3) O-Y, wherein: - B = O, S; (see above formula) wherein R1, R2, R3, R4, equal to or different from each other, are H, F, C1-C8 linear or branched perfluoroalkyl, NO2, CN; with the proviso that at least one of the two end groups T1, T2 is CH2-B-Y or CH(CF3)O-Y as above defined; W1, W2, equal to or different from each other, are -F, -CF3; Rf is a (per)fluoropolyoxyalkylene chain having a number average molecular weight from 400 to 10,000.

METHOD FOR PRODUCING LUBRICATING OILS WITH ANTI-RUST PROPERTIES

Lubricating oils exhibiting anti rust-properties are obtained by adding to the lubricating oil an acidic anti-rust additive and an acid scavenger such as carbodiimide, in a specific sequence.

THREADED JOINT FOR STEEL PIPE AND METHOD FOR SURFACE TREATMENT OF THE THREADED JOINT

A threaded joint for steel pipe formed on a pin and a box having a contact surface including a threaded parts and a non-threaded metal contact part and capable of preventing a galling by repeated fastening and loosening operations without applying compound grease thereto, wherein a solid lubricating film including lubricating powder such as molybdenum disulfide and resin binder is formed on the contact surface of at least one of the pin and the bo by drying the film by primary heating in the temperature range of 70 .degree.C to 150 .degree.C and by a secondary heating in the range of from higher than 150 .degree.C to 380 .degree.C, the solid lubricating film thus obtained has a Rockwell M scale hardness of 70 to 140, an adhesive strength of 500 N/m or higher obtained by the SAICAS (Surface And Interfacial Cutting Analysis System) method, and excellent galling resistance and airtightness even in a high temperature well environment, and, when ultraviolet ray shielding particles such as titanium ...

A METHOD OF IMPROVING THE COMPATIBILITY OF AN OVERBASED DETERGENT WITH OTHER ADDITIVES IN A LUBRICATING OIL COMPOSITION

A method of improving the compatibility of an overbased detergent with other additives in a lubricating oil composition. The method includes the step of adding an oil-soluble, hydrocarbyl sulphonic acid to the detergent.

CONTINUOUS GREASE MAKING

MIST LUBRICATION WITH OIL CONTAINING A POLYMERIC ADDITIVE

METHOD FOR CONTROLLING VISCOSITY OF ORGANIC LIQUIDS

A method for controlling the viscosity of organic liquids, said organic liquids having a solubility parameter of from about 6.0 to about 10.5, which comprises incorporating in said organic liquid a minor amount of an ionomeric polymer and polar cosolvent having a solubility parameter of from about 10 to 20, the solubility parameter of said solvent being at least 1.0 unit higher than the solubility parameter of said organic liquid.

PREPARATIVE PROCEDURE FOR HIGH DROPPING POINT LUBRICATING GREASE

(PER)FLUOROPOLYETHER ADDITIVES

Compounds usable as stabilizing additives of perfluoropolyether fluids working at high temperatures, higher than 200.degree.C, and/or in the presence of metals and/or in the presence of Lewis acids, are formed of (per)fluoropolyether chains and of end groups having a heteroaromatic structure, according to the following general formula: T1-CFW1-O-R f-CFW2-T2 (I) wherein - T1, T2, equal to or different from each other, have the following meanings: - F, CF3, C2F5, (C2F4)Cl - -CH2-B-Y, -CH(CF3)O-Y, wherein: - B = O, S; - Y is a substituent formed of a ring having a heterocyclic structure having the following formula: (see above formula) wherein: R1, R2, R3, R4, equal to or different from each other are H, linear or branched C1-C8 perfluoroalkyl, NO2, CN, preferably H; with the proviso that at least one of the two end groups T1, T2 is -CH2-B-Y or -CH(CF3)O-Y, wherein B and Y are as above; - W1, W2, equal to or different from each other, are -F, -CF3; Rf is a (per)fluoropolyoxyalkylene chain ...

MIST LUBRICATION WITH OIL CONTAINING A POLYMERIC ADDITIVE

PREPARATION OF STERICALLY HINDERED HYDROXYPHENYLCARBOXYLIC ACID ESTERS

A novel manufacturing process is described for producing hindered phenolic alkyl esters, which may be useful as antioxidants. This process simplifies catalyst neutralization and removal during the preparation of hindered phenolic esters. Compositions that comprise the hindered phenolic esters produced according to these methods are also described.

PREMIUM SYNTHETIC LUBRICANTS

Premium synthetic lubricants comprise a synthetic isoparaffinic hydrocarbon base stock and an effective amount of at least one, and typically a plurality of lubricant additives such as a detergent, dispersant, antioxidant, antiwear additive, pout point depressant, VI improver and the like. The base stock is derived from a waxy, paraffinic, Fischer-Tropsch synthesized hydrocarbon feed fraction having an initial boiling point in the range of about 650-750~F and continuously boiling up to at least 1050~F, by a process which comprises hydroisomerizing the feed and dewaxing the isomerate. The waxy feed has a T90- T10 temperature difference of at least 350~F and is preferably hydroisomerized without any pretreatment, other than optional fractionation. The lubricant may also contain hydrocarbonaceous and synthetic base stock material. Lubricants, such as fully formulated multigrade automotive crankcase and transmission oils formed by adding a suitable additive package to the isoparaffinic base ...

COMPOSITION AND METHOD OF MANUFACTURING CALCIUM MAGNESIUM SULFONATE GREASES WITHOUT A CONVENTIONAL NON-AQUEOUS CONVERTING AGENT

An overbased calcium magnesium sulfonate grease composition and method of making such grease without using any conventional non-aqueous converting agents, such as hexylene glycol, as a pre-conversion ingredient. The addition of magnesium sulfonate as an ingredient prior to conversion appears to act as a new, non-conventional converting agent, resulting in greases with improved thickener yield and excellent dropping point.

CATALYTIC DEPOLYMERISATION OF POLYMERIC MATERIALS

BIOGENIC LOW VISCOSITY INSULATING OIL

A method of producing a non-petroleum based electrical insulating oil, the method comprising providing a primary mixture of non-petroleum origin, comprising isomerized straight chain hydrocarbons; performing a distillation and/or stripping of the primary mixture; collecting a paraffinic base oil as a product of the distillation and/or stripping, comprising a mixture of isoalkanes and alkanes; and mixing the base oil with an antioxidant additive.

SYNTHESIS OF DIESTER-BASED LUBRICANTS FROM ENZYMATICALLY-DIRECTED EPOXIDES

The present invention is generally directed to a process comprising: a) epoxidizing an olefin having a carbon number of from 8 to 18 to form an epoxide comprising an epoxide ring, wherein such epoxidizing is enzymatically-driven; and b) directly esterifying the epoxide with a C2 t0 C18 carboxylic acid to form a diester species having viscosity and pour point suitable for use as a lubricant or component thereof In some embodiments, the processes for making such diester-based lubricants utilize a biomass precursor and/or low value (e.g., Fischer-Tropsch (FT) olefins and/or alcohols) so as to produce high value diester-based lubricants. In some embodiments, such diester-based lubricants are derived from FT olefins and fatty acids. The fatty acids can be from a bio-based source (i.e., biomass, renewable source) or can be derived from FT alcohols via oxidation.

EXTREME-PRESSURE ADDITIVE, PROCESS FOR PRODUCING THE SAME, CUTTING FLUID, AND GRINDING FLUID

The present invention provides a sulfur-based extreme-pressure additive that is completely soluble in water without using a surfactant, and has satisfactory odor and hue. In addition, the present invention provides a cutting liquid and grinding liquid having superior defoaming property and rust preventive characteristics, while also having high load resistance and lubrication performance comparable to cutting oils and grinding oils of the prior art. The above objects are achieved by an extreme-pressure additive comprising the salt of a condensation product of a sulfurized hydroxy-unsaturated fatty acid, the condensation product having a sulfur content of 8 to 15% by weight (mass), color of 6 or less, and acid value of 80 to 200, and a grinding liquid comprising that extreme-pressure additive and water.

THREADED JOINT FOR STEEL PIPES

A threaded joint for steel pipes for use in an oil well which has improved galling resistance and which is protected from rusting comprises a pin and a box each having a contact surface including a threaded portion and an unthreaded metalcontact portion. The contact surface of at least one of the pin and the box has a lower layer of a viscous liquid or semisolid lubricating coating comprising at least wax and a fatty acid alkaline earth metal salt and not containing a harmful heavy metal such as lead and an upper layer of a dry solid coating formed from an aqueous resin coating composition, an organic solvent type coating composition, or an ultraviolet curing coating composition.

METHOD FOR REDUCING THE VISCOSITY OF VISCOUS FLUIDS

... ²²²A viscous fluid, such as heavy crude oil which is too viscous to enable it to ²be pumped from a flowing phase of a reservoir into and along a pipeline for ²delivery to a refinery or other storage facility, may be contacted with a ²formulation to reduce its viscosity. The formulation comprises a polymeric ²material AA which includes -O- moieties pendent from a polymeric backbone ²thereof and said material is optionally cross-linked. In one embodiment, the ²formulation may comprise polyvinyl alcohol. In an alternative embodiment, the ²formulation may comprise a cross-linked polymeric material, such as cross-²linked polyvinyl alcohol. After the viscous composition has been transported ²to a desired location, it may be separated from the other components.² ...

NITRATED EXTREME PRESSURE ADDITIVES

This invention relates to processes for making nitro compounds derived from C2-C30 unsaturated fatty acids; C2-C30 unsaturated fatty oils; esters derived from the reaction of C1-C20 alcohols with unsaturated C2-C30 fatty acids; C2-C20 polyolefins; C4-C20 polydiolefins; C8-C20 copolymers derived from polyolefins and vinyl aromatics; and C4-C30 alkylated phenols using nitric acid or gaseous nitrogen dioxide. This class of extreme-pressure additives was found extremely effective in processing steel, stainless steel and special titanium and nickel or low-iron alloys.

A PROCESS FOR MAKING BORATED ALKALINE EARTH METAL TOLUENE SULFONATES

Provided is a new and improved process for preparing a borated alkaline eart h metal toluene sulfonate salt.

LUBRICATION BY EXPOSURE TO LIGHT

... ²² The present invention concerns a method for a location and/or time-dependent ²alteration of the friction coefficient and/or adhesion force between two ²bodies, which ²includes irradiation of one or both contact surfaces between the bodies with ²radiation, use of the method according to the invention for location and/or ²time-dependent alteration of the friction coefficient and/or adhesion force ²between to ²bodies, a system that includes two bodies in which the friction coefficient ²and/or the ²adhesion force between the bodies can be temporarily or permanently altered, ²and a ²device for location and/or time-dependent regulation of the friction ²coefficient and/or ²adhesion force which includes the system according to the invention and a ²control ²unit.² ...

LOW POUR POINT TRIMETHYLOLPROPANE ESTERS

The present invention relates to polyol esters that are particularly suitable for use as insulating oils in electrical equipment where an effective cooling action is required, such as electrical transformers. In particular the invention relates to esters of trimethylolpropane with monocarboxylic acids of nine and /or ten carbon atoms, wherein the monocarboxylic acids of nine and/or ten carbon atoms comprise 5-15 mol % of branched acids and 85-95 mol % of linear acids with respect to the total moles of the monocarboxylic acids.

PROCESS FOR PREPARING A PARA-BRANCHED ALKYL-SUBSTITUTED HYDROXYAROMATIC COMPOUND

Disclosed herein is a process for preparing an isomeric mixture comprising a major amount of a para-branched mono-alkyl-substituted hydroxyaromatic compound. The process involves the steps of: (a) subjecting an isomeric mixture comprising a major amount of a para-di(alkyl-substituted)aromatic compound; wherein a first alkyi substituent is a C3 to C8 alkyi moiety and a second alkyi substituent is a C4+n to C8+n branched alkyi moiety, wherein n is 0 to 42 and further wherein the second alkyi substituent is at least one carbon atom greater than the first alkyi substituent to oxidation conditions to a mixture of hydroperoxide compounds followed by converting the hydroperoxide moiety to a hydroxyl group.

Application-specific finished lubricant compositions comprising a bio-derived ester component and methods of making same

The present invention is generally directed to methods of making application-specific finished lubricant compositions comprising bio-derived diester species. In some embodiments, bio-derived fatty acid moieties are reacted with Fischer-Tropsch/gas-to-liquids reaction products and/or by-products (e.g., gas-to-liquids-produced α-olefins) to yield bio-derived diester species that can then be selectively blended with base oil and one or more additive species to yield an application-specific finished lubricant product having a biomass-derived component.

Fuel and base oil blendstocks from a single feedstock

A method comprising the steps of providing a quantity of biologically-derived oil comprising triglycerides; processing the biologically derived oil so as to transesterify at least some of the triglycerides contained therein to yield a quantity of saturated monoesters and unsaturated monoesters; oligomerizing at least some of the unsaturated monoesters to yield a quantity of fatty acid ester oligomers; separating at least some of the saturated monoesters from the fatty acid ester oligomers; and hydrotreating at least some of the fatty acid ester oligomers to yield a quantity of alkanes.

Azeotropic and azeotrope-like compositions of methyl perfluoroheptene ethers and heptane and uses thereof

The present disclosure provides azeotropic and azeotrope-like compositions comprised of methylperfluoroheptene ethers and heptane. The present disclosure also provides for methods of use for the azeotropic and azeotrope-like compositions.

Method for producing a two phase lubricant composition

This invention provides a method for producing a lubricant composition that is comprised of a continuous phase and a discontinuous phase. The method involves mixing together high viscosity ester, ether or combination thereof, and polar diluent or solvent, to produce a solution. The solution is then added to a low viscosity Group IV base oil to produce a discontinuous phase dispersed throughout a continuous phase.

Novel materials as additives for advanced lubrication

This invention relates to carbon-based materials as anti-friction and anti-wear additives for advanced lubrication purposes. The materials have various shapes, sizes, and structures and are synthesized by autogenic reactions under extreme conditions of high temperature and pressure. The lubricant compositions comprise carbon-based particles suspended in a liquid hydrocarbon carrier. Optionally, the compositions further comprise a surfactant (e.g., to aid in dispersion of the carbon particles). Specifically, the novel lubricants have the ability to significantly lower friction and wear, which translates into improved fuel economies and longer durability of mechanical devices and engines.

Microencapsulated engine lubricant additives

An engine lubricating system for an internal combustion engine. The system comprises a vehicle engine; a circulation system for providing a continuing flow of lubricant to the vehicle engine and engine components; and a lubricant disposed within the circulation system. The lubricant comprises a base oil and at least one microencapsulated oil additive. The microencapsulated oil additive is selectively released into the lubricant based one or more localized event. The localized event may include a predetermined temperature change, a predetermined pH change, a localized high friction contact, and combinations thereof.

Activated Gaseous Species for Improved Lubrication

The present application is directed to methods and devices for altering material properties of lubricants and other cross-linkable compounds comprising organic or organometallic materials through exposure to energized gaseous species. The energized gaseous species may create reactive sites among lubricant molecules that may alter their material properties by cross-linking at least a portion of the lubricant molecules. The cross-linked lubricant may reduce the ability of the lubricant to migrate away when force is applied between lubricated sliding friction surfaces.

CARBON FILM LAMINATE, METHOD OF MANUFACTURING SAID LAMINATE, AND LUBRICANT USING SAID LAMINATE

An object of the invention is to provide a carbon film laminate having a sliding surface with low friction, low abrasion, and low counterpart aggressiveness using high adhesiveness to a base material, hardness, surface flatness, low counterpart aggressiveness, transparency, and high thermal conductivity which are provided to the carbon film without using liquid and semiliquid lubricants such as lubricating oil. Provided is a carbon film laminate including a base material, a carbon film adhesion reinforcing layer which is provided on the base material and which is formed from silicon oxide (SiOx, x=1 to 2) containing fluorine atoms (F) in a concentration of 1×10atoms/cmor more, and a carbon film that is formed on the carbon film adhesion reinforcing layer. The carbon film contains fluorine atoms in the film in a concentration of 1×10to 1×10atoms/cm, and has an approximate spectrum curve obtained by superimposing, on a peak fitting curve A at a Bragg angle (2θ±0.5°) of 43.9° in an X-ray diffraction spectrum by CuKαrays, a peak fitting curve B at 41.7° and a baseline. 1. A carbon film laminate comprising:a base material;{'sub': 'x', 'sup': 19', '3, 'a carbon film adhesion reinforcing layer which is provided on the base material and which is formed from silicon oxide (SiO, x=1 to 2) containing fluorine atoms (F) in a concentration of 1×10atoms/cmor more; and'}a carbon film that is formed on the carbon film adhesion reinforcing layer,{'sup': 19', '21', '3, 'sub': '1', 'wherein the carbon film contains fluorine atoms in the film in a concentration of 1×10to 1×10atoms/cm, and has an approximate spectrum curve obtained by superimposing, on a peak fitting curve A at a Bragg angle (2θ±0.5°) of 43.9° in an X-ray diffraction spectrum by CuKαrays, a peak fitting curve B at 41.7° and a baseline (here, the fitting curve A is expressed with a curve of a Pearson VII function, the fitting curve B is expressed with a curve of an asymmetric normal distribution function, and the ...

LOW FRICTION WEAR RESISTANT GRAPHENE FILMS

A low friction wear surface with a coefficient of friction in the superlubric regime including graphene and nanoparticles on the wear surface is provided, and methods of producing the low friction wear surface are also provided. A long lifetime wear-resistant surface including graphene exposed to hydrogen is provided, including methods of increasing the lifetime of graphene containing wear surfaces by providing hydrogen to the wear surface. 1. A method of forming a low friction wear surface comprising:disposing over a substrate a solution comprising nanodiamonds and a h-BN 2D material to form a first sliding component, the h-BN 2D material forming patches on the first sliding component;sliding the first sliding component against a second sliding component having a diamond-like carbon on a sliding surface;forming scrolls of the h-BN 2D material around the nanodiamonds; andgraphitizing the nanodiamonds, converting the scrolled nanodiamonds into nano-onions.2. The method of claim 1 , further comprising establishing a dry environment over the substrate.3. The method of claim 1 , wherein disposing the solution over the substrate comprises forming patches of the material on the substrate.4. The method of claim 1 , wherein forming patches of the material on the substrate comprises spraying a liquid containing the material onto the substrate.5. The method of claim 1 , wherein disposing the nanoparticles over the substrate comprises spraying a liquid containing the nanoparticles onto the substrate.6. A low friction wear surface comprising:a substrate;graphene disposed over the substrate; and{'sub': 3', '4, 'nanoparticles disposed over the substrate, the nanoparticles selected from the group consisting of diamond, Ni, Fe, Pt, Co, SiNand combinations thereof;'}wherein the nanoparticles are free from oxidation.7. The low friction wear surface of claim 6 , wherein the nanoparticles comprise iron.8. The low friction wear surface of claim 6 , wherein the substrate comprises at ...

PROCESS FOR PRODUCING RENEWABLE PRODUCTS

The present disclosure relates to a method for producing renewable ketones, paraffin waxes, base oil components and alkenes from a feedstock of biological origin, wherein the method includes ketonisation of esters of fatty acids and monohydric alcohols wherein the alcohols have carbon chain length of two or more. 1. A method for producing simultaneously renewable ketones and renewable alkenes from a feedstock of biological origin , the method comprising steps of:a) providing a feedstock of biological origin containing fatty acids and/or fatty acid esters;b) subjecting the feedstock to esterification reaction in a presence of a monohydric alcohol, wherein the monohydric alcohol has a carbon chain length of two or more, yielding esters of the fatty acids and the monohydric alcohol, in proviso that when the feedstock includes esters of fatty acids and a monohydric alcohol, wherein the monohydric alcohol has a carbon chain length of two or more, step b) is optional,c) subjecting the esters of the fatty acid and the monohydric alcohol to ketonisation reaction in a presence of a metal oxide ketonisation catalyst, yielding an intermediate product stream containing ketones, alkenes and carbon dioxide; andd) separating the alkenes from the intermediate product stream yielding an alkene depleted intermediate product stream and the separated alkenes.2. The method according to claim 1 , comprising:subjecting the feedstock to prehydrogenation reaction in a presence of hydrogenation catalyst prior to step b).3. The method according to claim 1 , comprising:purifying the feedstock prior to step b).4. The method according to claim 1 , comprising:purifying the ester of fatty acid and the monohydric alcohol prior to step c).5. The method according to claim 1 , comprising:subjecting the ester of fatty acid and the monohydric alcohol to prehydrogenation reaction in a presence of hydrogenation catalyst prior to step c).6. The method according to claim 1 , wherein the ketonisation ...

Simultaneous Production of Base Oil and Fuel Components from Renewable Feedstock

The present invention provides a method for simultaneous production of components suitable for production of base oil and fuel components. In the method a feedstock comprising fatty acids and/or fatty acid esters is entered into a reaction zone and subjected to a ketonisation reaction in the presence of a dual catalyst system. This system is configured to perform a ketonisation reaction and a hydrotreatment reaction, under hydrogen pressure. Subsequently ketones are obtained. 1. A method for simultaneous production of components suitable for production of base oil and fuel components , comprising the steps of:a) introducing a feedstock comprising fatty acids and/or fatty acid esters into a reaction zone, andb) subjecting said feedstock to a ketonisation reaction in said reaction zone in the presence of a dual catalyst system configured to perform a ketonisation reaction and a hydrotreatment reaction, under hydrogen pressure, andc) obtaining from said ketonisation reaction ketones in addition to linear hydrocarbons from said fatty acids and/or fatty acid esters.2. The method according to claim 1 , wherein said obtained ketones are further hydrodeoxygenated to form linear hydrocarbons.3. The method according to claim 1 , wherein said fatty acid esters are triglycerides.4. The method according to claim 1 , wherein said feedstock is at least partly claim 1 , preferably completely claim 1 , in liquid form when entered into said reaction zone.5. The method according to claim 1 , wherein the pressure in said reaction zone is less than 10 MPa claim 1 , preferably from 0.1 to 5 MPa.6. The method according to claim 1 , wherein the temperature in said reaction zone is from 200 to 450° C.7. The method according to claim 1 , wherein the ratio of hydrogen to feedstock is from 100 to 600 NI/I claim 1 , preferably from 100 to 500 NI/I.8. A method for simultaneous production of base oil components and fuel components claim 1 , comprising the steps of(i) introducing a feedstock ...

PROCESS FOR PRODUCING NAPHTHENIC BASE OILS

A process for producing naphthenic base oils from low quality naphthenic crude feedstocks. The naphthenic base oils produced by the process have improved low temperature properties at high yields based on feedstock. 153.-. (canceled)54. A process for producing a naphthenic base oil comprising the steps of:a) hydrotreating a naphthenic feedstock having a sulfur content of up to about 5% by weight (as measured by ASTM D4294) and a nitrogen content of up to about 3% by weight (as measured by ASTM D5762) in the presence of a hydrotreating catalyst and hydrotreating conditions to produce a hydrotreated naphthenic effluent;b) dewaxing the hydrotreated naphthenic effluent having a sulfur content of about 0.0005% to about 0.5% by weight (as measured by ASTM D4294) and a nitrogen content of up to about 0.1% by weight (as measured by ASTM D5762) in the presence of a dewaxing cracking catalyst and under catalytic dewaxing conditions to produce a dewaxed effluent;c) hydrofinishing the dewaxed effluent in the presence of a hydrofinishing catalyst and under catalytic hydrofinishing conditions to produce a dewaxed hydrofinished effluent having reduced levels of polycyclic aromatic hydrocarbon compounds and reduced levels of unstable olefinic compounds; andd) fractionating the dewaxed hydrofinished effluent to remove one or more low viscosity high volatility fractions and provide a naphthenic base oil having a pour point (as measured by ASTM D5949) below about −5° C., at a yield greater than 85% of total naphthenic base oil over total hydrotreated naphthenic feedstock.55. The process of claim 54 , wherein the naphthenic feedstock comprises naphthenic crude claim 54 , waxy naphthenic crude claim 54 , naphthenic distillate or a mixture thereof.56. The process of claim 54 , wherein the naphthenic feedstock comprises a blend of naphthenic crude claim 54 , waxy naphthenic crude or a naphthenic distillate with paraffinic feedstock claim 54 , paraffinic distillate claim 54 , light or ...

CONTINUOUS PROCESS FOR THE MANUFACTURE OF GREASE

This disclosure relates to a continuous process for preparing a grease thickener product in which operating conditions of the continuous process can be varied to obtain desired grease product properties. The process includes: (a) introducing a Cto Chydroxy fatty acid or a Cto Chydroxy fatty acid ester, and a metal base into a reaction zone; (b) operating the reaction zone at a temperature between 100° C. and 240° C. to react the Cto Chydroxy fatty acid or the Cto Chydroxy fatty acid ester, and the metal base, to produce a grease thickener product; (c) introducing the grease thickener product of step (b) into a flash chamber zone; and (d) operating the flash chamber zone at a temperature sufficient to remove volatiles from the grease thickener product of step (b). The continuous process conditions afford a production throughput of grease thickener product of greater than 8,000 pounds per hour. 1. A continuous process for preparing a grease thickener product , said process comprising:{'sub': 3', '30', '3', '30, '(a) introducing a Cto Chydroxy fatty acid or a Cto Chydroxy fatty acid ester, and a metal base into a reaction zone;'}{'sub': 3', '30', '3', '30, '(b) operating the reaction zone at a temperature between about 100° C. and about 240° C. to react the Cto Chydroxy fatty acid or the Cto Chydroxy fatty acid ester, and the metal base, to produce a grease thickener product;'}(c) introducing the grease thickener product of step (b) into a flash chamber zone; and 'wherein continuous process conditions afford a production throughput of grease thickener product of greater than about 8,000 pounds per hour.', '(d) operating the flash chamber zone at a temperature sufficient to remove volatiles from the grease thickener product of step (b);'}2. The continuous process of claim 1 , further comprising:(e) passing the grease thickener product of step (b) through a reaction zone back pressure valve operated between about 10 and about 300 psig;(f) passing the grease thickener ...

Durable surface coatings

Described herein are durable coatings, i.e. for medical devices, and methods of forming the coatings.

MINERAL BASE OIL AND LUBRICATING OIL COMPOSITION

Provided is a mineral base oil having a kinematic viscosity at 40° C. of 4.0 mm/s or more and less than 6.0 mm/s, a kinematic viscosity at 100° C. of 1.0 mm/s or more and less than 2.0 mm/s, and a flash point of 140° C. or higher. A lubricating oil composition containing the mineral base oil has a high flash point while having a low viscosity and thus having excellent fuel-saving performance when used as a driving system oil and the like. 1: A mineral base oil having:{'sup': 2', '2, 'a kinematic viscosity at 40° C. of 4.0 mm/s or more and less than 6.0 mm/s,'}{'sup': 2', '2, 'a kinematic viscosity at 100° C. of 1.0 mm/s or more and less than 2.0 mm/s, and'}a flash point of 140° C. or higher.2: The mineral base oil according to claim 1 , wherein a temperature gradient Δ|η*| of complex viscosity between two temperature points −10° C. and −25° C. is 0.1 Pa·s/° C. or less as measured with a rotary rheometer under conditions at an angular velocity of 6.3 rad/s and a strain amount of 0.1 to 100%.3: The mineral base oil according to claim 1 , wherein the kinematic viscosity at 100° C. is 1.5 mm/s or more and less than 2.0 mm/s.4: The mineral base oil according to claim 1 , wherein a feedstock oil for the mineral base oil has a proportion of an n-paraffin component of 50% by volume or less based on 100% by volume of the total amount of an aroma component claim 1 , a naphthene component claim 1 , the n-paraffin component claim 1 , and an isoparaffin component.5: The mineral base oil according to claim 1 , wherein a feedstock oil for the mineral base oil has a 10 volume percent distillation temperature of 250° C. or higher and a 90 volume percent distillation temperature of 320° C. or higher in a distillation test in accordance with JIS K2254.6: The mineral base oil according to claim 1 , wherein a feedstock oil for the mineral base oil has a kinematic viscosity at 40° C. of 4.0 to 6.0 mm/s and a kinematic viscosity at 100° C. of 1.0 to 2.0 mm/s.7: The mineral base oil ...

STABLE LUBRICANT EMULSION

A stable lubricant emulsion composition for use in engine and gear applications is provided. The emulsion includes a base petroleum oil, an aqueous salt solution that functions as a friction/wear modifier, and a polymeric non-ionic surfactant composition having a hydrophilic-lipophilic balance value in the range of 2.5 to 7 and an average molecular weight in the range of 1,000 to 3,000. The surfactant composition may include a polyester surfactant, a PIB succinimide surfactant, a PIB amine surfactant, or a mixture thereof. 1. A lubricant composition , said composition comprising a water-in-oil emulsion comprising:a base oil;a friction modifier in the form of an aqueous salt solution; and 'wherein the dispersant has an average molecular weight in the range of 1,000 to 3,000 and a hydrophilic-lipophilic balance value in the range of 2.5 to 7.', 'a polymeric dispersant in an amount effective to form a stable emulsion,'}2. The lubricant composition of claim 1 , wherein the dispersant has a hydrophilic-lipophilic balance value in the range of 4 to 6.3. The lubricant composition of claim 1 , wherein the dispersant has an average molecular weight in the range of 1 claim 1 ,000 to 2 claim 1 ,000.4. The lubricant composition of claim 1 , wherein the dispersant comprises a polyester surfactant claim 1 , a PIB succinimide surfactant claim 1 , a PIB amine surfactant claim 1 , or a mixture thereof.5. The lubricant composition of claim 1 , wherein the dispersant comprises a polyester surfactant mixed with a PIB succinimide surfactant.6. The lubricant composition of claim 1 , wherein the dispersant comprises a polyester surfactant mixed with a PIB amine surfactant.7. The lubricant composition of claim 1 , wherein the emulsion is stable for at least six weeks.8. A method for formulating a water-in-oil emulsion comprising: a base oil; a friction modifier in the form of an aqueous salt solution; and a polymeric dispersant having an average molecular weight in the range of 1 claim 1 , ...

ELECTRORHEOLOGICAL FLUID

The present invention provides an electrorheological fluid, which includes a dielectric particle, a conductor particle and insulating oil, and the dielectric particle is evenly dispersed in the insulating oil; wherein the conductor particle is evenly dispersed in the insulating oil or inlaid in an interior and on a surface of the dielectric particle. The electrorheological fluid has the advantages of high shear stress, long service life, good temperature stability and small leakage current. 1. An electrorheological fluid , comprising a dielectric particle , a conductor particle and insulating oil , wherein the dielectric particle is evenly dispersed in the insulating oil , and the conductor particle is evenly dispersed in the insulating oil or inlaid in an interior and on a surface of the dielectric particle.2. The electrorheological fluid according to claim 1 , wherein the dielectric particle has a dielectric constant greater than 10 and a resistivity greater than 10 Ω·m.3. The electrorheological fluid according to claim 2 , wherein the dielectric particle is selected from one or more of TiO claim 2 , CaTiO claim 2 , BaTiO claim 2 , SrTiOand LaTiO.4. The electrorheological fluid according to claim 1 , wherein when a temperature is less than 20° C. claim 1 , the conductor particle is a solid with a resistivity less than 10Ω·m claim 1 , and the conductor particle is selected from one or more of metal claim 1 , carbon and a conductive organic matter.5. The electrorheological fluid according to claim 4 , wherein the metal is one or more of Ag claim 4 , Al claim 4 , Au claim 4 , Cu claim 4 , Fe claim 4 , Hf claim 4 , In claim 4 , Nd claim 4 , Ni claim 4 , Pd claim 4 , Pt claim 4 , Rh claim 4 , Ru claim 4 , Sm claim 4 , Sn claim 4 , Ti claim 4 , V claim 4 , Y and Zr;the carbon is one or more of amorphous carbon, graphite, graphene and reduced graphene oxide; andthe conductive organic matter is one or more of polyacetylene, polythiophene, polypyrrole, polyaniline, ...

Detergent for lubricant oil and production process thereof

A lubricant oil detergent and a producing process thereof are disclosed. A process for producing a lubricant oil additive having a TBN from about 100 to about 400 includes reacting, at an elevated temperature, of composition (A) an alkyl salicylic acid or an alkyl salicylate ester, composition (B) an alkaline earth metal hydroxide added by one time or plural times during the reaction; composition (C) which contains at least one compound which is (i) an alcohol, or (ii) an carboxylic acid or an carboxylic anhydride; composition (D) base oil; and composition (E) carbon dioxide introduced after the composition (B) by one time, or introduced each time when the composition (B) is added if the composition (B) is added by plural times; solvent having a low boiling point is removed from the reacted mixture after the overbasing under vacuum, and the reacted mixture is filtered to obtain a clear liquid product.

UREA GREASE

A urea grease of the invention is prepared by applying shear to a mixture of a monoamine compound and a diisocyanate compound to cause a reaction in the mixture, in which the monoamine compound consists of an alicyclic monoamine, and the urea grease has Peak High32-64s of 10 or less and Level High32-64s of 40 or less according to an FAG method. 1: A urea grease , prepared by a method comprising:applying shear to a mixture of a monoamine compound and a diisocyanate compound to cause a reaction in the mixture,whereinthe monoamine compound consists of an alicyclic monoamine, andthe urea grease has Peak High32-64s of 10 or less and Level High32-64s of 40 or less according to an FAG method.2: The urea grease according to claim 1 , whereinthe alicyclic monoamine consists of cyclohexylamine.3: The urea grease according to claim 1 , wherein{'sup': 2', '−1, 'the shear is applied at a shear rate of 10sor more.'}4: The urea grease according to claim 1 , wherein{'sup': 3', '−1, 'the shear is applied at a shear rate of 10sor more.'}5: The urea grease according to claim 1 , whereinthe mixture is prepared by mixing a first base oil comprising the monoamine compound and a second base oil comprising the diisocyanate compound.6: The urea grease according to claim 5 , whereinthe shear is applied to the mixture within 15 minutes after mixing the first base oil and the second base oil.7: The urea grease according to claim 1 , wherein{'sup': 7', '−1, 'the shear is applied at a shear rate of 10sor less.'}8: The urea grease according to claim 1 , whereinratio of a maximum shear rate to a minimum shear rate in the shear applied to the mixture is 70 or less. The present invention relates to a urea grease.A typical manufacturing method of a urea grease includes: mixing a base oil with isocyanate to prepare a first solution and heat the first solution to about 60 degrees C.; mixing a base oil with amine to prepare a second solution and heat the second solution to about 60 degrees C.; adding ...

Additive Tackifier Agent for Water-Soluble Lubricants

A composition for an aqueous tacky lubricant, specifically targeted towards increasing lubricant retention to the moving components of chainsaws. More specifically, the composition includes a novel additive composition for environmentally-neutral lubricants. The ideal function of the composition would be to increase the adhesive qualities of an aqueous lubricant without compromising the coolant and lubricant roles of such a substance. To accomplish this, the composition includes an additive compound, that is made of a linear anionic polyamide and a cationic surfactant. The reaction between the linear anionic polyamide and the cationic surfactant creates a viscoelastic tackifier that helps the lubricant to cling to a moving chain thus preventing the lubricant from flinging off the chain when in motion. In other words, the additive compound is a tackifier agent, presented as novel both as an independent composition and in addition to extant lubricants. 1. A composition for a water-soluble lubricant with increased adhesive quality , comprising:a quantity of an anionic linear polyamide;a quantity of a cationic surfactant;a quantity of a water-soluble lubricant;the quantity of the anionic linear polyamide and the quantity of the cationic surfactant, being homogeneously mixed into a lubricant additive;the quantity of the water-soluble lubricant and the lubricant additive being homogeneously mixed into an aqueous tacky lubricant.2. The composition of claim 1 , wherein the anionic linear polyamide being a compound comprising linear 2-propenoic acid claim 1 , sodium salt claim 1 , and polymer with 2-propenamide.3. The composition of claim 1 , wherein the lubricant additive being a viscoelastic tackifier.4. The composition for aqueous tacky lubricant claimed in comprises:the quantity of the anionic linear polyamide ranging between 0.001 percentage by weight (wt. %) and 20 wt. % of the aqueous tacky lubricant.5. The composition for aqueous tacky lubricant claimed in comprises: ...

LUBRICANTS THAT INCLUDE ALKYL ESTERS AND FATTY ACIDS

One or more embodiments presently described are directed to lubricants and methods for making such lubricants. According to one embodiment, a lubricant suitable for use in a water-based drilling fluid may comprise one or more alkyl esters and a fatty acid blend comprising one or more medium-chain fatty acids. The one or more medium-chain fatty acids may be at least 50 weight percent (wt. %) of the fatty acid blend. The weight ratio of the one or more alkyl esters to the fatty acid blend may be from 1:1 to 3:1. 1. A lubricant suitable for use in a water-based drilling fluid , the lubricant comprising:one or more alkyl esters; anda fatty acid blend comprising one or more medium-chain fatty acids, where the one or more medium-chain fatty acids are at least 50 wt. % of the fatty acid blend,where the weight ratio of the one or more alkyl esters to the fatty acid blend is from 1:1 to 3:1.2. The lubricant of claim 1 , where the one or more medium-chain fatty acids comprise at least caproic acid and caprylic acid.3. The lubricant of claim 2 , where the molar ratio of caproic acid to caprylic acid is from 10:90 to 90:10.4. The lubricant of claim 1 , where each of the one or more medium-chain fatty acids have a melting point of less than or equal to 50° C.5. The lubricant of claim 1 , where the one or more alkyl esters are derived from vegetable oil.6. The lubricant of claim 1 , where the one or more alkyl esters are from 50 wt. % to 75 wt. % of the lubricant.7. The lubricant of claim 1 , where the fatty acid blend is from 25 wt. % to 50 wt. % of the lubricant.8. The lubricant of claim 1 , where the fatty acid of the lubricant is a liquid.9. A method for making a drilling fluid lubricant claim 1 , the method comprising:mixing one or more medium-chain fatty acids to make a liquid fatty acid blend;mixing the liquid fatty acid blend with one or more alkyl esters to from a lubricant precursor; andheating the lubricant precursor to a temperature of at least 50° C. and mechanically ...

LUBRICANTS THAT INCLUDE ALKYL ESTERS AND FATTY ACIDS

One or more embodiments presently described are directed to lubricants and methods for making such lubricants. According to one embodiment, a lubricant suitable for use in a water-based drilling fluid may comprise one or more alkyl esters and a fatty acid blend comprising at least palmitic acid and stearic acid. The sum of the weight percent of the palmitic acid and stearic acid may be at least 50 wt. % of the fatty acid blend. The weight ratio of the one or more alkyl esters to the fatty acid blend may be from 1:1 to 3:1. The molar ratio of palmitic acid to stearic acid may be from 20:80 to 40:60. 1. A lubricant suitable for use in a water-based drilling fluid , the lubricant comprising:one or more alkyl esters; anda fatty acid blend comprising at least palmitic acid and stearic acid, where the sum of the weight percent of the palmitic acid and stearic acid is at least 50 wt. % of the fatty acid blend, and where the fatty acid blend is a liquid,where the weight ratio of the one or more alkyl esters to the fatty acid blend is from 1:1 to 3:1; andthe molar ratio of palmitic acid to stearic acid is from 20:80 to 40:60.2. The lubricant of claim 1 , where the weight ratio of the one or more alkyl esters to the fatty acid blend is from 1.5:1 to 2.5:1.3. The lubricant of claim 1 , where the molar ratio of palmitic acid to stearic acid is from 24:76 to 32:68.4. The lubricant of claim 1 , where the one or more alkyl esters are derived from vegetable oil.5. The lubricant of claim 1 , where the one or more alkyl esters are from 50 wt. % to 75 wt. % of the lubricant.6. The lubricant of claim 1 , where the fatty acid blend is from 25 wt. % to 50 wt. % of the lubricant.7. (canceled)8. A method for making a drilling fluid lubricant claim 1 , the method comprising:mixing solid palmitic acid and solid stearic acid to make a solid fatty acid blend;heating the solid fatty acid blend to form a liquid fatty acid blend;mixing the liquid fatty acid blend with one or more alkyl esters to ...

Catalytic Depolymerisation of Polymeric Materials

A process for converting a molten polymeric material is provided. The process includes effecting disposition of a molten polymeric material, having at least one carbon-carbon double bond, in sufficient proximity to a catalyst material within a reaction zone, to affect a reactive process that effects generation of a reaction product. The reactive process effects cleaving of at least one carbon-carbon double bond. The catalyst material includes [Fe—Cu—Mo—P]/AlOprepared by binding a ferrous-copper complex to an alumina support to generate an intermediate material and reacting the intermediate material with a heteropolyacid. 1. A wax prepared by a method , said method comprising:(a) selecting a waste polymeric feed,(b) heating said waste polymeric feed to create a molten polymeric material; and(c) depolymerizing said molten material in a reaction vessel until a predetermined pressure is reached to create said wax.2. The wax of wherein said depolymerization is aided by a catalyst.3. The wax of wherein said catalyst is [Fe—Cu—Mo—P]/AlO.4. The wax of wherein said waste polymeric feed comprises at least 90% polypropylene.5. The wax of wherein the temperature in said reaction vessel is between 300° C. to 400° C. during said depolymerization.6. The wax of wherein the temperature of the wall of said reaction vessel does not exceed 500° C.7. The wax of wherein said wax has a melting point between 100 and 170° C.8. The wax of wherein said depolymerization is aided by a catalyst claim 4 , wherein said catalyst is [Fe—Cu—Mo—P]/AlO.9. The wax of wherein said catalyst claim 8 , wherein said catalyst is between 1 to 6 percent weight of the total weight of the mixture of said molten polymeric material and said catalyst material.10. The wax of wherein said predetermined pressure is within the range of 10 to 10 claim 4 ,000 psi.11. The wax of wherein said waste polymeric feed comprises at least 90% polyethylene.12. The wax of wherein the temperature in said reaction vessel is between ...

Plasma treatment of liquid surfaces

A method of decreasing a water contact angle and/or increasing a surface energy of a liquid is disclosed herein, the method comprising exposing the liquid to a plasma treatment. Further disclosed is a plasma-treated liquid exhibiting a decreased water contact angle and/or increased surface energy, compared to the water contact angle and/or surface energy, respectively, of a non-treated corresponding liquid. Methods for combining a first liquid and a second liquid, or for enhancing an adhesion between a liquid and a surface of another substance, the methods comprising exposing a liquid to plasma treatment, are further disclose herein, as well as a method of predicting an apparent contact angle of a liquid droplet on a surface of a substance.

Process for Preparing Polymers and Compositions Thereof

The present invention provides a process for preparing a polymer, employing the steps of: (1) contacting a free radical initiator; a chain transfer agent containing a thiocarbonyl thio group and a free radical leaving group; and a radically polymerisable monomer, to form a polymer chain; and (2) contacting the polymer chain of step (1) with at least one of a polyvalent coupling agent, a polymerisation inhibitor, a grafting acylating agent, an amine and an oil of lubricating viscosity. The invention further provides compositions and uses for the polymer. 1. A composition comprising an oil of lubricating viscosity and a star polymer derived from at least two monomers comprising:(a) at least 50 wt % of a mixture of C12 to C15 alkyl substituted (meth)acrylate monomers; and(b) less than 50 wt % of an alkyl (meth)acrylate monomer containing 1 to 30 carbon atoms in the alkyl group, other than the C12 to C15 alkyl substituted (meth)acrylate monomer;(c) optionally containing less than 20 wt % styrene; and(d) optionally containing less than 10 wt % alkyl methacrylamide, wherein the star-polymer has about 7 to about 50 arms present on the star polymer, and wherein the star polymer is prepared by a reversible addition-fragmentation chain transfer controlled radical polymerisation process.2. The composition of claim 1 , wherein the star polymer is derived from at least two monomers consisting essentially of:(a) at least 50 wt % of a mixture of C12 to C15 alkyl substituted (meth)acrylate monomers; and(b) less than 50 wt % of an alkyl (meth)acrylate monomer containing 1 to 30 carbon atoms in the alkyl group, other than the C12 to C15 alkyl substituted (meth)acrylate monomer.3. The composition of claim 1 , wherein the star polymer is derived from at least two monomers comprising:(a) at least 50 wt % of a mixture of C12 to C15 alkyl substituted (meth)acrylate monomers; and(b) less than 50 wt % of an alkyl (meth)acrylate monomer containing 1 to 30 carbon atoms in the alkyl group, ...

GREASE AND METHOD FOR MANUFACTURING GREASE

A grease of the invention contains a base oil and a thickener, where, when the volumetric-based arithmetic mean particle size of particles contained in the grease measured using laser diffraction/scattering method is A (unit: μm), a formula A≦3 (1) is satisfied. 1: A grease , comprising:a base oil; anda thickener, {'br': None, 'i': 'A≦', '3\u2003\u2003(1).'}, 'wherein A (unit: μm) representing a volumetric-based arithmetic mean particle size of particles comprised in the grease calculated using laser diffraction/scattering method satisfies a formula (1)2: The grease according to claim 1 , wherein the thickener is one of urea claim 1 , a thickener for a simple soap grease claim 1 , and a thickener for a complex grease.3: The grease according to claim 2 , wherein the thickener is one of a calcium soap claim 2 , a lithium soap claim 2 , a sodium soap claim 2 , a calcium complex soap claim 2 , a lithium complex soap claim 2 , and a calcium sulfonate complex soap.4: The grease according to claim 2 , wherein;the thickener is urea,the urea is a reaction product of a monoamine and a diisocyanate, andthe monoamine is composed of a single amine compound or is a mixture of a plurality of amine compounds.5: The grease according to claim 1 , wherein the grease is prepared by mixing the thickener or a precursor of the thickener in the base oil to provide a mixture solution claim 1 , and applying a minimum shear rate of 10sor more to the mixture solution.6: The grease according to claim 1 , wherein the grease is prepared by mixing a first base oil comprising a first thickener precursor and a second base oil comprising a second thickener precursor to prepare a mixture solution claim 1 , and applying a minimum shear rate of 10sor more to the mixture solution.7: A manufacturing method of a grease claim 1 , the method comprising:{'sup': 2', '−1, 'applying a minimum shear rate of 10sor more to at least one of a first base oil comprising a first thickener precursor and a second base oil ...

Method for Reducing Piston Deposits in a Marine Diesel Engine

A method of reducing the incidence of deposits on the pistons of a 4-stroke marine diesel engine during operation of the engine when it is fuelled with a marine residual fuel meeting the ISO 8217 2017 fuel standard for marine residual fuels and having a sulphur content of more than 0.1% and less than 0.5% by mass. The method includes the step of lubricating the engine using a lubricating oil composition comprising: a) at least 50% by mass, based on the mass of the composition, of an oil of lubricating viscosity; (b) 5 to 25% by mass, based on the mass of the composition, of an oil-soluble or oil-dispersible alkali metal or alkaline earth metal salicylate detergent, or a mixture of two or more oil-soluble or oil-dispersible alkali metal or alkaline earth metal salicylate detergents; (c) 0.1 to 10% by mass, based on the mass of the composition of one or more oil-soluble or oil-dispersible ashless dispersants; and optionally, (d) 0.1 to 10% by mass, based on the mass of the composition of a polyalkylene-substituted succinic anhydride.

Novel water based metal working fluid composition

This invention is a composition of an ester resulting from the reaction of an oligomer of ethylene oxide in presence or a catalyst, with fatty acids. The resulting water based metal working fluid additive is useful as it imparts property of stable micro-emulsion and helps improving the wear life, coefficient of friction and other tribological properties among other uses.

Processes of preparing estolide base oils and lubricants that include transesterification

Provided herein are processes of producing estolide base oils, including the process comprising providing at least one fatty acid ester, and contacting the at least one fatty acid ester with at least one fatty acid to form an estolide base oil. Exemplary processes include the use of transesterification to form the at least one fatty acid ester and/or estolide base oil.

AQUEOUS ACIDIC COMPOSITION FOR TREATING METAL SURFACES, TREATING METHOD USING THIS COMPOSITION AND USE OF TREATED METAL SURFACE

An aqueous acidic composition for treating metal surfaces, the composition including the following components: 1. An aqueous acidic composition for treating metal surfaces , said composition comprising the following components:a) at least one water soluble or water dispersable anionic polyelectrolyte;b) at least one organofunctional silane comprising one or more reactive functional groups selected from the group comprising amino, mercapto, methacryloxy, epoxy and vinyl;c) at least one water dispersible solid wax;wherein the weight ratio between components a:b is in the range of 1:2-4:1, based on dry matter;the weight ratio between components (a+b):c is in the range of 1:3-3:1, based on dry matter, and wherein components a and b may be present—at least partially—as their graft reaction product,wherein the at least one anionic polyelectrolyte has an acid value of at least 250.2. The aqueous acidic composition according to claim 1 , wherein the at least one anionic polyelectrolyte has an acid value of at least 400 mg KOH/g.3. The aqueous acidic composition according to claim 2 , wherein the at least one anionic polyelectrolyte has an acid value of at least 600 mg KOH/g.4. The aqueous acidic composition according to claim 2 , wherein the at least one anionic polyelectrolyte has an acid value of at least 700 mg KOH/g.5. The aqueous acidic composition according to claim 1 , wherein the at least one anionic polyelectrolyte is present in an amount of 0.6-40 g/L.6. The aqueous acidic composition according to claim 5 , wherein the at least one anionic polyelectrolyte is present in an amount of 1.6-20 g/L.7. The aqueous acidic composition according to claim 1 , wherein the at least one organofunctional silane is present in an amount of 0.3-40 g/L.8. The aqueous acidic composition according to claim 7 , wherein the at least one organofunctional silane is present in an amount of 0.8-20 g/L.9. The aqueous acidic composition according to claim 1 , wherein the at least one water ...

Lubricant Composition and Methods of Manufacture

A lubricant made by a method of modifying fluid suspended metal sulfide particles that does not require use of hazardous additives. The base oil is derived from a proprietary ester lubricant. The formulation process includes a centrifugation step to remove non-colloidal metal sulfide particles. These non-colloidal particles may be collected and turned into colloidal particles for use in future batches of lubricant.

Lubricant Viscosity Modification System

A system for modifying viscosity of a lubricant. The system including a viscosity modification device configured to change viscosity of the lubricant between a first viscosity and a second viscosity. The second viscosity is lower than the first viscosity. 1. A system for modifying viscosity of a lubricant , the system comprising:a viscosity modification device configured to change viscosity of the lubricant between a first viscosity and a second viscosity, the second viscosity is lower than the first viscosity.2. The system of claim 1 , wherein the lubricant includes engine oil claim 1 , transmission oil claim 1 , or engine cylinder lubricant.3. The system of claim 1 , wherein the viscosity modification device is a frequency pulse generator configured to:generate a first frequency pulse and pass the first frequency pulse through the lubricant to provide the lubricant at the first viscosity; andgenerate a second frequency pulse that is lower than the first frequency pulse and pass the second frequency pulse through the lubricant to provide the lubricant at the second viscosity.4. The system of claim 3 , wherein:the first frequency pulse is above a natural resonance frequency of the lubricant; andthe second frequency pulse is below the natural resonance frequency of the lubricant.5. The system of claim 1 , wherein the viscosity modification device is an electric pulse generator configured to:generate a first electric pulse and pass the first electric pulse through the lubricant to provide the lubricant at the first viscosity; andgenerate a second electric pulse that has a lower voltage than the first electric pulse and pass the second electric pulse through the lubricant to provide the lubricant at the second viscosity.6. The system of claim 1 , wherein at the first viscosity claim 1 , molecules of the lubricant are claim 1 , overall claim 1 , closer together as compared to the second viscosity.7. The system of claim 1 , wherein the lubricant includes nanoparticles ...

Catalytic system for preparation of high branched alkane from olefins

The present invention discloses a catalytic system for preparing highly branched alkane from olefin, which contains novel nickel or palladium complexes. In the presence of the catalytic system, highly branched oily alkane mixture can be efficiently obtained from olefins (such as ethylene) under mild conditions. The alkane mixture has a low bromine number, and can be used as a processing aid(s) and lubricant base oil with high-performance. Provides also was a method for preparing the catalyst and a method for preparing an oily olefin polymer.

Process For Applying Nanoparticle Hard Coatings On Parts

A process for applying a low coefficient of friction coating to interacting parts of a mechanical device. The low coefficient coating is comprised of nanoparticles of a metal melting below about 400° C., preferably bismuth. Interacting parts of a mechanical device, prior to assembly of the mechanical device, are submerged in a dispersion of the nanoparticles, then heated to an effective temperature, then cooled, thereby resulting in a coating of the nanoparticles onto the interacting parts. 1. A process for applying a low coefficient of friction coating to interacting parts having interacting surfaces , of a mechanical device , prior to assembly of the device , which process comprises:i) dispersing about 0.001 wt. % to about 2 wt. % of nanoparticles of one or more metals having a melting point less than about 400° C. in a lubricating oil, thereby forming a dispersion;ii) placing at least a portion of the interacting surfaces of said interacting parts to be coated into said nanoparticle dispersion for an effective amount of time to enable nanoparticles to be adhered to at least a fraction of the interacting surfaces;iii) heating said interacting parts to a temperature effective to initiate sintering of said metal nanoparticles thereby resulting in the adhered nanoparticles to form a coating on said interacting surfaces; andiv) cooling the coated interacting parts thereby resulting in a final coated interacting parts ready for assembly into a machine for which the part was designed.2. The process of wherein the metal is selected from bismuth claim 1 , cadmium claim 1 , tin claim 1 , indium claim 1 , and lead.3. The process of wherein the metal is bismuth.4. The process of wherein the mean particle size of the metal nanoparticles is from about 2 to 60 nm.5. The process of wherein the lubricant is selected from lubricating oils and greases.6. The process of wherein the lubricant is a lubricating oil.7. The process of wherein the lubricating oil is a natural lubrication ...

Method of inspecting lubricating oil composition and method of producing lubricating oil composition

The invention provides a method of inspecting a lubricating oil composition and a method of producing a lubricating oil composition. The inspecting method is capable of stably reproducing wear resistance characteristics by using a relatively easy measuring method even in the case where the lubricating oil composition contains a fullerene. In the method of inspecting the lubricating oil composition, the particle size (r) of particles present in the lubricating oil composition containing a base oil and fullerene is measured, and the lubricating oil composition is sorted on the basis of a predetermined range of the particle size (r) set by the relationship between the measured value of the particle size (r) and the measured value of the wear coefficient of the lubricating oil composition.

Blown and stripped plant-based oils

A method for producing a high viscosity, low volatiles blown stripped plant-based oil is provided. The method may include the steps of: (i) obtaining a plant-based oil; (ii) heating the oil to at least 90C; (iii) passing air through the heated lilt to produce a blown oil having a viscosity of at least 200 cSt at 40C; (iv) stripping the blown oil from step (iii) to reduce an acid value of the blown oil to from 5 mg KOH/g to about 9 rag KOH/g; (v) adding a polyol to the stripped oil from (iv), and (vi) stripping the oil from step (v) to reduce the acid value of the oil to less than 5.0 mg KOH/g or less.

Lubricant composition having improved high-temperature durability

The present disclosure relates to a lubricant composition including a base oil, a thickener and a thickener supplement, and a method of manufacturing the same. The lubricant composition of the present disclosure is effective at improving performance at high-temperature by maintaining the evaporation amount and friction characteristics even at high temperatures, thus inhibiting oil contamination of powertrain parts and the like and maintaining sticking phenomenon even in a high-temperature environment, thereby increasing the durability of parts.

Highly Wear-Resistant Plant Genetic Lubricant Oil Additive, Preparation Method and Application Thereof

A highly wear-resistant plant genetic lubricant oil additive, a preparation method and an application thereof are disclosed. The additive includes 90-97% of a plant base oil and 3-10% of an aerogel. The plant base oil is prepared from a mixed plant oil of soybean oil, rapeseed oil, sesame oil, peanut oil, olive oil, castor seed oil, salad oil, sunflower seed oil and tung oil. The highly wear-resistant plant genetic lubricant oil additive is added to various lubricant oils for being used to devices, and a colloidal substance is generated after the devices are driven and heat is generated, so that the lubricant oils are firmly adhered to the surface of components. The lubricant oil additive not only has characteristics of high abrasion resistance, high and low temperature resistance, and oxidation resistance, but also the used lubricant oil can be regenerated and recycled after being recovered and filtered. 1. A highly wear-resistant plant genetic lubricant oil additive , which comprises by volume percentage:92-97% of a plant base oil prepared from a mixed plant oil of soybean oil, rapeseed oil, sesame oil, peanut oil, olive oil, castor seed oil, salad oil, sunflower seed oil and tung oil; and3-8% of an aerogel.2. The highly wear-resistant plant genetic lubricant oil additive claim 1 , as recited in claim 1 , wherein the aerogel is a porous material with a pore diameter in a range of 50-150 nm.3. The highly wear-resistant plant genetic lubricant oil additive claim 1 , as recited in claim 1 , wherein the mixed plant oil comprises 5-15% of the soybean oil claim 1 , 5-15% of the rapeseed oil claim 1 , 5-15% of the sesame oil claim 1 , 5-20% of the peanut oil claim 1 , 5-15% of the olive oil claim 1 , 5-20% of the castor seed oil claim 1 , 5-15% of the salad oil claim 1 , 5-20% of the sunflower seed oil claim 1 , and 5-8% of the tung oil by volume percentage.4. The highly wear-resistant plant genetic lubricant oil additive claim 1 , as recited in claim 1 , wherein the ...

CATALYTIC UPCYCLING OF POLYOLEFINS INTO LUBRICANTS

A method of upcycling polymers to useful hydrocarbon materials. A catalyst with nanoparticles on a substrate selectively docks and cleaves longer hydrocarbon chains over shorter hydrocarbon chains. The nanoparticles exhibit an edge to facet ratio to provide for more interactions with the facets. 1. A method producing a lubricant comprising:exposing, at a temperature of 150-350° C. and a pressure of 100-200 psi for 12-72 hours, a plurality polymer molecules to a catalyst comprising a substrate having a plurality of catalytic nanoparticles deposited thereon;docking a first polymer molecule of the plurality of polymer molecules to the catalyst;cleaving at least one carbon-carbon bond of the first polymer molecule;forming a plurality of hydrocarbon fragments from the cleaving;selectively docking to the catalyst a second polymer molecule of the plurality of polymer molecules, preferentially over the plurality of hydrocarbon fragments;cleaving at least one carbon-carbon bond of the second polymer molecule; andforming a second plurality of hydrocarbon fragments.2. The method of claim 1 , wherein exposing the plurality of polymer molecules is for at least 24 hours.3. The method of claim 1 , wherein the plurality of catalytic nanoparticles comprise Pt or Ni.4. The method of claim 1 , wherein the substrate comprises a perovskite.5. The method of claim 4 , wherein the substrate comprises strontium titanate.6. The method of claim 3 , wherein the substrate comprises alumina.7. The method of claim 1 , wherein the plurality of polymer molecules are solvent-free.8. The method of claim 1 , wherein the plurality of polymer molecules have a molecular weight ranging from 400-1000 Da.9. The method of claim 8 , wherein the plurality of hydrocarbon fragments are C30 to C76 alkanes.10. The method of claim 9 , wherein the plurality of hydrocarbon fragments have 10 branches per 1000 carbon to 400 branches per 1000 carbon.11. The method of claim 10 , wherein the plurality of hydrocarbon ...

LUBRICATING GREASE OF POLYUREA/HIGH BASE NUMBER CALCIUM SULFONATE COMPOSITE

The invention discloses a lubricating grease with thixotropy and a preparation method thereof. The lubricating grease comprises a polyurea/high base number calcium sulfonate composite thickener, colloidally dispersed calcium carbonate solid particles in the form of calcite, a calcium borate or calcium borate composite, and a calcium soap of fatty acid having 12 to 24 carbon atoms. The above components are uniformly dispersed in an oil phase medium. The content of high base number calcium sulfonate in the lubricating grease is less than 22 wt %. 1. A high performance , thixotropic polyurea/overbased calcium sulfonate complex hybrid grease comprising:70 to 85 wt % oleaginous medium in which there is homogeneously dispersed:at least 8 but less than 20 wt % overbased calcium sulfonate complex thickener comprising fine particles of calcium carbonate in calcite form;0.5 to 6.5 wt % polyurea thickener;0.05 to 3 wt % calcium borate or calcium borate complex;{'sub': '12-24', '0.5 to 3.5 wt % calcium soap of Caliphatic fatty acids; and'}0 to 3 wt % lime or calcium hydroxide,wherein all percentages are weight % based on the total weight of the grease.2. The grease as claimed in comprising:75 to 85 wt % oleaginous medium;10 to 19 wt % overbased calcium sulfonate complex thickener comprising fine particles of calcium carbonate in calcite form;0.8 to 5 wt % polyurea thickener;0.1 to 3 wt % calcium borate or a calcium borate complex;{'sub': '12-24', '0.8 to 3.5 wt % calcium soap of Chydroxy aliphatic fatty acids; and'}0 to 3 wt % lime or calcium hydroxide.3. The grease as claimed in claim 1 , wherein the calcium soap of a fatty acid of 12 to 24 carbon atoms comprises a calcium soap of a hydroxy fatty acid of 12 to 24 carbon atoms.4. The grease as claimed in claim 3 , wherein the calcium soap of hydroxy fatty acid of 12 to 24 carbon atoms comprises a calcium soap of hydroxystearic acid.5. The grease as claimed in claim 1 , wherein the calcium soap of Caliphatic fatty acids ...

IMPROVED PRODUCTION OF HEAVY API GROUP II BASE OIL

A process for heavy base oil production, comprising: a. performing an aromatic extraction of a first hydrocarbon feed to produce an aromatic extract, and a waxy raffinate; b. mixing the aromatic extract with a second hydrocarbon feed to make a mixed feed having greater than 2,000 wt ppm sulfur; c. feeding the mixed feed to a hydroprocessing unit to produce a heavy API Group II base oil having a kinematic viscosity at 70° C. from 22.6 to 100 mm/s. An integrated refinery process unit for making heavy base oils, comprising: a. an aromatic extraction unit fluidly connected to a solvent dewaxing unit and a hydroprocessing unit; b. a first line from the aromatic extraction unit, that feeds an aromatic extract to a second hydrocarbon feed to make a mixed feed having greater than 2,000 wt ppm sulfur; and c. a connection that feeds the mixed feed to the hydroprocessing unit. 1. A process for heavy base oil production , comprising:a. performing an aromatic extraction of a first hydrocarbon feed to produce an aromatic extract, and a waxy raffinate for further solvent dewaxing;b. mixing the aromatic extract with a second hydrocarbon feed to make a mixed feed having greater than 2,000 wt ppm sulfur;{'sup': '2', 'c. feeding the mixed feed to a hydroprocessing unit configured to produce a heavy API Group II base oil having a kinematic viscosity at 70° C. from 22.6 to 100 mm/s'}2. The process of claim 1 , wherein the aromatic extract comprises from 30 to 80 vol % aromatics.3. The process of claim 1 , wherein the hydroprocessing unit performs hydrotreating claim 1 , catalytic dewaxing claim 1 , and hydrofinishing.4. The process of claim 1 , wherein the waxy raffinate is solvent dewaxed and hydrofinished to produce a heavy API Group I base oil.5. The process of claim 1 , wherein the mixed feed has an initial boiling point less than 340° C.6. The process of claim 1 , wherein the mixed feed comprises from 5 to 20 wt % of the aromatic extract.7. The process of claim 1 , wherein the ...

Lithium-Based Grease and Preparation Method Thereof

A lithium-based grease and the preparation method thereof are provided. The raw materials for preparing the lithium-based grease include in parts by weight: 75-88 parts of base oil, 0.5-2.5 parts of antiwear agent, 0.1-1.5 parts of antirust agent, 0.1-1.5 parts of antioxidant, 5-25 parts of lubricant, 5-15 parts of thickening agent, and 0.6-2.0 parts of saponifying agent. The raw materials also include hydroxyl compound-containing modified graphene containing quaternary ammonium salt or aromatic ring. The grease has good colloid stability and mechanical stability, can greatly improve the antiwear property. More than that, the grease has excellent oxidation resistance, and can significantly shorten the reaction time of the saponification, reduce the reaction temperature of the saponification. 1. A lithium-based grease , characterized in that , the raw materials for preparing the lithium-based grease comprise in parts by weight:75-88 parts of base oil,0.5-2.5 parts of antiwear agent,0.1-1.5 parts of antirust agent,0.1-1.5 parts of antioxidant,5-25 parts of lubricant,5-15 parts of thickening agent, and0.6-2.0 parts of saponifying agent.2. The lithium-based grease according to claim 1 , characterized in that claim 1 , the raw materials for preparing the lithium-based grease further comprise in parts by weight: 0.001-1.5 parts of graphene material.3. The lithium-based grease according to claim 1 , characterized in that claim 1 , the raw materials for preparing the lithium-based grease further comprise in parts by weight: 0.001-1.5 parts of modified graphene.4. The lithium-based grease according to claim 3 , characterized in that claim 3 , the modified graphene is a hydroxyl compound-containing modified graphene.5. The hydroxyl compound-containing modified graphene according to claim 4 , characterized in that claim 4 , the hydroxyl compound-containing modified graphene is a hydroxyl compound-containing modified graphene containing a quaternary ammonium salt.6. The ...

CATALYTIC DEPOLYMERISATION OF POLYMERIC MATERIALS

A process for converting a molten polymeric material is provided. The process includes effecting disposition of a molten polymeric material, having at least one carbon-carbon double bond, in sufficient proximity to a catalyst material within a reaction zone, to affect a reactive process that effects generation of a reaction product. The reactive process effects cleaving of at least one carbon-carbon double bond. The catalyst material includes [Fe—Cu—Mo—P]/AlOprepared by binding a ferrous-copper complex to an alumina support to generate an intermediate material and reacting the intermediate material with a heteropolyacid. 1. A wax prepared by a method , said method comprising:(a) selecting a waste polymeric feed,(b) heating said waste polymeric feed to create a molten polymeric material; and(c) depolymerizing said molten material in a reaction vessel until a predetermined pressure is reached to create said wax.2. The wax of wherein said depolymerization is aided by a catalyst.3. The wax of wherein said catalyst is [Fe—Cu—Mo—P]/AlO.4. The wax of wherein said waste polymeric feed comprises at least 90% polypropylene.5. The wax of wherein the temperature in said reaction vessel is between 300° C. to 400° C. during said depolymerization.6. The wax of wherein the temperature of a wall of said reaction vessel does not exceed 500° C.7. The wax of wherein said wax has a melting point between 100 and 170° C.8. The wax of wherein said depolymerization is aided by a catalyst claim 4 , wherein said catalyst is [Fe—Cu—Mo—P]/AlO.9. The wax of wherein said catalyst is between 1 to 6 percent weight of the total weight of the mixture of said molten polymeric material and said catalyst.10. The wax of wherein said predetermined pressure is within the range of 10 to 10 claim 4 ,000 psi.11. The wax of wherein said waste polymeric feed comprises at least 90% polyethylene.12. The wax of wherein the temperature in said reaction vessel is between 300° C. to 600° C. during said ...

Methods for making foams using blowing agents comprising unsaturated fluorocarbons

Disclosed herein are blowing agents comprising fluorocarbons and/or hydrofluorocarbons useful in foamable compositions. Also disclosed are methods for forming a foam comprising the aforementioned blowing agents.

GREASE, MECHANICAL COMPONENT, AND METHOD FOR PRODUCING GREASE

Provided is a grease containing a base oil and a hydrophilic nanofiber, the hydrophilic nanofiber having a thickness (d) of 0.01 to 500 nm being dispersed therein. The grease is low in an environmental load and excellent in safety on the human body and also has an appropriate worked penetration and has a high dropping point, and therefore, it is also excellent in heat resistance. 1. A grease , comprising a base oil and a hydrophilic nanofiber , the hydrophilic nanofiber having a thickness (d) of 0.01 to 500 nm being dispersed therein.2. The grease according to claim 1 , wherein a content of the hydrophilic nanofiber is from 0.1 to 20% by mass on a basis of a total amount of the grease.3. The grease according to claim 1 , wherein a hydrophilic nanofiber having an aspect ratio of 5 or more is dispersed.4. The grease according to claim 1 , wherein the hydrophilic nanofiber comprises at least one polysaccharide selected from the group consisting of cellulose claim 1 , carboxymethyl cellulose claim 1 , chitin claim 1 , and chitosan.5. The grease according to claim 1 , further comprising a water resistance improver.6. A grease obtained by mixing a hydrophilic nanofiber having a thickness (d′) of 0.01 to 500 nm and a base oil.7. The grease according to claim 6 , obtained by mixing an aqueous dispersion in which a hydrophilic nanofiber having a thickness (d′) of 0.01 to 500 nm is blended in water claim 6 , a base oil claim 6 , and a dispersion solvent claim 6 , to prepare a mixed solution claim 6 , and then removing water and the dispersion solvent from the mixed solution.8. A mechanical component claim 1 , comprising the grease according to .9. A method for producing a grease claim 1 , the method comprising:Step (1): mixing an aqueous dispersion in which a hydrophilic nanofiber having a thickness (d′) of 0.01 to 500 nm is blended in water, a base oil, and a dispersion solvent, to prepare a mixed solution.10. The method for producing a grease according to claim 9 , further ...

PROCESS FOR PRODUCING NAPHTHENIC BRIGHT STOCKS

A process for producing naphthenic bright stocks from low quality naphthenic crude feedstocks. The naphthenic bright stocks produced by the process have improved low temperature properties at high yields based on feedstock. 133.-. (canceled)34. A process for producing a naphthenic bright stock comprising the steps of:a) dewaxing a naphthenic oil feedstock having a sulfur content of about 0.01 up to about 0.5% by weight (as measured by ASTM D4294) and a nitrogen content of about 0.01 up to about 0.1% by weight (as measured by ASTM D5762) in the presence of a dewaxing cracking catalyst and under catalytic dewaxing conditions to produce a dewaxed naphthenic effluent;b) hydrofinishing the dewaxed naphthenic effluent to produce a dewaxed hydrofinished naphthenic effluent having reduced levels of polycyclic aromatic hydrocarbon compounds and reduced levels of unstable olefinic compounds; andc) fractionating the dewaxed hydrofinished naphthenic effluent to separate the dewaxed hydrofinished naphthenic effluent into one or more gaseous fractions and one or more liquid fractions and to provide a naphthenic bright stock having a pour point (as measured by ASTM D5949) reduced by 10° C. compared to that of the naphthenic oil feedstock, at a yield greater than 85% of total naphthenic bright stock over total naphthenic oil feedstock.35. The process of claim 34 , wherein the naphthenic oil feedstock comprises hydrotreated deasphalted naphthenic crude claim 34 , hydrotreated deasphalted waxy naphthenic crude claim 34 , hydrotreated deasphalted naphthenic distillate or a mixture thereof.36. The process of claim 34 , wherein the naphthenic oil feedstock comprises a blend of hydrotreated deasphalted naphthenic crude claim 34 , hydrotreated deasphalted waxy naphthenic crude claim 34 , or a hydrotreated deasphalted naphthenic distillate with paraffinic feedstock claim 34 , paraffinic distillate claim 34 , light or heavy cycle oil claim 34 , deasphalted oil claim 34 , cracker residue ...

Method of producing lubricating base oil from feedstock comprising diesel fraction, and lubricating base oil produced thereby

Disclosed is a method of producing a lubricating base oil, including providing a feedstock including a diesel fraction, subjecting the feedstock to catalytic dewaxing, and recovering a lubricating base oil from a product of the catalytic dewaxing. A lubricating base oil produced thereby and a lubricant product including the lubricating base oil are also provided.

Superlubrious high temperature coatings

A low friction wear surface operable at high temperatures and high loads with a coefficient of friction in the superlubric regime including MoS 2 and graphene-oxide on the wear surface is provided, and methods of producing the low friction wear surface are also provided. The low friction wear surface remains with a coefficient of friction in the superlubric regime at temperatures in between about 200° C. and 400° C.

SUB-STOICHIOMETRIC METAL NITRIDES

A non-stoichiometric nanocomposite coating and method of making and using the coating. The non-stoichiometric nanocomposite coating is disposed on a base material, such as a metal or ceramic; and the nanocomposite consists essentially of a matrix of an alloy selected from the group of Cu, Ni, Pd, Pt and Re which are catalytically active for cracking of carbon bonds in oils and greases and a grain structure selected from the group of borides, carbides and nitrides. 1. A super lubricious apparatus comprising:a substrate;a nanocomposite coating on the substrate, the nanocomposite consisting essentially of a matrix of a catalytically active element embedded in the matrix, the matrix selected from nitrides, borides, carbides, and nitrocarbides of Cu, Ni, Pd, Pt and Re and mixtures thereof and the grains selected from the group of transition metal carbides, transition metal nitrides, transition metal carbo-nitrides, transition metal borides, refractory metal carbides, refractory metal nitrides, refractory metal carbo-nitrides, refractory metal borides;a hydrocarbon lubricant; anda carbon film disposed between the nanocomposite coating and the hydrocarbon lubricant.2. The method as defined in wherein the alloy is about 1% to 10% by weight and the particles from about 90% to 99% by weight.3. The method as defined in wherein the substrate is selected from the group of a metal and a ceramic.4. The method as defined in wherein the base material comprises a steel based material.5. The method as defined in wherein the oil is essentially free of additives.6. The method as defined in where the carbon film consists essentially of diamond like carbon.7. The method as defined in where the grains are selected from the group of refractory metal carbides claim 1 , carbo-nitrides claim 1 , nitrides and borides.8. A method for lubricating materials in wear contact claim 1 , comprising the steps of:providing a base material;disposing a nanocomposite coating on the base material, the ...

Entry sheet for drilling use

The present invention relates to an entry sheet for drilling use, which exhibits excellent hole position accuracy even when transported at ambient temperature for a long time and/or stored under a thermal environment having a higher temperature than in Japan, more specifically to an entry sheet for drilling use for a laminated board or a multi-layered board comprising a metallic support foil and a layer of water-soluble resin composition formed on at least one surface of the metallic support foil, wherein the water-soluble resin composition comprises a water-soluble resin, a water-soluble lubricant and a linear unsaturated fatty acid salt, the layer of water-soluble resin composition is formed by cooling from a cooling start temperature of 120° C. to 160° C. to a cooling end temperature of 25° C. to 40° C. within 60 seconds at a cooling rate of not less than 1.5° C./sec, the water-soluble resin composition has a degree of crystallinity of not less than 1.2, the layer of water-soluble resin composition has a standard deviation σ of surface hardness of not more than 2, and a surface hardness of not less than 8.5 to not more than 25 N/mm 2 .

High Viscosity Index Comb Polymer Viscosity Modifiers and Methods of Modifying Lubricant Viscosity Using Same

A comb copolymer viscosity modifier may be made by polymerization comprising at least, or consisting essentially of, the following monomers: (a) a hydrogenated polybutadiene-based (alk)acrylate ester macromonomer (which repeat units may comprise from 7.0 wt % to 18 wt % of the repeat units of the comb copolymer viscosity modifier); (b) a C-Calkyl (alk)acrylate ester monomer (which repeat units may comprise from 40 wt % to 71 wt % or from 45 wt % to 64 wt % of the repeat units of the comb copolymer viscosity modifier); and (c) a C-Calkyl (alk)acrylate ester monomer, wherein repeat units based on the C-Calkyl (alk)acrylate ester monomer comprise at least 21.0 wt % (and optionally up to 35.0 wt %) of repeat units of the comb copolymer viscosity modifier. Lubricant compositions comprising the comb copolymer viscosity modifier, as well as uses thereof and methods for modifying viscosity, are also contemplated herein. 2. The lubricant composition of claim 1 , wherein the comb copolymer viscosity modifier comprises substantially no repeat units based on styrene monomer claim 1 , and wherein repeat units based on the C-Calkyl (alk)acrylate ester monomer comprise up to 35.0 wt % of repeat units of the comb copolymer viscosity modifier.3. The lubricant composition of claim 1 , wherein repeat units based on the hydrogenated polybutadiene-based (alk)acrylate ester macromonomer comprise from 7.0 wt % to 18 wt % of the repeat units of the comb copolymer viscosity modifier.4. The lubricant composition of claim 1 , wherein repeat units based on the C-Calkyl (alk)acrylate ester monomer comprise from 40 wt % to 71 wt % of the repeat units of the comb copolymer viscosity modifier.5. The lubricant composition of claim 4 , wherein repeat units based on the C-Calkyl (alk)acrylate ester monomer comprise from 45 wt % to 64 wt % of the repeat units of the comb copolymer viscosity modifier.6. The lubricant composition of claim 1 , wherein:{'sub': 3', '8, '(i) the C-Calkyl (alk)acrylate ester ...

METHODS FOR MAKING A PLASTICIZED POLYMER, METHODS FOR MAKING A COMPOSITION USING THE PLASTICIZED POLYMER, AND COMPOSITIONS COMPRISING THE PLASTICIZED POLYMER

A method for making a plasticized polymer comprises polymerizing a polymerizable monomer, such as an ethylenically unsaturated monomer, in a plasticizer, such as mineral oil, and in the presence of a catalyst system. The plasticized polymer may be mixed with a tackifying resin in a method for making an adhesive. A composition, which may be useful as an adhesive, comprises a polymer system comprising a first polymer; a plasticized system comprising a first plasticizer that was in the presence of the first polymer during the polymerization step to make the first polymer; and a tackifier. The method can be used to make compositions having polymers with a low density or a low molecular weight or both. The final compositions made by methods of the invention include adhesives, sealants, coating, or lubricants. 1. A method for making a plasticized polymer comprising the step of:polymerizing a polymerizable monomer in a plasticizer and in the presence of a catalyst system for a time and temperature sufficient to form the plasticized polymer.2. The method of claim 1 , wherein the polymerizing step is a batch process.3. The method of claim 1 , wherein the polymerizing step is a continuous process.4. The method of claim 1 , wherein the molecular weight of the polymer is between about 5 claim 1 ,000 to about 200 claim 1 ,000 g/mol claim 1 , preferably between about 7 claim 1 ,500 g/mol to about 150 claim 1 ,000 g/mol claim 1 , more preferably between about 10 claim 1 ,000 g/mol to about 100 claim 1 ,000 g/mol claim 1 , and most preferably between about 10 claim 1 ,000 g/mol to about 80 claim 1 ,000 g/mol.5. The method of claim 1 , wherein the amount of monomer added is sufficient to provide an amount of polymer in the plasticized polymer of from about 2 wt % to an amount just below the solubilization limit of the plasticized polymer at 230° C.6. The method of claim 1 , wherein the monomer comprises an unsaturated monomer.7. The method of claim 6 , wherein the unsaturated ...

PRODUCTION OF RENEWABLE BASE OIL AND DIESEL BY PRE-FRACTIONATION OF FATTY ACIDS

Methods are disclosed for producing renewable base oil and a diesel oil from low-value biological oils. Low-value biological oils containing free fatty acids and fatty acid esters can be processed into a renewable base oil and a renewable diesel oil by first separating at least part of the saturated free fatty acids from the feedstock and then processing separately this saturated free acid feed in a ketonisation reaction followed by hydrodeoxygenation and hydroisomerisation reactions to yield a renewable base oil stream. The remaining free fatty acid depleted feed may be processed in a separate hydrodeoxygenation and hydroisomerisation step to yield a renewable diesel stream. 1. A method for producing a renewable base oil from a feedstock of biological origin , the method comprising:a) providing a feedstock, the feedstock containing at least 5 wt % of a mixture of saturated free fatty acids and at most a remainder of one or more compounds selected from the list consisting of: unsaturated free fatty acids, fatty acid esters, fatty amides, fatty alcohols, as well as fatty acid glycerols such as mono-glycerides, di-glycerides and tri-glycerides of fatty acids; {'sub': 'n', 'a saturated fatty acid feed containing at least 90 wt % saturated Cfree fatty acids, no more than 3 wt % unsaturated free fatty acids, where n is selected from one of the integer values; 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 21, 22, 23, 24; and one or more saturated fatty acid depleted feed(s);'}, 'b) separating the feedstock into at leastc) subjecting the saturated fatty acid feed to ketonisation reaction conditions where two fatty acids react to yield a ketone stream, the ketone stream including as a major part saturated ketones having a carbon number of 2n−1; andd) subjecting the ketone stream to both hydrodeoxygenation reaction conditions and to hydroisomerisation reaction conditions, simultaneously or in sequence, to yield a deoxygenated and isomerised base oil stream containing the ...

LUBRICATING GREASE OF POLYUREA/HIGH BASE NUMBER CALCIUM SULFONATE COMPOSITE

The invention discloses a lubricating grease with thixotropy and a preparation method thereof. The lubricating grease comprises a polyurea/high base number calcium sulfonate composite thickener, colloidally dispersed calcium carbonate solid particles in the form of calcite, a calcium borate or calcium borate composite, and a calcium soap of fatty acid having 12 to 24 carbon atoms. The above components are uniformly dispersed in an oil phase medium. The content of high base number calcium sulfonate in the lubricating grease is less than 22 wt %, and the lubricating grease has a worked cone penetration of 295 or less. 1. A high performance , thixotropic polyurea/overbased calcium sulfonate complex hybrid grease , comprising a polyurea/overbased calcium sulfonate complex thickener; solid , finely divided particles of colloidally dispersed calcium carbonate in the form of calcite; calcium borate or a complex of calcium borate , and a calcium soap of a fatty acid of 12 to 24 carbon atoms , evenly dispersed in an oleaginous medium , characterized in that the grease contains 70 wt % or more of the oleaginous medium and less than 22 wt % of overbased calcium sulfonate based on the total weight of the grease.2. The grease as claimed in having a worked cone penetration rating of 295 or less.3. The grease as claimed in comprising:70 to 85 wt % oleaginous medium in which there is homogeneously dispersed:8 to 21 wt % overbased calcium sulfonate complex thickener comprising fine particles of calcium carbonate in calcite form;0.5 to 6.5 wt % polyurea thickener;0.05 to 3 wt % calcium borate or calcium borate complex;{'sub': '12-24', '0.05 to 5 wt % calcium soap of Caliphatic fatty acids; and'}0 to 3 wt % lime or calcium hydroxide,wherein all percentages are weight % based on the total weight of the grease.4. The grease as claimed in comprising:75 to 85 wt % oleaginous medium;10 to 19 wt % overbased calcium sulfonate complex thickener comprising fine particles of calcium carbonate ...

Liquid-Infused Surfaces Featuring Reduced Drag Characteristics, and Methods for Fabricating the Same

In a broad aspect of the invention there are provided liquid infused surfaces that feature drag reducing characteristics. In a further broad aspect, the present invention provides methods for designing and fabricating liquid infused surfaces that feature drag reducing characteristics. In a yet further broad aspect the present invention provides methods for increasing the operating efficiency of systems in which a flowing bulk fluid is in contact with a patterned surface, the increased operating efficiency specifically being realized from a reduction of the drag forces due to the bulk fluid flowing over the patterned surface.

PROCESS FOR THE MANUFACTURE OF BASE OIL

Processes are provided for producing hydrocarbon base oils from alcohols, including by converting one or more alcohols into linear alpha olefins, and then forming branched oligomers with one or more olefin feedstock(s) which are subsequently hydrogenated and fractionated. A process for the preparation of a mixture of branched saturated hydrocarbons can include (a) forming an oligomerization reaction mixture having an oligomerization catalyst system and an olefin monomer mixture, wherein the olefin monomer mixture has an average carbon number in the range of 9.5 to 13, and at least 10% of the olefin monomers in the olefin monomer mixture have a carbon number difference of at least four carbons, (b) oligomerizing the olefin monomers in the oligomerization reaction mixture to produce an oligomer product, (c) separating unreacted olefin monomer from the oligomer product to produce a purified oligomer product, (d) hydrogenating the purified oligomer product, and (e) distilling the hydrogenated oligomer product. 1. A process for the preparation of a mixture of branched saturated hydrocarbons , the process comprising:(a) forming an oligomerization reaction mixture comprising an oligomerization catalyst system and an olefin monomer mixture, wherein the olefin monomer mixture has an average carbon number in the range of 9.5 to 13, and at least 10% of the olefin monomers in the olefin monomer mixture have a carbon number difference of at least four carbons,(b) oligomerizing the olefin monomers in the oligomerization reaction mixture to produce an oligomer product comprising dimers, trimers, and higher oligomers,(c) separating unreacted olefin monomer from the oligomer product to produce a purified oligomer product,(d) hydrogenating the purified oligomer product to form a mixture of branched saturated hydrocarbons having a Bromine Index below 1000 as determined in accordance with ASTM D2710-09, and(e) distilling the hydrogenated oligomer product.2. The process of wherein the ...

METHOD OF MAKING A GREASE THICKENER AND THE THICKENER MADE BY THE METHOD

A continuous process for producing a polyurea concentrate or powder. The process includes combing at least one amine and an isocayante in the presence of a liquid diluent or a base oil in a rotor stator mixer. The concentrate comprises a polyurea in a base oil wherein the concentration of from about 20 weight percent to about 50, or 40 or 35 or 30 weight percent of polyurea based on total weight of grease thickener. The powder has particle size of 2 to 400 microns. This concentrate or powder can then be formulated by grease manufacturers to the desired final properties without the need for handling of the isocyanate and amine raw materials. 1. A process comprising providing at least one amine and a first base oil to a rotor stator mixer which is operating at a shear rate of less than 5000 reciprocal seconds (1/sec) , adding a isocyanate to the mixer in the shear zone and in a position such that a residence time in the mixer after addition of the isocyanate is less than 20 seconds to produce a paste comprising a polyurea.2. The process of characterized in that the process is continuous.3. The process of wherein the at least one amine is a mixture comprising a first linear primary amines having six to eighteen carbon atoms and either a second linear primary amines having six to eighteen carbon atoms or a cyclic primary amine.4. The process of wherein the residence time is less than 10 seconds.5. The process of wherein the residence time is less than 5 seconds.6. The process of wherein the at least one amine is a primary amine and the isocyanate is a di-isocyanate such that the poly urea formed is a diurea.7. The process of wherein the at least one amine comprises an alkylamine and a fatty amine.8. The process of wherein the paste comprises at least 20 weight percent of the polyurea.9. The process of wherein the first base oil is selected from API Groups I claim 1 , II claim 1 , III claim 1 , IV or V.10. The process of further comprising diluting the paste with a ...

Lubricant and srt material

The invention provides an SRT material (lubricant) applicable to machine elements such as bearings, seals or guides (guiding mechanisms) that constitute a slide part of a machine. A lubricant and an SRT material are disclosed.

POLYMER GREASE MANUFACTURING PROCESS

A process for the manufacture of a lubricating grease composition, the process comprising steps of: (a) providing an essentially homogeneous liquid composition comprising a lubricating oil and a thickening polymer, and (b) flowing the liquid composition through a shear-mixing device to mix and cool the liquid composition to form a lubricating grease composition. 1. A process for a manufacture of a lubricating grease composition , the process comprising steps of:providing an essentially homogeneous liquid composition comprising a lubricating oil and a thickening polymer;flowing the essentially homogeneous liquid composition through a shear-mixing device to mix and cool the essentially homogeneous liquid composition to form the lubricating grease composition,wherein the thickening polymer forms from 5 to 20 wt % of the essentially homogeneous liquid composition,wherein the liquid composition flows through the shear-mixing device along a flow-path provided with one or more temperature-controlled portions to each at least one of heat and cool the liquid composition,wherein the shear-mixing device comprises at least one pair of heat-transfer plates between which the liquid composition is flowed,wherein the surface of at least one plate is provided with surface features in a flow path of the liquid composition which act as baffles for the flow of the liquid composition, causing shear-mixing.2. The process according to claim 1 , wherein the essentially homogeneous liquid composition is provided at a temperature of from 150 to 350° C. from 200 to 250° C.3. The process according to claim 1 , wherein the lubricating oil comprises oils selected from mineral oils claim 1 , synthetic hydrocarbons claim 1 , ester oils claim 1 , vegetable oils and mixtures of two or more thereof.4. The process according to claim 1 , claims claim 1 , the thickening polymer further comprising a polymer selected from polyamides claim 1 , polyesters claim 1 , polyethylene oxides claim 1 , polyethylene ...

BASE OILS AND METHODS OF MAKING THE SAME

A process for the preparation of saturated hydrocarbon base oils is provided, comprising oligomerization of a feed mixture that has an average carbon number in the range of 14 to 18 to produce an oligomer product comprising dimers, trimers, and higher oligomers, where the dimer has a branching proximity (BP) of 20 or greater, isomerization of at least the dimer portion, and hydrogenation of the isomerized product. The dimer portion is separated from the oligomer product, and a saturated hydrocarbon base oil is obtained comprising greater than 90% dimers having an average carbon number in the range of from 29 to 36, and the dimer portion having a weight average molecular weight in the range of 422 to 510, where the dimers have an average Branching Index (BI) in a range of 22 to 26 and an average paraffin branching proximity (BP) in a range of from 18 to 26. 1. A process for the preparation of a saturated hydrocarbon base oil , comprising:forming an oligomerization reaction mixture comprising an oligomerization catalyst system and an olefin monomer feed mixture, wherein the olefin monomer feed mixture has an average carbon number in the range of 14 to 18;oligomerizing the olefin monomer feed mixture in the reaction mixture to produce an oligomer product comprising dimers, trimers, and higher oligomers,isomerizing at least the dimer portion of the oligomer product in the presence of an acid catalyst to form a mixture of branched hydrocarbons;{'sub': '2', 'hydrogenating the isomerized branched hydrocarbons, to a Bromine Index below 1000 mg Br/100 g as determined in accordance with ASTM D2710-09; and'}separating the dimer portion of the hydrogenated oligomer product, whereby a saturated hydrocarbon base oil is obtained comprising greater than 90 wt % dimers having an average carbon number in the range of from 29 to 36, the dimer portion having a weight average molecular weight in the range of from 422 to 510,{'sub': '2', 'wherein the dimers of the oligomer product, in a ...

Method for Making Electrorheological Fluids

Dispersions are prepared by dispersing a polymer precursor such as a polyol into a non-aqueous fluid. The resulting droplets of the polymer precursor is partially polymerized to produce liquid or partially gelled droplets, and then sized to a target particle size. The sized particles are then cured to form solid particles. The process allows for close control of particle size, allows for good control of temperature, and is amenable to batch, semi-continuous or even continuous operation. The resulting dispersions are useful as electrorheological fluids. 1. A method of forming a rheological fluid , comprising the steps of:a) dispersing (1) at least one curable polymer precursor that has reactive groups which engage in a curing reaction to form a cured polymer into (2) a non-aqueous liquid in which the curable polymer precursor is substantially insoluble, to form a dispersion of droplets of the curable polymer precursor in a continuous phase of the non-aqueous liquid;b) forming a partially cured dispersion by curing the curable polymer precursor in the dispersed droplets to the extent of 1 to 25% of full cure without solidifying the droplets, to form partially cured droplets;c) sizing the partially cured droplets to a final target droplet size range; and thend) under non-resizing conditions, curing the curable polymer precursor in the sized, partially cured droplets to form a dispersion of solid polymer particles in the non-aqueous fluid.2. The method of claim 1 , wherein in steps b) and d) claim 1 , the curable polymer precursor is cured by adding a curing agent and reacting the curing agent with the curable polymer precursor claim 1 , wherein in step b) enough curing agent is added to react with 1 to 25 mole percent of the reactive groups of the curable polymer precursor.3. The method of claim 2 , wherein step c) is performed by passing the partially cured dispersion formed in step b) through a static mixer or rotor-stator.4. The method of claim 2 , wherein step a) ...

METHOD FOR SIMULTANEOUSLY AND STABLY DISPERSING SPHERICAL NANOPARTICLES IN OIL MEDIUM BY USING LAYERED NANOSHEETS AND APPLICATION THEREOF

Provided are a method for simultaneously and stably dispersing spherical nanoparticles in an oil medium by using layered nanosheets and an application thereof. The method comprises: (1) mixing the layered nanosheets and oil-soluble alkylamines to obtain a first mixture containing intercalated/exfoliated nano sheets; (2) mixing spherical nanoparticles and the oil medium to obtain a second mixture; and (3) mixing the first mixture, the second mixture and the oil medium to obtain a third mixture. 1. A method for simultaneously and stably dispersing spherical nanoparticles in an oil medium by using layered nanosheets , comprising:mixing the layered nanosheets and oil-soluble alkylamines to obtain a first mixture containing intercalated/exfoliated nanosheets;mixing the spherical nanoparticles and the oil medium to obtain a second mixture; andmixing the first mixture, the second mixture and the oil medium to obtain a third mixture.2. The method according to claim 1 , wherein the layered nanosheets and the oil-soluble alkylamines are mixed by means of heat treatment claim 1 , ultrasonic treatment or mechanical agitation.3. The method according to claim 1 , wherein the layered nanosheets are at least one selected from α-zirconium phosphate claim 1 , θ-zirconium phosphate claim 1 , γ-zirconium phosphate claim 1 , layered metal phosphates claim 1 , clays claim 1 , layered double hydroxides claim 1 , layered disulfide metal salts and layered tungsten acid metal salts.4. The method according to claim 1 , wherein the layered nanosheets are of a particle size of 10 to 4000 nm claim 1 , preferably 10 to 3000 nm.5. The method according to claim 1 , wherein the oil-soluble alkylamines are primary amines claim 1 , secondary amines claim 1 , tertiary amines or cyclic amines.6. The method according to claim 1 , wherein the oil-soluble alkylamines are Guerbet primary amines claim 1 , aliphatic amines or poly-aliphatic amines.9. The method according to claim 8 , wherein the aliphatic ...

Base oil hydrotreating catalyst and process of use

An improved hydrotreating catalyst and process for making a base oil product wherein the catalyst comprises a base extrudate that includes a high nanopore volume amorphous silica alumina (ASA) and a second amorphous silica alumina. The catalyst and process generally involve the use of a base extrudate comprising the high nanopore volume ASA and the second ASA in a catalyst to produce hydrotreated dewaxed base oil products by contacting the catalyst with a hydrocarbon feedstock. The catalyst base extrudate advantageously comprises a first amorphous silica alumina having a pore volume in the 11-20 nm pore diameter range of 0.2 to 1.0 cc/g and a second amorphous silica alumina having a pore volume in the 11-20 nm pore diameter range of 0.02 to 0.2 cc/g, with the base extrudate formed from the amorphous silica alumina and the alumina having a total pore volume in the 2-50 nm pore diameter range of 0.12 to 1.80 cc/g. The catalyst further comprises at least one modifier element from Groups 6 to 10 and Group 14 of the Periodic Table. The catalyst and process provide improved aromatics saturation.

PROCESSES FOR PRODUCING POLY ALPHA OLEFINS AND APPARATUSES THEREFOR

The present disclosure provides processes and apparatus for producing poly alpha olefins. In at least one embodiment, a process to produce a poly alpha olefin includes introducing a first olefin monomer to a first catalyst and an activator in a first reactor to form a first reactor effluent comprising olefin dimers and olefin timers. The process includes heating the first reactor effluent to form an isomerized product and introducing the isomerized product to a filtration unit to form a filtration effluent. The process may include introducing the filtration effluent to a first distillation unit to form a first distillation effluent. The process may include introducing the first distillation effluent to a second distillation unit to form a second distillation effluent. The process includes introducing the first distillation effluent and/or the second distillation effluent to a second catalyst in a second reactor to form a second reactor effluent comprising the olefin timers. 1. A process to produce a poly alpha olefin , the process comprising:introducing a first olefin monomer to a first catalyst and an activator in a first reactor to form effluent comprising a vinylidene olefin dimer;heating the effluent to isomerize the vinylidene dimers to form tri-substituted olefin dimers to form an isomerized product;introducing the isomerized product and a second olefin monomer to a second catalyst in a second reactor to form a second reactor effluent comprising olefin trimer formed by the oligomerization of the tri-substituted olefin dimers and the second olefin monomer.2. The process of claim 1 , wherein heating the effluent to isomerize the vinylidene dimers is performed without added isomerization catalysts.3. The process of claim 1 , wherein the second olefin monomer is the same as the first olefin monomer.4. The process of claim 1 , wherein the second olefin monomer is different from the first olefin monomer.5. The process of claim 1 , further comprising introducing the ...

Coated substrate

The invention to which this application relates is improvements to the provision of Molybdenum and/or Tungsten containing coatings of the type which can be used to improve certain characteristics of the surface of a substrate to which the coating is applied. In one embodiment the coating also includes Ti to provide the advantages of high adhesion, high humidity and wear resistance of the coating and TiB 2 to promote the formation of a relatively uniform, dense, coating, so strengthening the coating which is formed and improving the high temperature performance of the coatings.

METHOD FOR MANUFACTURING OIL GEL CAPSULES AND METHOD FOR MANUFACTURING CONTACT PART FOR VEHICLE, INCLUDING OIL GEL CAPSULES

The present disclosure relates to manufacturing oil gel capsules and adding the same to an overlay layer of a contact part for a vehicle. The present disclosure may provide a method for manufacturing oil gel capsules and a method for manufacturing a contact part for a vehicle, including the oil gel capsules. The oil gels in the oil gel capsules manufactured by the present disclosure may respond to the temperature environment of a contact part for a vehicle, and an aggregation phenomenon of gelators or an aggregation phenomenon of surfactants may not occur even after an oil is released. Therefore, as oil gel capsules are added to an overlay layer, the present disclosure may improve low friction characteristics and seizure resistance characteristics of a contact part for a vehicle without any side effects caused by the above-described aggregation phenomenon. 1. A method for manufacturing oil gel capsules , the method comprising:(a) manufacturing oil gels by mixing an oil and a gelator; and(b) producing at least one or more oil gel capsules by mixing the oil gels and an aqueous surfactant solution.2. The method of claim 1 , wherein the oil gel capsules are produced by surrounding the oil gel with a surfactant.3. The method of claim 1 , wherein the oil gels in step (b) are in a liquid state.4. The method of claim 1 , wherein the oil gel capsules have a size of 0.1 μm or more and less than 10 μm.5. The method of claim 1 , wherein the oil gel capsules have a size of 0.1 μm or more and 1 μm or less.6. The method of claim 1 , wherein in step (a) claim 1 , the oil and the gelator are mixed using an ultrasonic grinder.7. The method of claim 1 , wherein in step (b) claim 1 , the oil gel and the aqueous surfactant solution are mixed using an ultrasonic grinder.8. The method of claim 1 , wherein the oil is an engine oil.9. The method of claim 1 , wherein the gelator is 12-hydroxyoctadecanoic acid.10. The method of claim 1 , wherein the oil is an engine oil claim 1 , the gelator ...

PROCESSES FOR PRODUCING POLY ALPHA OLEFINS AND METHOD OF ANALYSIS AND APPARATUSES THEREFOR

The present disclosure provides processes and apparatus for producing poly alpha olefins. In at least one embodiment, a process to produce a poly alpha olefin includes introducing a first olefin monomer to a first catalyst and an activator in a first reactor to form a first reactor effluent comprising an olefin dimer and an olefin trimer. The process includes introducing the first reactor effluent to a filtration unit to form a filtration effluent, and introducing the filtration effluent to a first distillation unit to form a first distillation effluent. The process includes introducing the first distillation effluent (or a second distillation effluent) to a second catalyst in a second reactor to form a second reactor effluent comprising the olefin trimer. The process includes removing a sample at any stage of the process and introducing the sample to a gas chromatograph. 1. A process to produce a poly alpha olefin , the process comprising:introducing a first olefin monomer to a first catalyst and an activator in a first reactor to form a first reactor effluent comprising an olefin dimer;introducing the first reactor effluent to a distillation unit to form a distillation effluent;introducing the distillation effluent to a second catalyst and a second olefin monomer in a second reactor to form a second reactor effluent comprising an olefin timer;removing a sample from (1) the first reactor, (2) a line coupling the first reactor to the distillation unit; (3) a line coupling the distillation unit to the second reactor;introducing the sample to a gas chromatograph via a split/split-less injection port; andmeasuring by gas chromatography an amount of one or more of vinylidene dimers and/or tri substituted dimers.2. The process of claim 1 , further comprising:isomerizing the vinylidene dimers to form tri-substituted dimers in the first reactor effluent or the distillation effluent, or both.3. The process of claim 1 , wherein introducing the sample to the gas chromatograph ...

CIRCULAR ECONOMY FOR PLASTIC WASTE TO POLYETHYLENE AND LUBRICATING OIL VIA CRUDE AND ISOMERIZATION DEWAXING UNITS

Provided is a continuous process for converting waste plastic into recycle for polyethylene polymerization. In one embodiment, the process comprises selecting waste plastics containing polyethylene and/or polypropylene and passing the waste plastics through a pyrolysis reactor to thermally crack at least a portion of the polyolefin waste and produce a pyrolyzed effluent. The pyrolyzed effluent is separated into offgas, a naphtha/diesel fraction, a heavy fraction, and char. The naphtha/diesel fraction is passed to a crude unit distillation column in a refinery where a straight run naphtha (C-C) fraction or a propane/butane (C-C) fraction is recovered. The straight run naphtha fraction (C-C) or the propane/butane (C-C) fraction is passed to a steam cracker for ethylene production. The heavy fraction from the pyrolysis unit can also be passed to an isomerization dewaxing unit to produce a base oil. 1. A continuous process for converting waste plastic into recycle for polyethylene polymerization comprising:(a) selecting waste plastics containing polyethylene and/or polypropylene;(b) passing the waste plastics from (a) through a pyrolysis reactor to thermally crack at least a portion of the polyolefin waste and produce a pyrolyzed effluent;(c) separating the pyrolyzed effluent into offgas, a naphtha/diesel fraction, a heavy fraction, and char;(d) passing the naphtha/diesel fraction to a crude unit in a refinery;{'sub': 5', '8, '(e) recovering a straight run naphtha (C-C) fraction from the crude unit;'}{'sub': 5', '8, '(f) passing the straight run naphtha fraction (C-C) to a steam cracker for ethylene production; and'}(g) passing the heavy fraction to an isomerization dewaxing unit to produce a base oil.2. The process of claim 1 , wherein the naphtha/diesel fraction of (c) is passed directly to a refinery crude unit and the contaminants are removed in a crude unit desalter.3. The process of claim 1 , wherein contaminants are removed at the pyrolysis site.4. The process of ...

CIRCULAR ECONOMY FOR PLASTIC WASTE TO POLYPROPYLENE AND LUBRICATING OIL VIA REFINERY FCC AND ISOMERIZATION DEWAXING UNITS

A continuous process for converting waste plastic into recycle for polypropylene polymerization is provided. The process integrates refinery operations to provide an effective and efficient recycle process. The process comprises selecting waste plastics containing polyethylene and polypropylene and then passing the waste plastics through a pyrolysis reactor to thermally crack at least a portion of the polyolefin waste and produce a pyrolyzed effluent. The pyrolyzed effluent is separated into offgas, a naphtha/diesel fraction, a heavy fraction, and char. The naphtha/diesel fraction is passed to a refinery FCC unit, from which is recovered a liquid petroleum gas Colefin/paraffin mixture. The Cparaffins and Colefins are separated into different fractions with a propane/propylene splitter. The Colefin fraction is passed to a propylene polymerization reactor. The Cparaffin fraction is optionally passed to a dehydrogenation unit to produce additional propylene and then the resulting Colefin is passed to a propylene polymerization reactor. The heavy fraction of pyrolyzed oil is passed to an isomerization dewaxing unit to produce a lubricating base oil. 1. A continuous process for converting waste plastic into recycle for polypropylene polymerization comprising:(a) selecting waste plastics containing polyethylene and/or polypropylene;(b) passing the waste plastics from (a) through a pyrolysis reactor to thermally crack at least a portion of the polyolefin waste and produce a pyrolyzed effluent;(c) separating the pyrolyzed effluent into offgas, a naphtha/diesel fraction, a heavy fraction, and char;(d) passing the naphtha/diesel fraction to a refinery FCC unit;{'sub': '3', '(e) recovering a liquid petroleum gas Colefin/paraffin mixture from the FCC unit;'}{'sub': 3', '3, '(f) separating the Cparaffin and Colefin into different fractions;'}{'sub': '3', '(g) passing the Colefin to a propylene polymerization reactor; and'}(h) passing the heavy fraction to an isomerization ...

METHOD FOR MANUFACTURING A MECHANICAL TIMEPIECE PART PROVIDED WITH A MAGNETIC FUNCTIONAL AREA

A method for manufacturing a mechanical timepiece part () including at least one functional area () wherein a lubricant () is able to be confined, the method including a step () of constructing a blank of the part () including the at least one functional area () and a step of transforming () the at least one functional area () into a magnetised functional area () capable of cooperating with the lubricant () when it has magnetic properties. 1. A method for manufacturing a mechanical timepiece part comprising at least one functional area wherein a lubricant is able to be confined , the method comprising a step of constructing a blank of said part including said at least one functional area and a step of transforming said at least one functional area into a magnetised functional area capable of cooperating with said lubricant having magnetic properties in achieving said confinement of the lubricant in said at least one area.2. The method according to claim 1 , wherein the transformation step comprises a sub-step of making at least one channel in a portion of the blank body located in said at least one functional area in particular behind a functional contact surface comprised in said at least one area.3. The method according to claim 1 , wherein the transformation step comprises a sub-step of arranging in said at least one channel a material developing a magnetic field.4. The method according to claim 1 , wherein the arrangement sub-step comprises:a phase of inserting a fluid, in particular a crosslinkable resin, comprising magnetic particles in said at least one channel;a phase of magnetising the magnetic particles comprised in said fluid;a phase of defining an orientation of the polarity of the magnetic particles comprised in said fluid relative to a polarity of said lubricant;a phase of curing said fluid comprising the magnetic particles magnetised and provided with an oriented polarity.5. The method according to claim 1 , wherein the magnetisation claim 1 , ...

LOW POUR POINT TRIMETHYLOLPROPANE ESTERS

The present invention relates to polyol esters that are particularly suitable for use as insulating oils in electrical equipment where an effective cooling action is required, such as electrical transformers. In particular the invention relates to esters of trimethylolpropane with monocarboxylic acids of nine and/or ten carbon atoms, wherein the monocarboxylic acids of nine and/or ten carbon atoms comprise 5-15 mol % of branched acids and 85-95 mol % of linear acids with respect to the total moles of the monocarboxylic acids. 1. An ester of trimethylolpropane with monocarboxylic acids of nine and/or ten carbon atoms , said monocarboxylic acids of nine and/or ten carbon atoms comprising 5-15 mol % of a branched acid and 85-95 mol % of a linear acid with respect to the total moles of the said monocarboxylic acids.2. The ester according to having a kinematic viscosity at 40 ° C. of less than 35 mm/s.3. The ester according having a pour point according to standard ISO 3016 of below −40 ° C.4. The ester according to having a flash point according to standard ISO 2719 (Pensky-Martens claim 1 , closed cup procedure) of above 200° C.5. The ester according to wherein said branched acid is selected from 3 claim 1 ,5 claim 1 ,5-trimethylhexanoic acid claim 1 , 7-methyloctanoic acid claim 1 , 2 claim 1 ,2-dimethylheptanoic acid claim 1 , 3 claim 1 ,3-dimethylheptanoic acid claim 1 , 8-methylnonanoic acid claim 1 , 2 claim 1 ,2-dimethyloctanoic acid and mixtures thereof.6. The ester according to wherein said linear acid is pelargonic acid.7. The ester according to having an hydroxyl number equal to or less than 2 mg KOH/g.8. A process for the preparation of an ester according to comprising the esterification of trimethylolpropane with monocarboxylic acids of nine and / or ten carbon atoms comprising 5-15 mol % of a branched chain and 85-95 mol % of linear a chain.9. The process according to wherein said esterification is carried out in the absence of catalyst.10. A process for ...

COATING COMPOSITIONS COMPRISING ADHESION PROMOTING BASE LAYER

Described herein are coatings and formulations thereof for coating a substrate for use in producing a lubricious coating on a substrate surface that is to be inserted into the body lumen of a subject. Said coatings all contain an adhesion promoting coating formulation for applying to a substrate material that is formed from a polymeric adhesion promoter, a monomeric or polymeric crosslinking agent and a photoinitiator, where the polymeric adhesion promoter is a block copolymer comprising hydrophobic hydrophilic polymer blocks and/or a hydrophilic polymer comprising hydrophilic functional groups, where from 10% to 100% of the hydrophilic functional groups are capped with a hydrophobic functional group and the formulations thereof further contain a solvent to enable the coating to be applied to a substrate surface. 2. An adhesion promoting coating for forming a base coating layer on a substrate material onto which a lubricious top layer coating can be formed , comprising:a polymeric adhesion promoter;a first crosslinked polymeric matrix formed by a first monomeric or polymeric crosslinking agent, whereinthe polymeric adhesion promoter is a block copolymer comprising hydrophobic and hydrophilic polymer blocks and/or a hydrophilic polymer comprising hydrophilic functional groups, where from 10% to 100% of the hydrophilic functional groups are capped with a hydrophobic functional group.3. The adhesion promoting coating formulation of claim 1 , wherein claim 1 , when the polymeric adhesion promoter is a block copolymer claim 1 ,the hydrophilic block is chosen from one or more of the group selected from polysaccharide (such as chitosan), poly(vinyl alcohol) (PVA), polymethacrylic acid, poly (ethylene glycol) (PEG), polyacrylamide (PAM), poly(2-oxazoline), and polyethylenimine (PEI), andthe hydrophobic block is chosen from one or more of the group selected from polystyrene (PS), polybutadiene (PB), polyisoprene (PI), poly(methyl methacrylate) (PMMA), poly(methylacrylate) ( ...

AN AQUEOUS COATING AGENT COMPOSITION AND A COATING COMPOSITION FOR AN AQUEOUS LUBRICATING FILM COMPRISING THE SAME

[Problem] To provide an aqueous coating agent composition (in particular, an aqueous coating composition for lubricating films that contains a solid lubricant) which as a whole is excellent in terms of flowability, applicability, and storage stability and which is capable of forming satisfactory and smooth coating films effective in stick-slip inhibition. [Solution] The problem can be solved with an aqueous coating agent composition which comprises (A) a curable resin in an aqueous emulsion form, (B) a surfactant, (C) solid particles, (D) one or more nitrogenous heterocyclic compounds, (E) a film-forming silicone in an aqueous emulsion form, and (F) water. In particular, it is preferable that the (C) component comprise a solid lubricant. In view of the environmental regulations, it is especially preferable that the (D) component be 1,3-dimethyl-2-imidazolidinone. 1. An aqueous coating agent composition which contains:(A) A curable resin in the form of an aqueous emulsion,(B) A surfactant,(C) Solid particles,(D) One or more types of nitrogen-containing heterocyclic compounds,(E) A film-forming silicone in the form of an aqueous emulsion, and(F) Water.2. The aqueous coating agent composition as specified in claim 1 , which includes 0.1 to 50 parts per mass of Component (B) specified above claim 1 , 5 to 200 parts per mass of Component (C) specified above claim 1 , 1 to 20 parts per mass of Component (D) specified above claim 1 , 0.1 to 10 parts per mass of the solid component of Component (E) specified above claim 1 , and 50 to 1 claim 1 ,000 parts per mass of Component (F) specified above per 100 parts per mass of the solid component of Component (A) specified above.3. The aqueous coating agent composition as specified in or claim 1 , wherein Component (E) corresponds to a film-forming silicone in the form of an aqueous emulsion comprising 100 parts per mass of (Ea) a polyorganosiloxane having at least two hydroxyl groups or hydrolyzable groups bonded to a silicon ...

Slips Surface Based on Metal-Containing Compound

A method of preparing an article having a slippery surface includes providing a metal-containing surface, chemically modifying the metal-containing surface to roughen the metal-containing surface, and disposing a lubricating layer on the roughened metal-containing surface, wherein the lubricating layer is substantially stabilized on the roughened metal-containing surface.

SULFUR- AND PHOSPHORUS-FREE EXTREME PRESSURE LUBRICANT AND PREPARATION METHOD AND APPLICATION THEREOF

The present invention belongs to the field of lubricant technologies, and specifically, to a sulfur-and phosphorus-free extreme pressure lubricant and a preparation method thereof. In the present invention, the lubricant prepared by using Turkey red oil, a cyclic anhydride compound, triethanolamine, nano polytetrafluoroethylene powder, an alcohol compound, and water as raw materials does not contain hazardous substances such as sulfur and phosphorus. This reduces the harm to the environment, equipment, and human body, and conforms to the development trend of modern industrial production. Moreover, the lubricant has excellent extreme pressure performance, and can effectively reduce the downhole friction and torque, thereby meeting the construction requirements of extended reach wells and horizontal wells. 1. A sulfur- and phosphorus-free extreme pressure lubricant , comprising the following raw materials: 20-30 parts by weight of Turkey red oil , 20-30 parts by weight of cyclic anhydride compound , 15-20 parts by weight of triethanolamine , 10-20 parts by weight of nano polytetrafluoroethylene powder , 5-10 parts by weight of alcohol compound , and water.2. The sulfur- and phosphorus-free extreme pressure lubricant according to claim 1 , wherein the cyclic anhydride compound comprises one or two of tetrahydrophthalic anhydride claim 1 , hexahydrophthalic anhydride claim 1 , and cis-1 claim 1 ,2 claim 1 ,3 claim 1 ,6-tetrahydrophthalic anhydride.3. The sulfur and phosphorus extreme pressure lubricant according to claim 1 , wherein a particle size of the nano polytetrafluoroethylene powder is 50-300 nm.4. The sulfur- and phosphorus-free extreme pressure lubricant according to claim 1 , wherein the alcohol compound comprises ethanol or isopropanol.5. A preparation method of a sulfur- and phosphorus-free extreme pressure lubricant claim 1 , comprising the following steps:mixing the cyclic anhydride compound, triethanolamine, and water, and conducting first-stage reaction ...

Natural oil based grease compositions and processes for making such compositions

A grease composition is disclosed, having from 50 to 99 weight percent of a lubricating base oil, from 1 to 30 weight percent of a thickener component including one or more of (i) one or more natural oil derivatives, (ii) one or more hydrogenated metathesized natural oils and/or natural oil derivatives, (iii) one or more amidated metathesized natural oils and/or natural oil derivatives, (iv) one or more, or two or more, carboxylic acids and/or derivatives thereof, and (v) one or more of a metal base compound, and from 1 to 15 weight percent of one or more optional additives. Processes for making grease compositions are also disclosed.

SUPERLUBRICATING GRAPHENE AND GRAPHENE OXIDE FILMS

A system and method for forming at least one of graphene and graphene oxide on a substrate and an opposed wear member. The system includes graphene and graphene oxide formed by an exfoliation process or solution processing method to dispose graphene and/or graphene oxide onto a substrate. The system further includes an opposing wear member disposed on another substrate and a gas atmosphere of an inert gas like N, ambient, a humid atmosphere and a water solution. 123-. (canceled)24. A method of interacting with reduced friction comprising:providing relative movement between a first surface having disposed thereon graphene oxide flakes and being substantially free of oil with a second surface having a diamond like coating;interacting the first surface with the second surface wherein the coefficient of friction is between 0.15 and 1.0.25. The method of claim 24 , further wherein the relative movement including an atmosphere surrounding the solution processed wear member consisting of at least one of ambient claim 24 , N claim 24 , Ar and a high vacuum.26. The method of claim 24 , wherein the substrate is selected from the group of a plastic injection mold surface claim 24 , a gun barrel claim 24 , a cutting blade and a bearing.27. The method of claim 24 , wherein the graphene oxide is a film on the first surface.28. The method of claim 24 , wherein the graphene oxide is a layer of graphene flakes on the first surface.29. A method of forming at least one of graphene and graphene oxide on a substrate claim 24 , comprising the steps of:disposing graphene oxide on the substrate substantially free of oil, thereby establishing a low friction wear surface.30. The method of claim 29 , wherein disposing graphene oxide comprises forming a layer of graphene oxide flakes.31. The method of claim 29 , wherein the layer of graphene flakes is formed by solution processing claim 29 , chemical exfoliation claim 29 , or mechanical exfoliation.32. The method as defined in wherein the step ...

BASE OILS AND METHODS OF MAKING THE SAME

A process for the preparation of saturated hydrocarbon base oils is provided, comprising oligomerization of a feed mixture that has an average carbon number in the range of 14 to 18 to produce an oligomer product comprising dimers, trimers, and higher oligomers, where the dimer has a branching proximity (BP) of 20 or greater, isomerization of at least the dimer portion, and hydrogenation of the isomerized product. The dimer portion is separated from the oligomer product, and a saturated hydrocarbon base oil is obtained comprising greater than 90% dimers having an average carbon number in the range of from 29 to 36, and the dimer portion having a weight average molecular weight in the range of 422 to 510, where the dimers have an average Branching Index (BI) in a range of 22 to 26 and an average paraffin branching proximity (BP) in a range of from 18 to 26. 1. A process for the preparation of a saturated hydrocarbon base oil , comprising:forming an oligomerization reaction mixture comprising an oligomerization catalyst system and an olefin monomer feed mixture, wherein the olefin monomer feed mixture has an average carbon number in the range of 14 to 18;oligomerizing the olefin monomer feed mixture in the reaction mixture to produce an oligomer product comprising dimers, trimers, and higher oligomers;isomerizing at least the dimer portion of the oligomer product in the presence of an acid catalyst to form a mixture of branched hydrocarbons;{'sub': '2', 'hydrogenating the isomerized branched hydrocarbons, to a Bromine Index below 1000 mg Br/100 g as determined in accordance with ASTM D2710-09; and'}separating the dimer portion of the hydrogenated oligomer product, whereby a saturated hydrocarbon base oil is obtained comprising greater than 90 wt % dimers having an average carbon number in the range of from 29 to 36, the dimer portion having a weight average molecular weight in the range of from 422 to 510,{'sub': '2', 'wherein the dimers of the oligomer product, in a ...

PROCESS FOR THE PREPARATION OF A LUBRICANT BASE STOCK COMPRISING THE SELECTIVE THERMAL DECOMPOSITION OF PLASTIC POLYOLEFIN POLYMER

The present invention relates to a process for the preparation of a lubricant base stock from the thermal decomposition of plastic polymer. The present invention provides a process for preparing a lubricant base stock from the thermal decomposition of plastic polyolefin polymer, the method comprising the steps of: 152-. (canceled)53. A process for preparing a lubricant base stock from the thermal decomposition of plastic polyolefin polymer , the method comprising the steps of:i) introducing plastic polyolefin polymer into a thermal reaction zone of a vacuum pyrolysis reactor;{'sub': 20', '60, 'ii) heating the plastic polyolefin polymer at sub-atmospheric pressure, wherein the temperature in the thermal reaction zone of the reactor is from 500° C. to 750° C., to induce thermal decomposition of the plastic polyolefin polymer and to form a thermal decomposition product effluent which comprises a major portion by weight of a Cto Cwax fraction;'}iii) condensing a vapor component of the thermal decomposition product effluent from the vacuum pyrolysis reactor; and{'sub': 20', '60, 'iv) subjecting the Cto Cwax fraction of the thermal decomposition product to catalytic hydroisomerization in a hydroisomerization reactor in the presence of hydrogen to form the lubricant base stock,'}wherein the plastic polyolefin polymer comprises polyethylene and polypropylene in a polyethylene to polypropylene weight ratio of from 60:40 to 90:10.54. A process according to claim 53 , wherein the plastic polyolefin polymer is introduced into the pyrolysis reactor by means of an extruder.55. A process according to claim 53 , wherein at least one member of a group consisting of: the temperature in the thermal reaction zone of the reactor is from 525 to 650° C. claim 53 , and the pressure in the thermal reaction zone of the vacuum pyrolysis reactor is less than 75 kPa absolute.56. A process according to wherein at least one member of a group consisting of:the plastic polyolefin polymer comprises ...

Process and Apparatus for the Preparation of a Cylinder Oil

A process for production of cylinder oil comprises providing used oil, providing fresh cylinder oil, and blending the used oil with the fresh cylinder oil. The used oil has a lower TBN value than the fresh cylinder oil. A process for the operation of an internal combustion engine comprises preparing cylinder oil as described and using the cylinder oil in the internal combustion engine. An apparatus for the preparation of a cylinder oil comprises a blending means for blending used oil and fresh cylinder oil. The blending means is in flow communication with at least one compartment of an internal combustion engine that comprises used oil or at least one storage compartment comprising used oil, at least one storage compartment for fresh cylinder oil, and at least one cylinder of an internal combustion engine. Used oil and fresh cylinder oil are used for the preparation of cylinder oil. 2. Process according to claim 1 , wherein the cylinder oil produced comprises at least 1% by weight used oil claim 1 , based on the total amount of cylinder oil produced and/or at least 1% by weight of fresh cylinder oil claim 1 , based on the total amount of cylinder oil produced.3. Process according to claim 1 , wherein the cylinder oil produced comprises at least 10% by weight used oil claim 1 , based on the total amount of cylinder oil produced and/or at least 10% by weight of fresh cylinder oil claim 1 , based on the total amount of cylinder oil produced.4. Process according to claim 1 , wherein the used oil has a lower kinematic viscosity than the cylinder oil.5. Process according to claim 1 , wherein the used oil comprises one or more oils selected from the group consisting of used hydraulic fluids claim 1 , used gear oils claim 1 , used system oils claim 1 , used trunk piston engine oils claim 1 , used turbine oils claim 1 , used heavy duty diesel oils claim 1 , used compressor oils and mixtures thereof.6. Process according to claim 1 , wherein the process is performed on a ...

Low viscosity lubricating polyolefins

A low viscosity oil has more than 50% by weight of 9-methyl-11,13-dioctyltricosane. A lubricating composition having this low viscosity oil as base oil and, optionally, another base oil or an additive. The low viscosity oil has a kinematic viscosity at 100° C., measured by the ASTM D445 standard, of 4 to 8 mm 2 ·s −1 . The low viscosity oil can be prepared using a metallocene catalyst, and the low viscosity oil as high performance lubricant can be used for lubrication in the field of motors, hydraulic fluids and gears, in particular bridges and transmissions.

LUBRICATION OF MACHINES USING HEAT ACTIVATED POLYMERS

A lubricating system includes a machine configured to operate in a first operating state and a second operating state; and a heat activated polymer material applied to at least a part of the machine and to remain solid during the first operating state and to soften upon being heated in the second operating state to lubricate the machine. The heat activated polymer material may soften due to increased friction incurred by the machine in the second operating state. A heating element may be operatively connected to any of the machine and the heat activated polymer material. The heat activated polymer material may soften due to being heated by the heating element in the second operating state. An injector may apply the heat activated polymer material to the machine. A channel may direct a flow of the heat activated polymer material as it softens in the second operating state. 1. A lubricating system comprising:a machine configured to operate in a first operating state and a second operating state; anda heat activated polymer material applied to at least a part of the machine and to remain solid during the first operating state and to soften upon being heated in the second operating state to lubricate the machine.2. The lubricating system of claim 1 , wherein the heat activated polymer material softens due to increased friction incurred by the machine in the second operating state.3. The lubricating system of claim 1 , comprising a heating element operatively connected to any of the machine and the heat activated polymer material.4. The lubricating system of claim 3 , wherein the heat activated polymer material softens due to being heated by the heating element in the second operating state.5. The lubricating system of claim 1 , comprising an injector to apply the heat activated polymer material to the machine.6. The lubricating system of claim 1 , wherein the machine comprises any of a gear and a bearing.7. The lubricating system of claim 1 , comprising a channel to ...

VIRTUAL LANDFILL TERMINAL

Handling of municipal solid waste (MSW) is described. A method for handling MSW in a single waste processing facility includes receiving the MSW at the waste processing facility. The MSW is separated into biomass, recyclables, and plastics. The biomass is processed at the waste processing facility to produce syngas using a gasifier. The plastics are also processed at the waste processing facility to produce naphtha, diesel fuel, and/or lubricants. Waste heat from the processing of the biomass and from the processing of the plastics is captured and used in the generating of electricity at the waste processing facility. Facilities for handling MSW are also described. 1. A method for processing municipal solid waste , the method comprising:receiving municipal solid waste (MSW) at a waste processing facility;separating the MSW into biomass, recyclables, and plastics;processing the biomass, at the waste processing facility, to produce syngas using a gasifier;processing the plastics, at the waste processing facility, to produce naphtha, diesel fuel, and lubricants;capturing waste heat from the processing of the biomass and from the processing of the plastics; andgenerating electricity, at the waste processing facility, using the syngas and waste heat.2. The method of claim 1 , wherein processing the plastics includes using a rotary reactor and catalyst to produce synthetic crude and/or synthetic diesel claim 1 , and using a distillation column to produce the naphtha claim 1 , diesel fuel claim 1 , and lubricants from the synthetic crude.3. The method of claim 1 , further comprising using a distillation column to produce the naphtha claim 1 , diesel fuel claim 1 , and lubricants from the synthetic crude and/or synthetic diesel.4. The method of claim 1 , wherein processing the biomass includes drying the MSW biomass claim 1 , feeding the dried biomass to the gasifier to create syngas from the gasifier.5. The method of claim 1 , wherein processing the biomass includes ...

METHOD FOR INSPECTING LUBRICATING OIL COMPOSITION AND METHOD FOR PRODUCING LUBRICATING OIL COMPOSITION

A method for inspecting a lubricant oil composition containing a base oil and a fullerene, the method including: measuring at least one of a lamellar length of the lubricating oil composition and a most abundant diameter in a particle size distribution obtained by a dynamic light scattering method, and selecting the lubricating oil composition whose measured value is within a set range. 1. A method for inspecting a lubricant oil composition containing a base oil and a fullerene , the method comprising:measuring at least one of a lamellar length of said lubricating oil composition and a most abundant diameter in a particle size distribution obtained by a dynamic light scattering method; andselecting said lubricating oil composition whose measured value is within a set range.2. The method for inspecting a lubricating oil composition according to claim 1 , wherein said lamellar length and said most abundant diameter are measured claim 1 , and said lubricating oil composition having both measured values within set ranges is selected.3. A method for producing a lubricating oil composition comprising a step of selecting a lubricating oil composition obtained by mixing a base oil and a fullerene by the method for inspecting a lubricating oil composition according to .4. A method for producing a lubricating oil composition comprising a step of selecting a lubricating oil composition obtained by mixing a base oil and a fullerene by the method for inspecting a lubricating oil composition according to . The present invention relates to a method for inspecting a lubricating oil composition and a method for producing a lubricating oil composition.Priority is claimed on Japanese Patent Application No. 2017-234587, filed Dec. 6, 2017, the content of which is incorporated herein by reference.In recent years, with the increase in speed, efficiency, and energy saving, there is a strong demand for improved performance of lubricating oils used in automobiles, home appliances, ...

Glue Grease and method of making

Glue Grease, has been designed and made as a lubricant to be used in moving mechanical parts in difficult environmental conditions as an anti-abrasion material in order to increase the longevity of parts prone to friction. 1- A method for making glue grease , comprisingIn a first mixer, a predetermined quantity of Latex and Ammonia are mixed till a homogenous white solution is created;then in a second mixer that is a kept at a predetermined temperature a second quantity of Mazut oil is mixed with a portion of said white solution; creating a second solution.2- The method of claim 1 , wherein said Mazut oil is composed of Alkane hydrocarbon chains containing from 20 to70 carbon atoms in each chain; and wherein said Mazut oil is low-Sulphur Mazut oil claim 1 , with a Sulphur content of 1.0-1.5%.3- The method of claim 2 , wherein said Latex is an adhesive polymer acquired both from natural sources (plant saps) and synthetically through polymerization of isoprene; wherein either form is suitable.43- The method of claim 3 , wherein said second mixer is turned on for hours claim 3 , wherein vulcanization process happens between said Latex and said Sulphur content of said Mazut oil.53- The method of claim 4 , wherein in said hours claim 4 , said Latex is oxidized and said Sulphur turns into Sulphide claim 4 , therefore a third solution with elasticity and anti-abrasion characteristic is created.6- The method of claim 5 , wherein after said 3 hours said second mixer is turned off and said third solution is let to rest for at least 12 hours claim 5 , creating a paste like black polymer that is oily and elastic (glue grease).7- The method of claim 6 , wherein said predetermined quantity is 400 grams of said Latex and 700 grams of said 44% Ammonia claim 6 , and wherein said portion of said white solution is 300 ml claim 6 , and wherein said second quantity is 1 liter of said low-Sulphur Mazut oil.8- The method of claim 7 , wherein said final glue grease solution comprises a lot ...

ESTER COMPOUND AND LUBRICATING OIL BASE OIL

[Problem] An ester compound having low viscosity, excellent fluidity even at low temperatures, and a high viscosity index; and a lubricating oil base oil containing said compound are provided. [Solution] The present invention provides an ester compound indicated by formula (I). Formula (I) (in formula (I), Ris a hydrocarbon group having 1 to 35 carbon atoms and at least one hydrogen in the hydrocarbon group may be independently substituted with a group indicated by formula (II)). Formula (II) (in formula (II), Ris a linear alkyl having 1 to 30 carbon atoms or a branched alkyl having 3 to 30 carbon atoms.) 5. A lubricating oil base oil , comprising:{'claim-ref': {'@idref': 'CLM-00001', 'claim 1'}, 'the ester compound according to .'}6. A method for producing the ester compound according to claim 1 , the method comprising:a step of subjecting 10-ethyl-7-tetradecanol and carboxylic acid to esterification reaction.9. A lubricating oil base oil claim 1 , comprising:{'claim-ref': {'@idref': 'CLM-00002', 'claim 2'}, 'the ester compound according to .'}10. A lubricating oil base oil claim 1 , comprising:{'claim-ref': {'@idref': 'CLM-00003', 'claim 3'}, 'the ester compound according to .'}11. A lubricating oil base oil claim 1 , comprising:{'claim-ref': {'@idref': 'CLM-00004', 'claim 4'}, 'the ester compound according to .'}12. A lubricating oil base oil claim 1 , comprising:{'claim-ref': {'@idref': 'CLM-00007', 'claim 7'}, 'the ester compound according to .'}13. A lubricating oil base oil claim 1 , comprising:{'claim-ref': {'@idref': 'CLM-00008', 'claim 8'}, 'the ester compound according to .'}14. A method for producing the ester compound according to claim 2 , the method comprising:a step of subjecting 10-ethyl-7-tetradecanol and carboxylic acid to esterification reaction.15. A method for producing the ester compound according to claim 3 , the method comprising:a step of subjecting 10-ethyl-7-tetradecanol and carboxylic acid to esterification reaction.16. A method for ...

Method for producing biolubricant from vegetable oil, and biolubricant

The present invention describes a process for obtaining a biolubricant from vegetable oil, which comprises the steps of (a) esterification reaction of the product of vegetable oil hydrolysis using a branched aliphatic alcohol; (b) epoxidation reaction of the esters obtained in step (a); and (c) nucleophilic substitution reaction of the epoxidated esters obtained in step (b) using a branched aliphatic alcohol. The present invention also describes a biolubricant obtained from the process. More specifically, a biolubricant is described that is produced from a ricinoleic fatty acid, whose formula is illustrated in FIG. 1 of the present invention, and where R1 is a hydroxyl or it is from the formula R3COO−, with R3 being an alkyl radical C1-C3, preferably a methyl radical; and R2 consists of a straight chain of hydrocarbons C4-C8 and a branched chain of hydrocarbons C1-C3.

DEVICE FOR ELECTRICALLY PROCESSING A FATTY SUBSTANCE OF PLANT ORIGIN

The present invention relates to a device for electrically processing a fatty substance of plant origin, comprising a series of electrodes ( and ) and an enclosure (), said device being characterised in that the enclosure () is provided with at least one electrical connector () placed on the outer surface () of the enclosure (), a series of electrical connections for connecting each electrode of said series of electrodes to said electrical connector (), with the current flow distances of the electrical connections being equal in relation to each other, and a first inlet () and a first outlet () for the fatty substance, and in that said device comprises a filter () having an inlet () in fluidic connection with said first fatty-substance outlet () of the enclosure () and an output () in fluidic connection with said first fatty-substance inlet () of the enclosure (). 2. Device according to claim 1 , wherein at least one electrode claim 1 , preferably each electrode claim 1 , of the series of electrodes is a metal plate having a thickness ranging between 0.5 mm and 5 mm claim 1 , preferably 1 mm and 3 mm.310123. Device according to claim 1 , wherein said immersion device further comprises a rotating shaft () attached to said electrodes ( and ) and attached to said dielectric material elements ().4104. Device according to claim 1 , wherein said immersion device further comprises a rotating shaft () attached to the enclosure ().54271010282728272712328123. Device according to claim 4 , wherein said immersion device further comprises claim 4 , in the enclosure () claim 4 , a disc () fixed to the rotating shaft () and arranged to be rotated by said shaft () claim 4 , and provided with a series of blades () peripherally positioned on said disc () claim 4 , each of said blades () having a longitudinal axis (L) parallel to an axis of rotation of said disc () claim 4 , said disc () having a common axis of rotation (R) with said electrodes ( and ) and with said dielectric ...

Tools and methods for forming or servicing a wellbore, and methods of coating surfaces of tools

A method of utilizing a wellbore tool in a subterranean formation includes disposing a wellbore tool in a borehole. The wellbore tool has a first body and a second body. The first body is translated relative to the second body while exposing at least one surface of at least one of the first and second bodies to a lubricant comprising an organometallic compound, and a protective coating forms over the first body and/or the second body. The protective coating formed includes a metal originating from the organometallic compound. A tool for forming or servicing a wellbore includes a first body; a second body configured to translate relative to the second body; and a lubricant adjacent the first body and the second body.

Composition and Method of Manufacturing and Using Extremely Rheopectic Sulfonate-Based Greases

An extremely rheopectic sulfonate-based grease composition and method comprising adding overbased calcium sulfonate, overbased magnesium sulfonate, and a facilitating acid, using a particular type of overbased calcium sulfonate and/or methods for adding overbased calcium sulfonate relative to the magnesium sulfonate and facilitating acid to favor the reaction between the magnesium sulfonate and facilitating acid. A preferred overbased calcium sulfonate comprises benzene rings having multiple alkyl groups. Preferred methods comprise (1) adding all calcium sulfonate after adding the magnesium sulfonate and facilitating acid, (2) adding a first portion of calcium sulfonate with the magnesium sulfonate before adding the facilitating acid and a second portion of calcium sulfonate after the facilitating acid, and/or (3) one or more calcium sulfonate delay periods relative to adding the facilitating acid. The extremely rheopectic grease is fluid and pourable and only takes on a grease structure after milling or shearing. 1. A sulfonate-based grease composition comprising the following ingredients: overbased calcium sulfonate , overbased magnesium sulfonate , and a facilitating acid , wherein the sulfonate-based grease composition is extremely rheopectic and wherein the overbased calcium sulfonate (1) comprises benzene rings having more than one alkyl group; (2) is a natural calcium sulfonate; (3) comprises benzene rings that are sterically hindered; or (4) a combination thereof.2. The sulfonate-based grease composition of wherein the composition is fluid and pourable prior to milling or shearing and only takes on a thickened grease structure after milling or shearing.3. The sulfonate-based grease composition of wherein the composition has an unmilled claim 1 , unworked penetration greater than 360.4. The sulfonate-based grease composition of wherein the composition has an unmilled claim 1 , unworked penetration greater than 400.5. The sulfonate-based grease composition of ...

Organosilica materials and uses thereof

Organosilica materials, which are a polymer of at least one independent monomer of Formula [Z 1 OZ 2 OSiCH 2 ] 3 (I), wherein each Z 1 and Z 2 independently represent a hydrogen atom, a C 1 -C 4 alkyl group or a bond to a silicon atom of another monomer and at least one other trivalent metal oxide monomer are provided herein. Methods of preparing and processes of using the organosilica materials, e.g., for catalysis etc., are also provided herein.

Liquid-Phase Hydroisomerization System And Process Therefor And Use Thereof

Provided are a liquid-phase hydroisomerization system and a process therefor and use thereof. The system comprises a gas-liquid mixer (), a hydroisomerization reactor () and a fractionating column (). An oil product and hydrogen are mixed as a liquid hydrogen-oil mixture, and are introduced into the hydroisomerization reactor for a hydroisomerization reaction, and after being fractionated, a target product is led out. A supplemental hydrogen-dissolving inner member is provided at least between a group of two adjacent catalyst bed layers in order to supplement hydrogen to the reactants. The process cancels a circulating hydrogen compressor, has a simple process flow, and can be applied to the production of a lubricant base oil by the hydroisomerization of a lubricant raw material or the production of a low freezing point diesel by the hydroisomerization of and the reduction in the freezing point of a diesel raw material. 1. A liquid-phase hydroisomerization system , characterized in that the system comprises:a hydrogen-dissolving unit, a hydroisomerization reactor, and a fractionating column;wherein the hydrogen-dissolving unit comprises an oil feed line, a hydrogen feed line and a hydrogen-oil-mixture line, the hydrogen-oil-mixture line is in communication with the bottom of the hydroisomerization reactor, and the top of the hydroisomerization reactor is in communication with the fractionating column;the hydroisomerization reactor includes at least two catalyst beds, and an internal dissolved-hydrogen replenishment member is provided between at least one pair of two adjacent catalyst beds;the internal dissolved-hydrogen replenishment member comprises a bottom sieve separating plate, a middle mixing space and a top separating plate, the top separating plate is provided with multiple liquid discharging pipes, and the middle mixing space is provided with a hydrogen inlet and a hydrogen outlet; hydrogen and oil are mixed in the middle mixing space, the liquid phase in ...

LUBRICANT COMPOSITIONS AND METHODS OF USE

The present disclosure relates to lubricant compositions for use on engine components. The lubricant compositions include, by volume: 30 to 50% graphite in alcohol solution; 0.1 to 5% surfactant; and 40 to 70% water. The present disclosure also relates to processes for preparing lubricant compositions and methods of using such compositions. 1. A lubricant composition comprising by volume:30 to 50% graphite in alcohol solution;0.1 to 5% surfactant; and40 to 70% water.2. The lubricant composition of claim 1 , wherein the percentage by volume of graphite in alcohol solution is 32.2 to 49.5% claim 1 , the percentage by volume of surfactant is 1.0 to 3.5% claim 1 , and the percentage by volume of water is 48.25 to 66%.3. The lubricant composition of claim 1 , wherein the percentage of surfactant by volume is 1.9 to 2.8%.4. The lubricant composition of claim 1 , wherein the surfactant is selected from the group consisting of nonionic surfactants claim 1 , anionic surfactants claim 1 , cationic surfactants claim 1 , nonionic surfactants claim 1 , and zwitterionic surfactants.5. The lubricant composition of claim 4 , wherein the surfactant is a nonionic surfactant.6. A process for preparing a lubricant composition comprising 30 to 50% graphite in alcohol solution claim 4 , 1.0 to 5% surfactant claim 4 , and 40 to 70% water by volume claim 4 , the process comprising:mixing the graphite in alcohol solution with water; andmixing the surfactant into the graphite and water mixture.7. A method of using a lubricant composition comprising 30 to 50% graphite in alcohol solution claim 4 , 1.0 to 5% surfactant claim 4 , and 40 to 70% water claim 4 , the method comprising:applying the lubricant composition to a surface; andallowing the lubricant composition to dry.8. The method of claim 7 , wherein the lubricant composition is applied by a method selected from the group consisting of a brush claim 7 , a spray claim 7 , a person's hand claim 7 , and a mechanical means.9. The method of ...

PROCESS FOR PREPARING A GREASE

The invention provides for a process for preparing a lubricating grease. The process can be carried out in the presence of a base oil and avoids the use of diisocyanate reagents. 2. The process according to claim 1 , wherein Ris an alkyl group having from 1 to 6 carbon atoms.3. The process according to claim 1 , wherein n is 2 and Ris chosen from arylene comprising from 6 to 14 carbon atoms or alkylene comprising from 2 to 12 carbon atoms.4. The process according to claim 1 , wherein Ris aryl having from 6 to 12 carbon atoms or is alkyl comprising from 2 to 18 carbon atoms.5. The process according to claim 1 , wherein the lubricating grease comprises the compound of formula (c) in a range of from 2 weight percent to 25 weight percent claim 1 , based on the total weight of the lubricating grease.7. The lubricating grease according to claim 6 , wherein Ris chosen from arylene comprising from 6 to 14 carbon atoms or alkylene comprising from 2 to 12 carbon atoms.8. The lubricating grease according to claim 6 , wherein Ris aryl having from 6 to 12 carbon atoms or is alkyl comprising from 2 to 18 carbon atoms.9. The lubricating grease according to claim 6 , wherein the lubricating grease comprises the compound of formula (c) in a range of from 2 weight percent to 25 weight percent claim 6 , based on the total weight of the lubricating grease. The invention relates to a process for preparing a lubricating grease.Greases are used to provide lubrication in a variety of applications including bearings for constant-velocity joints, ball joints, wheel bearings, alternators, cooling fans, ball screws, linear guides of machine tools, sliding areas of construction equipment, and bearings and gears in steel equipment and various other industrial mechanical facilities.U.S. Pat. No. 3,119,869 discloses a thixotropic grease comprising an abietyl oxamide compound having the general formula (x):wherein R and R′ are the same or different abietyl radicals selected from the group ...

BASE OILS AND METHODS OF MAKING THE SAME

Aspects of the present disclosure relate to a process for producing synthetic hydrocarbon base oils having advantageous properties for formulation of engine oils, and the base oils obtained by such processes, involving the production of branched alkenes from the oligomerization of C14-C18 olefins. According to one embodiment, the base oils are obtained by first forming a mixture of two or more olefins ranging from C14-C18, where one of the olefins is an alpha olefin and the other has an average double bond position between 1.5-5.0, and oligomerizing this mixture in the presence of a catalyst to form one or more branched alkenes, hydrogenating the branched alkenes, and fractionating to form base oils. According to one aspect, advantageous properties can be obtained by controlling one or more of the degree of branching, branch length, branching positions, selection of the C14-C18 olefins, and catalytic isomerization, during or after the oligomerization process. 1. A saturated hydrocarbon base oil comprising: [ {'br': None, 'branching index (BI)=(number of methyl group hydrogens/total number of hydrogens)*100, and\u2003\u2003(1)'}, 'an average branching index (BI) of the oil as determined by 1H NMR is in a range of from 22 to 26, wherein the branching index (BI) is equivalent to the following equation (1), {'br': None, 'paraffin branching proximity (BP)=(number of ε carbon groups/total number of carbon groups)*100,\u2003\u2003(2)'}, 'an average paraffin branching proximity (BP) as determined by 13C NMR in a range of from 18 to 26, wherein the paraffin branching proximity (BP) is equivalent to the following equation (2)], 'dimers of C14-C18 olefin monomers, the dimers having an average carbon number in a range of from 29 to 36, the dimers being present in an amount of at least 95 wt % of the saturated hydrocarbon base oil, wherein the saturated hydrocarbon base oil is characterized in that 'wherein the saturated hydrocarbon base oil comprises a Noack Volatility that is ...

Process for producing a dry polyamide-imide film with high galling resistance on a threaded tubular component from an aqueous dispersion which is free of carcinogenic substances

The invention concerns a process for producing a dry film with a high galling resistance on a threaded element for drilling and/or operating a hydrocarbon well, characterized in that it comprises at least the following steps: forming a stable dispersion comprising a polyamide-imide powder, a polar aprotic solvent with a boiling point of more than 180° C. at 760 mm Hg, and water; applying the dispersion to one of the ends ( 1, 2 ) of said threaded element at a temperature in the range 20° C. to 40° C.; drying the coated end.

LOW PARTICULATE LUBRICIOUS COATING WITH VINYL PYRROLIDONE AND ACIDIC POLYMER-CONTAINING LAYERS

Embodiments of the disclosure include lubricious coatings. In an embodiment the disclosure includes a lubricious coating for a medical device including first and second coated layers. The first coated layer is between the second coated layer and the device surface and includes a vinyl pyrrolidone polymer and a photo reactive group. The second coated layer is in direct contact with the first coated layer and is a top coating that includes an acrylic acid polymer. The second coated layer can optionally include photoreactive groups. The coating was found to have a very low number of particulates (e.g., 10 μm or greater) which is very desirable for in vivo use. 1. A lubricious coating comprising:a first coated layer comprising a vinyl pyrrolidone polymer and photoreactive groups, wherein the photoreactive groups are pendent from the vinyl pyrrolidone polymer or on a first cross-linking agent comprising at least two photoreactive groups, or both; anda second coated layer that is a top coating comprising an acrylic acid polymer, wherein the second coated layer is in direct contact with the first coated layer, wherein the first coated layer is between the second coated layer and a substrate surface.2. The coating of wherein the second coated layer further comprises an acrylamide polymer comprising at least one photo reactive group.3. The coating of wherein the acrylamide polymer comprises acrylamide- claim 2 , sulfonate- claim 2 , and alkylene oxide-containing subunits.4. The coating of claim 2 , wherein the vinyl pyrrolidone polymer and the acrylamide polymer are present in the coating at a weight ratio in the range of approximately 3:1 to 1:3 (wt./wt.) claim 2 , respectively.5. The coating of claim 2 , wherein the acrylic acid polymer and the acrylamide polymer are present in the coating at a weight ratio in the range of approximately 2:1 to 1:2 (wt./wt.) claim 2 , respectively6. The coating of comprising a first or second cross-linking reagent claim 1 , wherein at least ...

A STABILIZED LUBRICANT COMPOSITION FOR CONTINUOUS CASTING PROCESSES

Described herein is a stabilized lubricant composition for use in steel casting, in particular in continuous casting processes. In particular, the lubricant composition for processes for producing steel by continuous casting includes a dispersion of a lubricant powder, for an ingot mold, in continuous casting, in an oily liquid means, and a stabilization additive, characterized in that it has the following shear thinning index values: 2. The lubricant composition according to claim 1 , wherein the stabilization additive is selected from:Organic additives including:secondary or tertiary amines with C4-C18 chains,amides or imides with C4-C18 chains,esters of mono- or di-carboxylic acids with C4-C18 chains with alcohols or polyols with C4-C18 chains,mono- or poly-carboxylic acids with C4-C18 chains,Salts of one or more of the aforesaid compounds; andamino acids and peptides up to 10 amino acidic units,Inorganic additives including:oxides or hydroxides of transition metals,carbonates or hydrogen carbonates of alkaline or alkaline earth metals,silica, alumina, silicates, aluminosilicates, fluoro silicates, phosphosilicates, andcarbon allotropes,and wherein the inorganic additives have a granulometry within the range of 1 nm-100 microns.3. The lubricant composition according to claim 2 , wherein the stabilization additive is selected from trihexylamine and titanium dioxide with a main particle size of about 20 nm.4. The lubricant composition according to claim 1 , wherein the stabilization additive is used in a concentration from 0.05% to 10% in mass with respect to the oil mass.5. The lubricant composition according to claim 1 , wherein the oily liquid means is selected from or comprises glyceric esters of fatty acids and/or poly-α-olefins.6. The lubricant composition according to claim 1 , wherein the oily liquid means has a kinematic viscosity claim 1 , μ claim 1 , from 25 to 150 mm/s at 40° C. (ASTM D445 claim 1 , gravimetric method with capillary viscometer) and a ...

METAL COMPOUNDS OF CALIXARENES, DETERGENT COMPOSITIONS CONTAINING THEM AND USE THEREOF IN LUBRICANT COMPOSITIONS

The present invention relates to a metal compound of calixarene not containing sulfur and dispersible in oil, which can be partially salified, or neutral, or basic or overbased, said calixarene having general formula (I) in which: a) R, R, Rand Rare independently selected from hydrogen, or a group containing carbon and hydrogen, or a group containing in addition to carbon and hydrogen also heteroatoms, provided that said heteroatoms are not sulfur; b) one of the two substituents Rand Ris hydrogen, while the other may be selected from hydrogen, or a linear or branched alkyl with a number of carbon atoms between 1 and 6, preferably methyl, ethyl, 1-propyl, 2-propyl, n-butyl, sec-butyl, more preferably methyl or ethyl; c) n is the number of units of the calixarene ring and is comprised in the range between 4 and 16, preferably between 5 and 12; said calixarene being characterized in that in at least one of the n units of the calixarene ring, at least one of the substituents R, R, Rand Rcontains at least one acid group of carboxylic type available for the reaction with a metal base, with the proviso that said acid group of carboxylic type is not contained in a unit of the calixarene ring derived from salicylic acid. 2. The metal compound according to wherein the calixarene having general formula (I) comprises at least two units of the n units of the calixarene ring in which at least one of the substituents R claim 1 , R claim 1 , Rand Rcontains at least one acid group of the carboxylic type claim 1 , with the proviso that said acid group of carboxylic type is not part of a unit of the calixarene ring derived from salicylic acid.3. The metal compound according to wherein the calixarene having general formula (I) comprises a number of units of the ring claim 1 , between 2 and n claim 1 , in which one of the substituents Rand Rcontains an acid group of carboxylic type claim 1 , with the proviso that said acid group of carboxylic type is not part of a unit of the calixarene ...

Lubricant transformable from solid to semi-solid

A lubricant composition includes a mixture of grease and wax formed into a block which is solid at atmospheric pressure and temperatures up to 150° F., and which transforms into a semi-solid under mechanical loading. The mixture is formed with 5-25% of melted wax. The block may be coated to form a shell to remain solid at elevated temperatures. The block may include other additives. The grease block is suitable for use in various applications, including on a 5th wheel trailer hitch plate.