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20-11-2000 дата публикации

ОБОРУДОВАНИЕ ДЛЯ ПРОИЗВОДСТВА РАСТИТЕЛЬНОГО МАСЛА

Номер: RU0000015887U1
Автор: Гусев В.Н., Кайдаш Н.Д., Кудра Ю.В., Шустов В.Т.
Принадлежит: Закрытое акционерное общество "НПФ "Российские семена"

1. Оборудование для производства растительного масла, содержащее установку для извлечения масла, выполненную с двумя выходами - выходом масла и выходом жмыха, устройство для охлаждения жмыха, бункер для жмыха, выполненный с возможностью загрузки в него жмыха с выхода жмыха установки для извлечения масла через устройство для охлаждения жмыха, установку для комплексной очистки масла, вход которой связан с выходом масла и которая выполнена с возможностью введения в нее отбельной земли через вход дренажного материала и выхода отработанной отбельной земли через его первый выход осадка, и которая выполнена с возможностью введения в нее перлита через вход фильтрующего средства и выхода отработанного перлита через второй выход осадка, по меньшей мере, один насос с трубопроводом для промывки водой установок, бак для зажиренной воды, вход которого связан с трубопроводом для промывки водой установок, отличающееся тем, что введены три дополнительных насоса с трубопроводами, транспортер, испарительная установка, смеситель для перемешивания отработанной отбельной земли и отработанного перлита, и выполненный с возможностью загрузки отработанной отбельной земли и отработанного перлита в смеситель через его вход, бак для зажиренной воды связан с входом испарительной установки посредством одного из дополнительных насосов с трубопроводом, испарительная установка связана с входом смесителя посредством второго из дополнительных насосов с трубопроводом, транспортер установлен на выходе жмыха установки для извлечения масла и выполнен с возможностью подачи жмыха в устройство для охлаждения жмыха, а смеситель связан посредством третьего дополнительного насоса с транспортером с возможностью подачи на него смеси из смесителя. 2. Оборудование по п.1, отличающееся тем, что введен транспортный шнек, связанный с первым и вторым выходами осадков установки для комплексной очистки масла и выполненный с возможностью перемещения отработанной отбельной земли и отработанного перлита в смеситель. (19) RU ...

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Номер записи: 1
27-12-2006 дата публикации

УСТРОЙСТВО ДЛЯ ЭКСТРАКЦИИ МАСЛОСОДЕРЖАЩИХ ОТХОДОВ

Номер: RU0000059567U1
Автор: Бордюков Юрий Юрьевич, Золотокопова Светлана Васильевна, Стоногина Анна Павловна
Принадлежит: Федеральное государственное образовательное учреждение высшего профессионального образования "Астраханский государственный технический университет"

Устройство для экстракции маслосодержащих отходов, содержащее сварную прямоугольную коробку из листовой стали, металлический пластинчатый транспортер, отличающееся тем, что оно дополнительно имеет емкость с флегматизатором и подающий насос, установленные в верхней части устройства и соединенные с экстракционной коробкой между второй и третьей зонами орошения. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 59 567 (13) U1 (51) МПК C11B 13/04 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ОПИСАНИЕ ПОЛЕЗНОЙ МОДЕЛИ К ПАТЕНТУ (21), (22) Заявка: 2006127012/22 , 24.07.2006 (24) Дата начала отсчета срока действия патента: 24.07.2006 (45) Опубликовано: 27.12.2006 (73) Патентообладатель(и): Федеральное государственное образовательное учреждение высшего профессионального образования "Астраханский государственный технический университет" (RU) U 1 5 9 5 6 7 R U Ñòðàíèöà: 1 U 1 Формула полезной модели Устройство для экстракции маслосодержащих отходов, содержащее сварную прямоугольную коробку из листовой стали, металлический пластинчатый транспортер, отличающееся тем, что оно дополнительно имеет емкость с флегматизатором и подающий насос, установленные в верхней части устройства и соединенные с экстракционной коробкой между второй и третьей зонами орошения. 5 9 5 6 7 (54) УСТРОЙСТВО ДЛЯ ЭКСТРАКЦИИ МАСЛОСОДЕРЖАЩИХ ОТХОДОВ R U Адрес для переписки: 414025, г.Астрахань, ул. Татищева, 16, ФГОУ ВПО "АГТУ", патентный отдел (72) Автор(ы): Золотокопова Светлана Васильевна (RU), Бордюков Юрий Юрьевич (RU), Стоногина Анна Павловна (RU) RU 5 10 15 20 25 30 35 40 45 50 59 567 U1 Техническое решение относится к инженерной экологии в области технологий утилизации отходов производства, а именно, к разработке устройства для экстракции маслосодержащих отходов. Известно техническое решение, которое нашло свое применение в технологии получения растительных масел (Щербаков В.Г. Технология получения растительных масел. - М.: Колос, 1992. - с.124). Наиболее близким по ...

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27-05-2009 дата публикации

УСТРОЙСТВО ДЛЯ ЭКСТРАКЦИИ ПРОМАСЛЕННЫХ ОТХОДОВ

Номер: RU0000083249U1
Автор: Бекенов Айткали Тахирович, Бордюков Юрий Юрьевич, Золотокопова Светлана Васильевна
Принадлежит: Государственный комитет Российской Федерации по рыболовству Федеральное государственное образовательное учреждение высшего профессионального образования Астраханский государственный технический университет (ФГОУ ВПО АГТУ)

Устройство для экстракции промасленных отходов, содержащее цилиндр, имеющий верхнее и нижнее днища, загрузочную горловину с крышкой, расположенной в верхней части устройства, вертикального вала с лопастями, отличающееся тем, что оно дополнительно имеет снаружи емкость с флегматизатором и подающим насосом, установленные в верхней части устройства и соединенные с экстрактором. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (13) 83 249 U1 (51) МПК C11B 13/04 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ОПИСАНИЕ ПОЛЕЗНОЙ МОДЕЛИ К ПАТЕНТУ (21), (22) Заявка: 2008148263/22, 08.12.2008 (24) Дата начала отсчета срока действия патента: 08.12.2008 (45) Опубликовано: 27.05.2009 R U 8 3 2 4 9 Формула полезной модели Устройство для экстракции промасленных отходов, содержащее цилиндр, имеющий верхнее и нижнее днища, загрузочную горловину с крышкой, расположенной в верхней части устройства, вертикального вала с лопастями, отличающееся тем, что оно дополнительно имеет снаружи емкость с флегматизатором и подающим насосом, установленные в верхней части устройства и соединенные с экстрактором. Ñòðàíèöà: 1 ru CL U 1 U 1 (54) УСТРОЙСТВО ДЛЯ ЭКСТРАКЦИИ ПРОМАСЛЕННЫХ ОТХОДОВ 8 3 2 4 9 (73) Патентообладатель(и): Государственный Комитет Российской Федерации по рыболовству Федеральное государственное образовательное учреждение Высшего профессионального образования Астраханский государственный технический университет (ФГОУ ВПО АГТУ) (RU) R U Адрес для переписки: 414025, г.Астрахань, ул. Татищева, 16, ФГОУ ВПО АГТУ, патентный отдел (72) Автор(ы): Золотокопова Светлана Васильевна (RU), Бекенов Айткали Тахирович (RU), Бордюков Юрий Юрьевич (RU) U 1 U 1 8 3 2 4 9 8 3 2 4 9 R U R U Ñòðàíèöà: 2 RU 5 10 15 20 25 30 35 40 45 50 83 249 U1 Техническое решение относится к инженерной экологии в области технологий утилизации отходов производства, а именно, к разработке устройства для экстракции промасленных отходов, образованных в результате эксплуатации автотранспорта ...

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10-12-2009 дата публикации

УСТРОЙСТВО ДЛЯ ЭКСТРАКЦИИ НЕФТЕСОДЕРЖАЩИХ ОТХОДОВ

Номер: RU0000089524U1
Автор: Золотокопова Светлана Васильевна, Исмагулов Амир Лазаревич, Кадралиева Ралина Рсланбековна
Принадлежит: Федеральное агентство по рыболовству Федеральное государственное образовательное учреждение высшего профессионального образования Астраханский государственный технический университет (ФГОУ ФПО АГТУ)

Устройство для экстракции нефтесодержащих отходов, содержащее металлический пластинчатый транспортер, отличающееся тем, что транспортер выполнен наклонным и снабжен щитками по всей длине. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 89 524 (13) U1 (51) МПК C11B 13/04 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ОПИСАНИЕ ПОЛЕЗНОЙ МОДЕЛИ К ПАТЕНТУ (21), (22) Заявка: 2009108699/22, 10.03.2009 (24) Дата начала отсчета срока действия патента: 10.03.2009 (45) Опубликовано: 10.12.2009 R U 8 9 5 2 4 Формула полезной модели Устройство для экстракции нефтесодержащих отходов, содержащее металлический пластинчатый транспортер, отличающееся тем, что транспортер выполнен наклонным и снабжен щитками по всей длине. Ñòðàíèöà: 1 ru CL U 1 U 1 (54) УСТРОЙСТВО ДЛЯ ЭКСТРАКЦИИ НЕФТЕСОДЕРЖАЩИХ ОТХОДОВ 8 9 5 2 4 (73) Патентообладатель(и): Федеральное агентство по рыболовству Федеральное государственное образовательное учреждение высшего профессионального образования Астраханский государственный технический университет (ФГОУ ФПО АГТУ) (RU) R U Адрес для переписки: 414025, г.Астрахань, ул. Татищева, 16, ФГОУ ВПО АГТУ, патентный отдел (72) Автор(ы): Золотокопова Светлана Васильевна (RU), Кадралиева Ралина Рсланбековна (RU), Исмагулов Амир Лазаревич (RU) RU 5 10 15 20 25 30 35 40 45 50 89 524 U1 Техническое решение относится к инженерной экологии в области технологий утилизации отходов производства, а именно, к разработке устройства для экстракции нефтесодержащих отходов. Известно устройство, которое нашло свое применение в технологии утилизации нефтесодержащих отходов экстракционным методом LANSCO.(Мазлова Е.А., Мещеряков С.В. Проблемы утилизации нефтешламов и способы их переработки. М., Издательский дом «Ноосфера», 2001, 28 с.) Недостатком работы данного устройства является то, что необходимо очень большое количество растворителя для утилизации отходов. Наиболее близким по сути является горизонтальный ленточный экстрактор МЭЗ, который имеет сварной ...

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Номер записи: 4
10-01-2015 дата публикации

УСТАНОВКА ДЛЯ ПЕРЕГОНКИ ЭФИРНОГО ГОРЧИЧНОГО МАСЛА ИЗ ГИДРОЛИЗАТА

Номер: RU0000149461U1
Автор: Крапивина Юлия Владиславовна, Парахневич Дмитрий Валерьевич, Парахневич Елена Дмитриевна, Попова Светлана Сергеевна, Русакова Галина Георгиевна, Русакова Мария Михайловна
Принадлежит: Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Волгоградский государственный технический университет" (ВолгГТУ)

1. Установка для перегонки эфирного горчичного масла из гидролизата, содержащая последовательно соединенные перегонный аппарат, холодильник и приемник, отличающаяся тем, что дополнительно содержит узел предварительной подготовки гидролизата для увеличения степени извлечения эфирного горчичного масла, установленный перед перегонным аппаратом и состоящий из парожидкостного инжектора для подачи транспортного агента, подогревателя и испарителя, последовательно соединенных нагнетательным трубопроводом. 2. Установка по п.1, отличающаяся тем, что в качестве транспортного агента используют острый пар. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (51) МПК C11B 13/00 (13) 149 461 U1 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ОПИСАНИЕ (21)(22) Заявка: ПОЛЕЗНОЙ МОДЕЛИ К ПАТЕНТУ 2014112404/13, 31.03.2014 (24) Дата начала отсчета срока действия патента: 31.03.2014 (45) Опубликовано: 10.01.2015 Бюл. № 1 (73) Патентообладатель(и): Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Волгоградский государственный технический университет" (ВолгГТУ) (RU) 1 4 9 4 6 1 R U Формула полезной модели 1. Установка для перегонки эфирного горчичного масла из гидролизата, содержащая последовательно соединенные перегонный аппарат, холодильник и приемник, отличающаяся тем, что дополнительно содержит узел предварительной подготовки гидролизата для увеличения степени извлечения эфирного горчичного масла, установленный перед перегонным аппаратом и состоящий из парожидкостного инжектора для подачи транспортного агента, подогревателя и испарителя, последовательно соединенных нагнетательным трубопроводом. 2. Установка по п.1, отличающаяся тем, что в качестве транспортного агента используют острый пар. Стр.: 1 U 1 U 1 (54) УСТАНОВКА ДЛЯ ПЕРЕГОНКИ ЭФИРНОГО ГОРЧИЧНОГО МАСЛА ИЗ ГИДРОЛИЗАТА 1 4 9 4 6 1 Адрес для переписки: 400005, г. Волгоград, пр. Ленина, 28, отдел интеллектуальной собственности ВолгГТУ R U Приоритет(ы): (22) Дата подачи ...

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Номер записи: 5
10-01-2015 дата публикации

УСТАНОВКА ДЛЯ ГИДРОЛИЗА СИНИГРИНА В ОТХОДАХ ГОРЧИЧНО-МАСЛОБОЙНОГО ПРОИЗВОДСТВА

Номер: RU0000149522U1
Автор: Мельниченко Татьяна Юрьевна, Парахневич Дмитрий Валерьевич, Парахневич Елена Дмитриевна, Русакова Галина Георгиевна, Русакова Мария Михайловна, Трегулова Анна Евгеньевна
Принадлежит: Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Волгоградский государственный технический университет" (ВолгГТУ)

Установка для гидролиза синигрина в отходах горчично-маслобойного производства, содержащая последовательно соединенные реактор с мешалкой и конденсатор, отличающаяся тем, что дополнительно содержит газо-газовый инжектор для нагнетания отходов горчично-маслобойного производства во взвешенном состоянии по нагнетательному трубопроводу в расходный бункер, дозатор для равномерной подачи отходов из расходного бункера в парогазовый инжектор, обеспечивающий нагнетание отходов в смеси с паром по нагнетательному трубопроводу в реактор с мешалкой, соединенный с вертикально установленным над ним конденсатором. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (51) МПК C11B 13/00 (13) 149 522 U1 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ОПИСАНИЕ (21)(22) Заявка: ПОЛЕЗНОЙ МОДЕЛИ К ПАТЕНТУ 2014112406/13, 31.03.2014 (24) Дата начала отсчета срока действия патента: 31.03.2014 (45) Опубликовано: 10.01.2015 Бюл. № 1 (73) Патентообладатель(и): Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Волгоградский государственный технический университет" (ВолгГТУ) (RU) 1 4 9 5 2 2 R U Формула полезной модели Установка для гидролиза синигрина в отходах горчично-маслобойного производства, содержащая последовательно соединенные реактор с мешалкой и конденсатор, отличающаяся тем, что дополнительно содержит газо-газовый инжектор для нагнетания отходов горчично-маслобойного производства во взвешенном состоянии по нагнетательному трубопроводу в расходный бункер, дозатор для равномерной подачи отходов из расходного бункера в парогазовый инжектор, обеспечивающий нагнетание отходов в смеси с паром по нагнетательному трубопроводу в реактор с мешалкой, соединенный с вертикально установленным над ним конденсатором. Стр.: 1 U 1 U 1 (54) УСТАНОВКА ДЛЯ ГИДРОЛИЗА СИНИГРИНА В ОТХОДАХ ГОРЧИЧНО-МАСЛОБОЙНОГО ПРОИЗВОДСТВА 1 4 9 5 2 2 Адрес для переписки: 400005, г. Волгоград, пр. Ленина, 28, отдел интеллектуальной собственности ВолгГТУ R U Приоритет(ы ...

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Номер записи: 6
18-12-2017 дата публикации

Установка по производству сырого таллового масла

Номер: RU0000175744U1
Автор: Брусенко Игорь Иванович, Середкин Антон Юлианович, Шадрин Евгений Дмитриевич
Принадлежит: Общество с ограниченной ответственностью "Техносервис"

Полезная модель относится к установкам по производству сырого таллового масла и может быть использована в целлюлозно-бумажной и лесохимической промышленности. Установка по производству сырого таллового масла имеет в своем составе статический смеситель 1, подсоединенный к трубопроводу подачи сульфатного мыла и через первый насос 2 подсоединенный к баку 3 серной кислоты. При этом выход статического смесителя 1 подсоединен к механическому смесителю 4, снабженному мешалкой. Установка имеет декантатор 5. Между декантатором 5 и механическим смесителем 4 имеется промежуточная вертикально ориентированная емкость 6. Декантатор 5 подсоединен своим верхним патрубком, выполненным на боковой стенке корпуса, к баку 7 таллового масла. Выгружной патрубок бака 7 таллового масла предназначен для подачи таллового масла на склад продукции. Конструкция содержит первый сборник 8 кислой воды, второй сборник 9 кислой воды и накопительную емкость 10 таллового масла. Декантатор 5 трубопроводом, подсоединенным к конусу днища, соединен с обоими сборниками кислой воды. Первый сборник 8 кислой воды соединен трубопроводом с накопительной емкостью 10 таллового масла и через нее с трубопроводом с установленным в нем вторым насосом 11 с баком 7 таллового масла. Другим трубопроводом с установленным в нем третьим насосом 12 первый сборник 8 кислой воды соединен со вторым сборником 9 кислой воды. К этому же трубопроводу подсоединен трубопровод для отведения нейтрализованного раствора лигнина и бисульфата натрия на выпарную станцию. К трубопроводу на выпарную станцию также подсоединен второй сборник 9 кислой воды, при этом второй сборник 9 кислой воды подсоединен к трубопроводу с четвертым насосом 13 для отвода нейтрализованной кислой воды на промывку мыла. К обоим сборникам 8 и 9 кислой воды подсоединен трубопроводами бак белого щелока 14. Поэтапное разделение продуктов реакции с использованием новых конструктивных элементов приводит к более полному разделению продуктов реакции, что уменьшает потери ...

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Номер записи: 7
01-03-2012 дата публикации

Bio-oil recovery systems

Номер: US20120051980A1
Автор: Charles C. Gallop, Kurt A. Dieker, Theron Cooper
Принадлежит: ICM Inc USA

An emulsion-breaking additive is combined with an emulsion concentrate to yield a reaction product and the emulsion concentrate is produced in a process stream and contains entrapped bio-oil. Subsequent phase separating can be accomplished with gravity separation and/or mechanical processing. The emulsion-breaking additive can be native to the process stream. Related systems and methods are also provided.

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Номер записи: 8
15-03-2012 дата публикации

Methods for producing a high protein corn meal from a whole stillage byproduct and system therefore

Номер: US20120064213A1
Автор: Chie Ying Lee
Принадлежит: Fluid Quip Inc

The present invention relates generally to corn dry-milling, and more specifically, to methods for producing a high protein corn meal from a whole stillage byproduct produced in a corn dry-milling process for making ethanol and a system therefore. In one embodiment, a method for producing a high protein corn meal from a whole stillage byproduct includes, in a corn dry-milling process for making ethanol, separating the whole stillage byproduct into an insoluble solids portion and a thin stillage portion. The thin stillage portion is separated into a protein portion and a water soluble solids portion. Next, the protein portion is dewatered then dried to define a high protein corn meal that includes at least 40 wt % protein on a dry basis.

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Номер записи: 9
02-08-2012 дата публикации

Composition of matter comprising of the creation of a low molecular weight hydrocarbon fluid exhibiting oligomerized pentenes mainly comprised of 2-Methyl-2-Butene subunits as well as related plant isoprenoids composed of 2-Methyl-1-Butene subunits and other hydrocarbons from hydrocarbon-bearing woody biomass and a process for the extraction and refinement in making the same composition through the creation of solvent permeable woody biomass particles and a multi-phase solvent extraction

Номер: US20120197049A1
Автор: Stephen Daniel Matthews
Принадлежит: Individual

A composition of matter with of the creation of a low molecular weight hydrocarbon fluid called Wood Phytoleum from woody Pinaceae and Myrtaceae biomass and a process for the extraction and refinement in making the same composition of matter through the reduction of the particle size of the raw woody biomass to form a solvent permeable particle and a phased multi-wash solvent system of extraction and refinement. A preferred embodiment includes the steps of the reduction of the particle size of the raw woody biomass to form a solvent permeable particle by shearing and chipping, the application of a phased multi-wash solvent system to the solvent permeable particle utilizing a non-polar solvent together with a bridge solvent soluble in both the non-polar solvent and in water, the application of a final bridge solvent wash to the solvent permeable particle, a mechanism for washing the particles of the woody biomass within the multi-wash solvent system, a mechanism for the collection of the solvent and Wood Phytoleum solution from the multi-wash solvent system, the extraction of the solvent from the solvent saturated particles of the woody biomass and the discharge for continued use of the woody biomass, and a process and mechanism for the extraction, collection and refinement of the solvent and Wood Phytoleum solution to discharge the solvents for reuse and to collect the Wood Phytoleum liquid oil including Pinene A and Pinene B and other oligomerized pentenes.

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Номер записи: 10
21-03-2013 дата публикации

Recovery of Oleaginous Tricyglycerols from Wastewater Title of Invention Treatment Plant Foams

Номер: US20130072706A1
Автор: Elizabeth J. Summer, Mei Liu, Sarah Dugleby
Принадлежит: PHASE BIOCONTROL RES LLC

Tricyglycerols that may be converted to biofuel are recovered from oleaginous organisms in the natural and induced foam of wastewater treatment process plants. Growing oleaginous organisms in the form of comparatively dry foam simplifies harvest and is more efficient and efficacious than skimming the biomass off the top of the liquids that rely on less efficient centrifugation or filtration methods typically required to concentrate cells grown in liquids.

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Номер записи: 11
13-06-2013 дата публикации

Application of Bacteriophages for the Control of Unwanted Bacteria in Biofuel Production Mediated by Bacterial Reactive Agents

Номер: US20130149759A1
Автор: Elizabeth J. Summer, Mei Liu
Принадлежит: Phage Biocontrol Res LLC

A method of reducing process interruptions in biofuel production systems mediated by bacterial reactive agents by reducing the amount of unwanted bacteria without reduction of wanted or useful bacteria. The method comprises applying a phage panel(s) containing phage virulent for unwanted bacteria that does not contain phage phages virulent wanted bacteria. The method includes, optionally, the selective production of solutions of phage for unwanted bacteria from which phages for wanted bacteria are screened out.

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Номер записи: 12
27-06-2013 дата публикации

SUSPENDED SOLIDS SEPARATION SYSTEMS AND METHODS

Номер: US20130165678A1
Автор: Dieker Kurt A., Gallop Charles C., Kohl Scott
Принадлежит:

A method that includes clarifying a thin stillage product in a mechanical processor to produce a fine suspended solids stream and a clarified thin stillage is provided. The method further includes providing the thin stillage product and the clarified thin stillage, separately or in a combined stream, to one or more evaporators to produce one or more reduced suspended solids streams, each stream having a reduced amount of suspended solids and a lower viscosity as compared to process streams having a comparable total solids content but containing a higher amount of suspended solids. The method can further included further processing of one or more of the reduced suspended solids streams to produce a bio-oil product. 1. A method comprising:clarifying a thin stillage product in a mechanical processor to produce a fine suspended solids stream and clarified thin stillage; andproviding the thin stillage product and the clarified thin stillage, separately or in a combined stream, to one or more evaporators to produce one or more reduced suspended solids streams, each stream having a reduced amount of suspended solids and a lower viscosity as compared to process streams having a comparable total solids content and which contains a higher amount of suspended solids.2. The method of claim 1 , wherein the suspended solids comprise less than about 10% by weight of the total solids content and the total solids content is between about 68% and about 72% by weight.3. The method of claim 1 , wherein at least one of the one or more reduced suspended solids stream has a total solids content comprising suspended solids and dissolved solids in an amount between about 30% and about 90% by weight claim 1 , wherein the suspended solids comprise less than 25% by weight of the total solids content.4. The method of claim 1 , wherein at least one of the one or more reduced suspended solids stream is clarified concentrated thin stillage claim 1 , which contains an amount of bio-oil which is ...

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Номер записи: 13
19-09-2013 дата публикации

METHOD OF EXTRACTING LIPIDS FROM TRAP GREASE WITH WASTE COOKING OIL

Номер: US20130239467A1
Автор: Lu Mingming, Tu Qingshi, Wang Jingjing
Принадлежит: University of Cincinnati

Describe are methods of extracting the lipid fraction from trap grease using vegetable oil, such as vegetable oils sourced from waste cooking oil. The method includes mixing a volume of vegetable oil with a volume of trap grease. The mixture is comprised of an aqueous fraction, a solid fraction, and a lipid fraction. The mixture is heated to a temperature in a range from about 50 degrees C. to about 100 degrees C. for a period of time sufficient to extract at least 80 percent of the lipids from the trap grease. The lipid fraction is then separated from the solid fraction. The method may further include a process of producing biodiesel from the extracted lipid fraction. 1. A method of extracting a lipid fraction from trap grease comprising:mixing a volume of vegetable oil with a volume of trap grease, wherein the mixture is comprised of an aqueous fraction, a solid fraction, and a lipid fraction;heating the mixture to a temperature in a range from about 50 degrees C. to about 100 degrees C. for a period of time sufficient to extract at least 80 percent of the lipids from the trap grease; andseparating a portion of the lipid fraction from the solid fraction.2. The method of claim 1 , wherein the vegetable oil is mixed with the trap grease at a ratio between about 1.5 ml:1 mg to about 4.5 ml:1 mg.3. The method of claim 1 , wherein the mixture of vegetable oil and trap grease is heated to a temperature in a range from about 55 degrees C. to about 85 degrees C.4. The method of claim 1 , wherein the mixture of vegetable oil and trap grease is heated to a temperature in a range from about 60 degrees C. to about 65 degrees C.5. The method of claim 1 , wherein the mixture of vegetable oil and trap grease is maintained at the desire temperature for a period of time from about 45 minutes to about 210 minutes.6. The method of claim 1 , wherein the separation step includes separating the lipid fraction from the solid fraction using a filtration process.7. The method of claim 1 , ...

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Номер записи: 14
19-09-2013 дата публикации

PROCESS AND APPARATUS FOR PURIFYING MATERIAL OF BIOLOGICAL ORIGIN

Номер: US20130245301A1
Автор: Kotoneva Jari, LAUMOLA Heli, NOUSIAINEN Jaakko, RISSANEN Arto, Ristolainen Matti
Принадлежит: UPM-KYMMENE CORPORATION

The present invention relates to a process and an apparatus for purifying a mixture of terpene material and tall oil material for the production of biofuels and components thereof. The present invention relates further to hydroprocessing of the purified material to obtain biofuels and components thereof. 1. A process for purifying a mixture of terpene material and tall oil material , comprising the following steps(a) evaporating the mixture of terpene material and tall oil material in a first evaporation step (E) to produce a first fraction comprising light hydrocarbons and water and a second fraction comprising fatty acids, resin acids, neutral substances and residue components,(b) evaporating said second fraction in at least one further evaporation step (G; F,G) to produce a third fraction comprising fatty acids, resin acids and light neutral substances, and a residue fraction, and(c) recovering said first fraction, third fraction and residue fraction.2. The process according to claim 1 , characterized in that the first evaporation step (E) is performed at a temperature of 50 to 250° C. and at a pressure of 5 to 100 mbar.3. The process according to claim 1 , characterized in that said at least one further evaporation step (G; F claim 1 ,G) is performed in one step (G) or in two steps (F claim 1 ,G).4. The process according to claim 3 , characterized in that said at least one further evaporation step (G; F claim 3 ,G) is performed in one step (G) at a temperature of 200 to 450° C. and at a pressure of 0 to 50 mbar.5. The process according to claim 3 , characterized in that said at least one further evaporation step (G; F claim 3 ,G) is performed in two steps (F claim 3 ,G) claim 3 , whereby the first (F) of said two further evaporation steps is performed at a temperature of 180 to 350° C. and at a pressure of 0.1 to 40 mbar and the second (G) of said two further evaporation steps is performed at a temperature of 200 to 450° C. and at a pressure of 0 to 50 mbar.6. ...

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Номер записи: 15
03-10-2013 дата публикации

PROCESS FOR ISOLATION OF FATTY ACIDS, RESIN ACIDS AND STEROLS FROM TALL OIL PITCH

Номер: US20130261284A1
Автор: HAMUNEN Antti
Принадлежит: RAVINTORAISIO OY

A process for recovering fatty acids, resin acids and sterols from tall oil pitch, said process comprising 1. A process for recovering fatty acids , resin acids and sterols from tall oil pitch , said process comprisinga) saponifying the tall oil pitch with an alkali to hydrolyse esters included in the pitch to free alcohols and organic acids in salt form,b) acidulating the saponified pitch with a mineral acid to convert the organic acids in salt form into free organic acids and to form an organic phase and an aqueous phase,c) separating the aqueous phase from the organic phase,d) evaporation fractionating the organic phase to obtain a distillate rich in sterols, fatty acids and resin acids,e) evaporation fractionating the distillate to obtain a bottom fraction rich in sterols, and a distillate rich in fatty acids and resin acids, andf) subjecting the sterols in the sterol-rich bottom fraction to crystallisation purification.2. The process of claim 1 , wherein the amount of the mineral acid in the acidulation is such that the pH of the aqueous phase is less than 4 claim 1 , preferably between 1.5 and 3.8 claim 1 , more preferably between 2.0 and 3.8 claim 1 , and most preferably between 3.0 and 3.5.3. The process of or claim 1 , wherein the sterols in the sterol-rich bottom fraction are subjected to purification by solvent crystallisation.4. The process of any of to claim 1 , wherein the distillate rich in fatty acids and resin acids is subjected to distillation to obtain separately fatty acids and resin acids.5. The process of any of to claim 1 , wherein the organic phase is treated with an alkali to destroy excess mineral acid used for acidulating the saponified pitch.6. The process of any of to claim 1 , wherein the organic phase is treated with an alkali in an amount in excess to that needed for destroying excess mineral acid used for acidulating the saponified pitch claim 1 , resulting in a partial saponification of fatty acids and resin acids claim 1 , the ...

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Номер записи: 16
23-01-2014 дата публикации

Separate Collection and Conversion Method and Plant For the Reuse of Natural and/or Synthetic Ester-Based Oils or Greases of Industrial Origin for Energy Purposes

Номер: US20140024847A1
Автор: Marini Leandro, Parodi Augusto
Принадлежит: A. & A. Fratelli Parodi S.p.A.

Separate collection and conversion method and plant for the reuse of used oils and greases for energy purposes, which method provides one or more of the following steps: producing and separating the waste from other substances or compounds, collecting the waste gathering/storing the waste in at least a collection and/or regeneration facility, regenerating or treating the waste, reusing the collected or regenerated or treated waste, an oil or a grease or a mixture containing at least a natural and/or synthetic ester-based oil and/or grease being considered as waste, which oil or grease or which mixture is the by-product or waste of industrial processes. 1. Separate collection and conversion method for the reuse of used oils and greases for energy purposes , which method provides one or more of the following steps:producing and separating the waste from other substances or compounds, gathering/storing the waste in at least a collection and/or regeneration facility,', 'regenerating or treating the waste,, 'collecting the waste'}reusing the collected or regenerated or treated waste,an oil or a grease or a mixture containing at least a natural and/or synthetic ester-based oil and/or grease being considered as waste, which oil or grease or which mixture is the by-product or waste of industrial processes.2. Method according to characterized in that the waste production and separation step provides natural and/or synthetic claim 1 , ester-based oils/greases to be separated from oils/greases with a different base claim 1 , particularly a mineral base.3. Method according to or claim 1 , characterized in that waste means one or more mixtures of the following substances: oils deriving from the deoiling of filtering and bleaching earths claim 1 , vegetable ester-based oils used into electric transformers claim 1 , synthetic ester-based oils used in electric transformers claim 1 , vegetable ester-based oils used in metal quenching claim 1 , oils used in metal cementation claim 1 ...

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Номер записи: 17
06-02-2014 дата публикации

Process for autocatalytic esterification of fatty acids

Номер: US20140039206A1
Автор: Bent Sarup, Susanne JONSSON
Принадлежит: ALFA LAVAL CORPORATE AB

The present invention relates to a process for isolation of micronutrients from deodorizer distillate comprising free fatty acids, the process comprises the following steps: (i) treating the deodorizer distillate in an esterification step with glycerol, which esterification step is autocatalysed, producing a feedstock of acyl glycerides, and discharging excess of glycerol and produced water; (ii) transferring the feedstock of acyl glycerides having a water content less than 1500 ppm and a free fatty acid content less than 3 wt % to a transesterification step and treating the feedstock of acyl glycerides with methanol to produce a crude biodiesel product; and (iii) refining the crude biodiesel product in a distillation step, and separating the crude biodiesel product into three fractions 1) fatty acid methyl esters, 2) micronutrient rich product comprising tocopherol, and 3) light hydrocarbons.

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Номер записи: 18
01-01-2015 дата публикации

SEPARATION OF BIOCOMPONENTS FROM DDGS

Номер: US20150001160A1
Автор: Roa-Espinosa Aicardo
Принадлежит:

A multi stage process for the progressive removal of protein and isolating streams containing cellulose fibers and oil from a waste stream containing Dried Distillers Grains with Solubles is disclosed. Targeted polymers are added to the source and separated streams prior to passing the streams through separation equipment including a rotary screen, a multi disk press, a dissolved air floatation device and optionally a centrifuge in which the waste stream is separated into a stream containing predominantly protein, a stream containing predominantly oil and a stream that contains predominantly cellulose and hemicellulose fibers.

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Номер записи: 19
04-01-2018 дата публикации

Non-Denatured Proteins Derived From a Biomass Source

Номер: US20180002374A1
Автор: Laubsch Kenneth L.
Принадлежит:

A biomass-derived protein compound has a high concentration of protein and can be made to have a very low concentration of fat and water; even when the biomass feedstock has a high fat concentration. The biomass-derived protein compound may be a whole protein that is non-denatured and enzymatically digestible. This unique protein compound can be produced from molecules from more than one source organism, including various animals and/or plant feedstocks. The unique protein compound is derived from a unique biomass method and apparatus for the treatment of a biomass stream to extract and separate an essentially solvent-free product from the biomass stream. In this unique method the solids content of the biomass stream is increased by bringing the biomass stream into contact with a moderately pressurized liquefied gas solvent, to create a high solids content biomass stream and introducing the high solids content biomass stream to an extraction apparatus. 1. A biomass-derived protein compound comprising:a mixture of protein molecules from more than one source organism wherein the mixture contains at least 65% whole, non-denatured protein molecules by weight, less than 15% fat by weight, and less than 10% water by weight.2. The biomass-derived protein compound of claim 1 , wherein at least 75% of the protein molecules in the compound contain each of the following essential amino acids: histidine claim 1 , isoleucine claim 1 , leucine claim 1 , lysine claim 1 , methionine claim 1 , phenylalanine claim 1 , threonine claim 1 , tryptophan claim 1 , and valine.3. The biomass-derived protein compound of claim 1 , wherein the biomass-derived protein compound has a neutral pH with a pH between 6 and 8.4. The biomass-derived protein compound of claim 1 , wherein a substantial portion of the protein molecules are enzymatically digested.5. The biomass-derived protein compound of claim 1 , wherein the biomass from which the protein compound is derived contains greater than 50% fat ...

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Номер записи: 20
07-01-2021 дата публикации

METHODS OF REFINING A GRAIN OIL COMPOSITION

Номер: US20210002584A1
Автор: Bly Steven T., Flittie Brett A., McCurdy Alex T., Milbrandt Jacob A., Sarks Cory J., Urban Shannon S.
Принадлежит:

The present disclosure relates methods and systems for refining grain oil compositions using water, and related compositions produced therefrom. The present disclosure also relates to methods of using said compositions. The present disclosure also relates to methods of using grain oil derived from a fermentation product in an anti-foam composition. 1. A method of refining a grain oil composition feedstock to provide a grain oil product , wherein the method comprises:combining the grain oil composition feedstock with water to form an oil-water mixture, wherein the grain oil composition comprises an impurity component, and wherein the oil-water mixture does not include chelating agent in an amount to aid in removal of metals and metal compounds from the grain oil composition feedstock;exposing the oil-water mixture to a temperature in the range from 0° C. to 50° C. for a time period at least until the oil-water mixture forms at least an oil phase and an emulsion phase; andseparating at least a portion of the oil phase from the emulsion phase to form the grain oil product, wherein an amount of the impurity component in the emulsion phase is greater than an amount of the impurity component in the grain oil product.2. The method of claim 1 , wherein the grain oil composition feedstock is derived from thin stillage by a method comprising:optionally evaporating at least a portion of water from the thin stillage to condense the thin stillage into a syrup; andseparating the thin stillage or syrup into a first oil fraction and a first aqueous fraction, wherein the first oil fraction is the grain oil composition feedstock.3. The method of claim 1 , wherein the grain oil composition feedstock is derived from thin stillage by a method comprising:optionally evaporating at least a portion of water from the thin stillage to condense the thin stillage into a syrup;separating the thin stillage or syrup into a first oil fraction and a first aqueous fraction, wherein the first oil ...

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Номер записи: 21
07-01-2021 дата публикации

POLYGLYCEROL FATTY ACID ESTERS (PGE) FOR CORN OIL EXTRACTION

Номер: US20210002585A1
Автор: RAAB Michael, Turunc Umit
Принадлежит:

An oil separation treatment composition providing a process stream mixture from a corn to ethanol process, and one or more polyglycerol esters of fatty acids (PGE) or mixture of PGE. A method for recovering oil in a corn to ethanol process wherein oil and solids are present in a process stream mixture, the method providing adding to the process stream mixture an oil separation treatment, the oil separation treatment comprises polyglycerol esters of fatty acids (PGE) or mixture of PGE. 1. An oil separation treatment composition , the composition comprising a process stream mixture from a corn to ethanol process , and one or more polyglycerol esters of fatty acids (PGE) or mixture of PGE.2. The oil separation treatment composition as recited in claim 1 , wherein the process stream mixture is present in a whole stillage process stream claim 1 , a thin stillage process stream claim 1 , an evaporator claim 1 , a syrup stream claim 1 , or at any time after the distillation stage but prior to the oil separation process.3. The oil separation treatment composition as recited in claim 1 , wherein the PGE is a member or members selected from the group consisting of polyglycerol-3-monooleate claim 1 , polyglycerol-3-dioleate claim 1 , polyglycerol-3-monostearate claim 1 , polyglycerol-6-distearate claim 1 , polyglycerol-10-caprylate/caprate claim 1 , polyglycerol-10-dipalmitate claim 1 , polyglycerol-10-monostearate claim 1 , polyglycerol-10-monooleate claim 1 , polyglycerol-10-dioleate claim 1 , polyglycerol-10-tetraoleate or polyglycerol-10-decaoleate.4. The oil separation treatment composition as recited in claim 1 , wherein the PGE is non-toxic and digestible.5. The oil separation treatment composition as recited in claim 1 , wherein the PGE is polyglycerol-3-monooleate.6. The oil separation treatment composition as recited in claim 1 , wherein the PGE is a blend of polyglyerol-3-monooleate claim 1 , polyglyerol-10-monooleate and polyglyerol-10-dioleate.7. The oil ...

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Номер записи: 22
20-01-2022 дата публикации

CONTINUOUS FRACTIONATION OF CRUDE TALL OIL TO REFINED TALL DIESEL

Номер: US20220017840A1
Автор: NAYDENOV Valeri
Принадлежит:

The present invention describes a process for continuous fractionation of CTO (crude tall oil) to RTD (refined tall diesel), said process comprising:—when removing a stream of TOP (tall oil pitch) the CTO is fed through at least two evaporation zones arranged in series so that one stream of CTO is fed from a first evaporation zone to a second evaporation zone, wherein a TOP stream is produced and fed from the second evaporation zone, wherein a first vapor stream is produced within the first evaporation zone and a second vapor stream is produced within the second evaporation zone and wherein there is a temperature difference of at least 10° C. between the first vapor stream and the second vapor stream; and—feeding the first vapor stream and the second vapor stream into a subsequent fractionation column to produce a stream of RTD from the fractionation column, wherein the first vapor stream and the second vapor stream are being fed to different positions, relative to the column height, in the fractionation column, where different conditions are applied to ensure suitable fractionations of a more fatty acid rich material and a more rosin rich material, respectively, and which different positions in the fractionation column are separated by packing means. 1. Process for continuous fractionation of CTO (crude tall oil) to RTD (refined tall diesel) , said process comprising:when removing a stream of TOP (tall oil pitch) the CTO is fed through at least two evaporation zones arranged in series so that one stream of CTO is fed from a first evaporation zone to a second evaporation zone, wherein a TOP stream is produced and fed from the second evaporation zone, wherein a first vapor stream is produced within the first evaporation zone and a second vapor stream is produced within the second evaporation zone and wherein there is a temperature difference of at least 10° C. between the first vapor stream and the second vapor stream; andfeeding the first vapor stream and the second ...

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Номер записи: 23
12-01-2017 дата публикации

METHOD AND SYSTEM FOR REDUCING RESIDUAL SOAP IN CRUDE TALL OIL

Номер: US20170009181A1
Автор: Kotoneva Jari
Принадлежит:

The present invention relates to a method and system for reducing residual soap in crude tall oil, wherein crude tall oil is supplied via piping to at least one vessel, soap number of the crude tall oil is determined using on-line measuring technique and sulphuric acid is added to the crude tall oil at a site of blending, where the dosing of the sulphuric acid is adjusted on-line to provide soap number of not more than 2. 1. A method for reducing residual soap in crude tall oil , characterized in the method comprises the steps , wherecrude tall is supplied to at least one vessel,soap number of the crude tall oil is measured on-line,an amount of sulphuric acid having concentration between 20-50 wt %, needed for adjusting the soap number to a value of not more than 2 is determined, andthe determined amount of sulphuric acid is added to the crude tall oil at a site of blending whereby treated crude tall oil having soap number not more than 2 is obtained.2. The method according to claim 1 , characterized in the method further comprises the steps wherethe measured soap number is transmitted as an input to a controlling unit, which controlling unit determines as an output the amount of sulphuric acid needed for adjusting the soap number to a value of not more than 2,the output of the amount of sulphuric acid is transmitted to a sulphuric acid dosing device, andthe amount of sulphuric acid is added to the crude tall oil according to the output, at a site of blending of crude tall oil and sulphuric acid.3. The method according to claim 1 , characterized in the crude tall oil is supplied via a line to at least one vessel.4. The method according to claim 2 , characterized in the soap number is measured from the crude tall oil running in the line.5. The method according to claim 1 , characterized in the crude tall oil is supplied using an unloading pump.6. The method according to claim 2 , characterized in the soap number of the crude tall oil running in the line is measured ...

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Номер записи: 24
18-01-2018 дата публикации

Sturgeon roe sack membrane-derived oil

Номер: US20180014564A1
Автор: Jemima BENNING, Kenneth BENNING
Принадлежит: SHAH CAVIAR Ltd

Preservation of newly-extracted roe sacks of sturgeons for subsequent harvesting of roe and caviar production, wherein said preservation employs an oil derived from roe sack membrane normally discarded in conventional caviar production. Such preservation enables roe sacks with retained roe derived from farmed or wild sturgeon to be stored and transported whereby export can be considered. The same oil, or fatty acid-containing fractions thereof, may also find use in dietary compositions, e.g. pet foods.

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Номер записи: 25
17-01-2019 дата публикации

Methodology for upgrading and cleaning of used tires, waste lubricants as well as any kind of oils and fats for utilization as feedstock in thermochemical conversion processes

Номер: US20190016959A1
Автор: Stylianos ARVELAKIS
Принадлежит: Individual

A methodology for cleaning and upgrading any kind of tires (cars, motorcycles, trucks, etc.), any kind of waste lubricants (internal combustion engines, industrial parts), any kind of oils as well as plant and animal fats by means of removal of the inorganic elements (potassium, sodium, chlorine, sulfur, phosphorus and heavy metals such as Pb, Cu, Cd, Zn, Hg, Mn, etc.) and the simultaneous addition of new such as calcium, magnesium and ammonium, in order to produce a clean and upgraded rubber material, lubricant as well as fat/oil, which can be used as raw material in thermochemical conversion processes such as flash (t<1 sec)/fast pyrolysis.

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Номер записи: 26
21-01-2021 дата публикации

METHODS FOR PRODUCING A HIGH PROTEIN CORN MEAL FROM A WHOLE STILLAGE BYPRODUCT AND SYSTEM THEREFORE

Номер: US20210017470A1
Автор: Lee Chie Ying
Принадлежит:

The present invention relates generally to corn dry-milling, and more specifically, to methods for producing a high protein corn meal from a whole stillage byproduct produced in a corn dry-milling process for making ethanol and a system therefore. In one embodiment, a method for producing a high protein corn meal from a whole stillage byproduct includes, in a corn dry-milling process for making ethanol, separating the whole stillage byproduct into an insoluble solids portion and a thin stillage portion. The thin stillage portion is separated into a protein portion and a water soluble solids portion. Next, the protein portion is dewatered then dried to define a high protein corn meal that includes at least 40 wt % protein on a dry basis. 1. A method for producing grain protein from a whole stillage comprising:separating a whole stillage byproduct, via a filtration centrifuge, a decanter centrifuge, a pressure screen, or a paddle screen, into an insoluble solids portion and a solubles portion, which includes protein;prior to any evaporation step, separating the solubles portion, via a nozzle centrifuge or a cyclone apparatus, into only a grain protein portion and a water soluble solids portion, wherein the grain protein portion is not subsequently subjected to an evaporator; anddrying the grain protein portion to define a grain meal that includes at least 40 wt % protein on a dry basis.2. A system for producing grain protein from a whole stillage , the system comprising:a first apparatus that receives a whole stillage byproduct, wherein the first apparatus separates the whole stillage byproduct into an insoluble solids portion and a solubles portion, which includes protein; anda second apparatus that is situated after the first apparatus and prior to any evaporator and that receives the soluble portion from the first apparatus, wherein the second apparatus separates the solubles portion into only a grain protein portion and a water soluble solids portion.3. The system ...

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Номер записи: 27
16-01-2020 дата публикации

Fractionation of biomass-based material

Номер: US20200017800A1
Автор: Kim VIKMAN, Ville NEVANLINNA
Принадлежит: Neste Oyj

A process is disclosed for fractionating biomass-based material. The process includes evaporating an evaporable part of biomass-based material in a short path evaporator, SPE, to produce a depitched lights fraction in liquid form, and a heavier pitch fraction. The depitched lights fraction may contain depitched tall oil in liquid form, and the heavier pitch fraction may contain tall oil pitch, TOP.

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Номер записи: 28
29-01-2015 дата публикации

Mobile processing systems and methods for producing biodiesel fuel from waste oils

Номер: US20150031097A1
Автор: James M. Rethore, Julie E. Wheeler, Luca Zullo
Принадлежит: Revolution Fuels Inc

The present invention improves biodiesel production in several ways. Unique combinations of unit operations and flow configurations are disclosed in mobile processing units that are feedstock-flexible and can be dynamically deployed in a distributed way. In some embodiments, a process includes introducing a waste oil and an alcohol into a reactor with an esterification-transesterification enzymatic catalyst. Free fatty acids are reacted with alcohol to produce fatty acid alkyl esters, and glycerides are reacted with alcohol to produce fatty acid alkyl esters and glycerin. A membrane separator removes glycerin, water, and alcohol. Unreacted free fatty acids are then separated and recycled, to generate a product stream with fatty acid alkyl esters. A genset may be provided for combusting glycerin to produce electrical power and thermal heat as co-products. This biodiesel process may be energy self-sufficient, require no external utilities, and avoid direct discharge of wastewater.

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Номер записи: 29
02-02-2017 дата публикации

METHOD FOR IMPROVING CORN OIL EXTRACTION USING ALKYL POLYGLYCOSIDES

Номер: US20170029742A1
Автор: Turunc Umit
Принадлежит:

Methods are provided for recovering oil from a process stream mixture in a corn to ethanol process. The method comprises adding an oil separation aid to the process stream wherein the oil separation aid is an alkyl polyglycoside (APG). 1. A method for recovering oil in a corn to ethanol process wherein oil and solids are present in a process stream mixture , said method comprising adding to said process stream mixture an oil separation aid , said oil separation aid comprising an alkyl polyglycoside (APG) or mixture of APGs.2. A method as recited in wherein said process stream mixture is present in a whole stillage process stream claim 1 , a thin stillage process stream claim 1 , in an evaporator claim 1 , in a syrup stream claim 1 , or in feed or make up water to a corn to ethanol fermentation process.4. A method as recited in wherein le is chosen from the group consisting of C-Calkyl groups claim 3 , C-Calkenyl groups and C-Calkynyl groups wherein said groups may be substituted or non-substituted and are straight or branched or contain aryl groups.5. A method as recited in wherein said APG is a member or members selected from the group consisting of caprylyl glucoside claim 3 , decyl glucoside claim 3 , undecyl glucoside claim 3 , lauryl glucoside claim 3 , myristyl glucoside claim 3 , hexadecyl d-glucoside claim 3 , octadecyl d-glucoside claim 3 , arachidyl glucoside claim 3 , caprylyl/capryl glucoside claim 3 , Calkyl glucoside claim 3 , Calkyl glucoside claim 3 , Calkyl glucoside claim 3 , Calkyl glucoside claim 3 , cetaryl glucoside claim 3 , Calkyl glucoside claim 3 , coco glucoside claim 3 , isostearyl glucoside claim 3 , octyldodecyl glucoside.6. A method as recited in wherein about 1 to about 5 claim 1 ,000 ppm of said oil separation aid are added to said process stream based upon one million parts of said process stream mixture.7. A method as recited in wherein about 100 to about 2500 ppm of said oil separation aid are added.8. A method as recited in ...

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Номер записи: 30
17-02-2022 дата публикации

PARTICULATE ADDITIVES FOR IMPROVED BIO-OIL RECOVERY

Номер: US20220049184A1
Автор: GRANDY Christopher A., Moore Kevin, ROACH Raymond P., Shepperd Paul W.
Принадлежит:

A method for recovering bio-oil from an emulsified bio-oil process stream, by adding a chemical additive system to the emulsified bio-oil process stream, wherein the chemical additive system comprises at least one surfactant and at least one hydrophobic particulate not based on silica. Bio-oil recovered from the method. A bio-oil recovery system, including a supply of emulsified bio-oil, a supply of chemical additive, wherein the chemical additive comprises at least one surfactant and at least one hydrophobic particulate not based on silica, a treatment unit for combining the chemical additive system with the emulsified bio-oil, and a centrifuge system for dewatering the treated emulsion and producing a concentrated bio-oil. 1. A method for recovering bio-oil from an emulsified bio-oil process stream , including the steps of:adding a chemical additive system to the emulsified bio-oil process stream in an amount of 20 to 2000 ppmv (mg/L) based on the weight of the chemical additive system and the volume of the emulsified bio-oil process stream, wherein the chemical additive system comprises at least one surfactant and at least one hydrophobic particulate chosen from the group consisting of fatty acids, salts of fatty acids, high melting point synthetic or semi-synthetic waxes (melting point greater than 110° C.), fatty acid coated calcium carbonate and organoclays;wherein the hydrophobic particulate comprises from 1-65% of the chemical additive system; andrecovering bio-oil.2. The method of claim 1 , wherein the emulsified bio-oil process stream is a process stream of an ethanol production process.3. The method of claim 2 , wherein the emulsified bio-oil process stream is chosen from the group consisting of whole stillage claim 2 , thin stillage claim 2 , concentrated thin stillage claim 2 , and syrup.4. The method of claim 1 , wherein fatty acids or salts of fatty acids comprise between 10-100% by weight of the hydrophobic particulate.5. The method of claim 1 , ...

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Номер записи: 31
04-02-2021 дата публикации

METHODS OF REFINING A GRAIN OIL COMPOSITION, AND RELATED COMPOSITIONS AND METHODS OF USING

Номер: US20210032564A1
Автор: Bly Steven T., Flittie Brett A., McCurdy Alex T., Milbrandt Jacob A., Sarks Cory J., Urban Shannon S.
Принадлежит:

The present disclosure relates methods and systems for refining grain oil compositions using water, and related compositions produced therefrom. The present disclosure also relates to methods of using grain oil derived from a fermentation product in an anti-foam composition and/or feedstock to make diesel. 1. A method of refining a grain oil composition feedstock to provide an anti-foam composition , wherein the method comprises:combining the grain oil composition feedstock with water to form an oil-water mixture;exposing the oil-water mixture to a temperature for a time period at least until the oil-water mixture forms at least an oil phase and an emulsion phase;separating at least a portion of the oil phase from the emulsion phase; anddehydrating the emulsion phase to form the anti-foam composition.2. The method of claim 1 , wherein grain oil in the grain oil composition feedstock has been exposed to one or more enzymes in a biorefinery to generate one or more fatty acid alkyl esters.3. The method of claim 2 , wherein the one or more enzymes are chosen from lipase claim 2 , esterase claim 2 , and combinations thereof claim 2 , wherein the one or more enzymes are endogenous enzymes and/or exogenous enzymes claim 2 , and wherein the one or more fatty acid alkyl esters comprise one or more fatty acid ethyl esters.4. The method of claim 1 , wherein the grain oil composition feedstock is derived from a stillage composition chosen from whole stillage claim 1 , thin stillage claim 1 , wet cake claim 1 , syrup claim 1 , and combinations thereof.5. The method of claim 4 , wherein the stillage composition is derived from a fermentation product derived from a method comprising fermenting a grain mash composition to form a beer comprising a biochemical claim 4 , wherein the grain mash composition comprises grain solids claim 4 , grain oil and sugar claim 4 , wherein fermenting comprises fermenting the grain mash in the presence of one or more enzymes to generate one or more ...

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Номер записи: 32
05-02-2015 дата публикации

METHOD AND SYSTEM FOR REDUCING FREE FATTY ACID CONTENT OF A FEEDSTOCK

Номер: US20150037852A1
Автор: Hosseini Majid, Ju Lu-Kwang
Принадлежит:

A method for reducing the free fatty acid content of a feedstock includes the steps of providing a free-fatty-acid-containing feedstock, treating the free-fatty-acid-containing feedstock to reduce the free fatty acid content thereof, where the step of treating includes combining at least one of an algae and a coagulant to the free-fatty-acid-containing feedstock, and producing a product from the treated feedstock. 1. A method for reducing the free fatty acid content of a feedstock comprising the steps ofcombining algae with a medium to form an algae-containing medium,combining a free-fatty-acid-containing feedstock with the algae-containing medium to form an algae treatment feedstock,allowing the algae to reduce the free-fatty-acid content of the algae treatment feedstock, and, after said step of allowing,producing a product from the algae treatment feedstock.2. The method of claim 1 , wherein the medium comprises water claim 1 , the method further comprising the steps ofagitating the algae treatment feedstock to form an upper oil phase, a lower aqueous phase, and a middle phase andcollecting said upper oil phase.3. The method of claim 2 , wherein the collected upper oil phase has a lower free fatty acid content than the free-fatty-acid-containing feedstock.4. The method of claim 2 , wherein the collected upper oil phase has a lower acid value than the free-fatty-acid-containing feedstock.5. The method of claim 1 , wherein the medium comprises water and waste cooking oil.6. The method of claim 1 , wherein the medium comprises a mineral medium.7. The method of claim 6 , wherein the mineral medium comprises one or more of the following components: glucose claim 6 , MgCO claim 6 , NHCl claim 6 , KHPO claim 6 , nitrilotriacetic acid claim 6 , peptone claim 6 , MgSO.7HO claim 6 , yeast extract claim 6 , CaCO claim 6 , NaEDTA claim 6 , FeCl.6HO claim 6 , HBO claim 6 , thiamine claim 6 , MnCl.4HO claim 6 , ZnSO.7HO claim 6 , CoCl claim 6 , 6HO claim 6 , NaMoO.2HO and ...

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Номер записи: 33
14-02-2019 дата публикации

SYSTEMS AND METHODS FOR EXTRACTING OIL FROM PLANT MATERIAL

Номер: US20190048286A1
Автор: Bly Steven T., Calar Kristin M., Flittie Brett A., Keeler John C., Oster Benjamin G., Rindsig Matthew J., Schnell Blake A.
Принадлежит:

Disclosed are methods and systems for recovering oil from processed plant materials and by-products formed during a milling process used for producing ethanol. 1. A method of extracting oil from a processed plant material , wherein the method comprises: i) processed plant material; and', 'ii) an aqueous carrier, wherein the slurry comprises a total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the slurry;, '(a) providing a slurry comprising(b) applying pressure to the slurry to move oil from the process plant material to the aqueous carrier;(c) separating the slurry into a liquid fraction and a solid fraction; and(c) recovering or separating oil from the liquid fraction.2. The method of claim 1 , wherein applying pressure and separating the slurry comprises mechanically pressing the processed plant material against a screen to separate the slurry into a liquid fraction and a solid fraction.3. The method of claim 1 , wherein applying pressure and separating the slurry comprises mechanically passing the processed plant material through a screw press to separate the slurry into a liquid fraction and a solid fraction.4. The method of claim 1 , wherein the average particle size of the slurry is reduced prior to applying pressure.5. The method of claim 1 , further comprising applying a pressure above ambient pressure to the slurry to generate a second slurry claim 1 , wherein the slurry comprises a first slurry.6. The method of claim 5 , wherein the applying pressure comprises applying pressure from about 200-600 psi.7. The method of claim 1 , further comprising heating the slurry above ambient temperature to generate a second slurry claim 1 , wherein the slurry comprises a first slurry.8. The method of claim 7 , wherein heating comprises heating from about 21° C. (70° F.) to about 100° C. (212° F.).9. The method of claim 1 , wherein the aqueous carrier comprises process water claim 1 , thin stillage claim 1 , ethanol claim 1 , or ...

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Номер записи: 34
01-03-2018 дата публикации

COMPLETE SAPONIFICATION AND ACIDULATION OF NATURAL OIL PROCESSING BYPRODUCTS AND TREATMENT OF REACTION PRODUCTS

Номер: US20180057771A1
Автор: BLANCHARD Cory, CHECK Christopher Thomas, KILLINGSWORTH Nathan, LONG Ryan, SUTTERLIN William R.
Принадлежит:

The present invention generally provides a process for treating a soapstock. The present invention more particularly provides systems and methods for treating a soapstock to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters. The present invention more particularly provides systems and methods for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to salts of fatty acids (soaps) and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters, wherein the soapstock comprises soaps and saponifiable lipids, e.g. glycerides and/or phospholipids, and the generating of free fatty acids and/or fatty acid is achieved without the use of a mineral acid. 1. A method for generating free fatty acids from a mixed lipid feedstock , the method comprising:providing the mixed lipid feedstock;combining the mixed lipid feedstock with a base to form a mixture;allowing the mixture to react in a reaction vessel;introducing carbon dioxide into the reacted mixture in the reaction vessel to form a first carbonic acid within the reaction vessel;mixing the first carbonic acid and the reacted mixture within the reaction vessel; allowing the first carbonic acid and reacted mixture to settle within the reaction vessel; anddraining a first aqueous layer from the reaction vessel.2. The method of claim 1 , further comprising filtering the first aqueous layer using a size exclusion filtration system claim 1 ,wherein optionally the filtering step further comprises a filter having a membrane having a plurality of pores, said pores allowing soaps and phosphates to pass through said membrane of said filter,and optionally the filtering step further comprises a filter having a membrane, said membrane allowing particles having a molecular weight less than the molecular weight of a salt,and optionally the filtering step further comprises ...

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Номер записи: 35
25-03-2021 дата публикации

Process For Isolating A Protein Composition And A Fat Composition From Mechanically Deboned Poultry

Номер: US20210084925A1
Автор: Fielding William R., Kelleher Stephen D., Saunders Wayne S.
Принадлежит: Proteus Industries, Inc

A protein fraction and an oxidation stable fat fraction are recovered from poultry containing fat, bone and protein. The poultry is comminuted, mixed with a food grade acid at pH 3.6 to 4.4 to form a liquid protein fraction and a solid fat fraction. The liquid fraction is mixed with a food grade alkali to precipitate the protein. 1) The process for recovering , from mechanically deboned poultry containing fat , bone and protein , and initial levels of calcium and sodium , and having a color , a protein composition with reduced levels of calcium and sodium as compared to the initial levels of calcium and sodium , wherein the deboned poultry has 65-85% by weight lean , wherein the protein composition retains most or all of the color of the mechanically deboned poultry , the process comprising the steps of:a) comminuting the poultry in water,b) adding a food grade acid to the comminuted poultry to effect a pH of 3.6 to 4.4 thereby to solubilize the protein, wherein calcium remains insoluble,c) after addition of the food grade acid in step b), separating solid fat from the solubilized protein, wherein calcium is separated together with the solid fat from the solubilized protein,d) adding a food grade alkali to the fat to neutralize acid in the fat and to the solubilized protein to neutralize acid in the protein and to precipitate the protein, wherein sodium remains soluble, ande) recovering from the precipitate the protein composition with reduced levels of calcium and sodium as compared to the initial levels of calcium and sodium, wherein the protein composition has 14% or greater by weight protein and less than 10% by weight fat, wherein the less than 10% by weight fat is stabilized against oxidation; and wherein the protein composition retains most or all of the color of the mechanically deboned poultry.2) The process of wherein said pH in step b is from 3.6 to 3.8.3) The process of wherein step a and step b are performed simultaneously.4) The process of wherein step ...

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Номер записи: 36
30-03-2017 дата публикации

METHOD FOR RECOVERING CRUDE TALL OIL

Номер: US20170088794A1
Автор: Finer Tiia, Timonen Olli
Принадлежит:

The present invention relates to a method for recovering crude tall oil from a soap which method comprises the steps of: determining a correlation between the crude tall oil content and the water content of the soap, determining an amount of acid and water needed in order to separate an optimal amount of crude tall oil from the soap dependent on the crude tall oil content of the soap, measuring the water content of the soap, adding the optimal amount of acid and water to the soap, mixing the added acid and water with the soap whereby an acidulated soap is formed and the crude tall oil is separated and recovering the separated crude tall oil from the acidulated soap. 1. A method for recovering crude tall oil from a soap comprising the steps of:(a) determining a correlation between the crude tall oil content and the water content of the soap,(b) determining an amount of acid and water needed in order to separate an optimal amount of crude tall oil from the soap dependent on the crude tall oil content of the soap,(c) measuring the water content of the soap,(d) adding the optimal amount of acid and water to the soap,(e) mixing the added acid and water with the soap whereby acidulated soap is formed and crude tall oil is separated, and(f) recovering the separated crude tall oil from the acidulated soap.2. The method according to wherein the water content is measured on-line on a soap flow.3. The method according to claim 1 , wherein the pH of the spent acid fraction of the acidulated soap after addition of the acid and water in step (e) is less than 5.4. The method according to claim 1 , wherein the temperature of the acidulated soap in step (e) is between 80 to 102° C.5. The method according to claim 1 , wherein step (e) is followed by a retention time before entering the recovery step (f).6. The method according to claim 1 , wherein the acid added in step (d) is a strong acid.7. The method according to claim 6 , wherein the acid added in step (d) is sulfuric acid which ...

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Номер записи: 37
28-03-2019 дата публикации

Methods and Devices for Producing Biodiesel and Products Obtained Therefrom

Номер: US20190093048A1
Автор: Albin Bradley N., Downey Jared A., Ellens Cody J., Slade David A., Winkel Derek J.
Принадлежит: Renewable Energy Group, Inc.

Methods and devices for economically producing a purified biodiesel product from feedstocks. Some embodiments of the methods comprise using at least one of a crude feedstock pretreatment process and a free fatty acid refining process prior to transesterification and the formation of crude biodiesel and glycerin. The crude biodiesel is then subjected to at least one biodiesel refining process which, in conjunction with feedstock pretreatment and free fatty acid refining produces a purified biodiesel product that meets multiple commercial specifications. A wide variety of feedstocks may be used to make biodiesel that otherwise would not meet the same commercial specifications, including corn oil, used cooking oil, poultry fats, fatty acid distillates, pennycress oil, and algal oils. The combination of feedstock refining and biodiesel refining processes is necessary to reduce problems associated with feedstocks having waxes, high free fatty acid levels, unacceptable color, high unsaponifiables levels, and high sulfur levels. 1. A method for producing a purified biodiesel from a first feedstock comprising:a. removing free fatty acids from said first feedstock to produce a refined feedstock and free fatty acids;b. transesterifying said refined feedstock to produce a first crude biodiesel;c. distilling said first crude biodiesel to produce the purified biodiesel and a distillation bottoms; andd. converting the free fatty acids to a second feedstock using a free fatty acid conversion process.2. The method of claim 1 , further comprising the step of using a transesterification process to convert said second feedstock to a second crude biodiesel.3. The method of claim 2 , further comprising the step of combining the second crude biodiesel with the first crude biodiesel and refining the first crude biodiesel and second crude biodiesel together in step (c).4. The method of claim 1 , further comprising the step of combining the second feedstock with the refined feedstock and ...

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Номер записи: 38
20-04-2017 дата публикации

Products Produced From Distillers Corn Oil

Номер: US20170107452A1
Автор: Dasari Mohan Prasad, Dieker Kurt A., Gallop Charles C., Knox Kidron Joel, Ravi Shashank, Warren Hugh Tallant
Принадлежит:

Products produced from distillers corn oil include once refined corn oil product, food grade corn oil product, and free fatty acid product which may be used in a variety of applications. The products have varying specifications for free fatty acid content and moisture content. The applications include food, feed, additives, and manufacture of industrial products. 1. A refined corn oil product produced from distillers corn oil , the refined corn oil product comprising:a free fatty acid content of less than about 1% by weight; anda moisture content ranging from about 0.09% to about 0.35% by weight.2. The product of claim 1 , further comprising an oxidative stability value of greater than 5.3. The product of claim 1 , wherein the refined corn oil product has a tocopherol content less than about 1 mg/g.4. The product of claim 1 , wherein the refined corn oil product has a beta-carotene content greater than about 2 μg/g.5. The product of claim 1 , wherein the refined corn oil product has transfat content of less than 1% by weight.6. A food grade corn oil product produced from distillers corn oil claim 1 , the food grade corn oil product comprising:a free fatty acid content less than 0.05% by weight percent; anda moisture content ranging from about 0.1 to about 0.5% by weight.7. The product of claim 6 , wherein the food grade corn oil product has a color ranging from 3.0 to 3.5R.8. The product of claim 6 , wherein the food grade corn oil product has an acid value less than 0.1% by weight.9. The product of claim 6 , wherein the food grade corn oil product has a peroxide value of less than 0.5 meg/kg.10. The product of claim 6 , wherein the food grade corn oil product has a transfat content of less than 1.0% by weight.11. A free fatty acid product produced from distillers corn oil claim 6 , the free fatty acid product comprising: 'and a moisture content less than about 1% by weight.', 'a free fatty acid content of greater than 50% by weight; and'}12. The product of claim 11 ...

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Номер записи: 39
28-04-2016 дата публикации

Oil Extraction Method And Composition For Use In The Method

Номер: US20160115425A1
Автор: Blankenburg Dean, Cumming Scott, Vassh John, Zouras Frank
Принадлежит:

A demulsifying composition is disclosed for aiding extraction of an emulsified oil from an oil and water emulsion. The composition includes one or more non-ionic surfactants having a HLB value of 6 or greater, wherein the non-ionic surfactant is selected from the group consisting of alkoxylated plant oils, alkoxylated plant fats, alkoxylated animal oils, alkoxylated animal fats, alkyl polyglucosides, alkoxylated glycerols, and mixtures thereof. The composition may include silicon containing particles. A method for recovering oil from a corn to ethanol process is also disclosed. The method includes the steps of adding the composition to a process stream of the corn to ethanol process, and extracting oil from the process stream. 1. A method for recovering oil from a corn to ethanol process , the method comprising:adding a composition to a process stream of the corn to ethanol process,wherein the composition comprises a non-ionic surfactant selected from the group consisting of alkoxylated plant oils, alkoxylated plant fats, alkoxylated animal oils, alkoxylated animal fats, alkyl polyglucosides, alkoxylated glycerols, and mixtures thereof.2. The method of wherein:the alkoxylated plant oil is selected from the group consisting of ethoxylated castor oil, ethoxylated soybean oil, ethoxylated palm kernel oil, ethoxylated almond oil, ethoxylated corn oil, ethoxylated canola oil, ethoxylated rapeseed oil, and ethoxylated coconut oil.3. The method of wherein:the alkoxylated plant oil is ethoxylated castor oil.4. The method of wherein:the composition further comprises an alkylene glycol ester of a fatty acid moiety present in a plant oil.5. The method of wherein:the alkoxylated plant oil is ethoxylated castor oil, andthe composition further comprises an alkylene glycol ester of a fatty acid moiety present in a plant oil, andthe composition further comprises silicon containing particles.6. The method of wherein:the non-ionic surfactant comprises an alkoxylated glycerol.7. The ...

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Номер записи: 40
24-07-2014 дата публикации

Compositions and methods for biofermentation of oil-containing feedstocks

Номер: US20140206048A1
Автор: Daniel J. Monticello, Paul Campbell, Ryan Black
Принадлежит: Glycos Biotechnologies Inc

The present invention provides compositions and methods for the use of oil-containing materials as feedstocks for the production the bioproducts by biofermentation. In one preferred embodiment, surfactants are not used in compositions and the methods of the invention. In one preferred embodiment the oil-containing feedstocks are the by-products of other industrial processes including microbial, plant and animal oil processing.

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Номер записи: 41
21-05-2015 дата публикации

STEAMCRACKING BIO-NAPHTHA PRODUCED FROM COMPLEX MIXTURES OF NATURAL OCCURRING FATS AND OILS

Номер: US20150141715A1
Автор: Van Gyseghem Nicolas, Vermeiren Walter
Принадлежит:

A process for making a bio-naphtha and optionally bio-propane from a complex mixture of natural occurring fats & oils, wherein 116-. (canceled)17. A process comprising:(a) making a bio-naphtha and optionally bio-propane from a complex mixture of natural occurring raw fats and oils, wherein the raw fats and oils are subjected to a refining pretreatment including a degumming and a bleaching for removing non-triglyceride and non-fatty acid components, thereby obtaining refined fats and oils; (c1) the refined fats and oils still containing free fatty acids or the physically refined triglycerides are sent to a hydrodeoxygenation section and converted into bio-naphtha and bio-propane; or', '(c2) the mixed fatty acids are sent to a hydrodeoxygenation section and converted into bio-naphtha or are sent to a decarboxylation section and converted into bio-naphtha; or', '(b2) the refined fats and oils are saponificated to recover soaps and glycerol or soaps are obtained during a chemical refining step of the raw fats and oils by a neutralisation step; or soaps are obtained via neutralisation of fatty acids obtained by steam splitting/hydrolysis of the refined fats and oils producing fatty acids and glycerol and the soaps are sent to a decarboxylation section and converted into bio-naphtha; and, '(b1) wherein the refined fats and oils are physically refined by vacuum distillation or steam distillation to recover mixed fatty acids as overhead product and triglycerides as bottom product; and wherein eitherwherein the complex mixture of natural occurring raw fats and oils comprises vegetable oils, animal fats, or mixtures thereof.18. The process of claim 17 , wherein the complex mixture of natural occurring raw fats and oils comprises inedible oils.19. The process of claim 17 , wherein the complex mixture of natural occurring raw fats and oils comprises highly saturated oils.20. The process of claim 17 , wherein the complex mixture of natural occurring raw fats and oils comprises ...

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Номер записи: 42
17-05-2018 дата публикации

Enhanced Separation of Corn Oil from the Ethanol Manufacturing Process

Номер: US20180134985A1
Автор: Eric Hakmiller
Принадлежит: Lincolnway Energy LLC

An ethanol production process and system for recovering high value oil products. The invention includes adding a heated lipid (oil) stream to a thin stillage stream to break the water/oil emulsion and free bound oil then recovering the oil. The lipid stream may be heated by use of existing process steam or other process energy source, or may be heated by the introduction of energy from an external source. The process uses oil as the heat transfer mechanism to increase both the volume and quality of the oil recovered.

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Номер записи: 43
07-08-2014 дата публикации

APPARATUS FOR TREATING FOOD WASTE AND EXTRACTING BIO OIL

Номер: US20140220646A1
Автор: Lim Won Im
Принадлежит: G&P BIOTECH CO., LTD.

An apparatus for treating food waste and extracting bio oil includes: a fermentation dryer which ferments and decomposes food waste for 24 hours to reduce moisture contained in the food waste to 40 to 50%, a crusher which crushes the food waste into small particles, a distillation tank which heats the crushed food waste at low pressure and temperature so that oil is gasified by means of low temperature thermal decomposition to form oil gas, a distillation tower in which the oil gas is cooled to be liquefied and separated into moisture (carbon liquid fertilizer) and oil, a vacuum storage tank which collects the separated oil, and a centrifugal separator which rectifies the oil. The apparatus extracts a carbon liquid fertilizer, bio oils, and activated carbon while treating organic substances such as food waste and residual product compost. 1. An apparatus for treating food waste and extracting bio oil , comprising:{'b': 40', '50, 'a fermentation dryer equipped with a mixing chamber into which a bulking agent and microorganisms are preliminarily introduced and in which a mixing vane which slowly mixes food waste is installed, an oxygen supplying apparatus, and an air cleaning apparatus, wherein the fermentation dryer ferments and decomposes food waste for 24 hours while mixing the food waste, thereby reducing moisture contained in the food waste to % to %, resulting in a decrease in the weight of the food waste;'}a crusher which crushes the food waste and organic substances which are deprived of a portion of moisture in the fermentation dryer into small particles and supplies the crushed food waste and organic substances to a distillation tank using a screw conveyer;the distillation tank including a heating chamber under which a burner is installed, and a tank equipped with an agitator which rotates by driving force of a motor and agitates organic particles is installed and a discharge opening formed at an upper end of the tank and connected to a distillation tower, ...

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Номер записи: 44
08-09-2022 дата публикации

MODIFIED LECITHIN FOR ASPHALT APPLICATIONS

Номер: US20220281900A1
Автор: KURTH Todd L., STAUDUHAR Suzanne, TABATABAEE Hassan Ali
Принадлежит: Cargill, Incorporated

Embodiments of the present invention provide a method, comprising obtaining a lecithin-containing material, in some aspects derived from a crude refining stream, comprising 20-80 wt % acetone insoluble matter, 1-30 wt % free fatty acid, and less than 10 wt % water, adding a fatty acid or carboxylic source to the lecithin-containing material to obtain a lecithin fatty acid blend or lecithin carboxylic acid blend and incorporating the blend into asphalt or oil field applications. 1. A method , comprising:(a) obtaining a lecithin-containing material, comprising 20-80 wt % acetone insoluble matter, 1-30 wt % free fatty acid, and less than 10 wt % water;(b) adding a fatty acid source to the lecithin-containing material to obtain a lecithin fatty acid blend; and(c) incorporating the lecithin fatty acid blend into asphalt or oil field applications.2. The method of claim 1 , wherein the lecithin-containing material comprises less than 5 wt % water.3. The method of claim 1 , wherein the lecithin-containing material comprises less than 2 wt % water.4. The method of claim 1 , wherein the lecithin-containing material comprises less than 1 wt % water.5. The method of claim 1 , wherein the lecithin-containing material comprises 10-20 wt % free fatty acid.6. The method of claim 1 , wherein the lecithin fatty acid blend has a Brookfield Viscosity at 25° C. of about 100 to 15000 cP.7. The method of claim 1 , wherein the lecithin fatty acid blend has a Brookfield Viscosity at 25° C. of about 2000 to 12000 cP.8. The method of claim 1 , wherein the lecithin fatty acid blend has a Brookfield Viscosity at 25° C. of about 5000 to 9000 cP.9. The method of claim 1 , wherein the lecithin fatty acid blend has an acid value of 1 to 100 mg KOH/g.10. The method of claim 1 , wherein the lecithin fatty acid blend has an acid value of 50 to 90 mg KOH/g.11. The method of claim 1 , wherein the lecithin fatty acid blend has an acid value of 10 to 70 mg KOH/g.12. The method of claim 1 , wherein the ...

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Номер записи: 45
08-09-2022 дата публикации

SYSTEMS AND METHODS FOR EXTRACTING OIL FROM PLANT MATERIAL

Номер: US20220282180A1
Автор: Bly Steven T., Calar Kristin M., Flittie Brett A., Keeler John C., Oster Benjamin G., Rindsig Matthew J., Schnell Blake A.
Принадлежит:

Disclosed are methods and systems for recovering oil from processed plant materials and by-products formed during a milling process used for producing ethanol. 1. A method of extracting oil from a biorefinery process stream , wherein the method comprises:diluting a biorefinery process stream to provide a diluted biorefinery process stream having a total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the diluted biorefinery process stream, wherein the biorefinery process stream comprises at least grain oil, grain fiber, and water; andapplying pressure to the diluted biorefinery process stream to separate the diluted biorefinery process stream into at least one liquid fraction and at least one solids fraction and to transfer oil into the at least one liquid fraction.2. The method of claim 1 , wherein applying pressure to the diluted biorefinery process stream comprises passing the diluted biorefinery process stream through a screw press to separate the diluted biorefinery process stream into a liquid fraction and a solids fraction.3. The method of claim 2 , wherein the biorefinery process stream is a first biorefinery process stream claim 2 , and wherein diluting comprises adding at least a portion of a second biorefinery process stream to the first biorefinery process stream to provide the diluted biorefinery process stream.4. The method of claim 3 , wherein the second biorefinery process stream is chosen from thin stillage claim 3 , syrup claim 3 , alcohol claim 3 , process water claim 3 , and combinations thereof.5. The method of claim 3 , wherein the second biorefinery process stream comprises thin stillage.6. The method of claim 2 , wherein the total solids content is in a range from 15 to 25% (wt/wt) based on the total weight of the diluted biorefinery process stream.7. The method of claim 2 , wherein the biorefinery process stream is a first solids fraction that is formed by separating an upstream biorefinery process ...

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Номер записи: 46
26-05-2016 дата публикации

Component Recovery from Metal Quenching Bath or Spray

Номер: US20160145120A1
Автор: Burke John Michael, Cross Alan Edward
Принадлежит:

The present invention provides processes for quenching metals which are more energy efficient and less expensive than the current metal quenching processes. The quenching processes utilize a water-soluble aqueous quenching fluid and hydraulic equipment which uses water-insoluble, fire-resistant hydraulic fluid for an immersion or spray application. During quenching of metal in a quenching immersion bath or by quenching spray process, the aqueous quenching fluid becomes contaminated with the hydraulic fluid and no longer meets its quenching specifications. The process and system described herein involves removing and heating the contaminated quenching fluid to enable separation of the quenching fluid from the contaminants and recycling of the used quenching fluid back into a functional quenching bath or functional quenching spray. The separated hydraulic fluid is then recycled as fuel, e.g., biofuel or waste fuel, thereby reducing the amounts of waste product associated with quenching metals. 1. A process for increasing the efficiency of a metal quenching process , said process comprising:(a)(1) providing a metal quenching bath tank comprising a used metal aqueous quenching fluid containing contamination with a water insoluble, fire resistant hydraulic fluid, wherein the bath is no longer within its quenching specifications; or(a)(2) collecting, in a collection tank in association with a quench barrel or quench ring, used metal aqueous quenching fluid after the fluid has been sprayed onto heated metal, wherein the collected used fluid is contaminated with a water insoluble, fire resistant hydraulic fluid, and wherein the collected fluid is no longer within its quenching specifications;(b) heating the bath tank (a)(1) or collection tank (a)(2) to a temperature of about 105 to 200° F. with agitation for less than 12 hours;(c) recovering the resulting uncontaminated aqueous quenching phase from the lower portion of the bath tank (a)(1) or collection tank (a)(2);(d) ...

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Номер записи: 47
10-06-2021 дата публикации

METHOD AND SYSTEM FOR REDUCING THE UNFERMENTABLE SOLIDS CONTENT IN A PROTEIN PORTION AT THE BACK END OF A CORN DRY MILLING PROCESS

Номер: US20210170419A1
Автор: Hora Michael, Jakel Neal, Kwik John
Принадлежит:

A method and system for reducing the unfermentable solids content in a protein portion, via a counter current wash, at the back end of a corn dry milling process for making alcohol is disclosed. The method can include separating the whole stillage byproduct into an insoluble solids portion and a stillage (centrate) portion, which includes protein. Thereafter, the stillage portion can be separated into a water soluble solids portion and a protein portion. The protein portion may be mixed with clean water to wash and dilute the protein portion. The diluted protein portion may be dewatered to form a dewatered protein portion and a centrate. A portion of the centrate may be used as a protein counter current wash when the protein portion is being separated from the stillage portion. The protein counter current wash reduces the amount of unfermentable solids in the protein portion and the centrate. 1. A method for reducing an unfermentable solids content in a protein portion at a back end of a starch-containing grain dry milling process for making biofuel and/or a biochemical , the method comprising:separating a whole stillage byproduct into an insoluble solids portion, which includes fiber, and a stillage portion, which includes protein;adding a counter current wash that is received from a later step in the method to the stillage portion and separating the stillage portion into a water soluble solids portion and a protein portion, wherein the addition of the counter current wash facilitates separation of a larger concentration of unfermentable solids into the water soluble solids portion;thereafter, separately adding a first wash water to the separated protein portion followed by dewatering the protein portion to separately provide a centrate portion, which includes first wash water, and a dewatered protein portion that defines a high protein grain meal that includes at least 40 wt % protein on a dry basis, wherein at least a portion of the centrate portion including the ...

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Номер записи: 48
10-06-2021 дата публикации

METHOD AND SYSTEM FOR REDUCING THE UNFERMENTABLE SOLIDS CONTENT IN A PROTEIN PORTION AT THE BACK END OF A CORN DRY MILLING PROCESS

Номер: US20210170420A1
Автор: Hora Michael, Jakel Neal, Kwik John
Принадлежит:

A method and system for reducing the unfermentable solids content in a protein portion, via a counter current wash, at the back end of a corn dry milling process for making alcohol is disclosed. The method can include separating the whole stillage byproduct into an insoluble solids portion and a stillage (centrate) portion, which includes protein. Thereafter, the stillage portion can be separated into a water soluble solids portion and a protein portion. The protein portion may be mixed with clean water to wash and dilute the protein portion. The diluted protein portion may be dewatered to form a dewatered protein portion and a centrate. A portion of the centrate may be used as a protein counter current wash when the protein portion is being separated from the stillage portion. The protein counter current wash reduces the amount of unfermentable solids in the protein portion and the centrate. 1. A system for reducing an unfermentable solids content in a protein portion at a back end of a starch-containing grain dry milling process for making biofuel and/or a biochemical , the system comprising:a first apparatus that receives a whole stillage byproduct produced via the starch-containing grain dry milling process, wherein the first apparatus separates the whole stillage byproduct into an insoluble solids portion, which includes fiber, and a stillage portion, which includes protein;a second apparatus that is situated after the first apparatus and prior to any evaporator, the second apparatus is configured to receive the stillage portion from the first apparatus and counter current wash water from a later apparatus in the system and to separate the stillage portion, via weights, into a water soluble solids portion and a protein portion, wherein the addition of the counter current wash water facilitates separation of a larger concentration of unfermentable solids into the water soluble solids portion; anda third apparatus that is situated after the second apparatus and ...

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Номер записи: 49
26-05-2016 дата публикации

Methods and Devices for Producing Biodiesel and Products Obtained Therefrom

Номер: US20160145536A1
Автор: Albin Bradley N, Downey Jared A, Ellens Cody J., Slade David A., Winkel Derek J
Принадлежит: Renewable Energy Group, Inc.

Methods and devices for economically producing a purified biodiesel product from feedstocks. Some embodiments of the methods comprise using at least one of a crude feedstock pretreatment process and a free fatty acid refining process prior to transesterification and the formation of crude biodiesel and glycerin. The crude biodiesel is then subjected to at least one biodiesel refining process which, in conjunction with feedstock pretreatment and free fatty acid refining produces a purified biodiesel product that meets multiple commercial specifications. A wide variety of feedstocks may be used to make biodiesel that otherwise would not meet the same commercial specifications, including corn oil, used cooking oil, poultry fats, fatty acid distillates, pennycress oil, and algal oils. The combination of feedstock refining and biodiesel refining processes is necessary to reduce problems associated with feedstocks having waxes, high free fatty acid levels, unacceptable color, high unsaponifiables levels, and high sulfur levels. 1. A method for producing a purified biodiesel from a feedstock comprising:a. removing free fatty acids from said feedstock in a free fatty acid stripping process to produce a first refined feedstock and a fatty acid distillate;b. transesterifying said refined feedstock to produce a first crude biodiesel; andc. distilling said first crude biodiesel to produce the purified biodiesel and a distillation bottoms.2. The method of claim 1 , further comprising the step of using an esterification process to convert said fatty acid distillate to a second crude biodiesel.3. The method of claim 1 , further comprising the step of using a glycerolysis process to convert said fatty acid distillate to a second refined feedstock.4. The method of claim 2 , further comprising the step of combining the second crude biodiesel with the first crude biodiesel and distilling the first crude biodiesel and second crude biodiesel together in step (c).5. The method of claim 3 ...

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Номер записи: 50
25-05-2017 дата публикации

METHOD OF SEPARATING OIL

Номер: US20170145341A1
Автор: Chen Xin, SUNGAIL CRAIG MICHAEL, Wang Min Ma
Принадлежит: CRODA, INC

A method of separating oil from a composition containing an oil and water emulsion, by adding a separation additive which is a fatty ester of alkoxylated glycerol, and performing at least one oil separation step. The method is particularly suitable for separating corn oil from stillage produced in a corn ethanol mill. 1. A method of separating oil from a composition comprising an oil and water emulsion , which comprises adding a separation additive to the composition and performing at least one oil separation step , wherein the separation additive comprises a fatty ester of alkoxylated glycerol.2. The method according to wherein the fatty ester is derived from fatty acids and/or derivatives thereof.3. The method according to wherein the fatty acids are selected from the group consisting of canola claim 2 , soya bean claim 2 , corn claim 2 , tall claim 2 , palm kernel claim 2 , coconut claim 2 , rapeseed claim 2 , high erucic rapeseed claim 2 , tallow fatty acids and mixtures thereof.4. The method according to wherein the fatty ester of alkoxylated glycerol comprises 1.0 to 2.0 ester bonds.5. The method according to wherein the fatty ester of alkoxylated glycerol comprises a polyalkylene oxide chain and wherein the average number of alkylene oxide groups in each polyalkylene oxide chain of the fatty ester of alkoxylated glycerol is 4 to 7.6. The method according to wherein the total number of alkylene oxide groups in the polyalkylene oxide chains of the fatty ester of alkoxylated glycerol is 12 to 30.7. The method according to wherein the separation additive is obtainable by alkoxylating a mixture of a triglyceride and glycerol.8. The method according to wherein the separation additive comprises greater than 75 wt % of fatty ester of alkoxylated glycerol.9. The method according to wherein the separation additive comprises 90 to 99.9 wt % of fatty ester of alkoxylated glycerol.10. The method according wherein the separation additive has a HLB value of 13 to 14.11. A ...

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Номер записи: 51
15-09-2022 дата публикации

METHOD AND SYSTEM FOR PRODUCING A HIGH PROTEIN MEAL FROM A WHOLE STILLAGE BYPRODUCT AND SYSTEM THEREFOR

Номер: US20220287332A1
Автор: Cannon Donald M., Franko Michael, Jakel Neal
Принадлежит:

A method and system for producing a high protein meal from a whole stillage byproduct produced in a grain dry-milling process for making ethanol, with optional back end milling options, is disclosed. In one embodiment, a method for producing a high protein meal from a whole stillage byproduct includes separating the whole stillage byproduct into an insoluble solids portion and a thin stillage/centrate portion, wherein at least one milling step can be applied to one or both of the insoluble solids portion and the whole stillage portion. Next, the centrate portion may be separated into a protein portion and a water-soluble solids portion. And then the protein portion can be dewatered and/or dried to define a high protein meal having at least 40 wt % protein on a dry basis. 1. A method for producing a high protein meal and an oil portion from a whole stillage byproduct comprising:separating a portion of the initial whole stillage byproduct into a first insoluble solids portion, including fiber and germ, and a first liquid portion;milling at least a portion of the first insoluble solids portion to further break up the fiber and germ and release oil and protein;combining the milled portion with the first liquid portion and recombining the combined milled portion and the first liquid portion with the initial whole stillage byproduct;after separating the portion of the initial whole stillage byproduct into the first insoluble solids portion and the first liquid portion, separating the remaining whole stillage byproduct, which includes at least a portion of the milled portion, into a second insoluble solids portion and a second liquid portion, which includes at least a portion of the oil and protein from the milling step;separating the second liquid portion into a protein portion and a water soluble solids portion, including oil, wherein the protein portion defines a high protein meal including at least 40 wt % protein on a dry basis; andseparating oil from the water ...

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Номер записи: 52
02-06-2016 дата публикации

PROCESS OF EXTRACTING OIL FROM THIN STILLAGE

Номер: US20160152922A1
Автор: Jump Joseph, Kreel Nathaniel
Принадлежит: NOVOZYMES A/S

The present invention relates to processes of recovering oil after liquefaction and/or from thin stillage and/or syrup/evaporated centrate from a fermentation product production process by adding a thermostable protease to the whole stillage, thin stillage and/or syrup. 1. A process of recovering oil , comprising(a) converting a starch-containing material into dextrins with an alpha-amylase; optionally recovering oil during and/or after step (a)(b) saccharifying the dextrins using a carbohydrate source generating enzyme to form a sugar;(c) fermenting the sugar in a fermentation medium into a fermentation product using a fermenting organism;(d) recovering the fermentation product to form a whole stillage;(e) separating the whole stillage into thin stillage and wet cake;(e′) optionally concentrating the thin stillage into syrup;(f) recovering oil from the thin stillage and/or optionally the syrup, wherein a protease having a thermostability value of more than 20% determined as Relative Activity at 80° C./70° C. is present and/or added during step (a) or steps (d)-(e′).2. The process of claim 1 , wherein the protease is present in and/or added in starch-containing material converting step (a).3. The process of claim 1 , wherein the temperature in step (a) is above the initial gelatinization temperature claim 1 , such as at a temperature between 80-90° C. claim 1 , such as around 85° C.4. The process of recovering oil of claim 1 , comprising(a) converting a starch-containing material into dextrins with an alpha-amylase at a temperature above the initial gelatinization temperature;(b) saccharifying the dextrins using a carbohydrate source generating enzyme to form a sugar;(c) fermenting the sugar in a fermentation medium into a fermentation product using a fermenting organism;(d) recovering the fermentation product to form a whole stillage;(e) separating the whole stillage into thin stillage and wet cake;(e′) optionally concentrating the thin stillage into syrup;(f) ...

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Номер записи: 53
02-06-2016 дата публикации

Processes for Recovering Oil from Fermentation Product Processes and Processes for Producing Fermentation Products

Номер: US20160152923A1
Автор: Clark Suzanne, Jump Joseph, Kreel Nathaniel, Matthews John
Принадлежит: NOVOZYMES A/S

The present invention relates to processes for recovering/extracting oil from fermentation product production processes based on starch-containing material, wherein an alpha-amylase, a high dosage of protease, and optionally a glucoamylase, are present and/or added in liquefaction. The invention also relates to processes for producing fermentation products and to enzyme compositions suitable for use in processes of the invention. 2. The process of claim 1 , wherein oil is recovered during and/or after liquefying the starch-containing material; from the whole stillage; from the thin stillage; or from the syrup.3Pyrococcus furiosusPyrococcus furiosusPyrococcus furiosusPyrococcus furiosusPyrococcus furiosus. The process of claim 1 , wherein 0.5-100 micro gram protease per gram DS claim 1 , such as 1-50 micro gram protease per gram DS claim 1 , such as 1-10 micro gram protease per gram DS claim 1 , such as 1.5-5 micro gram protease per gram DS claim 1 , such as around or more than 1.5 micro gram protease per gram DS are present and/or added in liquefaction step a).4Pyrococcus furiosus. The process of claim 1 , wherein the protease is one having at least 80% claim 1 , such as at least 85% claim 1 , such as at least 90% claim 1 , such as at least 95% claim 1 , such as at least 96% claim 1 , such as at least 97% claim 1 , such as at least 98% claim 1 , such as at least 99% identity to SEQ ID NO: 13 herein.5. The process of claim 1 , wherein no nitrogen-compound is present and/or added in steps a)-c) claim 1 , such as during saccharification step b) claim 1 , fermentation step c) claim 1 , or simultaneous saccharification and fermentation (SSF).6. A process for producing fermentation products from starch-containing material comprising the steps of: an alpha-amylase;', {'i': 'Pyrococcus furiosus', 'more than 2 micro gram protease per gram dry solids (DS);'}], 'a) liquefying the starch-containing material at a temperature above the initial gelatinization temperature usingb) ...

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Номер записи: 54
15-09-2022 дата публикации

Low iron hydrous phospholipid and method for separating low-iron hydrous phospholipids from soybean oil sediments

Номер: US20220289770A1
Автор: Ziqian Xu
Принадлежит: Inner Mongolia Bobeyman Technology Co Ltd, Shanghai Taiwei Pharmaceutical Corp Ltd

The invention belongs to the technical field of phospholipid processing, in particular to a low-iron hydrous phospholipid and a method for separating low-iron hydrous phospholipids from soybean oil sediments. The main components of low-iron water-containing phospholipids are phospholipids, oil and water; its water content is 70-80 g/100 g; on a dry basis, the content of acetone-insoluble matter is 92.5-95.5 g/100 g; in terms of acetone-insoluble matter, the iron content is less than or equal to 18 mg/kg. The low-iron water-containing phospholipid of the present invention is prepared from soybean oil by a hydration method, and is used to solve the defects of low acetone-insoluble content of the water-containing phospholipid, inability to remove iron ions and the industry's long-term dependence on the solvent method to prepare the powdered phospholipid; At the same time, the method solves the technical problem that “the preparation of powder phospholipid by hydration method cannot realize industrial production”.

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Номер записи: 55
07-06-2018 дата публикации

Process for the Conversion of Free Fatty Acids to Glycerol Esters and Production of Novel Catalyst systems

Номер: US20180154325A1
Автор: Glenn Richards, Michael Phillip Doyle
Принадлежит: AG Chem LLC

Animal and seed based triglycerides are oils used in cosmetics, pharmaceuticals, animal feed, energy generation, etc. These triglycerides or glycerol esters are a mixture of triglycerides and free fatty esters (FFA) along with unsaponifiables and gums (MIU). FFA may range from very low, 1% or less, to more than 40% in some rendered animal oils. Corn oil from the wet or dry process of ethanol production may have from 7 to 15% FFA. The varying amount of FFA presents numerous process issues for downstream users of these oils especially in the production of biodiesel, fatty acid methyl ester (FAME). FFA about 1 or 2% requires esterification as well as transesterification for the production of FAME. What is needed is a method to perform Glycerolysis. This disclosure describes an improved catalyst system as well as process equipment and operating conditions to allow economical commercialization of Glycerolysis.

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Номер записи: 56
22-09-2022 дата публикации

SELF-AGGREGATING HYDROUS PHOSPHOLIPID AND PREPARATION METHOD THEREOF

Номер: US20220298184A1
Автор: Xu Ziqian
Принадлежит:

The invention belongs to the technical field of phospholipid processing, in particular to a self-aggregating hydrous phospholipid and a preparation method thereof. The self-aggregating hydrous phospholipid, the main components of the self-aggregating hydrous phospholipid are phospholipids, oil and water, the water content is 70-80 g/100 g, and the acetone-insoluble content on a dry basis is 92.5-95.5 g/100 g. Preferably, the self-aggregating hydrous phospholipid is a brown translucent fluid. The present invention is used to overcome the defects of low acetone-insoluble content of the hydrous phospholipid prepared by the existing method and the long-term dependence of the industry on the solvent method to prepare powder phospholipid, and to solve the technical problem that the hydration method powder phospholipid cannot realize industrial production. 1. A self-aggregating hydrous phospholipid , wherein the main components of the self-aggregating hydrous phospholipid are phospholipids , oil and water , the water content is 70-80 g/100 g , and the acetone-insoluble content on a dry basis is 92.5-95.5 g/100 g.2. The self-aggregating hydrous phospholipid according to claim 1 , wherein the sensory index of the self-aggregating hydrous phospholipid is a brown translucent fluid.3. A preparation method of the self-aggregating hydrous phospholipid according to claim 1 , comprising the steps of: soaking soybean oil sediments in water to obtain saturated water-absorbing oil sediments claim 1 , and settling naturally to obtain final product.4. A preparation method of the self-aggregating hydrous phospholipid according to claim 2 , comprising the steps of: soaking soybean oil sediments in water to obtain saturated water-absorbing oil sediments claim 2 , and settling naturally to obtain final product.5. The preparation method according to claim 3 , wherein the mass ratio of described soybean oil sediment and water is 1:1-3.5.6. The preparation method according to claim 3 , wherein ...

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Номер записи: 57
18-06-2015 дата публикации

SEMI-CONTINUOUS ACIDULATION PROCESS

Номер: US20150166931A1
Автор: Bowles Robert E, Griffin Joseph H
Принадлежит: Arizona Chemical Company, LLC

A semi-continuous acidulation process for converting tall oil soap to crude tall oil is disclosed. Reactants are continuously mixed, and the product mixture is continuously transferred to a settling tank having a conical lower section and a capacity at least 25 times that of the mixer. Batches settle to give a solid phase comprising calcium sulfate, a clean spent acid phase, a dirty spent acid phase, and a crude tall oil phase. Each phase is removed sequentially through a port at or near the bottom of the settling tank. Compared with traditional batch acidulation, continuous mixing minimizes the corrosive environment and enables the use of less expensive materials for the settling tank. Sequential removal of four phases from one port allows calcium sulfate to be purged from every batch, permits clean separation of clean spent acid from dirty spent acid, and enables clean recovery of tall oil. Compared with processes that isolate product continuously, inherent difficulties in using centrifuges or continuous decanters to separate four phases are avoided. The process facilitates generation of clean alkaline brine and integration of new soap washing methods that enable improved conversion yields of CTO and better removal of calcium from the soap. 1. A semi-continuous acidulation process for converting tall oil soap to crude tall oil , comprising:(a) in one or more mixers, continuously mixing reactants comprising a tall oil soap, sulfuric acid, and water at a temperature within the range of 80° C. to 100° C.;(b) continuously transferring the reaction mixture(s) from step (a) to a settling tank having a conical lower section and a capacity at least 25 times that of the mixer;(c) allowing batches of the transferred reaction mixture to settle to give, in order of decreasing density, a solid phase comprising calcium sulfate, a clean spent acid phase, a dirty spent acid phase comprising lignin, and a crude tall oil phase; and(d) for each batch, removing each phase ...

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Номер записи: 58
30-05-2019 дата публикации

METHOD AND SYSTEM FOR REDUCING THE UNFERMENTABLE SOLIDS CONTENT IN A PROTEIN PORTION AT THE BACK END OF A CORN DRY MILLING PROCESS

Номер: US20190160470A1
Автор: Hora Michael, Jakel Neal, Kwik John
Принадлежит:

A method and system for reducing the unfermentable solids content in a protein portion, via a counter current wash, at the back end of a corn dry milling process for making alcohol is disclosed. The method can include separating the whole stillage byproduct into an insoluble solids portion and a stillage (centrate) portion, which includes protein. Thereafter, the stillage portion can be separated into a water soluble solids portion and a protein portion. The protein portion may be mixed with clean water to wash and dilute the protein portion. The diluted protein portion may be dewatered to form a dewatered protein portion and a centrate. A portion of the centrate may be used as a protein counter current wash when the protein portion is being separated from the stillage portion. The protein counter current wash reduces the amount of unfermentable solids in the protein portion and the centrate. 1. A method for reducing an unfermentable solids content in a protein portion at a back end of a starch-containing grain dry milling process for making biofuel and/or a biochemical , the method comprising:separating a whole stillage byproduct into an insoluble solids portion, which includes fiber, and a stillage portion, which includes protein;adding counter current wash water that is received from a later step in the method to the stillage portion and separating the stillage portion, via weights, into a water soluble solids portion and a protein portion, wherein the addition of the counter current wash water facilitates separation of a larger concentration of unfermentable solids into the water soluble solids portion; andrecovering the protein portion to define a high protein corn meal that includes at least 40 wt % protein on a dry basis.2. The method of further comprising adding wash water to the separated protein portion and claim 1 , thereafter claim 1 , dewatering the protein portion to provide a dewatered protein portion that defines the high protein corn meal and a ...

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Номер записи: 59
15-06-2017 дата публикации

Systems and methods to improve co-product recovery from grains and/or grain components used for biochemical and/or biofuel production using emulsion disrupting agents

Номер: US20170166834A1
Автор: Neal Jakel
Принадлежит: Fluid Quip Process Technologies LLC

Systems and methods are provided for improving co-product recovery, such as oil recovery, from grains and/or gain components used for biochemical and/or biofuel production, such as alcohol (e.g., ethanol) production, using surfactants, flocculants, and/or other emulsion-disrupting agents. At one or more points prior to or during emulsion formation, as well as after emulsion formation, surfactants and/or flocculants are added to the biochemical and/or biofuel production process to prevent emulsions or break those already formed to improve co-product recovery, such as oil recovery.

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Номер записи: 60
21-05-2020 дата публикации

SURFACTANT COMPOSITION

Номер: US20200157470A1
Автор: Chen Xin, Penfield Kevin Wade, Wang Min Ma
Принадлежит: CRODA, INC.

A process for making a surfactant composition is disclosed. In the process, a mixture comprising a sugar alcohol and fatty is formed. The mixture contains less than 5% by weight of water based on the total weight of the mixture. The mixture is reacted with an alkylene oxide to make a surfactant composition containing an alkoxylated sugar alcohol fatty acid ester and a polyalkylene glycol fatty acid ester. A surfactant composition and use of the surfactant composition to separate an oil phase and/or an aqueous phase from an emulsion is also disclosed. 1. A process for making a surfactant composition , comprising:a. forming a mixture comprising a sugar alcohol and a fatty acid, wherein the mixture comprises less than 5% water by weight based on the total weight of the mixture;b. reacting the mixture with an alkylene oxide to make a surfactant composition comprising an alkoxylated sugar alcohol fatty acid ester and a polyalkylene glycol fatty acid ester.2. A process according to wherein step b. occurs at a temperature in the range from 100° C. to 200° C.3. A process according to wherein step a. occurs at a temperature of at most 170° C.4. A process according to wherein the sugar alcohol is sorbitol.5. A process according to wherein the fatty acid has 6 to 24 carbon atoms.6. A process according to wherein the alkylene oxide is ethylene oxide.7. A process according to wherein the molar ratio of alkylene oxide to sugar alcohol which is reacted in step b. is from 40:1 to 80:1.8. A surfactant composition obtainable by a process according to .9. A surfactant composition comprising at least 40 wt % of alkoxylated sugar alcohol fatty acid ester and at least 10 wt % of polyalkylene glycol fatty acid ester claim 1 , wherein the polyalkylene glycol fatty acid ester comprises mono-ester and di-ester and wherein the weight ratio of mono-ester to di-ester of polyalkylene glycol fatty acid ester in the surfactant composition is from 3:1 to 1:3.10. A method of separating an oil phase ...

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Номер записи: 61
06-06-2019 дата публикации

Lipid composition and method for producing same

Номер: US20190169530A1
Автор: Junichi Okuyama, Koretaro TAKAHASHI, Takeya Yoshioka, Tomomi YAJIMA
Принадлежит: IHI Corp

The method of producing a lipid composition comprises an extraction treatment step to extract a lipid comprised in a hydrated raw material by using an extraction solvent comprising a polar solvent and a nonpolar solvent, and a separation treatment step to separate an extract solution obtained in the extraction treatment step into a polar solvent phase comprising a first lipid fraction and a nonpolar solvent phase comprising a second lipid fraction.

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Номер записи: 62
02-07-2015 дата публикации

Oil extraction aids in grain processing

Номер: US20150184112A1
Автор: III Paul W., Lewis Scott R., Shepperd
Принадлежит:

A method is provided for the use of a process additive system to improve the separation of oil from a process stream (whole stillage, thin stillage, or syrup) generated as a byproduct in grain to ethanol production. 1. A method for recovering oil from grain to ethanol production , the method comprising the addition of a process additive system to a process stream in a grain to ethanol production wherein the method comprises adding at least one chemical additive and at least one hydrophobic silica with particle size of at least 0.01 μm , wherein the total silica content of the process additive system is in an amount of from 3% to 50% by weight based on the weight of the process additive system and wherein the chemical additive comprises at least one functionalized polyol derived from a sorbitol , a sorbitan , isosorbide , sucrose , or glycerol.2. The method of wherein the functionalized polyol comprises at least one alkoxylated sorbitan alkylate.3. The method of wherein the chain length of the alkylate is from 6 to 24 carbons.4. The method of wherein the alkoxylated sorbitan alkylate has been alkoxylated with from 5 to 60 moles of alkyl oxide.5. The method of wherein the alkyl oxide is selected from ethylene oxide claim 4 , propylene oxide and mixtures thereof.6. The method of wherein the alkoxylated sorbitan alkylate is selected from the group consisting of an alkoxylated sorbitan monolaurate claim 2 , alkoxylated sorbitan monooleate claim 2 , alkoxylated sorbitan monopalmitate alkoxylated sorbitan monostearate and combination thereof.7. The method of wherein the alkoxylated sorbitan alkylate comprises an alkoxylated sorbitan monolaurate.8. The method of wherein the alkoxylated sorbitan alkylate comprises an alkoxylated sorbitan monooleate.9. The method of wherein the median particle size of silica is from about 0.01 to about 200 μm.10. The method of further comprising one or more modifiers to adjust the sedimentation stability claim 1 , rheological properties claim ...

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Номер записи: 63
28-05-2020 дата публикации

SYSTEMS AND METHODS FOR EXTRACTING OIL FROM PLANT MATERIAL

Номер: US20200165540A1
Автор: Bly Steven T., Calar Kristin M., Flittie Brett A., Keeler John C., Oster Benjamin G., Rindsig Matthew J., Schnell Blake A.
Принадлежит:

Disclosed are methods and systems for recovering oil from processed plant materials and by-products formed during a milling process used for producing ethanol. 120.-. (canceled)21. A method of extracting oil from a grain in a biochemical process , comprising:(a) grinding grain to reduce a size of the grain to form ground grain;(b) fermenting the ground grain to produce beer;(c) distilling the beer to recover a biochemical from the beer and to form whole stillage;(d) separating at least a portion of at least one of the beer, the whole stillage, or a combination thereof into a first liquid fraction and a first solids fraction;(e) applying pressure to the first solids fraction to separate the first solids fraction into a second liquid fraction and a second solids fraction and to transfer oil into the second liquid fraction; and(f) recovering or separating oil from the second liquid fraction.22. The method of claim 21 , wherein applying pressure comprises mechanically pressing the first solids fraction against a screen to separate the first solids fraction into the second liquid fraction and the second solids fraction.23. The method of claim 21 , wherein applying pressure comprises passing the first solids fraction through a screw press to separate the first solids fraction into the second liquid fraction and the second solids fraction.24. The method of claim 21 , wherein prior to applying pressure to the first solids fraction claim 21 , further reducing particle size of the first solids fraction.25. The method of claim 21 , wherein the applying pressure to the first solids fraction comprises applying pressure from about 200-600 psi.26. The method of claim 21 , further comprising heating the first solids fraction from about 21° C. (70° F.) to about 100° C. (212 ° F.).27. The method of claim 21 , further comprising prior to step (e) claim 21 , treating the first solids fraction with one or more enzymes.28. The method of claim 27 , wherein the one or more enzymes are ...

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Номер записи: 64
28-05-2020 дата публикации

USE OF AN ESTERASE TO ENHANCE ETHYL ESTER CONTENT IN FERMENTATION MEDIA

Номер: US20200165642A1
Автор: Bly Steven T., Breitling Brandon James, Gacke Benjamin P., Lewis Stephen M., McCurdy Alexander T.
Принадлежит:

Methods to prepare vegetable oil compositions having an elevated ethyl ester content are provided. 1. A method for enhancing vegetable oil properties from ground vegetable material , comprising:providing a first composition comprising water and ground vegetable material comprising vegetable fat;combining an amount of an exogenous esterase and the first composition under conditions to form a second composition comprising vegetable oil, wherein the exogenous esterase is in an amount that is at least 0.001 and up to about 0.4% w/w of the weight of the vegetable fat; andisolating vegetable oil from the second composition, wherein the vegetable oil has a fatty acid ethyl ester content that is greater than 2%.2. The method of claim 1 , wherein the fatty acid ethyl ester content is greater than 5% w/w in the total weight of the vegetable oil portion of the second composition.3. The method of claim 1 , wherein the fatty acid ethyl ester content is greater than 10% w/w in the total weight of the vegetable oil portion of the second composition.4. The method of claim 1 , wherein the fatty acid ethyl ester content is greater than 30% w/w in the total weight of the vegetable oil portion of the second composition.5. The method of claim 1 , wherein the esterase is in an amount that is up to 0.01% w/w of the weight of the vegetable fat.6. The method of claim 1 , wherein the esterase is in an amount that is up to 0.04% w/w of the weight of the vegetable fat.7. The method of claim 1 , wherein the esterase is in an amount that is from 0.01% to 0.4% w/w of the weight of the vegetable fat.8. The method of claim 1 , further comprising fermenting the first composition to produce the second composition.9. The method of claim 1 , wherein the exogenous esterase is further combined with the second composition.10. The method of claim 1 , wherein the ground vegetable material in the composition comprises 20 to 50 wt-% ground vegetable material including vegetable fat.11. The method of wherein ...

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Номер записи: 65
28-06-2018 дата публикации

LECITHIN COMPOSITIONS AND METHODS OF MAKING AND USING SUCH LECITHIN COMPOSITIONS

Номер: US20180178178A1
Автор: Baseeth Shireen
Принадлежит:

The present invention is directed towards compositions comprising a lecithin; a sugar alcohol, a sugar, or combinations of any thereof; and an alcohol. Compositions comprising a water soluble surfactant are further disclosed. Methods of separating oil from a mixture are disclosed. Methods of dispersing an oil are further disclosed. Compositions comprising a water-dilutable microemulsion are disclosed. Methods of making chewing gum are disclosed. Methods of recovering oil from a mixture are further disclosed. 134-. (canceled)35. A composition comprising:a lecithin;a sugar alcohol, a sugar, or combinations of any thereof;and an alcohol.3637-. (canceled)38. The composition of claim 35 , further comprising a cosurfactant.39. The composition of claim 38 , wherein the cosurfactant is selected from the group consisting of cationic surfactants claim 38 , anionic surfactants claim 38 , nonionic surfactants claim 38 , biobased emulsifiers claim 38 , and combinations of any thereof.4047-. (canceled)48. The composition of claim 35 , wherein the lecithin is selected from the group consisting of crude lecithin claim 35 , fluid lecithin claim 35 , deoiled lecithin claim 35 , fractionated lecithin claim 35 , high phosphatidyl choline (PC) fraction lecithin claim 35 , acetylated lecithin claim 35 , hydrolyzed lecithin claim 35 , hydroxylated lecithin claim 35 , lecithin comprising enzyme modified phospholipids claim 35 , and combinations of any thereof.49. (canceled)50. The composition of claim 35 , wherein the sugar alcohol comprises 3-12 carbon atoms.5152-. (canceled)53. The composition of claim 50 , wherein the sugar alcohol comprises a solution having from about 55% of the sugar alcohol to about 85% of the sugar alcohol.54. The composition of claim 35 , wherein the sugar alcohol is present in an amount of at least about 5% by weight of the composition.55. (canceled)56. The composition of claim 35 , wherein the sugar is selected from the group consisting of corn syrup claim 35 , ...

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Номер записи: 66
04-06-2020 дата публикации

PROCESS AND METHOD FOR STILLAGE FERMENTATION

Номер: US20200170206A1
Автор: Crotteau Adam
Принадлежит:

The present invention generally relates to a novel process in which thin stillage is processed to produce algae oil and protein rich biomass as well as other energy rich byproducts. In accordance with a preferred embodiment, thin stillage is removed from an evaporator during the evaporation process to produce mid-stillage. This mid-stillage is preferably routed to a new process where it is directed to a pre-treatment centrifuge to remove suspended solids, sludge and corn oil. Thereafter, the mid-stillage is preferably cooled and then directed to a fermentation tank where the mid-stillage is subject to a batch fermentation process with algae “seed” fed from an algae inoculation system. Once the batch is harvested, the oil-rich algae/mid-stillage is then preferably heated to rupture the cells and liberate the oil. Thereafter, the oil-rich algae/mid-stillage is preferably processed by a centrifuge which produces solids, a light phase oil and a “clean” mid-stillage stream that can be evaporated to a very high level of solids. 1. A process of producing bioproducts following the distillation of biomass , wherein the process comprises the steps of:separating ethanol and whole stillage;routing the whole stillage to a centrifuge;centrifuging the whole stillage to remove solids and to produce a thin stillage, wherein the thin stillage is comprised of 5-8% solids;routing the thin stillage to an evaporator;evaporating water content from the thin stillage to produce mid-stillage, wherein the mid-stillage is comprised of 9-27% solids;separating the mid-stillage into light phase oil, a sludge layer and clarified mid-stillage, wherein the clarified mid-stillage is in water phase with less than 1% suspended solids;cooling the clarified mid-stillage;routing the clarified mid- stillage to an algae fermentation tank;adding algae seed from an algae inoculation system to achieve a starting concentration of 1.5-3.0 grams/L algae;injecting air into the algae fermentation tank to support an ...

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Номер записи: 67
04-06-2020 дата публикации

Process For Isolating A Protein Composition And A Fat Composition From Deboned Poultry

Номер: US20200170275A1
Автор: Fielding William R., Kelleher Stephen D., Saunders Wayne S.
Принадлежит: Proteus Industries, Inc.

A protein fraction and an oxidation stable fat fraction are recovered from poultry containing fat, bone and protein. The poultry is comminuted, solubilized with a food grade acid or base to form a liquid protein fraction and a solid fat fraction. The protein in liquid fraction is precipitated and the protein product retains the color of raw meat. 2) process of ) claim 1 , the protein composition has 14% or greater by weight protein and less than 10% by weight fat.3) process of ) claim 1 , wherein said pH in Step B) is from 3.6 to 3.8.4) The process of ) claim 1 , wherein Step A) and Step B) are performed simultaneously.5) The process of ) claim 1 , wherein precipitating the protein from the solubilized liquid protein solution includes bringing the pH to a value in the range of between about 4.9 and about 6.4.6) The process of ) claim 5 , wherein adjusting the pH of the comminuted poultry of Step A) comprises adding of a food grade acid to obtain a pH value in the range between about 3.6 and about 4.4 and the step of precipitating the protein of Step D) includes adding a base to increase the pH to a value in the range of between about 4.9 and about 6.4.7) The process of ) claim 5 , wherein adjusting the pH of the comminuted poultry of Step A) comprises adding of a food grade base to obtain a pH value in the range between about 8.3 and about 10.5 and the step of precipitating the protein of Step D) includes adding an acid to decrease the pH to a value in the range of between about 4.9 and about 6.4.8) The process of ) claim 1 , wherein the addition of a food grade acid in Step B) comprises adding a food grade acid selected from the group consisting of: citric acid claim 1 , phosphoric acid claim 1 , ascorbic acid claim 1 , hydrochloric acid and any combination thereof.9) The process of ) claim 1 , wherein the addition of a food grade base in Step B) comprises adding a food grade base selected from the group consisting of: solution sodium bicarbonate claim 1 , sodium ...

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Номер записи: 68
09-07-2015 дата публикации

METHOD OF PROCESSING ETHANOL BYPRODUCTS AND RELATED SUBSYSTEMS

Номер: US20150191675A1
Автор: Cantrell David F., Winsness David J.
Принадлежит:

In one aspect of the invention, a method recovers oil from a concentrated byproduct, such as evaporated thin stillage formed during a dry milling process used for producing ethanol. The method includes forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct. Further, the step of separating the oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil from thin stillage. 1. A method of recovering oil from thin stillage in a dry milling corn-to-ethanol plant , the method comprising:dry milling corn at the ethanol manufacturing facility by converting starch in the corn to sugar;fermenting the sugar to produce ethanol and whole stillage;separating the whole stillage in a separator to produce a distillers wet grains and a thin stillage, wherein each of the distillers wet grains and the thin stillage contain corn oil;evaporating the thin stillage in an evaporator in the ethanol manufacturing facility to remove water and form a concentrated byproduct, wherein the concentrated byproduct contains corn oil;centrifuging the concentrated byproduct in a centrifuge located downstream from the evaporator in the ethanol manufacturing facility to separate at least a portion of the corn oil from the concentrated byproduct; andrecovering the separated oil.2. The method of claim 1 , further comprising mixing the concentrated byproduct remaining after centrifuging with distillers wet grains to form a mixture; and drying the mixture in a dryer downstream from the evaporator and centrifuge to make distillers dried grains with solubles.3. The method of claim 1 , wherein the concentrated byproduct has a moisture content of greater than 30% and less than 90% by weight.4. The method of claim 1 , wherein evaporating the thin stillage in the evaporator to remove ...

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Номер записи: 69
04-06-2020 дата публикации

OIL RECOVERY AID

Номер: US20200172828A1
Автор: Fowlie David A., Murphy Christopher B.
Принадлежит:

Compositions for increasing corn oil recovery and embodiments of methods for using the composition for corn oil separation are described. The composition(s) incorporate an admixture that includes a polymer selected from a polyglycol ester, a polyethyleneoxide-polypropyleneoxide block copolymer, a poloxamine, or a mixture thereof. The methods include admixing the compositions with a process stream for, for example, the extraction of oil from milled corn and residues from a fermentation step, including stillage (e.g., thin stillage or mid stillage), distiller's wet grain, distiller's dry grain and distiller's dry grains with solubles. 1. A method comprising:adding a polymer selected from a polyethyleneoxide-polypropyleneoxide block copolymer, a poloxamine, and a mixture thereof to a corn-to-ethanol process stream, wherein the polymer provides an Oil Separation Rating of at least 2 at a polymer dosage of 350 ppm.2. The method of claim 1 , wherein the polymer provides an Oil Separation Rating of at least 2 at a polymer dosage of 250 ppm.3. The method of claim 2 , wherein the polymer provides an Oil Separation Rating of at least 2 at a polymer dosage of 150 ppm.4. The method of claim 1 , wherein the polymer provides an Oil Separation Rating of 3 at a polymer dosage of 350 ppm.5. The method of claim 4 , wherein the polymer provides an Oil Separation Rating of 3 at a polymer dosage of 250 ppm.6. The method of claim 5 , wherein the polymer provides an Oil Separation Rating of 3 at a polymer dosage of 150 ppm.7. The method of claim 1 , wherein the polymer includes a polyethyleneoxide-polypropyleneoxide block copolymer.8. The method of claim 7 , wherein the polymer includes a mixture of polyethyleneoxide-polypropyleneoxide block copolymers.9. The method of claim 1 , wherein the polymer includes a poloxamine that has a formula (R)N[(CH)NR]R claim 1 , wherein each Ris claim 1 , independently claim 1 , selected from a hydrogen atom claim 1 , a hydroxyethyl group claim 1 , a ...

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Номер записи: 70
16-07-2015 дата публикации

Light phase product recovery methods and systems

Номер: US20150197707A1
Автор: Steven Redford
Принадлежит: Poet Research Inc

Methods and systems for recovering a desired co-product from a feedstock to ethanol production process are provided. The methods involve a multi-step separation of a fermentation-derived feedstock, in which an initial separation produces a discharge stream and an output feed stream including the co-product, and a final separation further purifies the output feed stream while also producing a recycle stream that is reintroduced into the separation process. The systems include at least an initial and at least a final separation device which are in fluid communication in both upstream and downstream directions. The initial separation device separates at least a portion of a non-co-product containing phase from a feed stream comprising the non-co-product containing phase and a co-product containing phase, and the final separation device separates at least a portion of the co-product containing phase from a stream comprising the co-product containing phase and a non-co-product containing phase.

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Номер записи: 71
05-07-2018 дата публикации

Lubricity additive for fuel with a low sulphur content

Номер: US20180187110A1
Автор: Hakim BEN SAHEL, Julien HEROU, Laurent Germanaud, Olivier Langlois
Принадлежит: Total Marketing Services SA

The invention relates to a lubricity additive for fuel, particularly for diesel fuel, directly obtained from the acidification of a soapstock produced by a method for refining at least one vegetable and/or animal oil. The lubricity additive according to the invention is more specifically used for fuels that have a low sulfur content, for example, lower than 500 ppm (by weight).

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Номер записи: 72
20-06-2019 дата публикации

Dry-milling process

Номер: US20190185885A1
Автор: Anthony Newton, Joseph P. Borst, Kenneth L. Zack
Принадлежит: BASF SE

A dry-milling process for the production of dried distiller's grains with solubles (“DDGS”) includes the steps of dry-milling corn kernels to form a corn flour comprising corn fiber; combining the corn flour with water to form a mash; separating the corn fiber from the mash; treating the separated corn fiber with a composition; combining the treated corn fiber with the mash having the corn fiber separated therefrom to form a slurry; fermenting the slurry to produce beer and carbon dioxide; distilling the beer to produce ethanol and whole stillage; and processing the whole stillage to produce DDGS. The composition includes an alkanesulfonic acid, water, an enzyme, and optionally a surfactant.

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Номер записи: 73
12-07-2018 дата публикации

Process for isolating a protein composition and a fat composition from mechanically deboned poultry

Номер: US20180192663A1
Автор: Fielding William R., Kelleher Stephen D., Saunders Wayne S.
Принадлежит: Proteus Industries, Inc.

A protein fraction and an oxidation stable fat fraction are recovered from poultry containing fat, bone and protein. The poultry is comminuted, mixed with a food grade acid at pH 3.6 to 4.4 to form a liquid protein fraction and a solid fat fraction. The liquid fraction is mixed with a food grade alkali to precipitate the protein. 1) The process for recovering , from mechanically deboned poultry containing fat , bone and protein and initial levels of calcium and sodium , a protein composition with reduced levels of calcium and sodium as compared to the initial levels of calcium and sodium , wherein the deboned poultry has 65-85% by weight lean , the process comprising the steps of:a) comminuting the poultry in water,b) adding a food grade acid to the comminuted poultry to effect a pH of 3.6 to 4.4 thereby to solubilize the protein, wherein calcium remains insoluble,c) after addition of the food grade acid in step b), separating solid fat from the solubilized protein, wherein calcium is separated together with the solid fat from the solubilized protein,d) adding a food grade alkali to the fat to neutralize acid in the fat and to the solubilized protein to neutralize acid in the protein and to precipitate the protein, wherein sodium remains soluble, ande) recovering from the precipitate the protein composition with reduced levels of calcium and sodium as compared to the initial levels of calcium and sodium, wherein the protein composition has 14% or greater by weight protein and less than 10% by weight fat, wherein the less than 10% by weight fat is stabilized against oxidation.2) The process of wherein said pH in step b is from 3.6 to 3.8.3) The process of wherein a food grade acid is added in step a.4) The process of wherein a food grade acid is added in step a.5) The process of wherein said food grade acid is hydrochloric acid and/or citric acid.6) The process of wherein said food grade acid is hydrochloric acid and/or citric acid.7) The process of wherein said food ...

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Номер записи: 74
29-07-2021 дата публикации

PROCESS AND METHOD FOR THE RECOVERY OF OIL FROM THE PROCESSING OF GRAINS INTO BIOFUELS AND OTHER CHEMICALS

Номер: US20210229000A1
Автор: Bleyer James Robert
Принадлежит: Trucent, Inc.

A method of recovering an extraction aid from distillers corn oil, by directing stillage containing distillers oil and an extraction aid to a centrifugal separator, recovering a light phase from the centrifugal separator, the light phase containing at least a portion of the distillers oil and at least a portion of the extraction aid, cooling the light phase and causing a precipitate to form, and recovering a precipitate from the cooled light phase containing at least a portion of the extraction aid. A method of recovering distillers oil. 1. A method of recovering an extraction aid from a stream containing oil and an extraction aid , including the steps of:directing a stream containing oil and an extraction aid to a separator;recovering a light phase from the separator, the light phase containing at least a portion of the oil and at least a portion of the extraction aid;cooling the light phase and causing a precipitate to form; andrecovering the precipitate from the cooled light phase.2. The method of claim 1 , further including the step of directing and recycling at least a portion of the recovered precipitate to the feed of a separator.3. The method of claim 1 , wherein said cooling step is further defined as cooling the light phase to a temperature at or below about 120 degrees F.4. The method of claim 3 , wherein said cooling step is further defined as cooling the light phase to a temperature at or below about 80 degrees F.5. The method of claim 1 , wherein the stream containing oil is from a fermentation process that produces ethanol.6. The method of claim 1 , wherein the feedstock to a fermentation process producing the stream is one or more of corn and milo.7. The method of claim 1 , where the stream containing oil and an extraction aid is directed to a centrifugal separator.8. The method of claim 7 , further including concentrating the stream containing oil before said directing step.9. The method of claim 8 , wherein said concentrating step is performed by a ...

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Номер записи: 75
18-06-2020 дата публикации

Process for purifying renewable feedstock comprising triglycerides

Номер: US20200190407A1
Автор: Andrea Gutierrez, Thomas Björklöf
Принадлежит: UPM Kymmene Oy

The present invention relates to a process for purifying renewable feedstock comprising triglycerides, said process comprising the steps, where the renewable feedstock comprising triglycerides, comprising at least one plant oil originating from a plant of the family Brassicaceae, is treated with an aqueous medium to obtain a mixture, and a first stream comprising water and a second stream comprising triglycerides are separated from said mixture, and the second stream is obtained as purified renewable feedstock.

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Номер записи: 76
18-06-2020 дата публикации

Process for purifying feedstock comprising fatty acids

Номер: US20200190426A1
Автор: Andrea Gutierrez, Thomas Björklöf
Принадлежит: UPM Kymmene Oy

The present invention relates to process for purifying renewable feedstock comprising at least one acidulated soap-stock, wherein said process comprises the steps, where the renewable feedstock comprising at least one fatty acid is treated in a treating step with an aqueous medium, and a first stream comprising water and a second stream comprising fatty acids are obtained, and the second stream is obtained as purified renewable feedstock.

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Номер записи: 77
18-06-2020 дата публикации

PROCESS FOR PURIFYING RENEWABLE FEEDSTOCK COMPRISING FATTY ACIDS

Номер: US20200190427A1
Автор: BJÖRKLÖF Thomas, GUTIERREZ Andrea
Принадлежит:

The present invention relates to a process for purifying renewable feedstock comprising fatty acids, said process comprising the steps, where the renewable feedstock comprising fatty acids comprises at least one acid oil and at least another renewable feedstock, and it is treated with an aqueous medium, to obtain a mixture, and a first stream comprising water is separated from said mixture and a second stream comprising fatty acids is obtained as purified renewable feedstock. 1. A process for purifying renewable feedstock comprising fatty acids , wherein said process comprises the steps , where the renewable feedstock comprising fatty acids comprises at least one acid oil and at least another renewable feedstock , and said renewable feedstock comprising fatty acids is treated with an aqueous medium , at the temperature from 140 to 195° C. , under a pressure from 0.1 to 70 bar (abs) , and where the ratio of the renewable feedstock comprising fatty acids to the aqueous medium is from 1:5 to 5:1 , respectively , to obtain a mixture , and a first stream comprising water and a second stream comprising fatty acids are separated from said mixture , and the second stream is obtained as purified renewable feedstock.2. The process according to claim 1 , wherein the purified renewable feedstock comprises not more than 50 mg/kg phosphorus claim 1 , preferably not more than 10 mg/kg phosphorus claim 1 , calculated as elemental phosphorus.3. The process according to claim 1 , wherein the purified renewable feedstock comprises not more than 100 mg/kg of alkali metals claim 1 , alkaline earth metals claim 1 , metals of the groups VIIB and VIIIB of the Periodic table of elements claim 1 , or combinations thereof claim 1 , preferably not more than 50 mg/kg claim 1 , calculated as elemental metals.4. The process according to claim 1 , wherein the first stream comprising water comprises not more than 10 000 mg/kg total organic carbon.5. The process according to claim 1 , wherein the ...

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Номер записи: 78
19-07-2018 дата публикации

Polymerized oils & methods of manufacturing the same

Номер: US20180201635A1
Автор: Hassan Ali Tabatabaee, Suzanne STAUDUHAR, Todd L. Kurth
Принадлежит: Cargill Inc

Embodiments of the present invention provide a method, comprising obtaining a lecithin-containing material, in some aspects derived from a crude refining stream, comprising 20-80 wt % acetone insoluble matter, 1-30 wt % free fatty acid, and less than 10 wt % water, adding a fatty acid or carboxylic source to the lecithin-containing material to obtain a lecithin fatty acid blend or lecithin carboxylic acid blend and incorporating the blend into asphalt or oil field applications.

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Номер записи: 79
26-07-2018 дата публикации

Applying measurement, control and automation to a dry corn milling ethanol production process to maximize the recovery of ethanol and co-products

Номер: US20180206526A1
Автор: Bret H. MAGNESS, James T. TURNBULL
Принадлежит: Buckman Laboratories International Inc, Cidra Corporated Services LLC

Apparatus features a signal processor or signal processing module configured to: receive signaling containing information about about a measurement of one or more constituents of an output stream from a centrifuge in a dry corn milling process, including to produce Ethanol; and determine corresponding signaling containing information about a real time feedback control of the dry corn milling process, based upon the signaling received. The signal processor or signal processing module is configured to provide the corresponding signaling as control signaling to provide the real time feedback control of the dry corn milling process.

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Номер записи: 80
13-08-2015 дата публикации

METHOD OF EXTRACTING LIPIDS FROM TRAP GREASE WITH WASTE COOKING OIL

Номер: US20150225658A1
Автор: Lu Mingming, Tu Qingshi, Wang Jingjing
Принадлежит:

Describe are methods of extracting the lipid fraction from trap grease using vegetable oil, such as vegetable oils sourced from waste cooking oil. The method includes mixing a volume of vegetable oil with a volume of trap grease. The mixture is comprised of an aqueous fraction, a solid fraction, and a lipid fraction. The mixture is heated to a temperature in a range from about 50 degrees C. to about 100 degrees C. for a period of time sufficient to extract at least 80 percent of the lipids from the trap grease. The lipid fraction is then separated from the solid fraction. The method may further include a process of producing biodiesel from the extracted lipid fraction. 1. A method of extracting a lipid fraction from trap grease comprising:mixing a volume of waste cooking oil with a volume of trap grease, wherein the mixture is comprised of an aqueous fraction, a solid fraction, and a lipid fraction, wherein the volume of waste cooking oil and the volume of trap grease are mixed at a ratio between 1.5 ml:1 mg to 4.5 ml:1 mg;heating the mixture to a temperature in a range from about 55 degrees C. to about 85 degrees C. and maintaining the temperature for a period of time from 45 minutes to 210 minutes to extract at least 80 percent of the lipids from the trap grease; andseparating a portion of the lipid fraction from the solid fraction using a process chosen from a filtration process and a heating process, wherein the heating process includes heating the mixture for a period of time sufficient for at least a majority portion of the aqueous fraction to evaporate.2. A method of extracting a lipid fraction from trap grease comprising:mixing a volume of vegetable oil with a volume of trap grease, wherein the mixture is comprised of an aqueous fraction, a solid fraction, and a lipid fraction;heating the mixture to a temperature in a range from about 50 degrees C. to about 100 degrees C. for a period of time sufficient to extract at least 80 percent of the lipids from the ...

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Номер записи: 81
03-08-2017 дата публикации

Producing recoverable oil from fermentation processes

Номер: US20170218298A1
Автор: Marco Kraemer, Vitaly SVETLITCHNYI
Принадлежит: BASF Enzymes LLC

The present technology relates to processes of fermenting a starch-containing material into a fermentation product comprising a fermentation step in the presence of a xylanase in combination with a pectinase on oil partitioning during post-fermentation processing. In particular, the enzyme(s) were added during simultaneous saccharification and fermentation. The finished beer was subjected to beer well incubation, distillation, and then decanting to separate thin stillage from the solids.

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Номер записи: 82
23-10-2014 дата публикации

Process for Obtaining a Diesel Like Fuel

Номер: US20140311018A1
Автор: Jan Warnqvist
Принадлежит: Invico Tech Ab

Disclosed is an enrichment method for obtaining components for the production of a diesel like fuel additive or a diesel like fuel from crude tall oil. In the method, lipophilic components, being present in said crude tall oil, are extracted with an organic solvent and the resulting extract is washed with sulfuric acid and water.

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Номер записи: 83
30-10-2014 дата публикации

Methods and systems for converting food waste oil into biodiesel fuel

Номер: US20140318631A1
Автор: James M. Rethore, Julie E. Wheeler, Steven G. Polski
Принадлежит: Revolution Fuels Inc

This invention provides the market with low-cost retrieval of valuable used cooking oil to customer distribution centers, where a mobile production unit visits to create biodiesel fuel, which can be immediately used by customers to fuel their fleet. In some variations, a method comprises identifying a network of customer distribution centers, collecting used cooking oil transported from users to customer distribution centers, providing a mobile reactor to convert used cooking oil into biodiesel fuel under effective reaction conditions, producing biodiesel fuel on-site at the customer distribution centers, and introducing the biodiesel fuel, directly or via a fuel blend, into fleet vehicles. Related systems and apparatus are also disclosed. This invention provides a clean source of energy from waste, a lower-cost alternatives to petroleum-derived diesel fuel, and improved environmental footprints including lower fuel use and lower total carbon emissions.

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Номер записи: 84
27-08-2015 дата публикации

PROCESS FOR REGENERATING FILTER AID USED IN A WINTERIZATION PROCESS

Номер: US20150240185A1
Автор: Bereznev Oleg, Golinski Stéphane, Kemeny Zsolt, Makarenko Andrey
Принадлежит: BUNGE NOVENYOLAJIPARI ZARTKORUEN MUKODO RESZVENYTARSASAG

The present invention relates to a process for in situ regeneration of spent filter aid including the steps of: a) circulating through a spent filter aid cake in a circulation loop a regenerating oil at a temperature of from 40° C. to 100° C., in a regenerating oil/spent filter aid (v/w) ratio of from 0.3/1 to 12/1; b) removing the regenerating oil from the treated spent filter aid cake; and c) recovering the regenerated filter aid. 1. A process for in situ regeneration of spent filter aid comprising the steps of:a) circulating a regenerating oil through a spent filter aid cake in a circulation loop at a temperature of from 40° C. to 100° C., in a regenerating oil/spent filter aid (v/w) ratio of from 0.3/1 to 12/1;b) removing the regenerating oil from the treated spent filter aid cake; andc) recovering the regenerated filter aid.2. A process according to claim 1 , wherein the regenerating oil is a non-refined claim 1 , partially refined or fully refined vegetable oil.3. A process according to claim 2 , wherein the vegetable oil is chosen as being partially refined or fully refined sunflower oil claim 2 , olive oil claim 2 , corn oil or cottonseed oil.4. A process according to claim 1 , wherein the regenerating oil is chosen as being the same oil as the oil being winterised in the process having generated the spent filter aid.5. A process according to claim 1 , wherein the regenerating oil circulates through the spent filter aid cake at a temperature of from 45° C. to 85° C.6. A process according to claim 1 , wherein the regenerating oil is circulating through the spent filter aid cake during 5 to 60 minutes.7. A process according to claim 1 , wherein the regenerating oil/spent filter aid (v/w) ratio of from 1/1 to 9/1.8. A process according to claim 1 , wherein the regenerating oil is removed from the treated spent filter aid cake by draining and then blowing said cake.9. A process according to claim 8 , wherein the treated spent filter aid cake is blown with air or ...

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Номер записи: 85
16-07-2020 дата публикации

METHODS FOR MAKING FREE FATTY ACIDS AND FATTY ACID DERIVATIVES FROM MIXED LIPID FEEDSTOCKS OR SOAPSTOCKS

Номер: US20200224121A1
Автор: "BLANCHARD Cory ONeil", KILLINGSWORTH Nathan, LONG Ryan Alexander
Принадлежит:

Provided are methods and systems for treating a soapstock. Provided are systems and methods for treating a soapstock to generate free fatty acids and/or fatty acid derivatives, and for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to fatty acids and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, wherein the soapstock comprises soaps and saponifiable lipids, and the generating of free fatty acids is achieved. Provided are systems and methods for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to salts of fatty acids and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, wherein the soapstock comprises soaps and saponifiable lipids, and the generating of free fatty acids is achieved. 1: A method or process for generating , and isolating or purifying , free fatty acids from a mixed lipid feedstock , the method comprising:(a) providing a first mixture comprising an aqueous solution or mixture comprising a mixed lipid feedstock, andwherein optionally the mixed lipid feedstock comprises: a soapstock; a triglyceride comprising material; a saponifiable material, optionally a glyceride or a phospholipid; a tall oil, optionally a “liquid rosin” tall oil, a soapstock; a gums product, optionally a chemically or enzymatically derived gums product; a crude biodiesel; a fatty acid, optionally from a distillation bottom; a fat splitter emulsion, optionally purged from fat splitter due to accumulation when recycled; or, any combination thereof,and optionally the mixed lipid feedstock comprises a soapstock, a wash-water comprising soaps or a combination thereof, optionally generated during the chemical refining of a crude natural oil,and optionally the mixed lipid feedstock comprises a mixture of fatty acid soaps, fatty acids or fatty acid soaps and ...

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Номер записи: 86
25-08-2016 дата публикации

Method of separating oil from a liquid stillage

Номер: US20160244694A1
Автор: Craig Michael SUNGAIL, Min Ma Wang, Ronald Eugene Bingeman, Xin Chen
Принадлежит: Croda Inc

A method of separating oil from a liquid stillage is disclosed. The stillage includes an aqueous phase and an oil phase. The method comprises adding a separation additive to the stillage and performing at least one separation operation on the stillage to separate an amount of the oil phase from the stillage. The separation additive comprises an ester of an alkoxylated non-cyclic polyol and a fatty acid.

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Номер записи: 87
23-08-2018 дата публикации

PROCESS OF EXTRACTING OIL FROM THIN STILLAGE

Номер: US20180237726A1
Автор: Jump Joseph, Kreel Nathaniel
Принадлежит: NOVOZYMES A/S

The present invention relates to processes of recovering oil after liquefaction and/or from thin stillage and/or syrup/evaporated centrate from a fermentation product production process by adding a thermostable protease to the whole stillage, thin stillage and/or syrup. 1. A process comprising:(a) converting a starch-containing material into dextrins with an alpha-amylase;(b) saccharifying the dextrins using a carbohydrate source generating enzyme to form a sugar;(c) fermenting the sugar in a fermentation medium into a fermentation product using a fermenting organism;(d) forming a whole stillage;{'i': 'Pyroccocus', 'wherein a protease selected from the group consisting of a bacterial protease, a fungal protease, and a protease is added during step (d).'}2. The process of claim 1 , further comprising adding the protease in starch-containing material converting step (a).3Rhizomucor mieheiThermoascus aurantiacus. The process of claim 1 , wherein the fungal protease is selected from the group consisting of the protease shown in SEQ ID NO: 9 or a variant thereof having at least 90% claim 1 , at least 95% claim 1 , at least 96% claim 1 , at least 97% claim 1 , at least 98% claim 1 , or at least 99% sequence identity to SEQ ID NO: 9 and the protease shown in SEQ ID NO: 3 herein with the mutations selected from the group consisting of:A27K+D79L+Y82F+S87G+D104P+A112P+A126V+D142L;D79L+Y82F+S87G+A112P+D142L;Y82F+S87G+S70V+D79L+D104P+A112P+D142L;Y82F+S87G+D79L+D104P+A112P+A126V+D142L.4. The process of claim 1 , wherein the bacterial protease is a bacterial serine protease.5Thermobifida fusca. The process of claim 4 , wherein the bacterial serine protease is a protease having the sequence shown in SEQ ID NO: 10 or is a variant thereof having at least 90% claim 4 , at least 95% claim 4 , at least 96% claim 4 , at least 97% claim 4 , at least 98% claim 4 , or at least 99% sequence identity to SEQ ID NO: 10.6Pyrococcus. The process of claim 1 , wherein the protease is the one shown ...

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Номер записи: 88
23-07-2020 дата публикации

Methods of extracting nutritionally valuable or biologically active components using animal products and extracts obtained by the same

Номер: US20200231897A1
Автор: Roland Laux, Tilo Huhn
Принадлежит: Unico-First Ag, Zuercher Hochschule fur Angewandte Wissenschaften Grueental

This invention relates to a method for obtaining nutritionally beneficial and/or biologically active components, such as aromatic substances and vitamins, from animal-derived products and to oil-based extracts which can be obtained from this method.

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Номер записи: 89
08-08-2019 дата публикации

Methods for producing a high protein corn meal from a whole stillage byproduct and system therefore

Номер: US20190241834A1
Автор: Chie Ying Lee
Принадлежит: Fluid Quip Inc

The present invention relates generally to corn dry-milling, and more specifically, to methods for producing a high protein corn meal from a whole stillage byproduct produced in a corn dry-milling process for making ethanol and a system therefore. In one embodiment, a method for producing a high protein corn meal from a whole stillage byproduct includes, in a corn dry-milling process for making ethanol, separating the whole stillage byproduct into an insoluble solids portion and a thin stillage portion. The thin stillage portion is separated into a protein portion and a water soluble solids portion. Next, the protein portion is dewatered then dried to define a high protein corn meal that includes at least 40 wt % protein on a dry basis.

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Номер записи: 90
07-09-2017 дата публикации

METHOD TO RECOVER FREE FATTY ACIDS FROM FATS AND OILS

Номер: US20170253830A9
Автор: Dasari Mohan Prasad A., Knox Kidron Joel, Warren Hugh Tallant
Принадлежит: RRIP, LLC

Methods for producing oil from fats and oils having high free fatty acid content are provided. In the method, fats and oils are treated with a mixture including an alcohol to result in a low-free fatty acid oily phase and an alcohol phase. The mixture may also include an alkali. The alcohol may be a monohydric alcohol and an aqueous alcohol, such as an aqueous alcohol having a concentration of at least about 15% alcohol-by-weight. The low-free fatty acid phase may include oil and at least one impurity. The low-free fatty acid phase may be cooled, and the oil may be separated from the at least one impurity. Fats and oils amenable to such a method may include, but are not limited to, waste fats, waste oils, high acid grease, high acid tallow, sorghum heat oil, and corn oil, such as corn oil produced at an ethanol production plant. 1. A method of producing oil comprising:treating fats and oils having a high free fatty acid content with a mixture comprising a monohydric alcohol to form a low-free fatty acid oily phase and an alcohol phase wherein said monohydric alcohol is a solvent;said low-free fatty acid oily phase comprising oil and at least one impurity;said monohydric alcohol having a concentration of at least about 15% alcohol by weight; andseparating said oil and said at least one impurity.2. The method of wherein said mixture comprising a monohydric alcohol further comprises an alkali.3. The method of wherein said at least one impurity is selected from the group consisting of free fatty acid soaps claim 2 , waxes claim 2 , unsaponifiables claim 2 , and combinations thereof.4. The method of wherein said at least one impurity is wax.5. The method of wherein both waxes and free fatty acid soaps are separated from said oil.6. The method of wherein the step of treating said fats and oils with a mixture comprising an alcohol and an alkali to form a low-free fatty acid oily phase and an alcohol phase is carried out at about 25 to 75 degrees Celsius and about ...

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Номер записи: 91
22-09-2016 дата публикации

METHOD TO RECOVER FREE FATTY ACIDS FROM FATS AND OILS

Номер: US20160272920A1
Автор: Dasari Mohan Prasad A., Knox Kidron Joel, Warren Hugh Tallant
Принадлежит: RRIP, LLC

Methods for producing oil from fats and oils having high free fatty acid content are provided. In the method, fats and oils are treated with a mixture including an alcohol to result in a low-free fatty acid oily phase and an alcohol phase. The mixture may also include an alkali. The alcohol may be a monohydric alcohol and an aqueous alcohol, such as an aqueous alcohol having a concentration of at least about 15% alcohol-by-weight. The low-free fatty acid phase may include oil and at least one impurity. The low-free fatty acid phase may be cooled, and the oil may be separated from the at least one impurity. Fats and oils amenable to such a method may include, but are not limited to, waste fats, waste oils, high acid grease, high acid tallow, sorghum heat oil, and corn oil, such as corn oil produced at an ethanol production plant. 1. A method of producing oil comprising:treating fats and oils having a high free fatty acid content with a mixture comprising a monohydric alcohol to form a low-free fatty acid oily phase and an alcohol phase wherein said monohydric alcohol is a solvent;said low-free fatty acid oily phase comprising oil and at least one impurity;said monohydric alcohol having a concentration of at least about 15% alcohol by weight; andseparating said oil and said at least one impurity.2. The method of wherein said mixture comprising a monohydric alcohol further comprises an alkali.3. The method of wherein said at least one impurity is selected from the group consisting of free fatty acid soaps claim 2 , waxes claim 2 , unsaponifiables claim 2 , and combinations thereof.4. The method of wherein said at least one impurity is wax.5. The method of wherein both waxes and free fatty acid soaps are separated from said oil.6. The method of wherein the step of treating said fats and oils with a mixture comprising an alcohol and an alkali to form a low-free fatty acid oily phase and an alcohol phase is carried out at about 25 to 75 degrees Celsius and about ...

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Номер записи: 92
22-08-2019 дата публикации

Process of extracting oil from thin stillage

Номер: US20190256799A1
Автор: Joseph Jump, Nathaniel Kreel
Принадлежит: Novozymes AS

The present invention relates to processes of recovering oil after liquefaction and/or from thin stillage and/or syrup/evaporated centrate from a fermentation product production process by adding a thermostable protease to the whole stillage, thin stillage and/or syrup.

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Номер записи: 93
11-12-2014 дата публикации

LIQUID/LIQUID EXTRACTION WITH A SOLVENT COMPRISING AT LEAST 5 CARBON ATOMS AND 1 OR 2 OXYGEN ATOMS

Номер: US20140363559A1
Автор: Legrand Jacques, Mercier Eglantine, Saunois Alex
Принадлежит: LABORATOIRES EXPANSCIENCE

The present invention relates to an extraction process of an unsaponifiable fraction contained in an oil or a vegetable butter, in an oil originating from a micro-organism, in a concentrate of oil or butter or of oil originating from a micro-organism, or in a co-product of the refining industry for vegetable oils, such as deodorisation exhaust and distillates of physical refining, or oils originating from micro-organisms, comprising at least: 118-. (canceled)20. The process according to claim 19 , further comprising claim 19 , after step A claim 19 , step A′ of adjusting the alcohol content of the hydro-alcoholic solution obtained after step A claim 19 , advantageously in order to obtain an alcohol content of between 10 and 50% by weight claim 19 , in particular between 11 and 40% by weight and typically between 12 and 28% by weight.21. The process according to claim 19 , further comprising claim 19 , after step B claim 19 , a step C of purifying the unsaponifiable.22. The process according to claim 21 , wherein purifying step C of the unsaponifiable is performed by using said first solvent system.23. The process according to claim 19 , wherein the first solvent system has a density less than 1.24. The process according to claim 19 , wherein the solvent comprising at least 5 carbon atoms and one or two oxygen atoms is selected from methylketones claim 19 , especially methyl isobutyl ketone (MIBK) claim 19 , 2-heptanone claim 19 , propionates claim 19 , especially ethyl propionate claim 19 , n-butyl propionate claim 19 , isoamyl propionate claim 19 , propylethers claim 19 , especially diisopropyl ether (DIPE) claim 19 , and mixtures thereof.25. The process according to claim 19 , wherein the first solvent system comprises a content in solvent comprising at least 5 carbon atoms and one or two oxygen atoms in the form of ether claim 19 , ketone or ester function of at least 60% claim 19 , especially at least 75% claim 19 , in particular at least 90% claim 19 , more ...

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Номер записи: 94
29-09-2016 дата публикации

METHOD AND ARRANGEMENT FOR THE SEPARATION OF TALL OIL PRODUCTS FROM BLACK LIQUOR

Номер: US20160281028A1
Автор: Hofstedt Anders Goran
Принадлежит:

A method and arrangement for separating tall oil products from a black liquor-containing boiling liquid that has been drained off, was produced within a kraft mill chip digester, and includes a fibrous cellulose material in a mixture with the black liquor and tall oil products, and where the boiling liquid is separated in a separation unit arranged to mechanically separate the boiling liquid into a fibrous cellulose material and a mixture of mixed black liquor and tall oil products, where the mixture of boiling liquid and tall oil products is brought to a separation tank, the separation tank being a gravity separation tank, and adapted to be emptied in a discontinuous manner of the tall oil product collected and concentrated therein, the tall oil products being floated on top of and above a fraction of mixed black liquor, where the tall oil products is brought to a centrifugal separator. 114-. (canceled)1533334523a. Method for the separation of tall oil products (soap products) from a black liquor comprising boiling liquid () that has been drained off , said boiling liquid () having been produced in a kraft mill chip digester (K) , where said boiling liquid () comprises a fibrous cellulose material in a mixture with said black liquor and tall oil products , adapted to a mixed black liquor by addition of intermediate black liquor , and where the boiling liquid () is mechanically separated in a separation unit (S) for the production of a fibrous cellulose material () and the mixture () of black liquor and tall oil products and where the mixture of black liquor is brought to a separation tank (SE) that employs a gravity separation , being adapted for being emptied of the collected and concentrated tall oil products in a discontinuous manner , said tall oil products becoming , through flotation , positioned above and resting on a fraction of mixed black liquor , and where the mentioned concentrated tall oil products are brought to a centrifugal separator (CS) , where ...

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Номер записи: 95
29-09-2016 дата публикации

Process and system for producing liquid biofuel from bio-based oils and/or fats

Номер: US20160281029A1
Автор: Annimari Lehtomäki, Mika Rautiainen
Принадлежит: BioGTS Oy

A process for utilizing bio-based oils and/or fats for producing biofuels includes the steps of: mixing alcohol with a raw material for forming a reaction mixture; pumping the reaction mixture to a reactor; mixing biogas as a catalyst with the reaction mixture in a selected process step either before or after the supply of the reaction mixture to a high-pressure pump, the biogas including methane and carbon dioxide; adjusting a temperature and pressure of the reactor so that the reaction mixture achieves a supercritical state; esterifying the reaction mixture to produce liquid biofuel and by-products; separating the by-products including methane and alcohol from the liquid biofuel; and recovering separated methane. An equivalent system for utilizing bio-based oils and/or fats for producing biofuels is also disclosed.

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Номер записи: 96
29-08-2019 дата публикации

TEMPERATURE EFFECTED PLANT MACERATION SYSTEM AND PROCESS

Номер: US20190264132A1
Автор: Maya Sergio Nates, Nates Enrique Maya, Richmond Matthew Gaines
Принадлежит:

A temperature controlled plant maceration and extraction system and method is provided comprising an extraction chamber, an end cap at an one end of the extraction chamber, and an inlet gas valve at a second end. A hollow temperature jacket is formed around the extraction chamber from the first wall and an outer wall defining a space there between that is sealed at the one end and second end. A frame having a first and second pass-through axle is provided, one each fixedly mounted on the jacket between the one end and second end of the extraction chamber. Wherein organic matter is introduced via the one end, a solvent is injected into the chamber at the inlet valve on the second end, the extraction chamber is then rotated about the axels enabling the solvent to repeatedly wash over the organic matter performing maceration of organic matter. 1. A temperature controlled plant maceration and extraction system comprising:a cylindrical extraction chamber having a hollow inner volume formed by a first wall, an end cap at an one end of the extraction chamber enabled to accept organic matter into the chamber, and at least one inlet valve at a second end, opposite the one end, enabled to inject a gas or liquid solvent into the inner volume;a hollow temperature jacket formed around the extraction chamber from the first wall and an outer wall defining a space there between that is sealed at the one end and second end; anda frame structure having a first and second pass-through axle, one each fixedly mounted on the jacket at opposite sides of the extraction chamber at a balanced center point along a length between the one end and second end of the extraction chamber, said axles supported by the frame structure enabled to hold the chamber at a height from ground enabling free rotation of the chamber about the axles;wherein organic matter is introduced via the one end, a solvent from a first gas tank is injected into the chamber at the inlet valve on the second end, with the one ...

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Номер записи: 97
27-09-2018 дата публикации

ROSIN-CONTAINING MATERIALS AND METHODS OF MAKING THEREOF

Номер: US20180273801A1
Автор: Nelson Lloyd A., OVERSTREET Tresha Ann, PHUN Lien H., Severance Rachel C., Williams Paul A.
Принадлежит: Arizona Chemical Company, LLC

Provided herein are rosin-containing materials, including crude tall oil (CTO), tall oil rosin (TOR), distilled tall oil (DTO), crude fatty acid (CFA), as well as methods of making thereof. The rosin-containing materials can exhibit improved color (e.g., a reduced Gardner color), reduced sulfur content, improved color stability, or a combination thereof. 189-. (canceled)90. A method of improving the properties of a rosin-containing material comprising contacting the rosin-containing material with a mesoporous adsorbent to form a decolorized rosin-containing material wherein the mesoporous adsorbent comprises:(a) a volume of mesopores of 0.2 mL/g or more;(b) a volume of micropores of from 0.05 mL/g to 0.3 mL/g; and(c) a volume of macropores of from 0.1 mL/g to 0.6 mL/g.91. The method of further comprising improving the color stability of a rosin-containing material to form a decolorized rosin-containing material wherein the decolorized rosin-containing material exhibits less than a 20% increase in Gardner color upon incubation at 23° C. for period of 7 days immediately following formation of the decolorized rosin-containing material.92. The method of claim 90 , wherein the rosin-containing material is selected from the group consisting of crude tall oil (CTO) claim 90 , tall oil rosin (TOR) claim 90 , distilled tall oil (DTO) claim 90 , crude fatty acid (CFA) claim 90 , and tall oil fatty acid (TOFA).93. The method of claim 91 , wherein the decolorized rosin-containing material is CTO and exhibits a Gardner color of 12 or less immediately following formation.94. The method of claim 91 , wherein the decolorized rosin-containing material is TOFA and exhibits a Gardner color of 4 or less immediately following formation.9590. The method of claim 91 , wherein the mesoporous adsorbent comprises an activated carbon or a blend of two or more activated carbons having different average pore sizes.96. The method of claim 90 , wherein contacting the rosin-containing material ...

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Номер записи: 98
27-09-2018 дата публикации

Chemical Additives to Improve Oil Separation in Stillage Process Operations

Номер: US20180273878A1
Автор: "Vant Hul Jason", Eastin Philip, Huang Xiaodong, Wang Xuejun, Xiao Lan
Принадлежит: ECOLAB USA INC.

The invention provides methods and compositions for recovering oil from stillage. The method comprises the addition of a surfactant and a microparticle comprising hydrophilic silica to a grain to ethanol stillage. The methods and compositions of the present invention release oil trapped in solid aggregates, increasing the total amount of oil extracted from the stillage. 1. A method of treating a grain to ethanol process stream comprising stillage and a surfactant , the method comprising adding hydrophilic colloidal silica to the grain to ethanol process stream comprising the stillage and the surfactant to form a treated process stream.2. The method of claim 1 , wherein the stillage is thick stillage.3. The method of claim 1 , wherein the stillage is thin stillage.4. The method of claim 1 , wherein the hydrophilic colloidal silica has a particle size of from about 0.01 to about 500 nm.5. The method of claim 1 , wherein the surfactant is an alkoxylated sorbitan alkylate.6. The method of claim 1 , wherein the surfactant is a polysorbate.7. The method of claim 1 , wherein the surfactant and hydrophilic colloidal silica are present in the treated process stream at a weight ratio of from about 15 to 1 to about 2 to 1.8. The method of claim 1 , wherein the surfactant and hydrophilic colloidal silica are present in the treated process stream at a weight ratio of from about 10 to 1 to about 1 to 1.9. The method of claim 1 , wherein the hydrophilic colloidal silica has an S-value of from about 24% to about 40%.10. The method of claim 1 , further comprising separating oil from the treated process stream.11. The method of claim 1 , wherein the .12. The method of claim 1 , wherein the grain to ethanol process stream is a dissolved air floatation (“DAF”) process stream.13. The method of claim 1 , wherein the hydrophilic colloidal silica has a specific surface area of from about 700 m/g to about 850 m/g.1420-. (canceled)21. The method of claim 1 , wherein the stillage is whole ...

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Номер записи: 99
25-11-2021 дата публикации

Desulfurized Crude Tall Oil Compositions and Processes for Producing

Номер: US20210363464A1
Автор: Lange Jos H.M., Rogers Randy, Steenkamer Sebastiaan J., Swan Francis E.
Принадлежит: Kraton Polymers LLC

A method to produce crude tall oil (CTO) having a reduced sulfur content is disclosed. Black liquor soap (BLS) is treated with 0.05 to 0.45% by weight HO. Hydrogen peroxide treated BLS compositions, CTO compositions, and chemical compositions derived thereof, including depitched CTO, TOP, depitched CTO distillation fractions, and products derived therefrom are disclosed. The use of a small amount of HOresults in a decreased degree of foaming. 1. A method to produce crude tall oil (CTO) comprising:{'sub': 2', '2, 'treating a black liquor soap (BLS) by mixing with 0.05 to 0.45% by weight HO, based on total weight of the BLS for 1 minute to 48 hours at a temperature of 0° C. to 105° C.;'}acidulating the treated BLS to a pH value ranging between 1 to 4, wherein a CTO phase, an aqueous phase and residual solids are formed;maintaining the acidulating temperature in the range of 70 to 103° C.; andseparating the CTO phase from the aqueous phase and from residual solids at a recovery yield of at least 75% CTO based on total weight of anhydrous BLS; andwherein the recovered CTO has a sulfur content of less than 900 ppm.2. The method of claim 1 , wherein the BLS is treated with 0.1 to 0.35% by weight HO claim 1 , at a temperature of 40° C. to 90° C.3. The method claim 2 , wherein the mixture of BLS and HOhas a volume increase of less than 50% during and after the treatment with HO.4. The method of claim 1 , wherein the BLS is treated for 5 minutes to 36 hours.5. The method of claim 1 , wherein the mixture of BLS and HOhas a volume increase of less than 20% during and after the treatment with HO.6. The method of claim 1 , wherein the acidulation temperature is maintained by any of the addition of steam.7. The method of claim 1 , wherein the recovered CTO has a sulfur content that is at least 15% lower than the sulfur content of CTO recovered from a BLS not treated with HO.8. The method of claim 1 , wherein the recovered CTO has an odor intensity reduction of at least 1 unit ...

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Номер записи: 100