09-05-2023 дата публикации
Номер: CN116081691A
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The invention discloses a method for preparing a W18O49/WO3 heterogeneous electrocatalyst by utilizing oxygen deficiency, the electrocatalyst and application, and the method comprises the following steps: respectively weighing tungsten chloride, cuprous oxide and urea, grinding to uniformly mix the tungsten chloride, the cuprous oxide and the urea, then adding the obtained mixture into a methanol solution, and stirring to obtain a uniformly mixed solution; loading the obtained uniformly mixed solution into a lining of a high-pressure kettle, mounting the lining into a stainless steel high-temperature and high-pressure reaction kettle, putting the sealed reaction kettle into an electric blast drying oven, setting parameters, controlling the temperature to be 120-220 DEG C and the reaction time to be 1-36 hours, after the reaction is finished, cooling the hydrothermal kettle to room temperature, disassembling the kettle, and cooling to room temperature; and carrying out suction filtration ...
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