18-04-2023 дата публикации
Номер: CN115974690A
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The present invention relates to the technical field of organic chemical industry, and discloses a 4-acetoxy-2-methyl-2-butene-1-aldehyde preparation method, which comprises: S1, mixing a chloride, urotropine and a water phase, carrying out a reaction for 8 h at a certain temperature, after the reaction is completed, carrying out standing layering, and removing the unreacted chloride to obtain a quaternary ammonium salt solution; s2, adding a certain amount of acid into the quaternary ammonium salt solution to adjust the pH value; s3, adding an organic phase solvent into the quaternary ammonium salt solution, adding a certain amount of a copper catalyst, performing hydrolysis at a certain temperature, and separating an organic phase after the reaction is finished; and S4, adding sodium carbonate with the concentration of 1% into a product obtained in S3 to adjust the product to be neutral, recovering an organic phase, and carrying out reduced pressure distillation to obtain the pentacarbonaldehyde ...
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