11-04-2023 дата публикации
Номер: CN115947370A
Принадлежит:
The invention relates to a method for preparing vanadium oxytrichloride from vanadium-containing refined tailings, which comprises the following steps: 1) carrying out high-temperature treatment on the vanadium-containing refined tailings in the presence of inert gas, and keeping the temperature for a period of time to obtain pretreated refined tailings; (2) the pretreated refined tailings are cooled, and mixed gas of oxygen and chlorine is continuously introduced for a reaction; 3) discharging the reacted mixed gas, and performing low-temperature condensation to obtain condensed liquid, namely crude vanadium oxytrichloride; and 4) filtering the coarse vanadium oxychloride to remove solid impurities to obtain fine vanadium oxychloride. According to the method, common vanadium-containing refined tailings are used as raw materials, low-temperature chlorination vanadium extraction production can be achieved, the problem of process control caused by high-temperature chlorination and the problem ...
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