30-06-2023 дата публикации
Номер: CN116354858A
Принадлежит:
The invention discloses a preparation method of dialkyl polysulfide, which specifically comprises the following steps: adding an alpha-olefin compound, elemental sulfur and a solid catalyst into a No.1 reaction kettle, raising the temperature to 110-130 DEG C in an inert gas atmosphere, and reacting for 8-12 hours; adding an alpha-olefin compound, elemental sulfur and a solid catalyst into the second reaction kettle, transferring the mixed material in the first reaction kettle into the second reaction kettle in an inert gas atmosphere and under a closed condition, raising the temperature to 110-130 DEG C, and reacting for 6-10 hours to obtain the dialkyl polysulfide. According to the method, only olefin and elemental sulfur are used as raw materials, a light-color product can be obtained on the premise that hydrogen sulfide, mercaptan and halogen-containing substances are not used, and the color of the prepared dialkyl polysulfide is basically consistent with that of a product prepared ...
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