25-08-2023 дата публикации
Номер: CN116640592A
Принадлежит:
The invention discloses a preparation method of a mesophase pitch precursor, which comprises the following steps: (1) crushing coal liquefied pitch, mixing with a solvent, heating, stirring and extracting; (2) carrying out centrifugal separation to respectively obtain a supernatant A and a heavy residue A; (3) carrying out high-speed centrifugal separation on the supernatant A to respectively obtain a supernatant B and a heavy residue B; (4) distilling the supernate B to recover the solvent, so as to obtain a mesophase pitch precursor; and (5) simultaneously, mixing the heavy slag A and the heavy slag B, and removing a solvent and volatile matters in a screw rod heating manner to obtain the coal pitch. According to the method, the coal liquefied pitch with high ash content and high quinoline content is taken as a raw material, polycyclic aromatic hydrocarbon is extracted, quinoline heavy slag is separated out, and inorganic ash content is removed through a solvent extraction and centrifugal ...
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