30-06-2023 дата публикации
Номер: CN116359262A
Принадлежит:
The invention discloses an electrolytic polishing method suitable for preparing a zinc and zinc alloy EBSD sample, and relates to an electrolytic polishing method for preparing an EBSD sample. The problems that the reaction rate of zinc and zinc alloy in electrolyte is too high, and corrosion and oxidation are prone to occurring are solved. The method comprises the following steps: grinding and mechanically polishing a to-be-polished surface of a sample; a stainless steel sheet is used as a cathode, a beaker is used as an electrolysis container, electrolyte is poured into the beaker, and the cathode is immersed below the liquid level of the electrolyte; the volume fraction of perchloric acid in the electrolyte is 5%, the volume fraction of methanol is 25-45%, and the balance is n-butyl alcohol; rotating the electrolyte at the temperature of-30 DEG C to-40 DEG C by adopting magnetic stirring; the sample is used as an anode to be placed in an electrolysis container and immersed below the ...
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