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Небесная энциклопедия

Космические корабли и станции, автоматические КА и методы их проектирования, бортовые комплексы управления, системы и средства жизнеобеспечения, особенности технологии производства ракетно-космических систем

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Мониторинг СМИ

Мониторинг СМИ и социальных сетей. Сканирование интернета, новостных сайтов, специализированных контентных площадок на базе мессенджеров. Гибкие настройки фильтров и первоначальных источников.

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Форма поиска

Поддерживает ввод нескольких поисковых фраз (по одной на строку). При поиске обеспечивает поддержку морфологии русского и английского языка
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Применить Всего найдено 544. Отображено 188.
20-09-2003 дата публикации

СПОСОБ ПОКРЫТИЯ ВНУТРЕННИХ СТЕНОК РЕАКТОРНЫХ ТРУБ В РЕАКТОРЕ ПИРОЛИЗА УГЛЕВОДОРОДОВ

Номер: RU2212283C2
Принадлежит: СК КОРПОРЕЙШН (KR)

Способ "on-line" нанесения непрерывной пленки покрытия на внутреннюю стенку реакторной трубы в реакторе пиролиза углеводорода для предотвращения образования и осаждения кокса на внутренних стенках. Этот способ включает стадии осаждения из паровой фазы смешанного раствора алкоксида металла и соединения хрома на внутренних стенках одновременно с введением носителя при расходе 1-5000 кг/ч/змеевик при 600-900oС под давлением 0-3 кг/см2, чтобы сформировать буферный слой на внутренних стенках, осаждение из паровой фазы алкоксида металла в качестве барьера на буферный слой и осаждение из паровой фазы соединения щелочного металла/щелочноземельного металла как такового или в смеси с алкоксидом металла в качестве удаляющего кокс слоя на барьере. Удаляющий кокс слой может быть дополнительно обеспечен на диффузионном барьере. Техническим результатом изобретения является увеличение продолжительности цикла работы реактора, сокращение издержек на сжигание кокса и повышение производительности целевых продуктов ...

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27-04-2012 дата публикации

СИСТЕМА ОКИСЛЕНИЯ С ВНУТРЕННИМ ВТОРИЧНЫМ РЕАКТОРОМ

Номер: RU2448766C2

FIELD: process engineering. SUBSTANCE: invention relates to production of terephthalic acid and reaction system to this end. Oxidation of multiphase reaction medium first part is conducted in reaction first zone selected inside outer reaction vessel. Oxidation of methyl-benzole acid vapors in second part of reaction medium is conducted in second reaction zone selected inside inner reaction vessel. Reaction medium suspension phase part is bled from reaction second zone and directed to further phases for additional treatment. Bubbling reaction column comprises outer reaction vessel and inner reaction vessel arranged, at least, partially inside outer reaction vessel. Inner reaction vessel has one or several holes to directly communicate via fluid first and second reaction zones. Inner reaction vessel has one or several discharge holes for fluid flow from second reaction zone but inhibiting direct communication between said first and second reaction zones. Over 50% of total effective cross-section area defined by direct communication holes falls on top half the inner reaction vessel. EFFECT: higher efficiency of oxidation, smaller amount of impurities. 49 cl, 31 dwg РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 2 448 766 (13) C2 (51) МПК B01J 10/00 (2006.01) C07C 51/265 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ОПИСАНИЕ ИЗОБРЕТЕНИЯ К ПАТЕНТУ (21)(22) Заявка: 2008131949/05, 20.12.2006 (24) Дата начала отсчета срока действия патента: 20.12.2006 (73) Патентообладатель(и): ИСТМАН КЕМИКАЛ КОМПАНИ (US) R U Приоритет(ы): (30) Конвенционный приоритет: 04.01.2006 US 60/756,137 01.03.2006 US 11/365,350 (72) Автор(ы): УАНДЕРЗ Алан Джордж (US), ВУДРАФФ Томас Эрл (US), ШЕППАРД Рональд Бафорд (US), СТРАССЕР Уэйн Скотт (US) (43) Дата публикации заявки: 10.02.2010 Бюл. № 4 2 4 4 8 7 6 6 (45) Опубликовано: 27.04.2012 Бюл. № 12 2 4 4 8 7 6 6 R U (85) Дата начала рассмотрения заявки PCT на национальной фазе: 04.08.2008 C 2 C 2 (56) Список документов, цитированных в отчете о ...

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12-02-2009 дата публикации

VERFAHREN ZUM BETREIBEN EINES RISERREAKTORS

Номер: DE602004018830D1

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30-01-1985 дата публикации

Process and apparatus for obtaining silicon from fluosilicic acid

Номер: GB0002142917A
Принадлежит:

Process for producing low cost, high purity solar grade Si wherein a reduction reaction, preferably the reduction of SiF4, by an alkali metal (Na preferred) is carried out by jetting a spray of reactants into a reaction chamber at a rate and temperature which causes the reaction to take place far enough away from the entry region to avoid plugging of reactants at the entry region and wherein separation in the melt is carried out continuously from the reaction and the Si can be cast directly from the melt.

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02-10-1996 дата публикации

Fast quench reactor and method

Номер: AU0005423596A
Принадлежит:

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25-11-2004 дата публикации

FLUIDIZED BED REACTOR WITH GAS COOLER

Номер: CA0002522674A1

A new reactor apparatus that can be used to carry out chemical reactions in a fluidized catalyst bed at high temperatures with reduced afterburning or other undesirable downstream side reactions. One application is the manufacture of acrylonitrile.

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26-06-2014 дата публикации

CONTROL OF THE VISCOSITY OF REACTION SOLUTIONS IN HYDROFORMYLATION METHODS

Номер: CA0002895375A1
Принадлежит:

The present invention relates to a method and a device for controlling the viscosity of reaction solutions in the hydroformylation of olefin-containing mixtures.

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31-08-1987 дата публикации

PROCEDURE AND MECHANISM FOR THE PRODUCTION OF SILICON FROM SILICON TETRAFLUORIDE.

Номер: CH0000661919A5
Автор: SANJURJO, ANGEL
Принадлежит: STANFORD RES INST INT, SRI INTERNATIONAL

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27-02-2007 дата публикации

СПОСОБ КОНВЕРСИИ ОКСИГЕНАТОВ В ОЛЕФИНЫ В ВЕРТИКАЛЬНОМ РЕАКТОРЕ

Номер: EA0200601209A1
Принадлежит:

В заявке описан способ повышения эффективности взаимодействия между твердыми частицами катализатора и исходным сырьем с одновременным снижением вероятности возникновения нежелательных побочных реакций. Исходное сырье в виде множества отдельных струй взаимодействует с твердыми частицами катализатора в реакторе, который имеет зону реакции с неоднородной структурой потока и зону реакции с однородной структурой потока.

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28-12-2007 дата публикации

СПОСОБ КОНВЕРСИИ ОКСИГЕНАТОВ В ОЛЕФИНЫ В ВЕРТИКАЛЬНОМ РЕАКТОРЕ

Номер: EA0000009365B1

В изобретении описан способ повышения эффективности взаимодействия между твердыми частицами катализатора и исходным сырьем с одновременным снижением вероятности возникновения нежелательных побочных реакций. Исходное сырье в виде множества отдельных струй взаимодействует с твердыми частицами катализатора в реакторе, который имеет зону реакции с неоднородной структурой потока и зону реакции с однородной структурой потока.

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30-12-2011 дата публикации

УПРАВЛЕНИЕ ХИМИЧЕСКИМИ РЕАКТОРАМИ

Номер: EA201170794A1
Принадлежит:

Способ управления одним или более химическими реакторами (12), в котором каждый химический реактор определяет первые потоковые каналы (15) для химического реакционного процесса, расположенные в непосредственной близости ко вторым потоковым каналам (16) для теплопередачи, и каждый химический реактор обеспечен соединениями для текучих сред для получения потоков соответствующих текучих сред через первые потоковые каналы и вторые потоковые каналы; при этом способ включает в себя этапы: выключение потоков текучих сред по меньшей мере через один из первых потоковых каналов и вторых потоковых каналов; последующее изменение соединений для текучих сред и вслед за этим повторное открытие соединений для текучих сред. В химический реакционный процесс, проводимый в реакторах, никаких изменений не вносится. Изменения в соединениях для текучих сред являются предпочтительно такими, чтобы достигнуть изменения направления потока на противоположное. Это может включать в себя поворот реактора (12) на 180° ...

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04-03-2020 дата публикации

MANUFACTURING PROCESS FOR CYCLODEXTRIN DERIVATIVES

Номер: PT0002814849T

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10-06-2010 дата публикации

DEVICE AND METHOD FOR CATALYTIC GAS PHASE REACTIONS AND USE THEREOF

Номер: WO2010063448A1
Принадлежит:

The invention relates to improved reactors for catalytic, exothermal gas phase reactions having an entrance zone (1), a reaction zone (2) comprising at least one catalyst (4) and an outlet zone (3) for the product gas, viewed in the flow direction of a reactant gas comprising at least one oxidizing agent and at least one component to be oxidized. The reactors have means, such as insulating jackets (6) and/or devices for transporting coolant, at least in the region of the entrance zone (1), wherein said coolants reduce the transport of heat generated in the reaction zone (2) into the entrance zone (1) and thus reduce the risks of advanced ignition of the reactant gas mixture used or the development of undesired secondary reactions in the entrance zone (1) and/or wherein the inside walls of the reactor are designed from inert material, at least in the region of the entrance zone (1). The reactant gas enters the entrance zone (1) as a homogenous gas mixture, with regard to the material composition ...

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21-07-2005 дата публикации

METHOD OF OPERATING A RISER REACTOR

Номер: WO2005066312A1
Автор: SMITH, Jeffrey, S.
Принадлежит:

A method for maximizing the contact between solid catalyst particles and a feedstock while minimizing undesirable side reactions is provided. A plurality of feedstock jets are contacted with solid catalyst particles in a reactor having a non–homogenous contact zone and a unified flow contact zone.

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24-11-2005 дата публикации

PROCESS FOR PRODUCING (METH)ACROLEIN OR (METH)ACRYLIC ACID

Номер: WO2005110956A1
Принадлежит:

A process for producing (meth)acrolein or (meth)acrylic acid, in which the operation can be continued without any decomposition reaction of acrolein, etc. There is provided a process for producing (meth)acrolein or (meth)acrylic acid, comprising carrying out a contact vapor-phase oxidation of propylene, propane or isobutylene by oxygen by means of a heat exchange type multitubular reactor including a tube bundle section consisting of a multiplicity of parallel arranged reaction tubes packed with a catalyst and a tube sheet disposed adjacent to understream of the reaction tube bundle section and providing a lead-out part for reaction gas, the reaction tube bundle section as a whole having a hollow cylindrical structure, characterized in that the tube sheet is fitted with a flow straightener.

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21-02-2008 дата публикации

Process for Producing (Meth)Acrolein or (Meth)Acrylic Acid

Номер: US20080045748A1
Принадлежит: MITSUBISHI CHEMICAL CORPORATION

An object of the invention is to provide a production method for (meth)acrolein or (meth)acrylic acid which can continue an operation without causing a decomposition reaction of acrolein or the like. According to the invention, provided is a production method for (meth)acrolein or (meth)acrylic acid, in which (meth)acrolein or (meth) acrylic acid is obtained by performing a catalytic gas phase oxidation on propylene, propane or isobutylene by using oxygen by means of a heat-exchange type multi-tubular reactor, having a tube bundle portion in which a multiple of reaction tubes each filled with a catalyst are aligned in parallel to one another and a tube plate which is adjacent to a downstream side of the tube bundle portion of the reaction tubes and forms a lead-out portion for a reaction gas, in which the tube bundle portion of the reaction tubes has a hollow-columnar constitution as a whole, and which is characterized in that a rectifier is provided on a tube plate.

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07-01-2020 дата публикации

Multitubular reactor for liquid phase alcohol dehydrogenation and method for liquid phase alcohol dehydrogenation

Номер: US0010526267B2
Принадлежит: FuZhou University, UNIV FUZHOU

The invention relates to a multitubular reactor for dehydrogenation of liquid phase alcohol dehydrogenation and a method of liquid phase alcohol dehydrogenation. Most of the alcohol dehydrogenation reaction is endothermic reaction, the reaction temperature is high and the equilibrium conversion rate is low.

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01-03-2016 дата публикации

Process for preparing alkenylhalosilanes and reactor suitable therefore

Номер: US0009272258B2
Принадлежит: EVONIK DEGUSSA GmbH

A process for preparing alkenylhalosilanes by reacting alkenyl halide in the gas phase in a reactor comprising a reaction tube (1) equipped with an inlet (2) at one end of the tube and with an outlet (3) at the other end of the tube, and having a gas inlet device (4) having a plurality of gas feed points (5) that are spaced apart in the direction of the longitudinal axis of the reaction tube (1) and open into the reaction tube (1). The process permits the preparation of alkenylhalosilanes in high yield and with high selectivity. The formation of soot is distinctly lower compared to conventional reactors.

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10-06-2021 дата публикации

FABRICATION PROCESS FOR EFFICIENT VISIBLE LIGHT PHOTOCATALYSTS

Номер: US20210170385A1
Принадлежит:

The present relates to the field of iron-doped TiO2 nanocrystals/photocatalysts and to a method of their production. The method comprising the steps: a) dissolving a compound comprising Fe (III); b) mixing an alcohol to the ferric solution to obtain a mixture; c) adjusting the pH of the mixture by adding a suitable acid to the mixture to obtain an acidic composition; d) producing a gelation reaction by mixing a titanium (IV) complex to the acidic composition, to obtain a dispersion comprising Fe-doped TiO2, e) drying the dispersion, to obtain a dried product substantially free of iron oxide contamination; f) grinding the dried product, to obtain a powder; g) washing the powder with an aqueous liquid, to obtain a washed powder comprising a Fe-doped TiO2 photocatalyst precursor; and h) drying the washed powder, to obtain the Fe-doped TiO2 photocatalyst precursor. The method further comprising calcining and grinding steps.

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07-09-2011 дата публикации

Oxidation system with internal secondary reactor

Номер: EP2363204A2
Принадлежит:

Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

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14-01-1987 дата публикации

REACTION APPARATUS

Номер: JP0062007431A
Принадлежит:

PURPOSE: To minimize the lowering of efficiency due to the interference with the wall surface of a downstream chamber or the diffusion of a stream, by constituting a reaction apparatus by arranging a flow control system by a contraction and expansion nozzle. CONSTITUTION: A flow control system by a contraction and expansion nozzle 1 is arranged to constituted a reaction apparatus and the stream of a stock material or reaction product is formed into a beam state. When the stream from the outflow port 1C of the contraction and expansion nozzle 1 comes to a proper expansion stream, said stream comes to one having speed distribution almost uniform in the cross-sectional direction along the inner wall surface direction of the outflow port 1C of the contraction and expansion nozzle 1 to be formed into a beam like stream. Because the stream is formed into the beam like one and the diffusion thereof is suppressed to a min. degree, the stock material or reaction product injected from the contraction ...

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20-12-2016 дата публикации

СПОСОБ ПОЛУЧЕНИЯ АЛКЕНИЛГАЛОГЕНСИЛАНОВ И ПРИГОДНЫЙ ДЛЯ ЕГО ОСУЩЕСТВЛЕНИЯ РЕАКТОР

Номер: RU2605553C2

Изобретение относится к способам получения алкенилгалогенсиланов. Предложен способ получения алкенилгалогенсиланов путем превращения алкенилгалогенида, выбранного из группы, включающей винилгалогенид, винилиденгалогенид и аллилгалогенид, с галогенсиланом, выбранным из группы, включающей моногалогенсилан, дигалогенсилан и тригалогенсилан, в исходном мольном отношении галогенсилана к алкенилгалогениду между 1,0 и 10 в газовой фазе в реакторе, представляющем собой реакционную трубу (1) с входным отверстием (2) на одном конце и выходным отверстием (3) на другом конце, а также снабженном газоподводящим устройством (4), которое имеет несколько мест ввода газа (5), расположенных вдоль продольной оси реакционной трубы (1) на определенном расстоянии друг от друга и выходящих внутрь реакционной трубы (1). Для осуществления способа моногалогенсилан, дигалогенсилан или тригалогенсилан подают через входное отверстие (2) в реакционную трубу (1), по которой он перемещается в направлении к выходному отверстию ...

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27-10-2015 дата публикации

КОЖУХОТРУБНЫЙ РЕАКТОР ДЛЯ ПОЛУЧЕНИЯ АНГИДРИДА МАЛЕИНОВОЙ КИСЛОТЫ

Номер: RU2566749C2
Принадлежит: БАСФ СЕ (DE)

FIELD: chemistry. SUBSTANCE: invention relates to an apparatus for producing maleic acid anhydride via heterogeneous catalytic gas-phase oxidation of an initials stream containing hydrocarbons with at least 4 carbon atoms per molecule, which includes a reactor with a bundle of reaction tubes in which there is a solid-phase catalyst on which an exothermic reaction of the initial stream and an oxygen-containing stream occurs, one or more pumps and one or more heat exchangers mounted outside the reactor, through which a heat carrier flows, which is a molten salt which follows through the space between the reaction tubes, thereby receiving the reaction heat, wherein temperature of the molten salt lies in the range between 350 and 480°C. The reaction tubes are made of heat-resistant alloy steel containing at least 0.25 wt % molybdenum, or at least 0.5 wt % chromium and at least 0.25 wt % molybdenum. EFFECT: apparatus is characterised by high stability. 5 cl, 4 ex РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (13) 2 566 749 C2 (51) МПК C07C 51/215 (2006.01) C07C 57/145 (2006.01) C07D 307/60 (2006.01) B01J 8/06 (2006.01) B01J 19/00 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ОПИСАНИЕ (21)(22) Заявка: ИЗОБРЕТЕНИЯ К ПАТЕНТУ 2012123724/04, 02.11.2010 (24) Дата начала отсчета срока действия патента: 02.11.2010 Приоритет(ы): (30) Конвенционный приоритет: (72) Автор(ы): ОЛЬБЕРТ Герхард (DE), БАССЛЕР Ханс-Юрген (DE), ШТАЙНИГЕР Михаэль (DE) 10.11.2009 EP 09175466.3 (43) Дата публикации заявки: 20.12.2013 Бюл. № 35 R U (73) Патентообладатель(и): БАСФ СЕ (DE) (45) Опубликовано: 27.10.2015 Бюл. № 30 C 2 C 2 (85) Дата начала рассмотрения заявки PCT на национальной фазе: 13.06.2012 (86) Заявка PCT: EP 2010/066597 (02.11.2010) 2 5 6 6 7 4 9 (87) Публикация заявки PCT: R U 2 5 6 6 7 4 9 (56) Список документов, цитированных в отчете о поиске: US 6803473 B2, 12.10.2004. US 7509928 B2, 02.08.2007. US 2008/0260605 A1, 23.10.2008. WO 2008/000740 A1, 03.01.2008. DE 102007025869 A1, ...

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20-02-2009 дата публикации

СПОСОБ ПОЛУЧЕНИЯ (МЕТ)АКРОЛЕИНА ИЛИ (МЕТ)АКРИЛОВОЙ КИСЛОТЫ

Номер: RU2346735C2

... (Мет)акролеин или (мет)акриловую кислоту получают путем каталитического окисления пропилена, пропана или изобутилена в газовой фазе с использованием молекулярного кислорода. Способ осуществляют в многотрубном реакторе-теплообменнике. Реактор содержит множество параллельно установленных реакционных трубок, каждая из которых заполнена катализатором. К нижней стороне части из пучка труб из реакционных трубок примыкает трубная доска, образуя выводную часть для реакционного газа. Трубная доска снабжена ректификатором. Таким образом обеспечивается беспрерывное протекание реакции без разложения акролеина, что повышает чистоту продукта реакции. 3 з.п. ф-лы, 1 ил.

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10-08-2014 дата публикации

СПОСОБ ПРЕОБРАЗОВАНИЯ УГЛЕРОДА, КРЕКИНГ УГЛЕВОДОРОДОВ И УСТРОЙСТВО ДЛЯ КРЕКИНГА УГЛЕВОДОРОДОВ

Номер: RU2012152275A

1. Способ преобразования углерода в оксид углерода, включающий приведение углерода в контакт с паром в присутствии материала со структурой типа карнегиита, имеющего формулу (NaO)Na[AlSiO], где 0<х≤1.2. Способ по п.1, в котором контакт осуществляют при температуре от приблизительно 400°C до приблизительно 1000°C.3. Способ по п.1, в котором контакт осуществляют при температуре от приблизительно 450°C до приблизительно 950°C.4. Способ по п.1, в котором контакт осуществляют при температуре от приблизительно 500°C до приблизительно 950°C.5. Способ по п.1, в котором контакт осуществляют при температуре от приблизительно 750°C до приблизительно 950°C.6. Способ по п.1, в котором материал со структурой типа карнегиита представляет собой материал формулы NaAlSiO.7. Способ по п.1, в котором материал со структурой типа карнегиита представляет собой смесь материалов формулы (NaO)Na[AlSiO].8. Способ по п.1, в котором оксид углерода включает диоксид углерода.9. Способ по п.8, в котором оксид углерода включает моноксид углерода.10. Способ крекинга углеводородов, включающий приведение по меньшей мере одного углеводорода в контакт с паром в устройстве, содержащем поверхность контакта, доступную по меньшей мере одному углеводороду и включающую материал со структурой типа карнегиита, имеющий формулу (NaO)Na[AlSiO], где 0<х≤1.11. Способ по п.10, в котором материал со структурой типа карнегиита представляет собой материал формулы NaAlSiO.12. Способ по п.10, в котором контакт осуществляют при температуре от приблизительно 500°С до приблизительно 870°С, и где меньшей мере один углеводород включает по меньше мере один из следующих углеводородов: этан, пропан, бутан, гептан, сжиженный нефтяной газ, ли� РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (51) МПК C10G 75/00 (13) 2012 152 275 A (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ЗАЯВКА НА ИЗОБРЕТЕНИЕ (21)(22) Заявка: 2012152275/04, 20.05.2011 (71) Заявитель(и): Дженерал Электрик Компани (US) Приоритет(ы): (30) ...

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10-01-2013 дата публикации

УСТРОЙСТВО И СПОСОБ ДЛЯ КАТАЛИТИЧЕСКИХ ГАЗОФАЗНЫХ РЕАКЦИЙ, А ТАКЖЕ ЕГО ПРИМЕНЕНИЕ

Номер: RU2011127178A
Принадлежит:

... 1. Реактор для каталитических газофазных реакций путем превращения исходного газа в газ-продукт с видимыми в направлении потока исходного газа входной зоной (1), по меньшей мере одной реакционной зоной (2), содержащей катализатор (4), и зоной выхода (3) для газа-продукта, причем через входную зону (1), которая представляет собой полую камеру или камеру, содержащую функциональные встроенные элементы, которые не служат для перемешивания, через один или более подающих трубопроводов (30) подают газовую смесь, гомогенную в отношении состава, которая содержит по меньшей мере один окислитель и по меньшей мере один окисляемый компонент, в качестве исходного газа, и по меньшей мере в области входной зоны (1) или реакционной зоны (2) предусмотрено средство, которое препятствует переносу теплоты реакции, которая образуется в реакционной зоне (2), во входную зону (1) и/или где внутренние стенки реактора по меньшей мере в области входной зоны (1) или в области реакционной зоны (2) изготовлены из инертного ...

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20-06-2008 дата публикации

СПОСОБ ПОЛУЧЕНИЯ (МЕТ)АКРОЛЕИНА ИЛИ (МЕТ)АКРИЛОВОЙ КИСЛОТЫ

Номер: RU2006144102A

1. Способ получения (мет)акролеина или (мет)акриловой кислоты, при котором (мет)акролеин или (мет)акриловую кислоту получают путем осуществления реакции каталитического окисления в газовой фазе пропилена, пропана или изобутилена при использовании молекулярного кислорода с помощью многотрубного реактора типа теплообменника, включающего часть из пучка труб, в которой множество реакционных трубок, каждая из которых заполнена катализатором, установлены параллельно одна другой, и трубной доски, которая примыкает к нижней стороне части из пучка труб из реакционных трубок и образует выводную часть для реакционного газа, в которой часть из пучка труб из реакционных труб имеет полое колоннообразное строение в целом, отличающийся тем, что трубная доска снабжена ректификатором.2. Способ получения (мет)акролеина или (мет)акриловой кислоты по п.1, отличающийся тем, что трубная доска снабжена ректификатором в центральной части.3. Способ получения (мет)акролеина или (мет)акриловой кислоты по п.1, отличающийся тем, что трубная доска снабжена ректификатором по периферической части.4. Способ получения (мет)акролеина или (мет)акриловой кислоты по п.1, отличающийся тем, что трубная доска снабжена ректификаторами в центральной части и по периферической части. ÐÎÑÑÈÉÑÊÀß ÔÅÄÅÐÀÖÈß (19) RU (11) 2006 144 102 (13) A (51) ÌÏÊ C07C 27/14 (2006.01) ÔÅÄÅÐÀËÜÍÀß ÑËÓÆÁÀ ÏÎ ÈÍÒÅËËÅÊÒÓÀËÜÍÎÉ ÑÎÁÑÒÂÅÍÍÎÑÒÈ, ÏÀÒÅÍÒÀÌ È ÒÎÂÀÐÍÛÌ ÇÍÀÊÀÌ (12) ÇÀßÂÊÀ ÍÀ ÈÇÎÁÐÅÒÅÍÈÅ (21), (22) Çà âêà: 2006144102/15, 25.10.2004 (71) Çà âèòåëü(è): ÌÈÖÓÁÈÑÈ ÊÅÌÈÊÀË ÊÎÐÏÎÐÅÉØÍ (JP) (30) Êîíâåíöèîííûé ïðèîðèòåò: 13.05.2004 JP 2004-143305 (43) Äàòà ïóáëèêàöèè çà âêè: 20.06.2008 Áþë. ¹ 17 (87) Ïóáëèêàöè PCT: WO 2005/110956 (24.11.2005) Àäðåñ äë ïåðåïèñêè: 129090, Ìîñêâà, óë. Á.Ñïàññêà , 25, ñòð.3, ÎÎÎ "Þðèäè÷åñêà ôèðìà Ãîðîäèññêèé è Ïàðòíåðû", ïàò.ïîâ. Å.Å.Íàçèíîé R U (57) Ôîðìóëà èçîáðåòåíè 1. Ñïîñîá ïîëó÷åíè (ìåò)àêðîëåèíà èëè (ìåò)àêðèëîâîé êèñëîòû, ïðè êîòîðîì (ìåò)àêðîëåèí èëè (ìåò)àêðèëîâóþ êèñëîòó ïîëó÷àþò ïóòåì ...

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11-06-2003 дата публикации

Slurry phase apparatus having a sparger with a backflow prevention system

Номер: GB0002382786A
Принадлежит:

Slurry phase apparatus 10 is provided which includes a slurry vessel 12 for holding a slurry comprising a liquid and solid particles such as catalyst particles and gas distribution means 14 for injecting a gas into the slurry. The gas distribution means 14 includes a sparger device 20 which includes an apertured sparger portion 24 inside the slurry vessel 12, an inlet portion 22 leading into the slurry vessel 12 and an outlet portion 26 leading from the slurry vessel 12. The gas distribution means 14 also includes closure means such as valve32, external of the slurry vessel 12 and being operable to allow or deny flow from the sparger portion 24 out through the outlet portion 26 of the sparger device 20. When the gas flow to the sparger 24 is interrupted, slurry can be cleared from sparger pipe 20 by establishing a lower pressure in collection vessel 30 and opening valve 32 so that slurry and settled solids are flushed into collection vessel 30. A purge fluid may also be introduced through ...

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03-12-1986 дата публикации

REACTION APPARATUS

Номер: GB0002175708A
Принадлежит:

A reaction apparatus is provided which comprises a flow control system provided with a convergent-divergent nozzle. This nozzle is operated under the optimum expansion condition, and the differential coefficient of the streamline of the channel inside the nozzle varies continuously and reaches zero at a throat of the nozzle.

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15-01-2009 дата публикации

PROCEDURE FOR THE OPERATION OF A RISERREAKTORS

Номер: AT0000419319T
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10-07-2007 дата публикации

THERMAL SYNTHESIS APPARATUS AND METHOD

Номер: CA0002408994C
Принадлежит: BECHTEL BWXT IDAHO, LLC

An apparatus for thermal conversion of one or more reactants to desired end products includes an insulated reactor chamber having a high temperature heater such as a plasma torch at its inlet end and, optionally, a restrictive convergent- divergent nozzle at its outlet end. In a thermal conversion method, reactants are injected upstream from the reactor chamber and thoroughly mixed with the plasma stream before entering the reactor chamber. The reactor chamber has a reaction zone that is maintained at a substantially uniform temperature. The resulting heated gaseous stream is then rapidly cooled by passage through the nozzle, which "freezes" the desired end product(s) in the heated equilibrium reaction stage, or is discharged through an outlet pipe without the convergent-divergent nozzle. The desired end products are then separated from the gaseous stream.

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28-02-2014 дата публикации

ПЕРЕМЕШИВАЮЩЕЕ УСТРОЙСТВО И СПОСОБ СМЕШИВАНИЯ ГАЗА И РАСТВОРА

Номер: EA0000019317B1
Принадлежит: ОТОТЕК ОЮЙ (FI)

Данное изобретение относится к перемешивающему устройству, обеспечивающему высокую перекачивающую способность. Это перемешивающее устройство предназначено для условий, когда обрабатываемый раствор или суспензия трудно поддаются технологической обработке и в них подают газ с целью его равномерного и эффективного распределения в растворе. Способ особенно подходит для гидрометаллургических процессов, в которых необходимо распределить газ в растворе и получить эффективное смешивание на микро- и макроуровне.

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27-07-2015 дата публикации

DEVICE AND METHOD FOR CATALYTIC GAS PHASE REACTIONS AND USE THEREOF

Номер: UA0000109106C2
Автор:
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31-08-2017 дата публикации

METHOD FOR CARRYING OUT EXOTHERMIC CATALYTIC REACTIONS AND A REACTOR FOR USE IN THE METHOD

Номер: EA0000027600B1
Принадлежит:

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30-12-2011 дата публикации

ПЕРЕМЕШИВАЮЩЕЕ УСТРОЙСТВО И СПОСОБ СМЕШИВАНИЯ ГАЗА И РАСТВОРА

Номер: EA0201100453A1
Принадлежит:

Данное изобретение относится к перемешивающему устройству, обеспечивающему высокую перекачивающую способность. Это перемешивающее устройство предназначено для условий, когда обрабатываемый раствор или суспензия трудно поддаются технологической обработке, и в них подают газ с целью его равномерного и эффективного распределения в растворе. Способ особенно подходит для гидрометаллургических процессов, в которых необходимо распределить газ в растворе и получить эффективное смешивание на микро- и макроуровне.

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31-03-2014 дата публикации

METHOD OF EXOTHERMIC CATALYTIC REACTIONS AND REACTOR, USED IN METHOD

Номер: EA0201490002A1
Автор:
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21-01-2014 дата публикации

OXIDATION SYSTEM WITH INTERNAL SECONDARY REACTOR

Номер: KR1020140008472A
Автор:
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29-07-2021 дата публикации

SOLUTION POLYMERIZATION PROCESS

Номер: SG11202105884XA
Принадлежит:

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19-07-2007 дата публикации

OXIDATION SYSTEM EMPLOYING INTERNAL STRUCTURE FOR ENHANCED HYDRODYNAMICS

Номер: WO000002007081513A1
Принадлежит:

Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

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22-04-1986 дата публикации

Process and apparatus for obtaining silicon from fluosilicic acid

Номер: US0004584181A1
Принадлежит: SRI International

An apparatus for producing low cost, high purity solar grade Si wherein a reduction reaction, preferably the reduction of SiF4, by an alkali metal (Na preferred) is carried out inside a reaction chamber. The chamber wall and bottom surfaces are formed of graphite and configured with drainage channels so as to facilitate the continuous separation of the products of reaction (Si and NaF) and removal of the molten salt by discharging the salt through one or more ports at the bottom of the reaction chamber. Such process is especially useful where it is desirable to discharge the reaction salt products from the reactor and retain silicon within the chamber for later removal.

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28-12-2021 дата публикации

Manufacturing process for cyclodextrin derivatives

Номер: US0011208500B2
Принадлежит: CyDex Pharmaceuticals, Inc.

A process and equipment assembly for reacting a substituent precursor with a cyclodextrin starting material to provide a raw product comprising a cyclodextrin derivative and 1% or less of an initial amount of the substituent precursor is provided. The process of the present invention provides cyclodextrin derivatives in substantially shorter time and with fewer side products than previous processes that utilize substantially the same starting materials.

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23-06-2005 дата публикации

Method of operating a riser reactor

Номер: US20050137439A1
Автор: Jeffrey Smith
Принадлежит:

A method for maximizing the contact between solid catalyst particles and a feedstock while minimizing undesirable side reactions is provided. A plurality of feedstock jets are contacted with solid catalyst particles in a reactor having a non-homogenous contact zone and a unified flow contact zone.

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22-01-1992 дата публикации

Номер: JP0004003254B2
Автор:
Принадлежит:

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27-01-2016 дата публикации

СПОСОБ ПРЕОБРАЗОВАНИЯ УГЛЕРОДА, КРЕКИНГ УГЛЕВОДОРОДОВ И УСТРОЙСТВО ДЛЯ КРЕКИНГА УГЛЕВОДОРОДОВ

Номер: RU2573833C2

FIELD: chemistry. SUBSTANCE: invention relates to method for transformation of carbon into carbon oxide. Claimed method includes bringing carbon in contact with vapour in presence of material with carnegieite-type structure, which has formula (Na 2 O) x Na 2 [Al 2 Si 2 O 8 ], wherein 0<x≤1. Invention also relates to method for cracking hydrocarbons and to device for cracking of hydrocarbons. EFFECT: claimed method makes it possible to effectively reduce amount of coke deposits. 20 cl, 4 dwg, 2 tbl, 4 ex РОССИЙСКАЯ ФЕДЕРАЦИЯ ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ОПИСАНИЕ (21)(22) Заявка: (19) RU (11) (51) МПК C10G 75/04 C01B 31/18 C01B 31/20 C01B 13/32 C10G 9/12 C10G 9/36 C01B 33/32 (13) 2 573 833 C2 (2006.01) (2006.01) (2006.01) (2006.01) (2006.01) (2006.01) (2006.01) ИЗОБРЕТЕНИЯ К ПАТЕНТУ 2012152275/04, 20.05.2011 (24) Дата начала отсчета срока действия патента: 20.05.2011 Приоритет(ы): (30) Конвенционный приоритет: (43) Дата публикации заявки: 10.08.2014 Бюл. № 22 (45) Опубликовано: 27.01.2016 Бюл. № 3 (73) Патентообладатель(и): Дженерал Электрик Компани (US) (86) Заявка PCT: C 2 C 2 (85) Дата начала рассмотрения заявки PCT на национальной фазе: 28.01.2013 US 2011/037288 (20.05.2011) (87) Публикация заявки PCT: 2 5 7 3 8 3 3 WO 2012/003055 (05.01.2012) R U 2 5 7 3 8 3 3 (56) Список документов, цитированных в отчете о поиске: US 3733186 A, 15.05.1973. SU 965360 A3, 07.10.1982. US 2009/0166259 A1, 02.07.2009. R.KLINGENBERG ET AL., Interstitial Cristobalite-type Compounds (Na2O)<=0.33Na [AlSiO4], JOURNAL OF SOLID STATE CHEMISTRY, 1986, vol.61, pp.40-46. R U 28.06.2010 CN 201010212803.5 (72) Автор(ы): ДЭН Чжиган (CN), ПЭН Вэньцин (US), ЛИНЬ Чуань (CN), ВАН Шичжун (US), ФУ Цицзя (US), ГУ Яньфэй (US), ВУ Чжаопин (US), ЛЯН Янган (US), ШЭ Минган (US) Адрес для переписки: 191036, Санкт-Петербург, а/я 24, "НЕВИНПАТ" (54) СПОСОБ ПРЕОБРАЗОВАНИЯ УГЛЕРОДА, КРЕКИНГ УГЛЕВОДОРОДОВ И УСТРОЙСТВО ДЛЯ КРЕКИНГА УГЛЕВОДОРОДОВ (57) Реферат: Изобретение относится к ...

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20-05-2011 дата публикации

СИСТЕМА ОКИСЛЕНИЯ, ИСПОЛЬЗУЮЩАЯ ВНУТРЕННЮЮ КОНСТРУКЦИЮ ДЛЯ УЛУЧШЕНИЯ ГИДРОДИНАМИКИ

Номер: RU2418629C2

Изобретение может быть использовано в химической промышленности для получения композиции поликарбоновых кислот. Барботажная реакторная колонна 600 включает внешнюю реакционную емкость и внутреннюю конструкцию 602, по меньшей мере, частично расположенную во внешней реакционной емкости. Зона реакции расположена внутри внешней реакционной емкости и вне внутренней конструкции 602. Зона покоя расположена внутри внутренней конструкции 602. Зона покоя включает в себя, по меньшей мере, один участок, который отстоит от зоны реакции на расстояние, равное приблизительно 0,2 метра или кратное максимальному горизонтальному диаметру внешней реакционной емкости с кратностью 0,05. Изобретение позволяет облегчить проведение реакций жидкофазного окисления. 3 н. и 37 з.п. ф-лы, 41 ил., 4 табл. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 2 418 629 (13) C2 (51) МПК B01J 10/00 (2006.01) B01J 8/22 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ОПИСАНИЕ ИЗОБРЕТЕНИЯ К ПАТЕНТУ (21)(22) Заявка: 2008131950/05, 20.12.2006 (24) Дата начала отсчета срока действия патента: 20.12.2006 (73) Патентообладатель(и): ИСТМАН КЕМИКАЛ КОМПАНИ (US) 2 4 1 8 6 2 9 (43) Дата публикации заявки: 10.02.2010 Бюл. № 4 (45) Опубликовано: 20.05.2011 Бюл. № 14 (56) Список документов, цитированных в отчете о поиске: GB 1301291 A, 29.12.1972. WO 2004058377 A1, 15.07.2004. SU 1012967 A, 23.04.1983. SU 1142159 A, 28.02.1985. 2 4 1 8 6 2 9 R U (86) Заявка PCT: US 2006/048644 (20.12.2006) C 2 C 2 (85) Дата начала рассмотрения заявки PCT на национальной фазе: 04.08.2008 (87) Публикация заявки РСТ: WO 2007/081513 (19.07.2007) Адрес для переписки: 129090, Москва, ул. Б.Спасская, 25, стр.3, ООО "Юридическая фирма Городисский и Партнеры", пат.пов. Е.Е.Назиной (54) СИСТЕМА ОКИСЛЕНИЯ, ИСПОЛЬЗУЮЩАЯ ВНУТРЕННЮЮ КОНСТРУКЦИЮ ДЛЯ УЛУЧШЕНИЯ ГИДРОДИНАМИКИ (57) Реферат: Изобретение может быть использовано в химической промышленности для получения композиции поликарбоновых кислот. Барботажная реакторная ...

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15-05-2017 дата публикации

РЕАКТОР И СПОСОБ ДЛЯ НЕПРЕРЫВНОЙ ПОЛИМЕРИЗАЦИИ

Номер: RU2619273C2

Изобретение относится к реактору в виде трубы и способу для непрерывной полимеризации. Реактор имеет корпус в форме трубы. Корпус реактора имеет проходящий по направлению течения вдоль геометрической центральной оси привод. Привод выполнен как центральный вал. Внутри корпуса реактора расположен с возможностью вращения скребок или очиститель, причем скребок или очиститель имеет по меньшей мере одну лопасть скребка или очистителя для прохождения вдоль внутренней стенки корпуса реактора. Корпус реактора имеет по меньшей мере один впуск и один выпуск. Выпуск выполнен таким образом, что выпускное отверстие расположено в основном по касательной к направлению вращения привода. Технический результат – влияние на условия реакции полимеризации, в частности установление желательного распределения по молекулярной массе посредством контроля времени пребывания. 2 н. и 25 з.п. ф-лы, 13 ил., 1 пр.

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10-02-2010 дата публикации

СИСТЕМА ОКИСЛЕНИЯ С ВНУТРЕННИМ ВТОРИЧНЫМ РЕАКТОРОМ

Номер: RU2008131949A
Принадлежит:

... 1. Способ получения композиции поликарбоновых кислот, при этом упомянутый способ включает ! (а) проведение для первой части многофазной реакционной среды окисления в первой зоне реакции, определенной внутри внешней реакционной емкости; ! (b) проведение для второй части упомянутой многофазной реакционной среды окисления во второй зоне реакции, определенной внутри внутренней реакционной емкости, где упомянутая внутренняя реакционная емкость, по меньшей мере, частично расположена в упомянутой внешней реакционной емкости; и ! (с) отбор, по меньшей мере, части фазы суспензии упомянутой реакционной среды из упомянутой второй зоны реакции с отправлением на последующие стадии технологической схемы для дополнительной переработки, где упомянутая фаза суспензии включает твердую и жидкую фазы. ! 2. Способ по п.1, дополнительно включающий введение ароматического соединения в упомянутую первую зону реакции, где, по меньшей мере, приблизительно 80 мас.% упомянутого ароматического соединения, вводимого ...

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27-03-2008 дата публикации

Ventil zum Einspeisen von Lösungen in Kristallisationsanlagen

Номер: DE102006047068A1
Принадлежит:

Die Erfindung betrifft ein Ventil mit mindestens einem Austrittsteil zum Eindüsen einer ersten Lösung in eine zweite Lösung, wobei das mindestens eine Austrittsteil (2) des Ventils (1) im Betriebszustand in der Strömung der zweiten Lösung angeordnet ist und von dieser umspült wird. Die Erfindung betrifft ebenfalls die Verwendung des Ventils in einer Kristallisationsanlage, eine Kristallisationsanlage und ein Verfahren zur kontinuierlichen Kristallisation.

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11-03-2004 дата публикации

Verfahren und Vorrichtung zum intermolekularen Transfer von Aktivierungsenergie zur Bindungsspaltung durch den Raum

Номер: DE0010237704A1
Принадлежит:

Die vorliegende Erfindung betrifft ein Verfahren zur Spaltung chemischer Bindungen, wobei die Aktivierungsenergie zur Bindungsspaltung durch den Raum von einem Trägermolekül geliefert wird, das von seinem Grundzustand in einen angeregten Zustand wechseln kann, indem es mit elektromagnetischer Strahlung bestrahlt wird. DOLLAR A Weiterhin betrifft die vorliegende Erfindung eine Vorrichtung für den intermolekularen Transfer der Aktivierungsenergie zur Bindungsspaltung von Trägermolekülen zu Zielmolekülen, die die zu spaltende Bindung enthalten, umfassend einen Vorratsbehälter, der die Trägermoleküle enthält, Mittel (113) zum Transport der Trägermoleküle durch einen Aktivierungsbereich (104), Aktivierungsmittel (102) und einen Austauschbereich (101), der das Zielmolekül enthält. Weiterhin betrifft die vorliegende Erfindung die Verwendung des erfindungsgemäßen Verfahrens und die Ausführung der lichtgesteuerten in-situ-Synthese in 5' nach 3' oder 3' nach 5' Richtung von Nukleinsäurederivaten ...

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08-08-1984 дата публикации

OBTAINING SILICON FROM FLUOSILICIC ACID

Номер: GB0008417388D0
Автор:
Принадлежит:

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14-08-1990 дата публикации

REACTION APPARATUS

Номер: CA1272661A
Принадлежит: CANON KK, CANON KABUSHIKI KAISHA

A reaction apparatus is provided which comprises a flow control system provided with a convergent-divergent nozzle. This nozzle is operated under the optimum expansion condition, and the differential coefficient of the streamline of the channel inside the nozzle varies continuously and reaches zero at a throat of the nozzle.

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20-08-2019 дата публикации

REACTION PROCESS WITH MEMBRANE SEPARATION

Номер: CA0002961693C
Принадлежит: VITO NV

Provided herein are processes for carrying out a chemical reaction of a substrate in a diluted reaction mixture. The processes comprise the conducting the reaction mixture comprising reaction product and solvent to a filtration membrane which is permeable to the solvent impermeable to the reaction product; and recycling solvent which permeates the filtration membrane for dilution of the substrate feed.

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05-07-2012 дата публикации

REACTOR AND METHOD FOR CONTINUOUS POLYMERIZATION

Номер: CA0002823101A1
Принадлежит:

The present invention relates to a reactor (10) and a method for continuous polymerization, the reactor (10) having a substantially tubular reactor housing (16). The reactor housing (16) has a drive (38) which runs along the geometric central axis (12) in the flow direction (22) and is configured as a central shaft. A rotatably arranged scraper or wiper (36) is provided within the reactor housing (16), the scraper or wiper (36) having at least one scraper or wiper blade (42) to run along an inner side (44) of the reactor housing (16). The rotational movement of the scraper or wiper (36) results in radial mixing of a flow within the reactor housing (16), which flow dominates gravity effects and, as a result of shaping of the scrapers or wipers, optionally makes possible plug flow, a loop flow or backflow within the reactor (10) or also via an additional external pumped circulation system (23). This allows the reaction conditions in the axial direction of the reactor housing (16) to be predicted ...

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22-04-2010 дата публикации

MIXER AND METHOD FOR MIXING A GAS AND SOLUTION

Номер: CA0002739043A1
Принадлежит:

The invention relates to a mixer providing a powerful pumping capacity. The mixer is intended for conditions in which the solution or slurry to be processed is difficult to treat and into which gas is conducted with the intention of dispersing it evenly and effectively into the solution. The method is especially suited to a hydrometallurgical process, whereby the purpose is to disperse the gas into the solution and obtain effective mixing both on the micro- and macro-level.

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30-06-1997 дата публикации

PRODUCTION OF TEREPHTHALIC ACID WITH EXCELLENT OPTICAL PROPERTIES THROUGH THE USE OF PURE OR NEARLY PURE OXYGEN AS THE OXIDANT IN P-XYLENE OXIDATION

Номер: CA0002194034A1
Принадлежит: Praxair Technology Inc

The production of terephthalic acid by the oxidation of p-xylene is carried out in such a manner that the oxygen concentration in the liquid phase is maximized through the use of pure or nearly pure oxygen, while simultaneously the hydrocarbon feed concentration is minimized through rapid dilution with the reactor contents.

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12-03-2019 дата публикации

Method and apparatus to reduce contamination of particles in a fluidized bed reactor

Номер: CN0109453729A
Принадлежит:

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14-11-2012 дата публикации

Oxidation system employing internal structure for enhanced hydrodynamics

Номер: CN101360553B
Принадлежит: Eastman Chemical Co

本发明公开了用于更有效和更经济地进行可氧化的化合物的液相氧化的优化方法和装置。该液相氧化在鼓泡塔反应器中进行,该反应器在相对低的温度下提供了高效的反应。当氧化的化合物为对-二甲苯且氧化反应的产物为粗制对苯二甲酸(CTA)时,该CTA产物可以通过相对于如果采用常规高温氧化方法来形成CTA时可以采用的技术更经济的技术来纯化和分离。

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09-01-2018 дата публикации

Tube bundle reactor

Номер: CN0103846062B
Автор:
Принадлежит:

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25-04-2003 дата публикации

Electrical heating to assist exothermic oxidation and endothermic pyrolysis reactions at high temperatures in a continuous flow hydrocarbon reforming reactor

Номер: FR0002831154A1
Принадлежит: PHYSIQUES ECP ET CHIMIQUES

The exothermic reaction is assisted by an electrical heater, raising the temperature in one zone of the reactor to up to 1250 deg C. The high temperature zone of the reactor contains a solid body (8) which is hot enough to ensure both a quick reaction and favorable thermodynamic conditions for the reactions to be achieved in a relatively small reformer. The exothermic reaction is assisted by an electrical heater, raising the temperature in one zone of the reactor to up to 1250 deg C. The high temperature zone of the reactor contains a solid body (8) which is hot enough to ensure both a quick reaction and favorable thermodynamic conditions for the reactions to be achieved in a relatively small reformer. The solid body is made of granular and/or porous refractory material, such as mineral or synthetic grains, metal wires or rods, or a metal or ceramic honeycomb. The material acts as a contact surface for the pyrolysis and/or partial oxidation of the hydrocarbon. The reactor contains an internal heat exchanger to increase the temperature in the reaction zone and of the body. The intrinsic inefficiency of the exchanger is corrected by adding heat which can be rapidly controlled by a local supply of electrical energy using the Joule effect as the electrical current passes across a resistance placed in the zone and the body. The heat exchanger also cools the flow leaving the body in the tube (2) and the surface of the exchanger is augmented by a structure (12) which may be in the form of conducting fins. The energy exchange is also increased by the turbulence around entering and leaving fluids. Thermal insulation (13) is placed around the reactor to conserve heat so the reactor can operate in quasi adiabatic conditions. The reactor is tubular, approximately 0.25 m diameter and 3 m high, and able to resist pressures of up to 4MPa.

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05-09-2013 дата публикации

REACTOR AND METHOD FOR CONTINUOUS POLYMERIZATION

Номер: KR1020130099222A
Автор:
Принадлежит:

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17-02-2006 дата публикации

REACTOR APPARATUS

Номер: KR1020060015596A
Принадлежит:

A new reactor apparatus that can be used to carry out chemical reactions in a fluidized catalyst bed at high temperatures with reduced afterburning or other undesirable downstream side reactions. © KIPO & WIPO 2007 ...

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17-06-2010 дата публикации

CHEMICAL REACTOR OPERATION

Номер: WO2010067097A3
Автор: WEST, David James
Принадлежит:

A method of operation of one or more chemical reactors (12), wherein each chemical reactor defines first flow channels (15) for a chemical reaction process in proximity to second flow channels (16) for heat transfer, and each chemical reactor is provided with fluid connections for bringing about flows of respective fluids through the first flow channels and the second flow channels, involves the steps of shutting down the flows of fluids through at least one of the first flow channels and the second flow channels, and then changing the fluid connections, and then reopening the fluid connections. There is no change in the chemical reaction process performed by the reactors. The change to the fluid connections is preferably such as to achieve a flow reversal. This may involve turning the reactor (12) itself around, or changing the arrangement of ducts connected to the reactor. This changes the thermal stress distribution within the reactor, and can consequently increase the reactor's operational ...

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26-02-2004 дата публикации

METHOD AND DEVICE FOR THE INTERMOLECULAR TRANSPORT OF BOND CLEAVAGE ACTIVATION ENERGY THROUGH SPACE

Номер: WO2004016349A2
Автор: STENGELE, Klaus-Peter
Принадлежит:

The present invention relates to a method for cleaving chemical bonds whereby the activation energy for bond cleavage is delivered through space by a carrier molecule, which can be switched from its ground state to an excited state upon irradiation. Furthermore, the present invention relates to a device for the intermolecular transfer of bond cleavage activation energy from carrier molecules to target molecules of the bond to be cleaved comprising a storage tank, comprising said carrier molecules, means (113) for delivering said carrier molecules through an activation area (104), activation means (102) and an exchange area (101) comprising the target molecule. Furthermore, the present invention addresses the use of the method according to the invention for effecting the light-addressed 5' to 3' or 3' to 5' in-situ synthesis of nucleic acid derivatives on solid supports for the production of biochips or genechips.

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21-10-2004 дата публикации

Thermal synthesis apparatus

Номер: US20040208805A1
Принадлежит:

An apparatus for thermal conversion of one or more reactants to desired end products includes an insulated reactor chamber having a high temperature heater such as a plasma torch at its inlet end and, optionally, a restrictive convergent-divergent nozzle at its outlet end. In a thermal conversion method, reactants are injected upstream from the reactor chamber and thoroughly mixed with the plasma stream before entering the reactor chamber. The reactor chamber has a reaction zone that is maintained at a substantially uniform temperature. The resulting heated gaseous stream is then rapidly cooled by passage through the nozzle, which “freezes” the desired end product(s) in the heated equilibrium reaction stage, or is discharged through an outlet pipe without the convergent-divergent nozzle. The desired end products are then separated from the gaseous stream.

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20-03-1990 дата публикации

Reaction apparatus which introduces one reacting substance within a convergent-divergent nozzle

Номер: US0004909914A1
Принадлежит: Canon Kabushiki Kaisha

A reaction apparatus is provided which comprises a flow control system provided with a convergent-divergent nozzle. This nozzle is operated under the optimum expansion condition, and the differential coefficient of the streamline of the channel inside the nozzle varies continuously and reaches zero at a throat of the nozzle.

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28-01-2020 дата публикации

Flow reactor

Номер: US0010543474B2
Принадлежит: KANEKA CORPORATION, KANEKA CORP

A flow reactor having two or more raw material feeding units, a mixing unit to mix raw materials fed from the raw material feeding units, and a reactor unit in which a mixed solution prepared in the mixing unit flows, wherein at least a part of an inner wall of the reactor unit is formed of a fluororesin containing a conductive filler.

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10-09-2016 дата публикации

СПОСОБ ПОЛУЧЕНИЯ АЛКЕНИЛГАЛОГЕНСИЛАНОВ И ПРИГОДНЫЙ ДЛЯ ЕГО ОСУЩЕСТВЛЕНИЯ РЕАКТОР

Номер: RU2015105915A
Принадлежит: Эвоник Индустрис Аг

1. Способ получения алкенилгалогенсиланов путем превращения алкенилгалогенида, выбранного из группы, включающей винилгалогенид, винилиденгалогенид или аллилгалогенид с галогенсиланом, выбранным из группы, включающей моногалогенсилан, дигалогенсилан или тригалогенсилан, в газовой фазе в реакторе, представляющем собой реакционную трубу (1) с входным отверстием (2) на одном конце и выходным отверстием (3) на другом конце, а также снабженном газоподводящим устройством (4), которое имеет несколько мест ввода газа (5), упорядоченных вдоль продольной оси реакционной трубы (1) на определенном расстоянии друг от друга и выходящих внутрь реакционной трубы (1), причем подаваемый в реакционную трубу (1) через входное отверстие (2) моногалогенсилан, дигалогенсилан или тригалогенсилан образует перемещающийся через реакционную трубу (1) в направлении к выходному отверстию (3) газовый поток, в который через места ввода газа (5) осуществляют дробную подачу винилгалогенида, винилиденгалогенида или аллилгалогенида.2. Способ по п. 1, отличающийся тем, что в качестве алкенилгалогенида используют винилхлорид, винилбромид, винилиденхлорид, винилиденбромид, аллилхлорид или аллилбромид, особенно винилхлорид или аллилхлорид, а в качестве галогенсилана -дихлорсилан, или трихлорсилан, или дибромсилан, или трибромсилан, предпочтительно дихлорсилан или трихлорсилан.3. Способ по п. 1, отличающийся тем, что в качестве алкенилгалогенида используют винилхлорид или аллилхлорид, а в качестве галогенсилана трихлорсилан.4. Способ по п. 1, отличающийся тем, что через входное отверстие (2) подают только моногалогенсилан, дигалогенсилан или тригалогенсилан, в то время как алкенилгалогенид РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (51) МПК C07F 7/12 (11) (13) 2015 105 915 A (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ЗАЯВКА НА ИЗОБРЕТЕНИЕ (21)(22) Заявка: 2015105915, 28.05.2013 (71) Заявитель(и): ЭВОНИК ИНДУСТРИС АГ (DE) Приоритет(ы): (30) Конвенционный приоритет: 24.07.2012 DE 102012212915.4 (85 ...

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10-02-2010 дата публикации

СИСТЕМА ОКИСЛЕНИЯ, ИСПОЛЬЗУЮЩАЯ ВНУТРЕННЮЮ КОНСТРУКЦИЮ ДЛЯ УЛУЧШЕНИЯ ГИДРОДИНАМИКИ

Номер: RU2008131950A
Принадлежит:

... 1. Способ получения композиции поликарбоновых кислот, при этом упомянутый способ включает ! (а) проведение для многофазной реакционной среды окисления в зоне реакции барботажной реакторной колонны, где упомянутая барботажная реакторная колонна включает внешнюю реакционную емкость и, по меньшей мере, одну внутреннюю конструкцию, по меньшей мере, частично расположенную в упомянутой внешней реакционной емкости; и ! (b) во время проведения стадии (а) использование упомянутой внутренней конструкции для определения одной или нескольких зон покоя в упомянутой барботажной реакторной колонне, где упомянутая внутренняя конструкция включает прямостоячие внутренние боковые стенки, которые по существу окружены упомянутой реакционной средой, где каждая из упомянутых зон покоя включает в себя, по меньшей мере, одну позицию, которая отстоит от упомянутой зоны реакции на расстояние, равное, по меньшей мере, приблизительно 0,2 м или кратное максимальному горизонтальному диаметру упомянутой зоны реакции с ...

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24-01-1985 дата публикации

Номер: DE0003390373T1
Автор:
Принадлежит:

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14-03-2019 дата публикации

Reaction process with membrane separation

Номер: AU2015316862B2
Принадлежит: Griffith Hack

Provided herein are processes for carrying out a chemical reaction of a substrate in a diluted reaction mixture. The processes comprise the conducting the reaction mixture comprising reaction product and solvent to a filtration membrane which is permeable to the solvent impermeable to the reaction product; and recycling solvent which permeates the filtration membrane for dilution of the substrate feed.

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14-08-1990 дата публикации

REACTION APPARATUS

Номер: CA0001272661A1
Принадлежит:

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08-06-2017 дата публикации

MULTI-VALVE UNI-DIRECTION BLOWDOWN SYSTEM FOR A HIGH PRESSURE TUBULAR REACTOR

Номер: CA0002950545A1
Принадлежит:

Provided herein is a unidirectional blow down system for a high-pressure tubular reactor with a hyper that minimizes the tube wall metal temperature during a decomposition event wherein the system prevents the reactor walls from reaching a temperature capable of causing the tube metal to austenize. Also provided are methods of designing and methods of operating a unidirectional blowdown system.

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19-09-1996 дата публикации

FAST QUENCH REACTOR AND METHOD

Номер: CA0002215324A1
Принадлежит:

A fast quench reaction includes a reactor chamber having a high temperature heating means such as a plasma torch at its inlet and a restrictive convergentdivergent nozzle at its outlet end. Reactants are injected into the reactor chamber. The resulting heated gaseous stream is then rapidly cooled by passage through the nozzle. This "freezes" the desired end product(s) in the heated equilibrium reaction stage.

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31-12-1997 дата публикации

METHOD OF MANUFACTURING A DRY POWDER PARTICLE, A POWDER PRODUCED WITH SAID METHOD, AND AN ELECTRODE AND AN APPARATUS FOR USE IN SAID METHOD

Номер: CA0002259253A1
Принадлежит:

The invention relates to a method of manufacturing a dry powder particle, preferably using electrohydrodynamic spraying, wherein two oppositely charged aerosol streams are contacted. The invention allows for the manufacture of powders having various, controllable compositions and shapes. In particular the method according to the invention may be used to perform physical and chemical reactions and allows for the manufacture of powders not previously obtainable. In addition, the invention also relates to an electrode (4, 4', 5, 10a, 10b) and an apparatus for applying the method according to the invention.

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08-07-2015 дата публикации

Vapor-grown graphite fiber composition production system

Номер: CN204455392U
Принадлежит:

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17-07-1981 дата публикации

DISPOSITIF D'ATOMISATION D'UN MELANGE REACTIONNEL

Номер: FR0002473360A
Принадлежит:

La présente invention concerne un dispositif d'atomisation d'un mélange réactionnel. Ce dispositif d'atomisation permet la pulvérisation du mélange réactionnel du réacteur 20 à l'aide d'au moins un premier gaz 8 et d'une buse d'atomisation 12. Ce dispositif comprend de plus une alimentation en un deuxième gaz chaud 22, situé au sommet du dispositif d'atomisation 14 ou 16, servant au séchage du mélange atomisé, une alimentation en un troisième gaz 26 et des moyens de distribution 27 de ce troisième gaz tel qu'il soit distribué dans le réacteur 20 sous la forme d'une couronne, le long de la paroi interne 24 du réacteur 20, de façon à éviter tout contact entre le mélange réactionnel et ladite paroi. Application à la pulvérisation d'un mélange réactionnel. (CF DESSIN DANS BOPI) ...

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06-02-2004 дата публикации

ELECTRIC ASSISTANCE WITH the REFORMING Of a HYDROCARBON MATTER

Номер: FR0002831154B1
Принадлежит:

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20-12-2012 дата публикации

METHOD FOR CARRYING OUT EXOTHERMIC CATALYTIC REACTIONS AND A REACTOR FOR USE IN THE METHOD

Номер: WO2012172065A1
Автор: THORHAUGE, Max
Принадлежит:

Method and a reactor for performing exothermic catalytic reactions. The method comprises the steps of providing a feed gas stream comprising reactants for the exothermic catalytic reaction to a fixed bed catalytic reactor comprising one or more catalyst beds each with catalyst particles filled sections with a catalyst volume; providing a feed gas bypass inside the reactor by arranging within at least one of the catalyst beds a number of bypass passageways without catalytic active particles inside the passageways and having a cooling surface area; passing a part of the feed gas stream through the bypass passageways and reminder of the stream through the catalyst particles filled sections; and removing heat from the feed gas stream being passed through the catalyst filled sections by indirect heat transfer to the part of the feed gas stream being passed through the bypass passageways.

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29-11-2007 дата публикации

Reactor Comprising a Heat Exchanger Area Comprising an Insert

Номер: US2007274882A1
Принадлежит:

The invention relates to a reactor at least comprising, connected with each other in fluid-communicating fashion: a reaction area, whereby the reaction area comprises at least one solid-state catalyst; a coolable heat exchanger area, whereby the heat exchanger area comprises at least one housing, whereby the housing accommodates at least partially an insert, whereby the insert comprises a plurality of elements, a process for oxidation of a hydrocarbon using the reactor, an oxidized hydrocarbon product obtainable by this process, chemical products, such as fibers, sheets, formed bodies and the like based on this oxidized hydrocarbon product as well as the use of this oxidized hydrocarbon product in chemical products of this type.

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01-08-2007 дата публикации

Distributor for delivery in pairs of two liquids to a plurality of feed-in locations in a reactor or a column

Номер: EP0001813347A1
Принадлежит:

Der Verteiler dient zu einer paarweisen Abgabe zweier Flüssigkeiten auf eine Vielzahl von Einspeisestellen (9), die in einem Reaktor oder einer Kolonne auf einer horizontalen Querschnittsfläche liegen. Mit dem Verteiler (1) lassen sich an jeder Einspeisestelle die Flüssigkeiten getrennt zuführen. Die Einspeisestellen sind mit einer Dichte von mindestens 50 Stellen pro m2 auf einer Mehrzahl von Linien angeordnet. Die genannte Querschnittsfläche ist längs dieser Linien jeweils durch ein Paar (10) von Nebenkanälen (11, 12) überspannt. Die Nebenkanäle sind an Hauptkanäle angeschlossen. Jedes Paar von Nebenkanälen bildet eine Einheit. Dieses Nebenkanalpaar (10) umfasst zwei durch Abkantung geformte Seitenteile (31, 32) sowie eine Trennwand (30). Auf den Seitenteilen erstrecken sich zwischen Kanalenden jeweils Böden (34, 34') der Nebenkanäle längs einer horizontalen Aussen- und Innenkante (4, 5), die auf einer horizontalen oder geneigten Ebene liegen. Die Seitenteile gehen bei den Innenkanten ...

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10-04-2006 дата публикации

РЕАКТОРНОЕ УСТРОЙСТВО

Номер: RU2005134690A
Принадлежит:

... 1. Реакторное устройство, содержащее реакционный сосуд, содержащий первую зону, по меньшей мере одну вторую зону и устройство для отделения катализатора, причем первая зона содержит по меньшей мере один впуск для реагента, а вторая зона содержит газовый холодильник, расположенный по меньшей мере частично внутри реакционного сосуда, пригодный для охлаждения газов, проходящих через газовый холодильник. 2. Реакторное устройство, содержащее реакционный сосуд, содержащий первую, вторую и третью зоны, газовый холодильник, расположенный по меньшей мере частично внутри реакционного сосуда, и устройство для отделения катализатора, причем первая зона содержит пластину для поддержки частиц катализатора и систему распределения газообразного реагента, расположенную в первой зоне и над пластиной. 3. Реакторное устройство по п.2, в котором реакционный сосуд имеет круговое горизонтальное поперечное сечение. 4. Реакционный сосуд по п.3, в котором вторая зона имеет больший диаметр, чем первая зона. 5. Реакторное ...

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10-02-2015 дата публикации

РЕАКТОР И СПОСОБ ДЛЯ НЕПРЕРЫВНОЙ ПОЛИМЕРИЗАЦИИ

Номер: RU2013135136A
Принадлежит:

... 1. Реактор для непрерывного синтеза полимеров, в особенности синтетических каучуков, включающий в себя, по меньшей мере один корпус реактора (16) по существу в форме трубы, причем корпус реактора (16) имеет в оснащении по меньшей мере- привод (38), который соединен по меньшей мере с одним скребком или очистителем (36), расположенным внутри корпуса реактора (16) с возможностью вращения, и причем скребок или очиститель (36) имеет по меньшей мере одну лопасть скребка или очистителя (42) для движения по внутренней стенке (44) корпуса реактора;- по меньшей мере одно входное устройство (20);- по меньшей мере одно выпускное устройство (24).2. Реактор по п. 1, отличающийся тем, что у него имеется центральный вал, который расположен по существу вдоль геометрической центральной оси (12).3. Реактор по п. 1, в котором выпускное устройство (24) выполнено таким образом, что отверстие выпуска (25) расположено по существу по касательной к направлению вращения (78) приводного механизма (38).4. Реактор по ...

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08-08-1984 дата публикации

OBTAINING SILICON FROM FLUOSILICIC ACID

Номер: GB0008417389D0
Автор:
Принадлежит:

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24-12-2002 дата публикации

METHOD OF MANUFACTURING A DRY POWDER PARTICLE, A POWDER PRODUCED WITH SAID METHOD AND AN ELECTRODE AND AN APPARATUS FOR USE IN SAID METHOD

Номер: CA0002259253C

The invention relates to a method of manufacturing a dry powder particle, preferably using electrohydrodynamic spraying, wherein two oppositely charge d aerosol streams are contacted. The invention allows for the manufacture of powders having various, controllable compositions and shapes. In particular the method according to the invention may be used to perform physical and chemical reactions and allows for the manufacture of powders not previously obtainable. In addition, the invention also relates to an electrode (4, 4', 5, 10a, 10b) and an apparatus for applying the method according to the inventio n.

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07-01-2016 дата публикации

PLANT FOR MANUFACTURING HYDROGEN SULFIDE GAS AND METHOD FOR EXHAUSTING HYDROGEN SULFIDE GAS

Номер: US20160002038A1
Принадлежит:

An object of the present invention is to reduce costs while maintaining safety in exhausting hydrogen sulfide gas. In exhaust facilities of a plant for manufacturing hydrogen sulfide gas, the concentrations of hydrogen sulfide gas leaking from a reaction facility, a cooling facility, and a sulfur removal facility, respectively, are measured by a measuring apparatus, and when a detected concentration is less than a predetermined concentration, a valve is controlled to exhaust hydrogen sulfide gas from a first exhaust pipe into the air, on the contrary, when a detected concentration is not less than a predetermined concentration, the valve is controlled to exhaust hydrogen sulfide gas from a second exhaust pipe to a gas treatment facility. 1. A plant for manufacturing hydrogen sulfide gas , the plant comprising at least: a reaction facility configured to generate hydrogen sulfide gas from sulfur and hydrogen gas; a cooling facility configured to cool generated hydrogen sulfide gas; a sulfur removal facility configured to remove sulfur contained in the hydrogen sulfide gas; and a gas treatment facility configured to render the hydrogen sulfide gas harmless ,wherein the plant has exhaust facilities which are provided in the reaction facility, the cooling facility, and the sulfur removal facility, respectively, and configured to exhaust hydrogen sulfide gas leaking from the facilities, andwherein each of the exhaust facilities comprises:an exhaust pipe whose one end branches out into a first exhaust pipe configured to exhaust leaking hydrogen sulfide gas to the air and a second exhaust pipe configured to exhaust leaking hydrogen sulfide gas to the gas treatment facility;a concentration measuring apparatus provided between the corresponding facility and a branch point in the exhaust pipe and configured to measure a concentration of the hydrogen sulfide gas; anda valve mechanism configured to perform control in such a manner that, when the concentration measuring apparatus ...

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14-01-2016 дата публикации

Medical waste break down and solid waste disposal system

Номер: US20160008860A1
Принадлежит: Edward Hermann, Milton Dallas, Russ Robers

A system for breaking down medical waste for safe disposal includes a novel disposal solution for dissolving and dispersing the medical waste, as well as a hardening agent that solidifies the disposal solution to prevent it from contaminating the environment after disposal. The novel disposal solution includes a dispersion agent that dissolves the medical waste in addition to a neutralizer, which binds to the dissolved medical waste to render it inert. The disposal solution can optionally include defoaming, preservation and/or anti-freeze agents. The system may also include a vessel with a vented cap for storing the disposal solution prior to and during use. The vessel may also be used to discard the disposal solution and broken-down medical waste after the disposal solution solidifies.

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03-02-2022 дата публикации

SHUT-DOWN PROCESS FOR THE PRODUCTION OF GLYCOLS

Номер: US20220033331A1
Принадлежит:

The invention provides a shut down method for a process for the preparation of glycols from a starting material comprising one or more saccharides in the presence 5 of hydrogen and a catalyst system comprising one or more retro-aldol catalysts comprising tungsten and one or more catalytic species suitable for hydrogenation in a reactor, said method comprising removing the one or more retro-aldol catalysts from the reactor whilst also in the presence of one or more agents suitable to suppress tungsten precipitation. 1. A shut-down method for a process for the preparation of glycols from a stream comprising one or more saccharides in the presence of hydrogen and a catalyst system comprising one or more retro-aldol catalysts comprising tungsten and one or more catalytic species suitable for hydrogenation in a reactor , said method comprising removing the one or more retro-aldol catalysts from the reactor whilst also in the presence of one or more agents suitable to suppress tungsten precipitation.2. The method according to claim 1 , wherein the one or more agents suitable to suppress tungsten precipitation comprise at least one of organic oxygenates or buffer systems comprising one or more organic acids claim 1 , their corresponding conjugated bases with alkali-metal as their counterions claim 1 , and mixtures thereof.3. The method according to claim 2 , wherein the one or more agents suitable to suppress tungsten precipitation comprise at least one of organic oxygenate solvents claim 2 , the stream comprising one or more saccharides claim 2 , glycols claim 2 , sugar alcohols claim 2 , carboxylic acids claim 2 , other products formed during the process claim 2 , and mixtures thereof.4. The method according to claim 1 , wherein the one or more retro-aldol catalysts are removed from the reactor prior to or along with removal of the one or more agents suitable to suppress tungsten precipitation.5. The method according claim 1 , wherein the reactor temperature is lowered ...

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26-01-2017 дата публикации

METHOD AND REACTOR FOR CRACKING HYDROCARBON

Номер: US20170022428A1
Принадлежит:

A method for cracking hydrocarbon, comprises: providing steam and hydrocarbon; and feeding steam and hydrocarbon into a reactor accessible to hydrocarbon and comprising a perovskite material of formula ABCDO, wherein 0 Подробнее

01-02-2018 дата публикации

METHOD FOR THE EPOXIDATION OF AN OLEFIN WITH HYDROGEN PEROXIDE

Номер: US20180030010A1
Принадлежит: EVONIK DEGUSSA GmbH

Epoxidation of an olefin is carried out by continuously reacting the olefin with hydrogen peroxide in the presence of a homogeneous epoxidation catalyst in a reaction mixture comprising an aqueous liquid phase and an organic liquid phase, using a loop reactor with mixing of the liquid phases. The loop reactor comprises a measuring section in which the liquid phases are temporarily separated, at least one pH electrode is arranged in the measuring section in contact with the separated aqueous phase, a pH of the separated aqueous phase is determined with the pH electrode and the pH is maintained in a predetermined range by adding acid or base to the loop reactor. 111-. (canceled)12. A method for the epoxidation of an olefin , comprising continuously reacting the olefin with hydrogen peroxide in the presence of a homogeneous epoxidation catalyst , wherein: i) a measuring section in which the liquid phases are temporarily separated into a separated aqueous phase and a separated organic phase;', 'ii) at least one pH electrode in said measuring section in contact with the separated aqueous phase;, 'a) the reaction is carried out in a reaction mixture comprising an aqueous liquid phase and an organic liquid phase using a loop reactor with mixing of the liquid phases, wherein the loop reactor comprisesb) a pH of the separated aqueous phase is determined with said pH electrode and said pH is maintained in a predetermined range by adding acid or base to the loop reactor.13. The method of claim 12 , wherein the liquid phases are temporarily separated by lowering the flow rate.14. The method of claim 13 , wherein the flow rate is lowered in the measuring section by enlarging the flow cross section.15. The method of claim 12 , wherein the measuring section is located in a side stream to the loop reactor.16. The method of claim 15 , wherein a valve is used for lowering the flow rate or temporarily stopping the flow in the measuring section.17. The method of claim 12 , wherein at ...

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18-03-2021 дата публикации

APPARATUS TO SIMULATE BIOCIDE PERFORMANCE IN CRUDE PIPELINE CONDITIONS

Номер: US20210079307A1
Принадлежит:

An apparatus to simulate biocide performance in crude oil pipeline conditions is disclosed. The apparatus includes: a reactor to simulate a two-phase crude oil pipeline which includes a crude oil phase above a water phase. The reactor has an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator. A crude oil inlet supplies crude oil to the reactor for the crude oil phase. A water inlet supplies water to the reactor for the water phase. A control circuit is configured by code to control a proportion of the water to the crude oil supplied to the reactor and to control the motor to drive a desired agitation rate of the agitator. A biocide inlet supplies biocide to the reactor. A water sample outlet enables sampling of the water phase of the reactor. 1. An apparatus to simulate biocide performance in crude oil pipeline conditions , the apparatus comprising:a reactor to simulate a two-phase crude oil pipeline and including a crude oil phase above a water phase, the reactor comprising an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator;a crude oil inlet to supply crude oil to the reactor for the crude oil phase;a water inlet to supply water to the reactor for the water phase; control a proportion of the water to the crude oil supplied to the reactor by the crude oil inlet and the water inlet, and', 'control the motor to drive a desired agitation rate of the agitator;, 'a control circuit configured by logic or code toa biocide inlet to supply biocide to the reactor; anda water sample outlet to sample the water phase of the reactor.2. The apparatus of claim 1 , whereinthe reactor further comprises a plurality of reactors each having a dedicated biocide inlet and a dedicated water sample outlet, andthe control circuit is further configured by logic or code to independently control the proportion of the water to the crude ...

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18-04-2019 дата публикации

MULTITUBULAR REACTOR FOR LIQUID PHASE ALCOHOL DEHYDROGENATION AND METHOD FOR LIQUID PHASE ALCOHOL DEHYDROGENATION

Номер: US20190112249A1
Принадлежит: FUZHOU UNIVERSITY

The invention relates to a multitubular reactor for dehydrogenation of liquid phase alcohol dehydrogenation and a method of liquid phase alcohol dehydrogenation. Most of the alcohol dehydrogenation reaction is endothermic reaction, the reaction temperature is high and the equilibrium conversion rate is low. 110-. (canceled)11. A multitubular reactor for liquid phase alcohol dehydrogenation , comprising:a reactor shell;a plurality of tubes spaced within the reactor shell, wherein the tubes are made of a gas selectively permeable membrane, which is permeable to hydrogen and oxygen but impermeable to liquid molecules, and wherein one end of the tubes is a liquid phase alcohol inlet, and another end of the tubes is a dehydrogenation product outlet;a dehydrogenation catalyst being provided inside the tubes;an oxidation catalyst being provided outside the tubes and in the reactor shell;at least one oxygen membrane tube disposed in the reactor shell, wherein one end of the oxygen membrane tube is an oxygen inlet, and another end of the oxygen membrane tube is closed; andan oxidation product outlet disposed on the reactor shell.12. The multitubular reactor for liquid phase alcohol dehydrogenation of claim 11 , wherein the gas selectively permeable membrane is made of a molecular sieve claim 11 , silica claim 11 , carbon claim 11 , ceramics claim 11 , porous stainless steel or a composite formed by two or more thereof.13. The multitubular reactor for liquid phase alcohol dehydrogenation of claim 11 , wherein the dehydrogenation catalyst is filled in the form of particles within the tubes claim 11 , and the dehydrogenation catalyst comprises:a supported noble metal and a support thereof, wherein the noble metal is Pd, Pt, Ru or Au, and the support is a metal oxide, a molecular sieve, a carbon material or an organic polymer; anda non-noble metal, wherein the non-noble metal is Cu, Zn, Mn, Ni, Co, Cr or V.14. The multitubular reactor for liquid phase alcohol dehydrogenation of ...

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01-09-2022 дата публикации

Method for preventing the fluidization of a catalytic fixed bed in a tubular upward-flow reactor of a steam methane reformer

Номер: US20220274080A1

The present invention relates to a method to prevent the fluidization of a catalytic fixed bed present in a tubular reactor operated in upward-flow configuration by estimating a pressure drop margin remaining before fluidization of the catalytic bed and adjusting the reactant gas flow in response. It relates also to a method to operate safely a furnace suitable for performing endothermic reactions containing a plurality of catalytic fixed bed reactors operated in upward-flow configuration, and to a method to debottleneck safely a catalytic fixed bed reactor involving a gas flowing in up flow direction.

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21-05-2020 дата публикации

Manufacturing process for cyclodextrin derivatives

Номер: US20200157252A1
Принадлежит: Cydex Pharmaceuticals Inc

A process and equipment assembly for reacting a substituent precursor with a cyclodextrin starting material to provide a raw product comprising a cyclodextrin derivative and 1% or less of an initial amount of the substituent precursor is provided. The process of the present invention provides cyclodextrin derivatives in substantially shorter time and with fewer side products than previous processes that utilize substantially the same starting materials.

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30-06-2016 дата публикации

Canister system for air separation module

Номер: US20160184793A1
Принадлежит: Hamilton Sundstrand Corp

An air separation module including a canister defining an interior chamber and having a first port at a first end and a second port at a second end, the canister configured to permit fluid to pass from the first port to the second port through the interior chamber, a first end cap located proximal to the first end of the canister and configured to releasably retain the first end of the canister, a second end cap located proximal to the second end of the canister and configured to releasably retain the second end of the canister, and a collar movably configured on the second end of the canister and configured to move from a first position to a second position, wherein the first position defines an engagement between the collar and the second end cap, and the second position defines a disengagement between the collar and the second end cap.

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23-07-2015 дата публикации

Process for preparing alkenylhalosilanes and reactor suitable therefor

Номер: US20150202590A1
Принадлежит: Evonik Industries AG

What is described is a process for preparing alkenylhalosilanes by reacting alkenyl halide selected from the group of vinyl halide, vinylidene halide and allyl halide with halosilane selected from the group of mono-, di- and trihalosilane in the gas phase in a reactor comprising a reaction tube ( 1 ) equipped with an inlet ( 2 ) at one end of the tube and with an outlet ( 3 ) at the other end of the tube, and having a gas inlet device ( 4 ) having a plurality of gas feed points ( 5 ) which are spaced apart in the direction of the longitudinal axis of the reaction tube ( 1 ) and open into the reaction tube ( 1 ). To perform the process, mono-, di- or trihalosilane is passed through the inlet ( 2 ) into the reaction tube ( 1 ) and flows through the reaction tube ( 1 ) in the direction of outlet ( 3 ), and vinyl halide, vinylidene halide or allyl halide flows through the gas feed points ( 5 ) in sections into the gas stream in the interior of the reaction tube ( 1 ). The process permits the preparation of alkenylhalosilanes in high yield and with high selectivity. The formation of soot is distinctly lower compared to conventional reactors. The invention also relates to a reactor for performance of gas phase reactions, which is characterized by the presence at least of the following elements: A) reaction tube ( 1 ) having B) an inlet ( 2 ) at one side of the tube, C) an outlet ( 3 ) at the other side of the tube, and D) having a gas inlet device ( 4 ) having a plurality of gas feed points ( 5 ) which are spaced apart in the direction of the longitudinal axis of the reaction tube ( 1 ) and open into the reaction tube ( 1 ).

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18-08-2016 дата публикации

Production system for vapor-grown carbon nanofibers

Номер: US20160236937A1

In a production system for vapor-grown carbon nanofibers includes a static mixer and a micro mist nozzle for preventing un-uniform input material from forming impurities, an anti-adhering coating covering an inner wall of a vertical tubular reactor for preventing a catalyst, raw material and carbon fibers from adhering to the inner wall of the vertical tubular reactor, and a sedimentation device into which a dispersant and water are inputted to separate produced carbon fiber compositions from particulate impurities in water.

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14-09-2017 дата публикации

REACTION PROCESS WITH MEMBRANE SEPARATION

Номер: US20170260229A1
Принадлежит:

Provided herein are processes for carrying out a chemical reaction of a substrate in a diluted reaction mixture. The processes include conducting the reaction mixture having reaction product and solvent to a filtration membrane which is permeable to the solvent but impermeable to the reaction product. Solvent which permeates the filtration membrane for dilution of the substrate feed is recycled. 117-. (canceled)18. A continuous process for carrying out a chemical reaction of a substrate in a diluted reaction mixture comprising a solvent , the process comprising the steps of:(a) simultaneously adding a substrate feed and a solvent for diluting said substrate feed to form a reaction mixture in a reactor; and causing said substrate to form a reaction product in said reaction mixture;(b) discharging, from an outlet of the reactor, reaction mixture comprising reaction product and solvent;(c) conducting the entire reaction mixture discharged in step (b) to a filtration membrane, whereby the filtration membrane is permeable to the solvent and provided to be impermeable to the reaction product, thereby obtaining a permeate and a retentate;(d) recycling solvent which permeates the filtration membrane for diluting said substrate feed in step (a); and(e) conducting the retentate from said filtration membrane to a reservoir other than said reactor, said retentate comprising reaction product.19. The process according to claim 18 , wherein said reaction is selected from the group consisting of a cyclization reaction claim 18 , a polymerization reaction claim 18 , an enzymatic reaction showing substrate inhibition claim 18 , an enzymatic reaction showing product inhibition claim 18 , a reaction showing precipitation of the substrate or of a co-reactant claim 18 , and combinations thereof.20. The process according to claim 18 , wherein said substrate feed and said solvent enter said reactor as separate streams which are mixed inside said reactor claim 18 , and wherein step (d) ...

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08-10-2015 дата публикации

METHOD FOR CONVERTING CARBON AND HYDROCARBON CRACKING AND APPARATUS FOR HYDROCARBON CRACKING

Номер: US20150284639A1
Принадлежит:

A method for converting carbon into a carbon oxide, comprises: contacting carbon with steam in presence of a carnegieite-like material of formula (NaO)Na[AlSi)], wherein 0 Подробнее

06-10-2016 дата публикации

SYSTEMS AND METHODS FOR REDUCING CORROSION IN A REACTOR SYSTEM USING ROTATIONAL FORCE

Номер: US20160288071A1
Принадлежит: EMPIRE TECHNOLOGY DEVELOPMENT LLC

Systems and methods for reducing or eliminating corrosion of components of a reactor system, including a supercritical water gasification system, are described. The reactor system may include various system components, such as one or more pre-heaters, heat exchangers and reactor vessels. The system components may be configured to receive a reactor fluid corrosive to an inner surface thereof and to separately receive a protective fluid that has a higher density and is substantially immiscible with the reactor fluid. A rotating element may be configured to generate a rotational force that forces at least a portion of the protective fluid to flow in a layer between the reactor fluid and at least a portion of the inner surface, the layer operating to reduce corrosion by forming a barrier between the reactor fluid and at least a portion of the inner surface. 163.-. (canceled)64. A method of reducing corrosion in a reactor system , the method comprising:providing a reactor vessel comprising an inner surface;receiving a reactor fluid at the reactor vessel corrosive to at least a portion of the inner surface;receiving a molten salt fluid at the reactor vessel, the molten salt fluid being substantially immiscible with the reactor fluid; androtating the reactor vessel at a speed such that at least a portion of the molten salt fluid forms a molten salt layer on the at least a portion of the inner surface, the molten salt layer operating to reduce corrosion by forming a barrier between the reactor fluid and the at least a portion of the inner surface.65. (canceled)66. The method of claim 64 , wherein providing the reactor vessel comprises providing a reactor vessel arranged in a substantially horizontal orientation and rotating the reactor vessel comprises rotating at a speed sufficient to generate a centripetal acceleration on at least a portion of the molten salt fluid greater than that of the acceleration of gravity on the at least a portion of the molten salt fluid entering ...

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15-10-2015 дата публикации

Method and System for Separating Rare Earth Elements

Номер: US20150292059A1
Принадлежит:

An objective of the invention is to provide a method and system for separating a particular rare earth element from a rare earth magnet at a high separation ratio and by a simple process. There is provided a rare earth separation method for separating a first and a second groups of rare earth elements contained in a magnet, the method including: a starting powder preparation step from the magnet; a magnet component oxidation heat treatment step; a rare earth oxide separation step from the magnet components oxide powder; a powder size optimization step; a chlorinating agent mixing step; a chlorination/oxychlorination heat treatment step of forming a “first group rare earth chlorides”/“second group rare earth oxychlorides” mixture; a selective dissolution step of selectively dissolving the first group rare earth chlorides in the solvent and leaving the second group rare earth oxychlorides undissolved in solid phase form; and a solid-liquid separation step. 1. A rare earth separation method for separating rare earth elements contained in a magnet wherein said magnet includes as components a first group of rare earth elements and a second group of rare earth elements , comprising the steps of:(a) a starting powder preparation step of preparing a starting powder from the magnet;(b) a magnet component oxidation heat treatment step of forming a powder of oxides of the magnet components, the oxides being formed by heating or combustion at a temperature from 300 to 1000° C. in an oxidizing atmosphere;(c) a rare earth oxide separation step of separating a rare earth oxide powder from the powder of the oxides of the magnet components, the rare earth oxide powder including first group rare earth oxides (=oxides of the first group of rare earth elements) and second group rare earth oxides (=oxides of the second group of rare earth elements);(d) a powder size optimization step of optimizing the rare earth oxide powder so as to have a desirable powder size distribution;(e) a ...

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05-10-2017 дата публикации

METHOD FOR CONVERTING CARBON AND HYDROCARBON CRACKING AND APPARATUS FOR HYDROCARBON CRACKING

Номер: US20170283712A1
Принадлежит:

A method for converting carbon into a carbon oxide, comprises: contacting carbon with steam in presence of a carnegieite-like material of formula (NaO)Na[AlSiO], wherein 0 Подробнее

04-10-2018 дата публикации

DETECTING AND CORRECTING PROBLEMS IN LIQUID LIFTING IN HEAT EXCHANGERS

Номер: US20180280914A1
Принадлежит:

A plant or refinery may include equipment such as reactors, heaters, heat exchangers, regenerators, separators, or the like. Types of heat exchangers include shell and tube, plate, plate and shell, plate fin, air cooled, wetted-surface air cooled, or the like. Operating methods may impact deterioration in equipment condition, prolong equipment life, extend production operating time, or provide other benefits. Mechanical or digital sensors may be used for monitoring equipment, and sensor data may be programmatically analyzed to identify developing problems. For example, sensors may be used in conjunction with one or more system components to detect and correct maldistribution, cross-leakage, strain, pre-leakage, thermal stresses, fouling, vibration, problems in liquid lifting, conditions that can affect air-cooled exchangers, conditions that can affect a wetted-surface air-cooled heat exchanger, or the like. An operating condition or mode may be adjusted to prolong equipment life or avoid equipment failure. 1. A system comprising:a reactor;a heater;a heat exchanger;a regenerator;a separator;one or more sensors associated with the heat exchanger; one or more processors of the data collection platform;', 'a communication interface of the data collection platform; and', receive, from the one or more sensors associated with the heat exchanger, sensor data comprising operation information associated with the heat exchanger;', 'correlate the sensor data from the one or more sensors with metadata comprising time data, the time data corresponding to the operation information associated with the heat exchanger; and', 'transmit the sensor data; and, 'memory storing executable instructions that, when executed, cause the data collection platform to], 'a data collection platform comprising one or more processors of the data analysis platform;', 'a communication interface of the data analysis platform; and', receive, from the data collection platform, the sensor data comprising ...

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22-10-2015 дата публикации

Control of the viscosity of reaction solutions in hydroformylation methods

Номер: US20150299079A1
Принадлежит: EVONIK DEGUSSA GmbH

The present invention relates to a method and a device for controlling the viscosity of reaction solutions in the hydroformylation of olefin-containing mixtures.

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24-12-2015 дата публикации

Method for Controlling the Production of a Biocide

Номер: US20150367315A1
Автор: BARAK Ayala
Принадлежит:

A method and apparatus for producing a biocide from a hypochlorite oxidant and an ammonium salt are provided. The method includes monitoring a control parameter to optimize the ratio between the hypochlorite oxidant and the ammonium salt. The control parameter may be oxidation-reduction potential, conductivity, induction or oxygen saturation. 1. A method for producing a biocide comprising:mixing a solution of a hypochlorite oxidant with a solution of an ammonium salt to produce a biocide; andmonitoring a control parameter that indicates when a maximum yield of said biocide, which yield is attainable without degradation of said biocide, has been reached;wherein said control parameter is not pH.2. The method according to claim 1 , wherein said hypochlorite oxidant is sodium hypochlorite.39-. (canceled)10. The method according to claim 1 , wherein said ammonium salt is selected from ammonium carbonate and ammonium carbamate.11. The method according to claim 1 , wherein said solution of an ammonium salt is prepared by diluting a commercial stock solution of about 15-50% with water or with said solution of a hypochlorite oxidant immediately prior to use.1216-. (canceled)17. The method according to claim 1 , wherein said control parameter is ORP.18. The method according to claim 1 , wherein said control parameter is conductivity or induction.19. The method according to claim 1 , wherein said control parameter is oxygen saturation.20. The method according to claim 1 , wherein said method comprises:providing a discrete amount of said solution of an ammonium salt;adding a plurality of discrete amounts of said solution of a hypochlorite oxidant to said discrete amount of said solution of an ammonium salt under mixing conditions; andmeasuring said control parameter after the addition of each discrete amount of said solution of a hypochlorite oxidant.21. The method according to claim 1 , wherein said method comprises:mixing a stream of a hypochlorite solution with a stream of ...

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19-12-2019 дата публикации

Plasma reactor and method of operating a plasma reactor

Номер: US20190381475A1
Автор: Olaf Kühl
Принадлежит: Ccp Technology GmbH

The problem addressed by the invention is that of providing a plasma reactor for decomposition of hydrocarbons which allows stable operation over a prolonged time period. This problem is solved by a plasma reactor for decomposing a hydrocarbon fluid, which comprises a reactor chamber surrounded by a reactor wall and further comprises at least one hydrocarbon inlet and an outlet. A plasma torch having at least two electrodes, which comprise a base part at a first end, is fixed to the reactor wall. At a second end, the electrodes comprise a burner part which projects into the reactor chamber, and a plasma zone is defined between the burner parts of adjacent electrodes. In a region between the plasma zone and the outlet, the hydrocarbon inlet opens into the reactor chamber, and the hydrocarbon inlet is oriented toward the plasma zone such that hydrocarbon fluid flowing therefrom is directed towards the plasma zone. In the plasma reactor disclosed herein, primarily small C particles are formed which prevent fouling or overgrowing of the reactor chamber. Furthermore some large and heavy C particles, which may statistically be formed, penetrate the plasma cloud and can attach specifically to the electrodes.

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05-10-2010 дата публикации

Systems and methods for detecting impurities in reactor systems

Номер: US7808227B2
Принадлежит: Univation Technologies Llc

The present invention is directed to various methods and systems for detecting at least one impurity in a bulk fluid. In certain embodiments, the methods are performed in conjunction with a polymerization reactor system such as a gas-phase reactor system.

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15-05-2019 дата публикации

Automated method for terminating an olefin polymerization reaction under emergency conditions

Номер: EP3483189A1
Принадлежит: Borealis AG

The present invention relates to a method for terminating an olefin polymerization reaction conducted in the presence of an olefin polymerization catalyst in a polymerization reactor under emergency conditions by automatically introducing a killing agent into the polymerization reactor the stop the polymerization reaction at a monitored increase of the polymerization temperature and/or pressure and automatically stopping the polymerization reaction at a monitored pressure drop in the vessel containing the killing agent. This method will feed the CO into the reactor independently of manual interaction e.g changing of empty CO bottles .

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16-06-2022 дата публикации

Reactor for a gas-phase olefin polymerization

Номер: WO2022122749A1
Принадлежит: BASELL POLYOLEFINE GMBH

A reactor for carrying out a gas-phase olefin polymerization in the presence of a polymerization catalyst, the reactor comprising at least a first polymerization zone adapted and arranged for growing polymer particles to flow upward under fast fluidization or transport conditions and at least a second polymerization zone adapted and arranged for the growing polymer particles to flow downward; and at least one set of bars for introducing feedstock and/or a barrier stream into the reactor, wherein each bar comprises a hollow space along the length of the bar and has a particle deviating top and each bar has openings arranged along the bottom half of the periphery of the bar.

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17-01-2008 дата публикации

Using electrical probes for detecting impurities in reactor systems

Номер: WO2008008169A2
Принадлежит: UNIVATION TECHNOLOGIES, LLC

The present invention is directed to various methods and systems for detecting at least one impurity in a bulk fluid (10), using at least one electrical probe (40). The methods are performed in conjunction with a polymerization reactor system (100) such as a gas-phase reactor system.

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03-04-2008 дата публикации

Using electrical probes for detecting impurities in reactor systems

Номер: WO2008008169A3

The present invention is directed to various methods and systems for detecting at least one impurity in a bulk fluid (10), using at least one electrical probe (40). The methods are performed in conjunction with a polymerization reactor system (100) such as a gas-phase reactor system.

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21-02-2008 дата публикации

Systems and methods for detecting impurities in reactor systems

Номер: US20080042655A1
Принадлежит: Univation Technologies Llc

The present invention is directed to various methods and systems for detecting at least one impurity in a bulk fluid. In certain embodiments, the methods are performed in conjunction with a polymerization reactor system such as a gas-phase reactor system.

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18-06-2020 дата публикации

Solution polymerization process

Номер: WO2020123973A1
Принадлежит: Dow Global Technologies LLC

Disclosed herein too is a method comprising charging to a reactor system a feed stream comprising a catalyst, a monomer and a solvent; reacting the monomer to form a polymer; where the polymer is contained in a single phase polymer solution; transporting the polymer solution to a pre-heater to increase the temperature of the polymer solution; charging the polymer solution to a liquid-liquid separator; reducing a pressure of the polymer solution in the liquid-liquid separator and separating a polymer-rich phase from a solvent-rich phase in the liquid-liquid separator; transporting the polymer-rich phase to a plurality of devolatilization vessels located downstream of the liquid-liquid separator, where each devolatilization vessel operates at a lower pressure than the preceding devolatilization vessel; and separating the polymer from volatiles present in the polymer rich phase.

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31-08-2021 дата публикации

SOLUTION POLYMERIZATION SYSTEM AND METHOD

Номер: BR112021011009A2
Принадлежит: Dow Global Technologies LLC

sistema para polimerização em solução, e, método. também é divulgado no presente documento um método que compreende carregar em um sistema de reator uma corrente de alimentação que compreende um catalisador, um monômero e um solvente; reagir o monômero para formar um polímero; em que o polímero está contido em uma solução de polímero monofásica; transportar a solução de polímero para um preaquecedor para aumentar a temperatura da solução de polímero; carregar a solução de polímero em um separador líquido-líquido; reduzir a pressão da solução de polímero no separador líquido-líquido e separar uma fase rica em polímero de uma fase rica em solvente no separador líquido-líquido; transportar a fase rica em polímero para uma pluralidade de recipientes de desvolatilização localizados a jusante do separador líquido-líquido, em que cada recipiente de desvolatilização opera a uma pressão mais baixa do que o recipiente de desvolatilização anterior; e separar o polímero dos voláteis presentes na fase rica em polímero. system for solution polymerization and method. Also disclosed herein is a method comprising charging a feed stream comprising a catalyst, a monomer and a solvent into a reactor system; reacting the monomer to form a polymer; wherein the polymer is contained in a single-phase polymer solution; transporting the polymer solution to a preheater to raise the temperature of the polymer solution; loading the polymer solution into a liquid-liquid separator; reducing the pressure of the polymer solution in the liquid-liquid separator and separating a polymer-rich phase from a solvent-rich phase in the liquid-liquid separator; conveying the polymer-rich phase to a plurality of devolatilization vessels located downstream of the liquid-liquid separator, wherein each devolatilization vessel operates at a lower pressure than the preceding devolatilization vessel; and separating the polymer from the volatiles present in the polymer-rich phase.

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12-11-2021 дата публикации

多位点流体分布装置和连续流硝化反应装置

Номер: CN113634198A
Автор: 洪亮, 洪浩, 王苗, 郑淞元, 陶建
Принадлежит: Asymchem Laboratories Tianjin Co Ltd

本发明提供了一种多位点流体分布装置和连续流硝化反应装置。该多位点流体分布装置包括:管式稳压腔室和至少两个支管路,各支管路的内径与目标反应器的入口端连通,且支管路的内径与目标反应器的内径之比≤1:4,目标反应器包括盘管反应器或柱状反应器。本申请提供的多位点流体分布装置包括稳压腔室和多个与稳压腔室连通的支管路,通过将目标反应器与支管路的内径比限定在上述范围内能够使其通过水力学流阻来调控各支管中的流量,从而实现提高各支管路中流体分配均匀性的效果。

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16-12-2004 дата публикации

Flow reactor of non-equilibrium open type

Номер: US20040254311A1
Автор: Koichiro Matsuno
Принадлежит: Individual

A flow reactor for liquid-phase polymerization reaction, which enables controlling the degree of polymerization for, for example, amino acid polymerization, wherein the liquid reaction mixture containing the organic reactive molecules to be polymerized is emitted from a high-temperature high-pressure part (A) to a low-temperature high-pressure part (B) via a circulation line (C), whereby inhibiting the decomposition of the polymer product in the low-temperature high-pressure part (B), after which the polymer product is once again sent to the high-temperature high-pressure part (A) through the circulation line for further polymerization, and the same cycle is repeated.

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26-07-2022 дата публикации

Detecting and correcting problems in liquid lifting in heat exchangers

Номер: US11396002B2
Принадлежит: UOP LLC

A plant or refinery may include equipment such as reactors, heaters, heat exchangers, regenerators, separators, or the like. Types of heat exchangers include shell and tube, plate, plate and shell, plate fin, air cooled, wetted-surface air cooled, or the like. Operating methods may impact deterioration in equipment condition, prolong equipment life, extend production operating time, or provide other benefits. Mechanical or digital sensors may be used for monitoring equipment, and sensor data may be programmatically analyzed to identify developing problems. For example, sensors may be used in conjunction with one or more system components to detect and correct maldistribution, cross-leakage, strain, pre-leakage, thermal stresses, fouling, vibration, problems in liquid lifting, conditions that can affect air-cooled exchangers, conditions that can affect a wetted-surface air-cooled heat exchanger, or the like. An operating condition or mode may be adjusted to prolong equipment life or avoid equipment failure.

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10-02-2021 дата публикации

Method for preventing fluidizazion in an upward-flow catalytic fixed bed reactor

Номер: EP3772372A1

The present invention relates to a method to operate safely a catalytic fixed bed reactor operated in upward-flow configuration by preventing fluidization of the catalyst fixed bed present in said reactor; it relates also to a method to operate safely a furnace suitable for performing endothermic reactions containing a plurality of catalytic fixed bed reactors operated in upward-flow configuration by preventing fluidization of the catalyst fixed bed, and to a method to debottleneck safely a catalytic fixed bed reactor involving a gas flowing in upflow direction where the method includes increasing the reactant gas flow in the reactor while preventing the risk of fluidization of the catalyst bed present in the reactor by preventing fluidization of the catalyst fixed bed; the prevention of the fluidization of the catalyst fixed bed comprising a step of control of a pressure drop margin remaining before fluidization of the catalytic bed.

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11-02-2021 дата публикации

Method for preventing the fluidization of a catalytic fixed bed in a tubular upward-flow reactor of a steam methane reformer

Номер: WO2021023613A1

The present invention relates to a method to prevent the fluidization of a catalytic fixed bed present in a tubular reactor operated in upward-flow configuration by estimating a pressure drop margin remaining before fluidization of the catalytic bed and adjusting the reactant gas flow in response. It relates also to a method to operate safely a furnace suitable for performing endothermic reactions containing a plurality of catalytic fixed bed reactors operated in upward-flow configuration, and to a method to debottleneck safely a catalytic fixed bed reactor involving a gas flowing in up flow direction.

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15-06-2017 дата публикации

Method for designing multi-valve uni-direction blowdown system for a high pressure tubular reactor

Номер: WO2017098389A1
Принадлежит: NOVA CHEMICALS (INTERNATIONAL) S.A.

Provided herein is a unidirectional blow down system for a high-pressure tubular reactor with a hyper that minimizes the tube wall metal temperature during a decomposition event wherein the system prevents the reactor walls from reaching a temperature capable of causing the tube metal to austenize. Also provided are methods of designing and methods of operating a unidirectional blowdown system.

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01-03-2022 дата публикации

烯键不饱和单体在聚合反应器中的高压聚合方法

Номер: CN113166283B
Принадлежит: BASELL POLYOLEFINE GMBH

一种用于在高压聚合系统中聚合乙烯的方法,包括连续操作的聚合反应器和反应器排放系统,该反应器排放系统包括应急阀、含有水性介质的反应器排放容器和反应器排放倾倒容器,其中该方法包括监测聚合系统的干扰发生情况,在允许聚合系统的内容物膨胀到反应器排放容器中的干扰的情况下,打开应急阀,使反应器排放容器中的内容物与水性介质接触以获得水性聚合物浆料,分离聚合物浆料和气态组分并将聚合物浆料转移到反应器排放倾倒容器。

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23-07-2014 дата публикации

减少流化床反应器内颗粒污染的方法和装置

Номер: CN103945932A
Принадлежит: REC SILICON INC

本发明公开一种减少或消除涂硅颗粒的污染的方法和流化床反应器。一个或多个流化床反应器组件的金属表面至少部分地涂布有包含650℃时极限拉伸强度为至少700MPa的材料的硬保护层。

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28-04-1999 дата публикации

PRODUCTION OF TEREFTALIC ACID WITH EXCELLENT OPTICAL PROPERTIES, THROUGH THE USE OF PURE OR ALMOST PURE OXYGEN, AS THE OXIDIZER IN P-XYLENE OXIDATION

Номер: AR005299A1
Автор: [UNK]
Принадлежит: Praxair Technology Inc

La producción de ácido tereftálico mediante la oxidación de p-xileno se lleva a cabo de tal forma que la concentración de oxígeno, en la fase líquida,se incrementa al máximo a través del uso de oxígeno puro o casi puro, mientras quesimultáneame nte la concentración de alimentación de hidrocarburos se reduceal mínimo a través de la rápida dilución con los contenidos del reactor. The production of terephthalic acid through the oxidation of p-xylene is carried out in such a way that the concentration of oxygen, in the liquid phase, is increased to the maximum through the use of pure or almost pure oxygen, while simultaneously the concentration Hydrocarbon feed is minimized through rapid dilution with the reactor contents.

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09-10-2019 дата публикации

Plasma reactor and method of operating a plasma reactor

Номер: EP3548426A1
Автор: Olaf Kühl
Принадлежит: Ccp Technology GmbH

The problem addressed by the invention is that of providing a plasma reactor for decomposition of hydrocarbons which allows stable operation over a prolonged period. This problem is solved by a plasma reactor (1) for cracking a hydrocarbon fluid which comprises a reactor chamber (2) which is surrounded by a reactor wall (3, 3a, 3b) and comprises at least one hydrocarbon inlet (5) and an outlet (15). A plasma burner (7) having at least two electrodes which comprise at a first end a base part (9) is fixed to the reactor wall. The electrodes comprise at a second end a burner part (11) which projects into the reactor chamber and a plasma zone (13) is defined between the burner parts of adjacent electrodes. In a region between the plasma zone and the outlet the hydrocarbon inlet opens into the reactor chamber and the hydrocarbon inlet is aligned with respect to the plasma zone such that hydrocarbon fluid issuing therefrom is conducted towards the plasma zone. In the plasma reactor disclosed herein primarily small C particles are formed which prevent fouling/closing-up of the reactor chamber. Furthermore some large and heavy C particles which may statistically be formed penetrate the plasma cloud and can attach to the electrodes in targeted fashion.

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25-11-2004 дата публикации

Fluidized bed reactor with gas cooler

Номер: WO2004101136A2
Принадлежит: The Standard Oil Company

A new reactor apparatus that can be used to carry out chemical reactions in a fluidized catalyst bed at high temperatures with reduced afterburning or other undesirable downstream side reactions. One application is the manufacture of acrylonitrile.

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28-10-2008 дата публикации

Reactor apparatus

Номер: US7442345B2
Принадлежит: INEOS USA LLC

A new reactor apparatus that can be used to carry out chemical reactions in a fluidized catalyst bed at high temperatures with reduced afterburning or other undesirable downstream side reactions.

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01-03-2006 дата публикации

Fluidized bed reactor with gas cooler

Номер: EP1628751A2
Принадлежит: Innovene USA LLC

A new reactor apparatus that can be used to carry out chemical reactions in a fluidized catalyst bed at high temperatures with reduced afterburning or other undesirable downstream side reactions. One application is the manufacture of acrylonitrile.

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07-06-2006 дата публикации

带有气体冷却器的流化床反应器

Номер: CN1784264A
Принадлежит: Standard Oil Co

一种新的反应装置,可用于在高温下在流化催化剂床中进行化学反应,并可减少二次燃烧或其它不合需要的下游副反应。一种应用是生产丙烯腈。

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30-10-2009 дата публикации

Reactor apparatus

Номер: MY139567A
Принадлежит: INEOS USA LLC

A NEW REACTOR APPARATUS THAT CAN BE USED TO CARRY OUT CHEMICAL REACTIONS IN A FLUIDIZED CATALYST BED AT HIGH TEMPERATURES WITH REDUCED AFTERBURNING OR OTHER UNDESIRABLE DOWNSTREAM SIDE REACTIONS.

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27-06-2009 дата публикации

Реакторное устройство

Номер: RU2359747C2
Принадлежит: ИНЕОС ЮЭсЭй ЭлЭлСи

Изобретение относится к химической промышленности и может быть использовано для проведения химических реакций в псевдоожиженном слое катализатора при высоких температурах и в газовой фазе с пониженным выгоранием или иными нежелательными побочными реакциями. В зоне плотного слоя реакторного устройства на решетке реакторного устройства находится слой порошкового катализатора. Над решеткой расположена система распределения газа. Зона выделения катализатора расположена над зоной плотного слоя. Зона разбавленной фазы расположена над зоной выделения. Внутри зоны разбавленной фазы размещен газовый холодильник. Внутри реакционного сосуда расположено устройство для отделения катализатора и средство для возврата отделенного катализатора в зону плотного слоя. Изобретение обеспечивает снижение степени неконтролируемого окисления и уменьшение потерь продуктов и исходных материалов. 17 з.п. ф-лы, 11 ил. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 2 359 747 (13) C2 (51) МПК B01J 8/18 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ОПИСАНИЕ ИЗОБРЕТЕНИЯ К ПАТЕНТУ (21), (22) Заявка: 2005134690/12, 06.05.2004 (24) Дата начала отсчета срока действия патента: 06.05.2004 (43) Дата публикации заявки: 10.04.2006 2 3 5 9 7 4 7 R U (85) Дата перевода заявки PCT на национальную фазу: 09.11.2005 C 2 C 2 (56) Список документов, цитированных в отчете о поиске: US 4158036 А, 12.06.1979. FR 937899 А, 30.08.1948. GB 2075360 А, 18.11.1981. ЕР 0446379 A1, 18.09.1991. GB 1121909 A, 31.07.1968. EP 1202017 A2, 02.05.2002. EP 0546677 A1, 16.06.1993. SU 1554202 A1, 20.06.1996. (73) Патентообладатель(и): ИНЕОС ЮЭсЭй ЭлЭлСи (US) (86) Заявка PCT: US 2004/014403 (06.05.2004) (87) Публикация PCT: WO 2004/101136 (25.11.2004) Адрес для переписки: 119034, Москва, Пречистенский пер., 14, стр.1, 4 этаж, "Гоулингз Интернэшнл Инк.", В.Н.Дементьеву (54) РЕАКТОРНОЕ УСТРОЙСТВО (57) Реферат: Изобретение относится к химической промышленности и может быть использовано для проведения ...

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16-01-2005 дата публикации

Reactor apparatus

Номер: TW200502199A
Принадлежит: Standard Oil Co

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06-01-2005 дата публикации

Reactor apparatus

Номер: US20050002837A1

A new reactor apparatus that can be used to carry out chemical reactions in a fluidized catalyst bed at high temperatures with reduced afterburning or other undesirable downstream side reactions.

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02-06-2005 дата публикации

Fluidized bed reactor with gas cooler

Номер: WO2004101136A3

A new reactor apparatus that can be used to carry out chemical reactions in a fluidized catalyst bed at high temperatures with reduced afterburning or other undesirable downstream side reactions. One application is the manufacture of acrylonitrile.

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20-04-2000 дата публикации

Device and method for filling and emptying a container charged with flammable and aggressive gas

Номер: DE19847786A1
Принадлежит: Degussa GmbH, Degussa Huels AG

Die vorliegende Erfindung betrifft eine Vorrichtung zum sicheren Befüllen oder Entleeren eines unter Druck stehenden und mit brennbarem und/oder aggressivem Gas beaufschlagten Behälters, welche durch eine obere Klappenkombination (1), einen Schleusenbehälter (2) mit Spülvorrichtung (3) und eine untere Klappenkombination (4) gekennzeichnet ist. DOLLAR A Die vorliegende Erfindung betrifft auch einen mit brennbarem und/oder aggressivem Gas beaufschlagten und unter Druck stehenden Reaktor, der mit einer erfindungsgemäßen Befüll- und einer entsprechenden Entaschungsschleusenvorrichtung ausgestattet ist, und seine Verwendung zur gleichzeitigen Herstellung von Tetrachlorsilan, Trichlorsilan und Wasserstoff. DOLLAR A Ferner betrifft die vorliegende Erfindung ein spezielles Verfahren zum Befüllen und Entleeren eines solchen Reaktors. The present invention relates to a device for the safe filling or emptying of a container under pressure and charged with combustible and / or aggressive gas, which comprises an upper flap combination (1), a lock container (2) with flushing device (3) and a lower flap combination ( 4) is marked. DOLLAR A The present invention also relates to a pressurized and / or aggressive gas pressurized reactor, which is equipped with a filling and a corresponding ash removal lock device according to the invention, and its use for the simultaneous production of tetrachlorosilane, trichlorosilane and hydrogen. DOLLAR A Furthermore, the present invention relates to a special method for filling and emptying such a reactor.

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03-08-2016 дата публикации

水解自动化控制系统

Номер: CN105817190A
Автор: 卓仲标

本发明属于化学技术领域,尤其涉及一种水解自动化控制系统。它解决了现有技术设计不合理等技术问题。本水解自动化控制系统包括用于放置原料的反应仓和向反应仓内注入水解液的水解液输入装置,所述的反应仓内设有对反应仓中水解液进行搅拌的均衡搅拌机构和对水解液进行pH值检测的pH值检测机构。本发明优点在于:1、设计更合理,搅拌过程更均匀,使得水解包膜后的云母的色泽均匀、光泽度高、珠光效果好。2、生产过程自动化,水解过程中,注料准确,同时节约劳动力,节约生产成本。

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28-08-2015 дата публикации

연속 중합을 위한 반응기 및 방법

Номер: KR101548440B1
Принадлежит: 란세스 인터내쇼날 에스에이

본 발명은, 실질적으로 관형인 반응기 하우징 (16)을 갖는 반응기 (10) 및 연속 중합 방법에 관한 것이다. 반응기 하우징 (16)은 유동 방향 (22)로 기하학적 중심축 (12)를 따라 진행되며 중심 샤프트로서 구성된 구동기 (38)을 갖는다. 회전가능하게 배열된 스크레이퍼 또는 와이퍼 (36)이 반응기 하우징 (16) 내에 제공되고, 스크레이퍼 또는 와이퍼 (36)은 반응기 하우징 (16)의 내면 (44)를 따라 진행되는 1개 이상의 스크레이퍼 또는 와이퍼 블레이드 (42)를 갖는다. 스크레이퍼 또는 와이퍼 (36)의 회전 운동은, 반응기 하우징 (16) 내의 유동의 방사 방향 혼합을 일으키고, 이 유동은 중력 효과를 억누르며, 또한 스크레이퍼 또는 와이퍼의 성형에 의해 임의로 반응기 (10) 내에서 또는 추가의 외부 펌핑 순환 시스템 (23)을 통해 플러그 유동, 루프 유동 또는 역류를 가능하게 한다. 이는 반응기 하우징 (16)의 축 방향으로의 반응 조건이 예측될 수 있게 하고, 반응기 하우징을 따라 개별적으로 적합한 반응 조건이 설정되고 조절될 수 있게 함으로써, 특히, 요망되는 분자량 분포가 설정될 수 있다.

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20-12-2007 дата публикации

Oxidation System with Internal Secondary Reactor

Номер: US20070292320A1
Принадлежит: Eastman Chemical Co

Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

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17-02-2009 дата публикации

Oxidation system with internal secondary reactor

Номер: US7491369B2
Принадлежит: Eastman Chemical Co

Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

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20-12-2013 дата публикации

Кожухотрубный реактор для получения ангидрида малеиновой кислоты

Номер: RU2012123724A
Принадлежит: БАСФ СЕ

1. Способ получения ангидрида малеиновой кислоты посредством гетерогенно-каталитического газофазного окисления исходного потока, содержащего углеводороды, по меньшей мере, с 4 углеродными атомами на молекулу в установке, включающей реактор с группой реакционных труб, в которых размещен твердофазный катализатор, на котором происходит экзотермическое взаимодействие исходного потока с содержащим кислород газовым потоком, один или несколько насосов и один или несколько установленных вне реактора теплообменников, через которые протекает теплоноситель, представляющий собой солевой расплав, который протекает через промежуточное пространство между реакционными трубами, воспринимая теплоту реакции, причем температура солевого расплава лежит в диапазоне между 350 и 480°С, отличающийся темчто реакционные трубы выполнены из легированной термостойкой стали, содержащей, по меньшей мере, 0,5 вес.% хрома или, по меньшей мере, 0,25 вес.% молибдена или, по меньшей мере, 0,5 вес.% хрома и, по меньшей мере, 0,25 вес.% молибдена, причем солевой расплав имеет эвтектический состав смеси нитрата калия, нитрита натрия и нитрата натрия.2. Способ по п.1отличающийся тем,что исходный поток содержит летучее фосфорное соединение, и твердофазный катализатор содержит ванадий, фосфор и кислород.3. Способ по п.1 или 2, отличающийся тем,что температура солевого расплава лежит в диапазоне между 380°С и 440°С.4. Способ по п.1 или 2, отличающийся темчто солевой расплав содержит 53 вес.% нитрата калия, 40 вес.% нитрита натрия и 7 вес.% нитрата натрия.5. Способ по п.1 или 2, отличающийся темчто в качестве углеводорода используют н-бутан.6. Способ по п.2, отличающийся темчто в РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (13) 2012 123 724 A (51) МПК C07C 51/215 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ЗАЯВКА НА ИЗОБРЕТЕНИЕ (21)(22) Заявка: 2012123724/04, 02.11.2010 (71) Заявитель(и): БАСФ СЕ (DE) Приоритет(ы): (30) Конвенционный приоритет: 10.11.2009 EP 09175466.3 (85) Дата начала ...

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25-08-2014 дата публикации

Hydrogen sulfide gas production plant and method for discharging a hydrogen sulfide gas

Номер: JP2014152090A
Принадлежит: SUMITOMO METAL MINING CO LTD

【課題】硫化水素ガスの排気の安全性を維持しつつ、コストを削減する。 【解決手段】硫化水素ガス製造プラントの排気設備において、反応設備、冷却設備及び硫黄除去設備から漏洩した硫化水素ガスの濃度を測定器で測定し、検出した濃度が所定の濃度未満の場合にはバルブを制御して第1の排気管から硫化水素ガスを大気中に排気し、所定の濃度以上の場合にはバルブを制御して第2の排気管から硫化水素ガスをガス処理設備に排気する。 【選択図】図1

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28-12-2017 дата публикации

Flow type reactor

Номер: WO2017222048A1
Принадлежит: 株式会社カネカ

The problem addressed by the present invention is to provide a flow type reactor that can use chargeable substances, such as organic solvents with low dielectric constants, and has excellent corrosion resistance. This flow type reactor is characterized by being provided with two or more raw material liquid feed units, a mixing unit for mixing the raw materials from these raw material liquid feed units, and a reactor unit through which a mixed liquid adjusted by the mixing unit flows, and in that at least part of the inner wall of the reactor unit is constituted of a fluororesin having a conductive filler.

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23-07-2021 дата публикации

Solution polymerization process

Номер: CN113164898A
Принадлежит: Dow Global Technologies LLC

本文也公开了一种方法,所述方法包括将包含催化剂、单体和溶剂的进料料流装入反应器系统中;使所述单体反应以形成聚合物;其中所述聚合物包含在单相聚合物溶液中;将所述聚合物溶液输送至预热器以提高所述聚合物溶液的温度;将所述聚合物溶液装入液‑液分离器中;降低所述液‑液分离器中的所述聚合物溶液的压力,并且在所述液‑液分离器中将富聚合物相与富溶剂相分离;将所述富聚合物相输送至位于所述液‑液分离器下游的多个脱挥发分容器中,其中每个脱挥发分容器在比前一脱挥发分容器更低的压力下操作;以及将所述聚合物与存在于所述富聚合物相中的挥发物分离。

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07-12-1982 дата публикации

Device for atomizing a reaction mixture

Номер: US4361965A
Принадлежит: Commissariat a lEnergie Atomique CEA

The present invention relates to a device for atomizing a reaction mixture, said device enabling the reaction mixture to be atomized in a reactor with the aid of at least a first gas and an atomizing nozzle. This device further comprises a supply of a second hot gas at the top of the atomizing device, serving to dry the atomized mixture, a supply of a third gas and means for distributing this third gas comprising an annular space of adjustable width and adapted to distribute in the reactor said third gas in the form of a ring along the inner wall of the reactor, so as to avoid any contact between the reaction mixture and said wall. The invention is applicable to the atomization of a reaction mixture.

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06-08-2020 дата публикации

Shell and tube reactor

Номер: DE102012023527B4
Принадлежит: MAN Energy Solutions SE

Rohrbündelreaktor zur Durchführung katalytischer Gasphasenreaktionen, mit- einem Bündel (2) Reaktionsrohre (3), die im Betrieb katalysatorgefüllt sind und von Reaktionsgas (10) durchströmt werden,- einem gaseintrittsseitigen und einem gasaustrittsseitigen Rohrboden (4), die mit den gaseintrittsseitigen bzw. den gasaustrittseitigen Enden der Reaktionsrohre (3) dicht verbunden sind und durch die hindurch die Reaktionsrohre (3) in einen Gaseintrittsraum bzw. einen Gasaustrittsraum (7) münden,- einem Reaktormantel (5), der das Rohrbündel (2) umschließt und mit den Rohrböden (4) dicht verbunden ist, um mit diesen einen Mantelraum (12) auszubilden, in dem die Reaktionsrohre (3) im Betrieb von einem Wärmeträger umspült werden,- wobei der gasaustrittsseitige Rohrboden (4) mindestens einen ersten Rohrbodenabschnitt (16) aufweist, der vom Rohrbündel (2) belegt ist, und mindestens einen zweiten Rohrbodenabschnitt (17) aufweist, der rohrbündelfrei ist, und- wobei im Gasaustrittsraum (7) mindestens ein erster Gasaustrittsraumabschnitt (18) vorhanden ist, der mit dem ersten Rohrbodenabschnitt (16) fluchtet, und mindestens ein zweiter Gasaustrittsraumabschnitt (19) vorhanden ist, der mit dem zweiten Rohrbodenabschnitt (17) fluchtet und einen Teilabschnitt (20) aufweist, und mit- mindestens einer Strömungsleiteinrichtung (8), die im zweiten Gasaustrittsraumabschnitt (19) angeordnet ist, dadurch gekennzeichnet, dass die mindestens eine Strömungsleiteinrichtung (8) als Strömungsleitblech mit einem Abschnitt (22, 31) ausgebildet ist oder Strömungsleitrohre (35) aufweist, der (22, 31) bzw. die (35) sich aus dem zweiten Gasaustrittsraumabschnitt (19) in den ersten Gasaustrittsraumabschnitt (18) hineinerstreckt/-erstrecken und einen Teilstrom des aus den Reaktionsrohren (3) austretenden Reaktionsgases (10) zwischen sich (8) und dem Rohrboden (4) aus dem ersten Gasaustrittsraumabschnitt (18) in einen Teilabschnitt (20) des zweiten Gasaustrittsraumabschnitts (19) hineinleitet/- leiten, ...

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06-06-2003 дата публикации

Slurry phase device and method.

Номер: NL1022077A1
Автор: Andre Steynberg
Принадлежит: Sasol Tech Pty Ltd

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13-09-2000 дата публикации

Process and apparatus for the oxidation of alhylaromatic compounds to aromatic carboxylic acids

Номер: EP0781754B1
Автор: Anne Katherine Roby
Принадлежит: Praxair Technology Inc

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12-01-2021 дата публикации

Preparation method of sucrose-6-ester

Номер: CN112218874A
Принадлежит: Anhui Jinhe Industrial Co Ltd

本申请提供了一种蔗糖‑6‑酯的制备方法,包括:将制备蔗糖和有机锡化物的反应溶液;将反应溶液进行雾化,形成小液滴;将小液滴与气化的脱水介质充分混合接触,使小液滴发生脱水反应,从而生成含有蔗糖有机锡酯小液滴的中间体混合物;将中间体混合物进行分离,得到蔗糖有机锡酯溶液和脱水气液混合物;将分离步骤中得到的蔗糖有机锡酯溶液回收并循环至雾化步骤和脱水步骤数次;将蔗糖有机锡酯溶液与有机酸酐进行酰化反应,生成蔗糖‑6‑酯。本申请能够在极短的时间内实现酯化反应的快速高效脱水,高效的制备出蔗糖有机锡酯中间体,极大程度上减少体系内糖类物质的分解和副反应的发生,且耗能低、产品收率高、选择性强、蔗糖反应程度更加彻底。

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29-04-2015 дата публикации

Method and device for separating rare earth elements

Номер: CN104583428A
Принадлежит: Hitachi Metals Ltd

提供以高分离率简便地从稀土磁铁中分离稀土元素的方法及用于实施该方法的分离装置。本发明稀土元素分离方法是从含有多种稀土元素的磁铁材料中分离稀土元素,具有:准备包含稀土磁铁粉末的起始粉末的工序、由上述起始粉末生成上述磁铁材料成分的氧化物的工序、从上述磁铁材料成分的氧化物中分离出多种稀土氧化物的工序、对分离的上述多种稀土氧化物的粒度进行调整的工序、将整粒了的上述多种稀土氧化物与氯化剂混合的工序、使氧化物/氯化剂混合物生成氯化物/氧氯化物混合物的工序、从上述氯化物/氧氯化物混合物中将上述稀土氯化物选择的提取到溶剂中的工序、将提取了上述稀土氯化物的液相与残留的上述稀土氧氯化物的固相进行固液分离的工序。

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30-11-2011 дата публикации

Hydrocarbon cracking method and reactor

Номер: CN102260519A
Принадлежит: General Electric Co

烃类裂解方法包括:提供蒸汽和烃类;将蒸汽和烃类输入接触烃类的表面含有化学式为A a B b C c D d O 3-δ 的钙钛矿材料的反应装置,其中0<a<1.2,0≤b≤1.2,0.9<a+b≤1.2,0<c<1.2,0≤d≤1.2,0.9<c+d≤1.2,-0.5<δ<0.5;A从钙(Ca)、锶(Sr)、钡(Ba)及其组合选取;B从锂(Li)、钠(Na)、钾(K)、铷(Rb)及其组合选取;C从铈(Ce)、锆(Zr)、锑(Sb)、镨(Pr)、钛(Ti)、铬(Cr)、锰(Mn)、铁(Fe)、钴(Co)、镍(Ni)、镓(Ga)、锡(Sn)、铽(Tb)及其组合选取;D从镧(La)、铈(Ce)、镨(Pr)、钕(Nd)、钷(Pm)、钐(Sm)、铕(Eu)、钆(Gd)、铽(Tb)、镝(Dy)、钬(Ho)、铒(Er)、铥(Tm)、镱(Yb)、镥(Lu)、钪(Sc)、钛(Ti)、钒(V)、铬(Cr)、锰(Mn)、铁(Fe)、钴(Co)、镍(Ni)、铜(Cu)、锌(Zn)、钇(Y)、锆(Zr)、铌(Nb)、钼(Mo)、锝(Tc)、钌(Ru)、铑(Rh)、钯(Pd)、银(Ag)、镉(Cd)、铪(Hf)、钽(Ta)、钨(W)、铼(Re)、锇(Os)、铱(Ir)、铂(Pt)、金(Au)、镓(Ga)、铟(In)、锡(Sn)、锑(Sb)及其组合选取。

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27-07-2005 дата публикации

Oligomerisation of olefins with zeolite catalyst

Номер: GB0512377D0
Автор: [UNK]
Принадлежит: ExxonMobil Chemical Patents Inc

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03-09-2020 дата публикации

Automation type powder washing device system for synthesis of high furity powder

Номер: KR102150884B1
Принадлежит: 한국세라믹기술원

자동화 방식의 도입으로 ZnS 나노분말 특성에 대한 균일성을 향상시킬 수 있는 고순도 분말 합성을 위한 자동화 방식의 분말 수세 장치 시스템에 대하여 개시한다. 본 발명에 따른 고순도 분말 합성을 위한 자동화 방식의 분말 수세 장치 시스템은 반응조; 상기 반응조에 ZnS 나노분말 슬러리를 공급하기 위한 슬러리 저장 탱크; 상기 반응조에 수세액을 공급하기 위한 수세액 저장 탱크; 상기 반응조의 내부로 공급되는 ZnS 나노분말 슬러리를 수세액으로 교반하면서 수세하기 위한 오버 헤드 스터러; 상기 반응조의 내부에 장착되며, 수세된 상기 ZnS 나노분말 슬러리를 여과하기 위한 여과 필터; 상기 여과 필터에 의해 필터링된 상기 ZnS 나노분말 슬러리를 건조하기 위해, 상기 반응조의 외부에 장착된 히팅 유닛; 및 상기 반응조의 하측에 장착되어, 상기 여과 필터를 통과한 여과액이 배출되는 여과액 저장 탱크;를 포함하는 것을 특징으로 한다. Disclosed is a powder washing device system of an automated method for synthesizing high-purity powders that can improve the uniformity of ZnS nanopowder properties by introducing an automated method. An automated powder washing device system for synthesizing high-purity powder according to the present invention comprises: a reaction tank; A slurry storage tank for supplying the ZnS nanopowder slurry to the reaction tank; A washing liquid storage tank for supplying a washing liquid to the reaction tank; An overhead stirrer for washing with water while stirring the ZnS nanopowder slurry supplied to the inside of the reaction tank with a water washing solution; A filtration filter mounted inside the reaction tank and configured to filter the washed ZnS nanopowder slurry; A heating unit mounted on the outside of the reaction tank to dry the ZnS nanopowder slurry filtered by the filtration filter; And a filtrate storage tank mounted below the reaction tank to discharge the filtrate that has passed through the filtration filter.

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08-09-2005 дата публикации

Reactor with an insert having a heat exchanger area

Номер: DE102004005863A1

Die Erfindung betrifft einen Reaktor miteinander fluidleitend verbunden mindestens aufweisend: DOLLAR A - einen Reaktionsbereich, DOLLAR A wobei der Reaktionsbereich mindestens einen Feststoffkatalysator aufweist; DOLLAR A - einen kühlbaren Wärmetauscherbereich, DOLLAR A wobei der Wärmeaustauscherbereich mindestens ein Gehäuse aufweist, DOLLAR A wobei das Gehäuse mindestens teilweise einen Einsatz aufnimmt, DOLLAR A wobei der Einsatz eine Mehrzahl von Elementen aufweist, DOLLAR A ein Verfahren zur Oxidation eines Kohlenwasserstoffs unter Einsatz des Reaktors, ein oxidiertes Kohlenwasserstoff-Produkt, erhältlich aus diesem Verfahren, chemische Produkte wie Fasern, Folien, Formkörper und dergleichen, basierend auf diesem oxidierten Kohlenwasserstoff-Produkt, sowie die Verwendung dieses oxidierten Kohlenwasserstoff-Produkts in derartigen chemischen Produkten. The invention relates to a reactor fluidly connected to each other at least comprising: DOLLAR A - a reaction region, DOLLAR A wherein the reaction region has at least one solid catalyst; DOLLAR A - a coolable heat exchanger area, DOLLAR A wherein the heat exchanger area comprises at least one housing, DOLLAR A wherein the housing at least partially receives an insert, DOLLAR A wherein the insert comprises a plurality of elements, DOLLAR A a method for the oxidation of a hydrocarbon using the Reactor, an oxidized hydrocarbon product, obtainable from this process, chemical products such as fibers, films, moldings and the like, based on this oxidized hydrocarbon product, as well as the use of this oxidized hydrocarbon product in such chemical products.

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22-01-1992 дата публикации

Patent JPH043254B2

Номер: JPH043254B2
Автор: [UNK]
Принадлежит: [UNK]

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20-04-2016 дата публикации

Miniature lubricating grease reaction kettle

Номер: CN105498668A
Автор: 卢小辉, 谢小鹏

本发明公开了一种小型润滑脂反应釜,包括釜体、设置在釜体内的搅拌轴、设置在釜体顶部的釜盖、设置在釜体的底座,以及设置在釜盖上的气动马达;所述气动马达通过马达支座与釜盖连接,气动马达的转轴通过联接套与搅拌轴连接。所述搅拌轴通过两个轴承与釜盖连接,搅拌轴在釜体内的一端装有搅拌浆,在该两个轴承之间增设有轴承定位套,通过轴承定位套将该两个轴承隔开。本与现有技术相比,本发明通过气动马达驱动搅拌装置,利用气阀可以方便地控制搅拌转速,并具有良好的防爆性能,适用于各种润滑脂的少量制备与研发。本发明技术手段简便易行,便于推广应用。

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24-03-2016 дата публикации

Reaction process with membrane separation

Номер: CA2961693A1
Принадлежит: VITO NV

Provided herein are processes for carrying out a chemical reaction of a substrate in a diluted reaction mixture. The processes comprise the conducting the reaction mixture comprising reaction product and solvent to a filtration membrane which is permeable to the solvent impermeable to the reaction product; and recycling solvent which permeates the filtration membrane for dilution of the substrate feed.

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03-04-2018 дата публикации

Method for converting carbon and hydrocarbon cracking and apparatus for hydrocarbon cracking

Номер: CA2802677C
Принадлежит: Bl Technologies Inc

A method for converting carbon into a carbon oxide, comprises: contacting carbon with steam in presence of a carnegieite-like material of formula (Na2O)xNa2[Al2Si2O8], wherein 0<x=l. Method and apparatus for hydrocarbon cracking are also described herein.

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14-05-2021 дата публикации

Apparatus and method for converting uranium hexafluoride to uranium dioxide

Номер: CN112805791A
Принадлежит: Framatome SA

用于将六氟化铀(UF 6 )转化为二氧化铀(UO 2 )的设备包括用于将UF 6 转化为氟氧化铀粉末(UO 2 F 2 )的水解反应器(4)、用于将由反应器(4)提供的UO 2 F 2 粉末转化为UO 2 粉末的高温水解炉(6)、包括用于注入UF 6 、水蒸汽或H 2 的试剂注入管道(10)的供给装置(8)以及被构造为控制供给装置(8)以在转化设备的停止或启动阶段期间向至少一个试剂注入管道(10)供给中性气体的控制系统(16)。

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05-07-2007 дата публикации

Oxidation system employing internal structure for enhanced hydrodynamics

Номер: US20070155986A1
Принадлежит: Individual

Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

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04-03-2020 дата публикации

Manufacturing process for cyclodextrin derivatives

Номер: EP2814849B8
Принадлежит: Cydex Pharmaceuticals Inc

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19-07-2007 дата публикации

Oxidation system employing internal structure for enhanced hydrodynamics

Номер: CA2635357A1

Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

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18-08-2021 дата публикации

Installation and method for converting uranium hexafluoride into uranium dioxide

Номер: EP3864674A1
Принадлежит: Framatome SA

The installation for converting uranium hexafluoride (UF 6 ) into uranium dioxide (U0 2 ) comprises a hydrolysis reactor (4) for converting UF 6 into uranium oxyfluoride powder (U0 2 F 2 ), a pyrohydrolysis furnace (6) for converting the U0 2 F 2 powder provided by the reactor (4) into U0 2 powder, a supply device (8) comprising reagent injection pipes (10) for injecting UF 6 , water vapor or H 2 , and a control system (16) configured to control the supply device (8) in such a way as to supply at least one of the reagent injection pipes (10) with a neutral gas during a phase of stopping or starting the conversion installation.

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31-12-2008 дата публикации

Method of operating a riser reactor

Номер: EP1702026B1
Автор: Jeffrey S. Smith
Принадлежит: ExxonMobil Chemical Patents Inc

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01-05-2013 дата публикации

Method for converting carbon and hydocarbon cracking and apparatus for hydrocarbon cracking

Номер: EP2585560A1
Принадлежит: General Electric Co

A method for converting carbon into a carbon oxide, comprises: contacting carbon with steam in presence of a carnegieite-like material of formula (Na 2 O) x Na 2 [Al 2 Si 2 O 8 ], wherein 0<x≤l. Method and apparatus for hydrocarbon cracking are also described herein.

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05-01-2012 дата публикации

Method for converting carbon and hydrocarbon cracking and apparatus for hydrocarbon cracking

Номер: CA2802677A1
Принадлежит: General Electric Co

A method for converting carbon into a carbon oxide, comprises: contacting carbon with steam in presence of a carnegieite-like material of formula (Na2O)xNa2[Al2Si2O8], wherein 0<x=l. Method and apparatus for hydrocarbon cracking are also described herein.

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10-07-2003 дата публикации

Slurry phase apparatus

Номер: US20030129110A1
Автор: Andre Peter Steynberg
Принадлежит: Sasol Technology Pty Ltd

Slurry phase apparatus is provided which includes a slurry vessel for holding a slurry comprising a liquid and solid particles and gas distribution means for injecting a gas into the slurry. The gas distribution means includes a sparger device which includes an apertured sparger portion inside the slurry vessel, an inlet portion leading into the slurry vessel and an outlet portion leading from the slurry vessel. The gas distribution means also includes closure means, external of the slurry vessel, and being operable to allow or deny flow from the sparger portion out through the outlet portion of the sparger device. The invention extends to a method of introducing or reintroducing a gas into a slurry vessel.

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18-06-2021 дата публикации

Device and process for gas-solid separation of catalytic cracking in a fluidized bed with side openings

Номер: FR3104469A1
Принадлежит: IFP Energies Nouvelles IFPEN

Dispositif et un procédé de séparation et de stripage d’un mélange gazeux et de particules solides comprenant une pluralité de chambres de séparation (12) et de préstripage (13) réparties autour d’un réacteur central (14), chaque chambre de préstripage (13) comprenant une paroi périphérique, une ouverture de sortie inférieure (24) de particules solides adaptée pour communiquer avec la chambre de stripage (23), une ouverture de sortie supérieure (31) du mélange gazeux et de gaz de stripage adaptée pour communiquer avec un second étage de séparation ; et une ouverture d’entrée latérale (28) du gaz de stripage. Figure 4 à publier Device and a method for separating and stripping a gas mixture and solid particles comprising a plurality of separation (12) and pre-stripping (13) chambers distributed around a central reactor (14), each pre-stripping chamber ( 13) comprising a peripheral wall, a lower outlet opening (24) of solid particles adapted to communicate with the stripping chamber (23), an upper outlet opening (31) of the gas mixture and stripping gas adapted to communicate with a second separation stage; and a side inlet opening (28) for stripping gas. Figure 4 to publish

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29-03-2022 дата публикации

Method of Preventing Fluidization of Catalyst Fixed Beds in Tubular Up-Flow Reactor of Steam Methane Reformer

Номер: KR20220038697A

본 발명은, 촉매 베드의 유동화 전의 잔류 압력 강하 마진을 추정하는 것 그리고 그에 응답하여 반응물 가스 유동을 조정하는 것에 의해서, 상향-유동 구성으로 동작되는 관형 반응기 내에 존재하는 촉매 고정 베드의 유동화를 방지하는 방법에 관한 것이다. 또한, 본 발명은 상향-유동 구성으로 동작되는 복수의 촉매 고정 베드 반응기를 포함하는 흡열 반응을 수행하기에 적합한 퍼니스를 안전하게 동작시키기 위한 방법, 그리고 상향 유동 방향으로 유동하는 가스를 포함하는 촉매 고정 베드 반응기를 안전하게 병목 현상 제거하기 위한 방법에 관한 것이다.

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19-03-2020 дата публикации

Shut-down process for the production of glycols

Номер: WO2020055796A1

The invention provides a shut down method for a process for the preparation of glycols from a starting material comprising one or more saccharides in the presence 5 of hydrogen and a catalyst system comprising one or more retro-aldol catalysts comprising tungsten and one or more catalytic species suitable for hydrogenation in a reactor, said method comprising removing the one or more retro-aldol catalysts from the reactor whilst also in the presence of one or more agents suitable to suppress tungsten precipitation.

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09-03-1999 дата публикации

Fast cooling reactor and method

Номер: JPH11502760A

(57)【要約】 高速冷却反応が、その入口におけるプラズマトーチ及びその出口端における制限的中軸ノズルなど高温加熱手段を有する反応器室を含む。反応物を反応器室に噴射する。こうして得られる加熱ガス流をノズルに通過させることにより急速に冷却する。これにより、加熱平行反応段階において所望の最終生成物を「凍結する」。

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