04-01-2018 дата публикации
Номер: US20180001298A1
The subject invention concerns metal or metalloid oxide-based sol-gel hybrid sorbent and methods of synthesis. In one embodiment, the sorbent is a ZrOpolypropylene oxide based sol-gel. The subject invention also concerns a hollow tube or capillary internally coated with a sorbent of the invention. Sorbent coated tubes and capillaries of the invention can be used in extraction and/or enrichment of samples to be analyzed for catecholamines and related compounds. 1. A metal or metalloid oxide-based sol-gel hybrid sorbent composition prepared from a biocompatible polymer or ligand comprising one or more sol-gel active end groups.2. The sorbent composition according to claim 1 , wherein the metal or metalloid of the sorbent composition is aluminum claim 1 , antimony claim 1 , arsenic claim 1 , barium claim 1 , beryllium claim 1 , bismuth claim 1 , boron claim 1 , cadmium claim 1 , cerium claim 1 , chromium claim 1 , cobalt claim 1 , copper claim 1 , dysprosium claim 1 , erbium claim 1 , europium claim 1 , gadolinium claim 1 , gallium claim 1 , gold claim 1 , hafnium claim 1 , holmium claim 1 , indium claim 1 , iridium claim 1 , iron claim 1 , lanthanum claim 1 , lithium claim 1 , magnesium claim 1 , manganese claim 1 , molybdenum claim 1 , neodymium claim 1 , nickel claim 1 , niobium claim 1 , osmium claim 1 , palladium claim 1 , platinum claim 1 , praseodymium claim 1 , rhodium claim 1 , ruthenium claim 1 , samarium claim 1 , scandium claim 1 , selenium claim 1 , silver claim 1 , strontium claim 1 , tellurium claim 1 , terbium claim 1 , thallium claim 1 , thulium titanium claim 1 , tantalum claim 1 , vanadium claim 1 , yttrium claim 1 , zirconium claim 1 , zinc claim 1 , tungsten claim 1 , or any combination thereof.3. The sorbent composition according to claim 1 , wherein the sorbent composition comprises ZrOpolypropylene oxide (ZrOPPO).5. The sorbent composition according to claim 1 , wherein the polymer or ligand used to prepare the sorbent composition comprises one ...
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