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Небесная энциклопедия

Космические корабли и станции, автоматические КА и методы их проектирования, бортовые комплексы управления, системы и средства жизнеобеспечения, особенности технологии производства ракетно-космических систем

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Мониторинг СМИ

Мониторинг СМИ и социальных сетей. Сканирование интернета, новостных сайтов, специализированных контентных площадок на базе мессенджеров. Гибкие настройки фильтров и первоначальных источников.

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Поддерживает ввод нескольких поисковых фраз (по одной на строку). При поиске обеспечивает поддержку морфологии русского и английского языка
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Применить Всего найдено 4987. Отображено 100.
07-06-2012 дата публикации

Green luminescent glass for ultraviolet led and preparation method thereof

Номер: US20120138854A1
Автор: Mingjie Zhou, Wenbo Ma, Zhaopu Shi
Принадлежит: Mingjie Zhou, Wenbo Ma, Zhaopu Shi

A green luminescent glass for ultraviolet LED and a preparation method for glass are disclosed. The preparation method includes: weighing raw materials of CaCO 3 , Al 2 O 3 , SiO 2 , CeO 2 and Tb 4 O 7 respectively and mixing the raw materials evenly; melting the raw materials at 1500˜1700 for 0.5˜3 hours and then molding to form a glass; annealing the formed glass in reducing atmosphere with temperature of 650˜1050 for 3˜20 hours; and cooling the glass to room temperature to obtain the green luminescent glass for ultraviolet LED. The green luminescent glass for ultraviolet LED prepared according to the preparation method of the disclosure has advantages of high luminous intensity, uniformity and stability.

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Номер записи: 1
08-11-2012 дата публикации

Glass with high frictive damage resistance

Номер: US20120282449A1
Автор: Timothy Michael Gross
Принадлежит: Corning Inc

A glass article exhibiting improved resistance to fictive surface damage and a method for making it, the method comprising removing a layer of glass from at least a portion of a surface of the article that is of a layer thickness at least effective to reduce the number and/or depth of flaws on the surface of the article, and then applying a friction-reducing coating to the portion of the article from which the layer of surface glass has been removed.

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Номер записи: 2
22-11-2012 дата публикации

Copper-contaning silica glass, method for producing the same, and xenon flash lamp using the same

Номер: US20120291488A1
Автор: Akira Fujinoki, Hidetsugu Yoshida, Hiroyuki Nishimura, Masahiro Nakatsuka, Michinari Ohuchi, Tetsuji Ueda
Принадлежит: OPTO ELECTRONICS Labs Inc, Shin Etsu Quartz Products Co Ltd

It is an object of the present invention to provide a copper-containing silica glass which emits fluorescence having a peak in a wavelength range of from 520 nm to 580 nm under irradiation of ultraviolet light with a wavelength of 400 nm or less, and which is excellent in long term stability even in the high output use. The copper-containing silica glass is made to have copper of from 5 wtppm to 200 wtppm, which emits fluorescence having a peak in a wavelength range of from 520 nm to 580 nm under irradiation of ultraviolet light with a wavelength ranging from 160 nm to 400 nm, and in which an internal transmittance per 2.5 mm thickness at a wavelength of 530 nm is 95% or more.

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Номер записи: 3
11-04-2013 дата публикации

Anti-Bird Glass and Method of Its Production and Use

Номер: US20130087720A1
Автор: Franz Krampl, Gerhard Cesnik, Guenther Arnold, Hans-Joachim Arnold, Simon Remschnig
Принадлежит: ISOLAR ISOLIERGLASERZEUGUNG GMBH

The present invention relates to a pane element with a protective device against bird strikes, whereby a protective structure is arranged on the outer area of a pane element which structure absorbs light in the wavelength range of approximately 320 nm to 420 nm, in particular at approximately 350 nm to 380 nm and emits by Stokes shift on the longer wave range, in particular in the UV range or near UV range into the visible wavelength range and is visible as a hindrance for a bird that cannot be flown through and is largely not visible to the human eye or seems translucent or can be recognized as an anti-bird structure, and relates to a method for the production and the use for avoiding the injuring or killing of birds.

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Номер записи: 4
02-05-2013 дата публикации

RARE EARTH IONS DOPED ALKALI METAL SILICATE LUMINESCENT GLASS AND THE PREPARATION METHOD THEREOF

Номер: US20130105734A1
Автор: Ma Wenbo, Qiao Yanbo, Zhou Mingjie
Принадлежит:

A preparation method of rare earth ions doped alkali metal silicate luminescent glass is provided. The steps involves: step 1, mixing the source compounds of cerium, terbium and alkali metals and putting the mixture into solvent to get a mixed solution; step 2, impregnating the nanometer micropores glass with the mixed solution obtained in step 1; step 3: calcining the impregnated nanometer micropores glass obtained in step 2 in a reducing atmosphere, cooling to room temperature, then obtaining the cerium and terbium co-doped alkali metal silicate luminescent glass. Besides, the rare earth ions doped alkali metal silicate luminescent glass prepared with aforesaid method is also provided. In the prepared luminescent glass, cerium ions can transmit absorbed energy to terbium ions under the excitation of UV light due to the co-doping of cerium ions. As a result, the said luminescent glass has higher luminous intensity than the glass only doped with terbium. 1. A preparation method of rare earth ions doped alkali metal silicate luminescent glass , comprising:step one: mixing the source compounds of cerium, terbium and alkali metal and dissolving them in a solvent to obtain a mixed solution;step two: submerging a nano-porous glass into the mixed solution obtained in step 1 for soaking;step three: sintering the soaked nano-porous glass obtained in step 2 in reductive atmosphere, then cooling to room temperature to obtain a cerium and terbium co-doped alkali metal silicate luminescent glass.2. The preparation method of claim 1 , wherein in step one the source compound of terbium is one or more selected from the group consisting of oxide claim 1 , nitrate claim 1 , chloride and acetate of terbium; the source compound of cerium is one or more selected from the group consisting of oxide claim 1 , nitrate claim 1 , chloride claim 1 , sulfate and acetate of cerium; the source compound of alkali metal is one or more selected from the group consisting of nitrate claim 1 , ...

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Номер записи: 5
20-06-2013 дата публикации

IONICALLY CONDUCTIVE MATERIAL AND PROCESS FOR PRODUCING SAME

Номер: US20130157172A1
Автор: Daiko Yusuke, Takase Hironori, YAMADA Takeshi, Yamazaki Hiroki, Yazawa Tetsuo
Принадлежит:

Provided is an ion-conducting material, comprising, as a composition in terms of mol o, 15 to 80% of PO, 0 to 70% of SiO, and 5 to 35% of RO, which represents the total content of LiO, NaO, KO, RbO, CsO, and AgO. 1. An ion-conducting material , comprising , as a composition in terms of mol % , 15 to 80% of PO , 0 to 70% of SiO , and 5 to 35% of RO , which represents a total content of LiO , NaO , KO , RbO , CsO , and AgO.2. The ion-conducting material according to claim 1 , wherein RO comprises at least two or more kinds of components among LiO claim 1 , NaO claim 1 , KO claim 1 , RbO claim 1 , CsO claim 1 , and AgO.3. The ion-conducting material according to claim 1 , wherein a content of POis 15 to 60% and a content of SiOis 10 to 60%.4. The ion-conducting material according to claim 1 , wherein the ion-conducting material has a molar ratio of (NaO+KO)/RO of 0.2 to 1.0.5. The ion-conducting material according to claim 1 , wherein the ion-conducting material has a molar ratio of NaO/RO of 0.2 to 0.8.6. The ion-conducting material according to claim 1 , wherein the ion-conducting material has a molar ratio of KO/RO of 0.2 to 0.8.7. The ion-conducting material according to claim 1 , further comprising 0.1 mol % or more of AlOin the composition.8. The ion-conducting material according to claim 1 , wherein the ion-conducting material has an ionic conductivity logσ (S/cm) at 500° C. of −5.5 or more and has a transport number of a proton at 500° C. of 0.7 or more.9. The ion-conducting material according to claim 1 , wherein the ion-conducting material has an areal resistance value (Ω.cm) at 500° C. of 30 or less.10. The ion-conducting material according to claim 1 , wherein the ion-conducting material is an amorphous material with a crystallinity of 50% or less.11. The ion-conducting material according to claim 1 , wherein the ion-conducting material has a thin-sheet shape and has a thickness of 1 to 500 μm.12. The ion-conducting material according to claim 1 , wherein ...

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Номер записи: 6
01-08-2013 дата публикации

GLASS COMPOSITIONS, DIELECTRIC COMPOSITIONS AND MULTILAYER CERAMIC CAPACITOR HAVING HIGH CAPACITANCE USING THE SAME

Номер: US20130196159A1
Автор: OH Young Joo, YOON Jung Rag
Принадлежит: SAMHWA CAPACITOR CO., LTD.

Disclosed are a glass composition and a dielectric composition enabling low temperature sintering, and a high capacitance multilayer ceramic capacitor using the same. In the glass composition used for sintering, the glass composition may be formed of a formula, aRO-bCaO-cZnO-dBaO-eBO-fAlO-gSiO, and the formula may satisfy a+b+c+d+e+f+g=100, 0≦a≦7, 1≦b≦3, 1≦c≦15, 10≦d≦20, 3≦e≦10, 0≦f≦3, and 55≦g≦72. Through this, when manufacturing the high capacity multilayer ceramic capacitor, the dielectric substance may enable the lower temperature sintering, thereby enhancing a capacitance and a reliability of the high capacitance multilayer ceramic capacitor. 1. A glass composition used for sintering , wherein the glass composition is formed of a formula , aRO-bCaO-cZnO-dBaO-eBO-fAlO-gSiO , and the formula satisfies a+b+c+d+e+f+g=100 , 0≦a≦7 , 1≦b≦3 , 1≦c≦15 , 10≦d≦20 , 3≦e≦10 , 0≦f≦3 , and 55≦g≦72.2. The glass composition of claim 1 , wherein the glass composition corresponds to a spherical nano powder having an average grain size of 30 nm to 200 nm.3. The glass composition of claim 2 , wherein the spherical nano powder is spheroidized or vaporized by performing thermal plasma processing of a glass powder having a size of 0.2 μm to 30 μm.4. The glass composition of claim 3 , wherein a temperature of the thermal plasma processing is 3000° C. to 8000° C.5. The glass composition of claim 4 , wherein a radio frequency (RF) plasma torch is used for the thermal plasma processing. This application claims the benefit of Korean Patent Application No. 10-2010-0086481, filed on Sep. 3, 2010, in the Korean Intellectual Property Office, the disclosure of which is incorporated herein by reference.1. Field of the InventionThe present invention relates to a glass composition, a dielectric composition, and a high capacitance multilayer ceramic capacitor using the same, and more particularly, to a glass composition and a dielectric composition enabling low temperature sintering, and a high ...

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Номер записи: 7
15-08-2013 дата публикации

Arsenic and antimony free, titanium oxide containing borosilicate glass and methods for the production thereof

Номер: US20130207058A1
Автор: Holger Wegener, Lenka Grygarova, Rainer Schwertfeger, Reinhard Kassner
Принадлежит: SCHOTT AG

Titanium oxide containing borosilicate glasses, which have been produced without the use of arsenic and antimony compounds, are provided. An environmentally friendly refining method for providing titanium oxide containing borosilicate glass is also provided. The method includes using oxygen containing selenium compounds as refining agents to provide glasses with good transmittance values in the infrared range and show no disturbing discolorations. The glasses of the present disclosure are particularly suitable for the production of IR light conductors, cover glasses for photo sensors, and UV filters.

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Номер записи: 8
19-09-2013 дата публикации

WHITE LIGHT-EMITTING GLASS, GLASS-COVERED LIGHT-EMITTING ELEMENT, AND LIGHT-EMITTING DEVICE

Номер: US20130241399A1
Автор: FUJIWARA Takumi, Masai Hirokazu, Matsumoto Syuji, Yoko Toshinobu
Принадлежит:

A glass emitting white light in itself, and a light-emitting element and a light-emitting device covered with the glass as stated above are provided. The white light-emitting glass is a glass emitting fluorescence at a region having a wavelength of 380 nm to 750 nm by excitation light with a wavelength of 240 nm to 405 nm, not containing crystal, and containing SnO(where x=1 to 2, typically x=1 or 2), PO, and MnO(where y=1 to 2, typically y=1 or 2). The light-emitting element and the light-emitting device are made up by covering a main surface of a semiconductor light-emitting element with the glass as stated above. 1. A white light-emitting glass emitting fluorescence at a region having a wavelength of 380 nm to 750 nm by excitation light with a wavelength of 240 nm to 405 nm and not containing a crystal , the glass containing:{'sub': x', '2', '5', 'y, 'SnO(where x=1 to 2, typically x=1 or 2), PO, ZnO and MnO(where y=1 to 2, typically y=1 or 2).'}2. The white light-emitting glass according to claim 1 ,wherein a chromaticity coordinating position X of a light-emission color is 0.22 to 0.40 and a chromaticity coordinating position Y is 0.25 to 0.35.3. The white light-emitting glass according to claim 1 ,{'sub': y', 'x, 'wherein an existence ratio of MnO(where y=1 to 2, typically y=1 or 2) does not exceed an existence ratio of SnO(where x=1 to 2, typically x=1 or 2).'}4. The white light-emitting glass according to claim 1 , containing:{'sub': 2', '5, 'from 27.5% to 44.4% of PO,'}{'sub': 'x', 'from 0.1% to 40% of SnO(where x=1 to 2, typically x=1 or 2),'}from 30% to 71% of ZnO:, and{'sub': m', 'n, 'from “0” (zero) % to 10% of MO(where M is an element selected from Ti, Zr, V, Nb, Cr, Ni, Cu, B, Al, Si, Cl, Ga, Ge, As, Se, Cd, In, Sb, Te, Hg, Tl, Bi, S and rare-earth elements, and m and n are integers of 1 or more) as expressed in mol % on an oxide basis, and further containing{'sub': 'y', 'from 0.1% to 2.4% of MnO(where y=1 to 2, typically y=1 or 2) in outer percentage ...

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Номер записи: 9
03-10-2013 дата публикации

BISMUTH BORATE GLASS ENCAPSULANT FOR LED PHOSPHORS

Номер: US20130256598A1
Автор: Aitken Bruce Gardiner, Badding Michael Edward, Borrelli Nicholas Francis, Lonnroth Nadja Teresia
Принадлежит:

Embodiments are directed to glass frits containing phosphors that can be used in LED lighting devices and for methods associated therewith for making the phosphor containing glass frit and their use in glass articles, for example, LED devices. 1. An article comprising a glass layer , wherein the layer comprises a glass comprising BiOand at least 30 mol % BO; and at least one phosphor , wherein the layer is a fired mixture of a frit comprising the BiOand BOand the at least one phosphor.2. The article according to claim 1 , wherein the layer is Pb free.3. The article according to claim 1 , wherein the glass comprises in mole percent:{'sub': 2', '3, '10-30% BiO;'}{'sub': '2', '0-20% MO, wherein M is Li, Na, K, Cs, or combinations thereof;'}0-20% RO, wherein R is Mg, Ca, Sr, Ba, or combinations thereof;{'sub': '2', '15-50% ZnO, ZnF, or a combination thereof;'}{'sub': 2', '3, '0-5% AlO;'}{'sub': 2', '5, '0-5% PO; and'}{'sub': 2', '3, '30-55% BO.'}4. The article according to claim 3 , comprising in mole percent:{'sub': 2', '3, '10-30% BiO;'}{'sub': '2', 'greater than 0% NaO;'}{'sub': '2', '15-50% ZnO, ZnF, or a combination thereof;'}{'sub': 2', '3, '30-55% BO;'}{'sub': '2', '0-3% SiO;'}{'sub': '3', '0-1% WO;'}0-12% BaO, CaO, SrO, or combinations thereof.5. The article according to claim 4 , comprising at least 1% NaO.6. The article according to claim 4 , comprising 15-50% ZnO.7. The article according to claim 4 , comprising:{'sub': 2', '3, '12-20% BiO;'}{'sub': '2', '5-12% NaO;'}20-30% ZnO;{'sub': 2', '3, '38-52% BO;'}{'sub': '2', '0-3% SiO;'}{'sub': '3', '0-1% WO;'}1-12% BaO, CaO, SrO, or combinations thereof.8. The article according to claim 7 , comprising:{'sub': 2', '3, '14-16% BiO;'}{'sub': '2', '5-11% NaO;'}22-27% ZnO;{'sub': 2', '3, '40-51% BO;'}{'sub': '2', '0-3% SiO;'}{'sub': '3', '0-1% WO;'}1-11% BaO, CaO, SrO, or combinations thereof.9. The article according to claim 8 , wherein the glass has a refractive index of 1.81-1.83 at 473 nm and a glass transition ...

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Номер записи: 10
07-11-2013 дата публикации

Light Emitting Device

Номер: US20130293099A1
Автор: Andrew J. Steckl, Steven C. Allen
Принадлежит: QUARKSTAR LLC

A light emitting device includes a base; a light emitting diode (LED) supported by the base; a layer spaced apart from the LED and including a light emitting material of refraction index n 1 . An enclosure formed by the layer and the base encloses the LED. A medium inside the enclosure between the LED and the layer has a refraction index n 0 <n 1 ; and an optic in contact with the layer and having a refraction index n 2 ≧n 1 . The layer is positioned between the optic and the LED. The optic has, at a surface of contact with the layer, a radius r measured along a ray originating from the LED, and, at an output surface of the optic, another radius R measured along the same ray, such that R≧r·(n 1 /n m ), where n m is a refraction index of a medium adjacent the output surface of the optic.

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Номер записи: 11
26-12-2013 дата публикации

Glass compositions with improved chemical and mechanical durability

Номер: US20130344263A1
Автор: Melinda Ann Drake, Paul Stephen DANIELSON, Robert Anthony Schaut, Robert Michael Morena, Santona Pal, Steven Edward DeMartino
Принадлежит: Corning Inc

The embodiments described herein relate to chemically and mechanically durable glass compositions and glass articles formed from the same. In another embodiment, a glass composition may include from about 70 mol. % to about 80 mol. % SiO 2 ; from about 3 mol. % to about 13 mol. % alkaline earth oxide; X mol. % Al 2 O 3 ; and Y mol. % alkali oxide. The alkali oxide may include Na 2 O in an amount greater than about 8 mol. %. A ratio of Y:X may be greater than 1 and the glass composition may be free of boron and compounds of boron. In some embodiments, the glass composition may also be free of phosphorous and compounds of phosphorous. Glass articles formed from the glass composition may have at least a class S3 acid resistance according to DIN 12116, at least a class A2 base resistance according to ISO 695, and a type HGA1 hydrolytic resistance according to ISO 720.

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Номер записи: 12
23-01-2014 дата публикации

Quantum Dot Luminescent Materials

Номер: US20140021368A1
Автор: Amin Himanshu Subhash, Chakravarthy Krishnan, Kamisetti Siddhartha Venkata
Принадлежит: NANOAXIS, LLC

A quantum dot dispersed glass article is disclosed herein and associated articles, products, and methods of making thereof. In an aspect, a glass material can incorporate one or more quantum dot dispersed therein, wherein the one or more quantum dot luminesces upon excitation from an excitation source. In another aspect, the quantum dot can take a variety of shapes and sizes. In another aspect, the quantum dot can be water soluble. In yet another aspect, the quantum dot can be dispersed within one or more glass cavities. 1. An article , comprising:a glass material incorporating one or more quantum dots dispersed therein, wherein the one or more quantum dots luminesce upon excitation from an excitation source.2. The article of claim 1 , wherein the at least one quantum dots are of at least one of the following shapes: teardrop claim 1 , arrow claim 1 , snowflake claim 1 , multi-leg luminescent nanoparticle claim 1 , multi-branched luminescent nanoparticle compound claim 1 , sphere claim 1 , luminescent tetrapod dot claim 1 , tetrapod claim 1 , rod claim 1 , or dendrimer.3. The article of claim 1 , wherein the at least one quantum dots have a longest diametric length greater than 1 nm and smaller than 999 nm.4. The article of claim 1 , wherein the at least one quantum dots are water-soluble.5. The article of claim 1 , wherein the at least one quantum dots comprise a water-soluble semiconductor comprising:a base semiconductor material; anda shell semiconductor material surrounding the base material.6. The article of claim 5 , wherein the base material is a II-IV semiconductor or a III-V semiconductor.7. The article of claim 5 , wherein the base semiconductor material is a II-IV semiconductor.8. The article of claim 5 , wherein the base semiconductor material is a III-V semiconductor.9. The article of claim 6 , wherein the base semiconductor material is at least one of: MgS claim 6 , MgSe claim 6 , MgTe claim 6 , CaS claim 6 , CaSe claim 6 , CaTe claim 6 , SrS claim 6 , ...

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Номер записи: 13
23-01-2014 дата публикации

ION EXCHANGEABLE LI-CONTAINING GLASS COMPOSITIONS FOR 3-D FORMING

Номер: US20140023865A1
Автор: Comte Marie Jacqueline Monique, Drake Melinda Ann, Geisinger Karen Leslie, Gomez Sinue, Morena Robert Michael, Smith Charlene Marie, Youngman Randall Eugene
Принадлежит:

According to one embodiment, a glass article may include SiO, AlO, LiO and NaO. The glass article may have a softening point less than or equal to about 810° C. The glass article may also have a high temperature CTE less than or equal to about 27×10/° C. The glass article may also be ion exchangeable such that the glass has a compressive stress greater than or equal to about MPa and a depth of layer greater than or equal to about 25 μm after ion exchange in a salt bath comprising KNOat a temperature in a range from about 390° C. to about 450° C. for less than or equal to approximately 15 hours. 1. A glass article comprising SiO , AlO , LiO and NaO , the glass article having:a softening point less than or equal to about 810° C.;{'sup': '−6', 'a high temperature CTE less than or equal to about 27×10/° C.; and'}{'sub': '3', 'a compressive stress greater than or equal to about 600 MPa and a depth of layer greater than or equal to about 25 μm after ion exchange in a salt bath comprising KNOin a temperature range from about 390° C. to about 450° C. for less than or equal to approximately 15 hours.'}2. The glass article of claim 1 , the glass article has L claim 1 , a* claim 1 , b* claim 1 , color coordinates of L from about 0 to about 5.0 claim 1 , a* from about −2.0 to about 2.0 claim 1 , and b* from about 0 to about −5.0.3. The glass article of claim 1 , wherein the glass article has an opacity greater than or equal to about 80% over a range of wavelengths from about 350 nm to about 750 nm.4. The glass article of comprising:{'sub': '2', 'from about 65 mol. % to about 71 mol. % SiO;'}{'sub': 2', '3, 'from about 7 mol. % to about 12 mol. % AlO;'}{'sub': '2', 'from about 1 mol. % to about 9 mol. % LiO;'}{'sub': '2', 'from about 6 mol. % to about 16 mol. % NaO;'}{'sub': '2', 'from about 0 mol. % to about 5 mol. % KO;'}from about 0.8 to about 10 mol. % of a divalent oxide, wherein the divalent oxide comprises at least one of MgO and ZnO; and{'sub': 2', '3', '2', '3, 'less ...

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Номер записи: 14
13-02-2014 дата публикации

Luminophore composition for uv-visible light conversion and light converter obtained therefrom

Номер: US20140042477A1
Автор: Alain Ibanez, Antonio Carlos Hernandes, Lauro June Queiroz Maia, Vinicius Ferraz Guimaraes
Принадлежит: CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE CNRS

A luminophore composition comprising amorphous aluminoborate powders is disclosed. The composition is obtainable by preparing an aluminoborate resin by a wet chemical route based on precursors solutions substantially free from monovalent and divalent cations; drying the resin to obtain a solid; grinding the solid to obtain a powder; pyrolyzing the powder at a pyrolysis temperature lower than the crystallization temperature of the composition; and calcinating the powder so pyrolyzed at a calcination temperature lower than the crystallization temperature of the composition. Furthermore, a process for the preparation of said composition is disclosed. The composition is particularly suitable for use in solid-state lighting, and for example for converting UV light into warm white visible light.

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Номер записи: 15
20-02-2014 дата публикации

GRADED FLUORESCENT MATERIAL

Номер: US20140048831A1
Автор: Fujino Shigeru
Принадлежит: EMPIRE TECHNOLOGY DEVELOPMENT LLC

Some embodiments in the present disclosure generally relate to fluorescent structures such as fluorescent glass, fluorescent substrates, and/or light emitting devices, which can include a gradient of fluorescent molecules across the structure, substrate, and/or light emitting device. In some embodiments, the fluorescent glass, fluorescent substrates, and/or light emitting devices can be porous and include at least one fluorescent molecule within the one or more pore. In some embodiments, this can allow for the creation of a gradient fluorescent material throughout the material. 1. A graded fluorescent glass comprising: silica; and', 'a gradient of fluorescent molecules, wherein the gradient of fluorescent molecules comprises a first concentration of fluorescent molecules at the first surface, and a second concentration of fluorescent molecules at the second surface., 'a silica structure comprising a first surface and a second surface, and wherein the silica structure comprises'}2. The graded fluorescent glass of claim 1 , wherein a concentration of fluorescent molecules is about 50 ppm to about 10 claim 1 ,000 ppm.3. The graded fluorescent glass of claim 2 , wherein the gradient of fluorescent molecules comprises an approximately linear change in concentration from the first surface to the second surface.4. A light-emitting apparatus comprising:at least one light source; and silica;', 'at least a first pore within the silica and a second pore within the silica; and', 'at least a first fluorescent molecule within the first pore and at least two or more second fluorescent molecules within the second pore., 'a fluorescent silica glass, wherein the fluorescent silica glass comprises5. The light-emitting apparatus of claim 4 , wherein: the first fluorescent molecule absorbs radiation at a first wavelength of light claim 4 , the second fluorescent molecule absorbs radiation at a second wavelength of light claim 4 , and the first wavelength and the second wavelength are ...

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Номер записи: 16
07-01-2016 дата публикации

Glass sheet with a high level of infrared radiation transmission

Номер: US20160002094A1
Автор: Audrey DOGIMONT, Thomas LAMBRICHT
Принадлежит: AGC Glass Europe SA

The invention relates to a glass sheet with a high level of infrared radiation transmission, that can be used especially in a tactile tablet, panel or screen. More precisely, the invention relates to a glass sheet having a composition comprising, as a content expressed in total weight percentages of glass: SiO2 55-78%; AI2O3 0-18%; B2O3 0-18%; Na2O 5-20%; CaO 0-15%; MgO 0-10%; K2O 0-10%; BaO 0-5%; total iron (expressed in the form of Fe2O3) 0.002-0.06%; and a chromium content (expressed in the form of Cr2O3) of between 0.002 and 0.06%.

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Номер записи: 17
07-01-2016 дата публикации

DECORATIVE POROUS INORGANIC LAYER COMPATIBLE WITH ION EXCHANGE PROCESSES

Номер: US20160002104A1
Автор: Lehuede Philippe, Monique Marie Jacqueline
Принадлежит:

Embodiments of methods for forming strengthened glass articles comprise providing an exchangeable glass substrate having a coefficient of thermal expansion (CTE) between about 60×10−7°/C. to about 110×10−7°/C., depositing at least one decorative porous inorganic layer onto at least a portion of the surface of the glass substrate, wherein the decorative porous inorganic layer comprises a glass transition temperature (Tg)≧450° C., a glass softening temperature (Ts)≧650° C., wherein the difference in CTE values between the glass substrate and the decorative porous inorganic layer is within 10×10−7°/C.; and curing the glass substrate and the deposited decorative porous inorganic layer at a temperature greater than the Ts of the decorative porous inorganic layer; and chemically strengthening the cured glass substrate and the decorative porous inorganic layer thereon via ion exchange at a temperature below the Tg of the decorative porous inorganic layer. 1. A method for forming a strengthened glass article , the method comprising:{'sup': −7', '−7, 'providing an ion exchangeable glass substrate having a coefficient of thermal expansion (CTE) ranging between about 60×10/° C. to about 110×10/° C.;'}{'sup': '−7', 'depositing at least one decorative porous inorganic layer onto at least a portion of the surface of the glass substrate, wherein the decorative porous inorganic layer comprises a glass transition temperature (Tg)≧450° C., a glass softening temperature (Ts)≦650° C., wherein the difference in CTE values between the glass substrate and the decorative porous inorganic layer is within 10×10° C.;'}curing the glass substrate and the deposited decorative porous inorganic layer at a temperature greater than the glass softening temperature (Ts) of the decorative porous inorganic layer; andchemically strengthening the cured glass substrate and the decorative porous inorganic layer thereon via ion exchange at a temperature above the glass transition temperature (Tg) of the ...

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Номер записи: 18
05-01-2017 дата публикации

GLASS FOR CHEMICAL STRENGTHENING, CHEMICALLY STRENGTHENED GLASS, AND METHOD FOR MANUFACTURING CHEMICALLY STRENGTHENED GLASS

Номер: US20170001903A1
Автор: Akiba Shusaku, KASE Junichiro, MIYASAKA Junko, OHARA Seiki, YAMAZAKI Shuji
Принадлежит: Asahi Glass Company, Limited

An object of the present invention is to provide a glass for chemical strengthening which is capable of improving strength as compared with an ordinary soda lime silicate glass even when the same chemical strengthening treatment as that in a conventional process is applied and has good devitrification characteristics, a chemically strengthened glass using the glass for chemical strengthening, and a method for producing the chemically strengthened glass. The present invention provides a glass for chemical strengthening having a specific glass composition described in the present specification. 1. A glass for chemical strengthening , comprising , as expressed by mass percentage based on oxides , 60 to 72% of SiO , 4.4 to 10% of AlO , 5 to 10.9% of MgO , 0.1 to 5% of CaO , 14 to 19% of NaO , and 0 to 3% of KO , wherein RO is 7% or more and 11% or less (wherein the RO represents the sum of alkaline earth metal oxides , i.e. , MgO , CaO , SrO , and BaO) and RO/(RO+RO) is 0.20 or more and 0.42 or less (wherein the RO represents the sum of alkali metal oxides).2. The glass for chemical strengthening according to claim 1 , wherein the RO/(RO+RO) is 0.40 or less.3. The glass for chemical strengthening according to claim 1 , comprising 5% or more of AlO.4. The glass for chemical strengthening according to claim 1 , comprising 6% or more of MgO.5. The glass for chemical strengthening according to claim 1 , comprising 10% or less of MgO.6. The glass for chemical strengthening according to claim 1 , further comprising 0 to 4% of BO claim 1 , 0 to 1% of FeOand 0 to 1% of TiO.7. The glass for chemical strengthening according to claim 1 , having a temperature (T) at which a viscosity is 10dPa·s of 1550° C. or lower.8. The glass for chemical strengthening according to claim 1 , which has been formed according to a float process.9. A chemically strengthened glass obtained by chemically strengthening the glass for chemical strengthening according to .10. The chemically strengthened ...

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Номер записи: 19
02-01-2020 дата публикации

Fluorophosphate glasses for active device

Номер: US20200002217A1
Автор: Eui Sam LEE, Ju Hyeon CHOI, June Park, Jung Whan IN
Принадлежит: Korea Photonics Technology Institute

Disclosed is fluorophosphate glasses for an active device, the fluorophosphate glasses including: a metaphosphate composition including Mg(PO3)2 of about 20 mol % to about 60 mol %; a fluoride composition including BaF2 of about 20 mol % to about 60 mol % and CaF2 of about 0 mol % to about 40 mol %; and dopants including rare earth elements, in which there is an effect of increasing a carrier lifetime at a metastable state energy level that is stimulated-emitted due to an efficient energy transfer phenomenon by composition optimization of dopants (e.g. Er and Yb).

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Номер записи: 20
02-01-2020 дата публикации

FLUOROPHOSPHATE GLASSES FOR ACTIVE DEVICE

Номер: US20200002218A1
Автор: CHOI Ju Hyeon, HWANG Yeon, IN Jung Whan, Kim Young Bok
Принадлежит:

The disclosed fluorophosphate glasses for an active device include: a metaphosphate composition including Al(PO); a fluoride composition including BaFand SrF; and a dopant composed of ErFand YbF, and have thermal and mechanical properties to be able to be used as a glass base material for an active device (e.g., optical fiber laser), have a high emission cross-section characteristic, have a reinforced upconversion and downconversion emission characteristic, and have high sensitivity S in a cryogenic environment. 1. Fluorophosphate glasses for an active device , comprising:{'sub': 3', '3, 'a metaphosphate composition including Al(PO);'}{'sub': 2', '2, 'a fluoride composition including BaFand SrF; and'}{'sub': 3', '3, 'a dopant composed of ErFand YbF.'}2. The fluorophosphate glasses of claim 1 , wherein the YbFis about 3 mol % to about 5 mol %.3. The fluorophosphate glasses of claim 2 , wherein the ErFis about 3 mol % and the YbFis about 3 mol % to about 5 mol %.4. The fluorophosphate glasses of claim 1 , wherein the Al(PO)is about 20 mol % to about 30 mol % claim 1 ,{'sub': '2', 'the BaFis about 10 mol % to about 60 mol %, and'}{'sub': '2', 'the SrFis about 10 mol % to about 70 mol %.'}5. The fluorophosphate glasses of claim 4 , wherein the Al(PO)is about 20 mol % claim 4 ,{'sub': '2', 'the BaFis about 40 mol % to about 60 mol %, and'}{'sub': '2', 'the SrFis about 20 mol % to about 40 mol %.'}6. The fluorophosphate glasses of claim 5 , wherein the ErFis about 3 mol % and the YbFis about 3 mol % to about 5 mol %.7. The fluorophosphate glasses of claim 4 , wherein the Al(PO)is about 20 mol % claim 4 ,{'sub': '2', 'the BaFis about 60 mol %, and'}{'sub': '2', 'the SrFis about 20 mol %.'}8. The fluorophosphate glasses of claim 7 , wherein the ErFis about 3 mol % and the YbFis about 3 mol % to about 5 mol %.9. The fluorophosphate glasses of claim 4 , wherein the Al(PO)is about 20 mol % claim 4 ,{'sub': '2', 'the BaFis about 50 mol %, and'}{'sub': '2', 'the SrFis about 30 ...

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Номер записи: 21
02-01-2020 дата публикации

TRANSPARENT, NEAR INFRARED-SHIELDING GLASS CERAMIC

Номер: US20200002220A1
Автор: Dejneka Matthew John, Kohl Jesse, Patil Mallanagouda Dyamanagouda
Принадлежит:

Optically transparent glass ceramic materials comprising a glass phase containing and a crystalline tungsten bronze phase comprising nanoparticles and having the formula MWO, where M includes at least one H, Li, Na, K, Rb, Cs, Ca, Sr, Ba, Zn, Cu, Ag, Sn, Cd, In, Tl, Pb, Bi, Th, La, Pr, Nd, Sm, Eu, Gd, Dy, Ho, Er, Tm, Yb, Lu, and U, and where 0 Подробнее

Номер записи: 22
01-01-2015 дата публикации

TEMPERED GLASS, TEMPERED GLASS PLATE, AND GLASS FOR TEMPERING

Номер: US20150004390A1
Автор: Kawamoto Kosuke, Murata Takashi, TOJYO Takako
Принадлежит: NIPPON ELECTRIC GLASS CO., LTD.

A tempered glass has a compressive stress layer in a surface thereof, includes as a glass composition, in terms of mass %, 50 to 80% of SiO, 10 to 30% of AlO, 0 to 6% of BO, 0 to 2% of LiO, and 5 to 25% of NaO, and is substantially free of AsO, SbO, PbO, and F. 1. A tempered glass having a compressive stress layer in a surface thereof , comprising as a glass composition , in terms of mass % , 50 to 80% of SiO , 10 to 30% of AlO , 0 to 6% of BO , 0 to 2% of LiO , and 5 to 25% of NaO , and being substantially free of AsO , SbO , PbO , and F.2. The tempered glass according to claim 1 , wherein the tempered glass comprises as a glass composition claim 1 , in terms of mass % claim 1 , 50 to 80% of SiO claim 1 , 10 to 30% of AlO claim 1 , 0 to 6% of BO claim 1 , 0 to 1.7% of LiO claim 1 , more than 7.0 to 25% of NaO claim 1 , and 0 to 2% of SrO.3. The tempered glass according to claim 1 , wherein the tempered glass comprises as a glass composition claim 1 , in terms of mass % claim 1 , 50 to 76% of SiO claim 1 , more than 16.0 to 30% of AlO claim 1 , 0 to 6% of BO claim 1 , 0 to 1.7% of LiO claim 1 , more than 7.0 to 25% of NaO claim 1 , 0 to 2% of SrO claim 1 , and 0 to 4.5% of TiO.4. The tempered glass according to claim 1 , wherein the tempered glass comprises as a glass composition claim 1 , in terms of mass % claim 1 , 50 to 76% of SiO claim 1 , more than 16.0 to 30% of AlO claim 1 , 0 to 6% of BO claim 1 , 0 to 1.7% of LiO claim 1 , more than 7.0 to 25% of NaO claim 1 , 0 to 2% of SrO claim 1 , 0 to 0.5% of TiO claim 1 , and 0 to 4% of ZrO.5. The tempered glass according to claim 1 , wherein the tempered glass comprises as a glass composition claim 1 , in terms of mass % claim 1 , 50 to 76% of SiO claim 1 , more than 16.0 to 30% of AlO claim 1 , 0 to 6% of BO claim 1 , 0 to 1.7% of LiO claim 1 , more than 7.0 to 25% of NaO claim 1 , 0 to 2% of SrO claim 1 , 0 to 0.5% of TiO claim 1 , 0 to 4% of ZrO claim 1 , and 0 to 1% of PO claim 1 , and has a molar ratio (MgO+CaO ...

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Номер записи: 23
13-01-2022 дата публикации

GLASS CERAMIC DEVICES AND METHODS WITH TUNABLE INFRARED TRANSMITTANCE

Номер: US20220009823A1
Автор: Dejneka Matthew John, Kohl Jesse
Принадлежит:

Devices, apparatuses, and methods are disclosed that include a glass or glass ceramic substrate with a bleached region and an unbleached region. Examples include a substrate with a region that transmits IR wavelength light, and a region that is substantially opaque to IR light. Examples include additional opacity in some or all regions to visible wavelength light and/or UV wavelength light. 1. A device comprising:a substrate comprising a glass or glass-ceramic material comprising from about 0.1% to about 50% by weight crystalline phase;the substrate comprising an unbleached region and a bleached discrete region comprising at least partially dissolved or altered crystalline phase wherein an average ratio of absorbance in the unbleached/bleached regions over the near infra-red (NIR) wavelength range of 700-2000 nm is equal to or greater than 7.5; andwherein the substrate is substantially opaque in the visible wavelength range of 400 nm to 700 nm.2. The device of claim 1 , wherein the substrate includes a modifiable crystalline phase consisting of an oxide or sub-oxide comprising tungsten and or molybdenum that may be doped with any combination of: Li claim 1 , Na claim 1 , K claim 1 , Rb claim 1 , Cs claim 1 , Be claim 1 , Mg claim 1 , Ca claim 1 , Sr claim 1 , Ba claim 1 , Ra claim 1 , Ti claim 1 , Zn claim 1 , Se claim 1 , Nb claim 1 , Ru claim 1 , Rh claim 1 , In claim 1 , Sn claim 1 , Pb claim 1 , Ce claim 1 , Pr claim 1 , Nd claim 1 , Pm claim 1 , Sm claim 1 , Eu claim 1 , Gd claim 1 , Tb claim 1 , Dy claim 1 , Ho claim 1 , Er claim 1 , Tm claim 1 , Yb claim 1 , and Lu claim 1 , wherein this modifiable component amount is from about 0.35 mol % to about 30 mol %.3. The device of claim 1 , wherein the substrate includes a dopant claim 1 , wherein the dopant includes an element chosen from a group consisting of Co claim 1 , Ni claim 1 , Cu claim 1 , Se claim 1 , Bi claim 1 , Cr claim 1 , V claim 1 , Fe claim 1 , and Mn.4. The device of claim 3 , wherein the dopant ...

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Номер записи: 24
13-01-2022 дата публикации

SYSTEM AND PROCESS FOR PRODUCING LITHIUM

Номер: US20220010447A1
Автор: Swonger Lawrence Ralph
Принадлежит:

A decoupled plating system is provided for producing lithium. In a general embodiment, the present disclosure provides a feed tank configured to supply a lithium-rich aqueous electrolyte stream, a plating tank that is configured to receive an organic electrolyte and plate out lithium metal from that organic electrolyte, and one or more lithium replenishment cells configured to receive both electrolytes, keep them separated, and selectively move lithium ions from the aqueous electrolyte into the spent organic electrolyte stream. The present system and process can advantageously reduce operating costs and/or improve energy efficiency in production of lithium metal and associated products. 1. A lithium producing system comprising:a plating tank configured to receive an organic electrolyte;an anode provided within the plating tank;a substrate spaced apart from the anode and provided within the plating tank, wherein the anode and the substrate are configured to apply a potential to the substrate, whereupon lithium is plated onto the substrate from the organic electrolyte, and a spent electrolyte stream is discharged; andone or more lithium replenishment cells configured to receive the spent electrolyte stream and to form one or more regenerate electrolyte streams.2. The lithium producing system of claim 1 , wherein the anode comprises a substantially planar mesh structure.3. The lithium producing system of claim 1 , wherein the substrate comprises a substantially planar body portion.4. The lithium producing system of claim 1 , wherein the plating tank includes one or more sidewalls claim 1 , and the anode and the substrate are coupled to the one or more sidewalls.5. The lithium producing system of claim 1 , wherein the substrate measures approximately 12.7 cm or greater in the longest dimension.6. The lithium producing system of claim 1 , wherein the organic electrolyte comprises a DMC-LiPF6 mix.7. The lithium producing system of claim 1 , wherein the one or more lithium ...

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Номер записи: 25
13-01-2022 дата публикации

Methods of making glass constructs

Номер: US20220013857A1
Автор: Bruce D. Katz, Steven J. Visco, Yevgeniy S. Nimon
Принадлежит: Polyplus Battery Co Inc

Manufacturing methods for making a substantially rectangular and flat glass preform for manufacturing a Li ion conducting glass separator can involve drawing the preform to a thin sheet and may involve one or more of slumping, rolling or casting the glass within a frame that defines a space filling region and therewith the shape and size of the preform. The thickness of the rectangular flat preform so formed may be about 2 mm or less. The frame may be slotted having a back surface and widthwise wall portion that define the height and width of the space filling region. The flat backing surface and surfaces of the widthwise wall portions are defined may be coated by a material that is inert in direct contact with the heated glass material, such as gold.

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Номер записи: 26
07-01-2021 дата публикации

COMPLIANT SOLID-STATE IONICALLY CONDUCTIVE COMPOSITE MATERIALS AND METHOD FOR MAKING SAME

Номер: US20210005889A1
Автор: Burdynska Joanna, Nasybulin Eduard, Rupert Benjamin, Teran Alexander, Uppal Simmi Kaur, Venugopal Saranya
Принадлежит:

Provided herein are ionically conductive solid-state compositions that include ionically conductive inorganic particles in a matrix of an organic material. The resulting composite material has high ionic conductivity and mechanical properties that facilitate processing. In particular embodiments, the ionically conductive solid-state compositions are compliant and may be cast as films. In some embodiments of the present invention, solid-state electrolytes including the ionically conductive solid-state compositions are provided. In some embodiments of the present invention, electrodes including the ionically conductive solid-state compositions are provided. The present invention further includes embodiments that are directed to methods of manufacturing the ionically conductive solid-state compositions and batteries incorporating the ionically conductive solid-state compositions. 180.-. (canceled)81. A solid-state electrode for use in an alkali ion or alkali metal battery , comprising an inorganic phase comprising an ionically conductive inorganic material , an electrochemically active material , and an electronically conductive additive; andan organic phase comprising a first component and a binder, wherein the first component is a non-ionically conductive polymer having a number average molecular weight of between 500 g/mol and 50,000 g/mol and the binder is a non-ion conducting polymer having a number average molecular weight of at least 100 kg/mol.82. The solid-state electrode of claim 81 , wherein the ionically conductive inorganic material constitutes between 15% and 60% by weight of the inorganic phase claim 81 , the electrochemically active material constitutes between 30% and 80% by weight of the inorganic phase claim 81 , and the electronically conductive additive constitutes between 5% and 25% of the inorganic phase.83. The solid-state electrode of claim 81 , wherein the first component constitutes between 50% and 99% by weight of the organic phase claim 81 ...

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Номер записи: 27
02-01-2020 дата публикации

Optoelectronic Component and Method for Producing an Optoelectronic Component

Номер: US20200006913A1
Автор: Angela Eberhardt, Florian Peskoller, Jörg Frischeisen, Jürgen Bauer, Michael Schmidberger, Thomas Huckenbeck
Принадлежит: OSRAM GMBH, OSRAM OLED GmbH

An optoelectronic component and a method for producing an optoelectronic component are disclosed. In an embodiment an optoelectronic component includes at least one laser source configured to emit at least one laser beam during operation and a self-supporting conversion element arranged in a beam path of the laser beam, wherein the self-supporting conversion element comprises a substrate followed by a first layer, the first layer being directly bonded to the substrate and comprising at least one conversion material embedded in a glass matrix, wherein the glass matrix has a proportion of 50 vol % to 80 vol % inclusive in the first layer, wherein the substrate is free of the glass matrix and of the conversion material and mechanically stabilize the first layer, and wherein the first layer has a layer thickness of less than 200 μm.

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Номер записи: 28
27-01-2022 дата публикации

GLASS PLATE AND PROCESS FOR PRODUCING THE SAME

Номер: US20220024803A1
Автор: Hijiya Hiroyuki, Kuroiwa Yutaka, MATSUO Yusaku, Ogawa Tomonori, Ono Kazutaka
Принадлежит: AGC Inc.

A glass plate has a dielectric dissipation factor at 10 GHz of tan δA and a glass transition temperature of Tg° C. The glass plate satisfies (tan δ100−tan δA)≥0.0004, where tan δ100 is a dielectric dissipation factor of the glass plate at 10 GHz after having been heated to (Tg+50)° C. and then cooled to (Tg−150)° C. at 100° C./min. 1. A glass plate having a dielectric dissipation factor at 10 GHz of tan δA and a glass transition temperature of Tg° C. ,wherein the glass plate satisfies (tan δ100−tan δA)≥0.0004, where tan δ100 is a dielectric dissipation factor of the glass plate at 10 GHz after having been heated to (Tg+50)° C. and then cooled to (Tg−150)° C. at 100° C./min.2. The glass plate according to claim 1 , having a relative permittivity at 10 GHz of εrA claim 1 ,wherein the glass plate satisfies 0.95≤(εr100/εrA)≤1.05, where εr100 is a relative permittivity of the glass plate at 10 GHz after having been heated to (Tg+50)° C. and then cooled to (Tg−150)° C. at 100° C./min.3. The glass plate according to claim 1 , comprising a principal surface with an area of 350 cmor larger.4. The glass plate according to claim 1 , having the dielectric dissipation factor at 10 GHz of 0.009 or less.5. The glass plate according to claim 1 , having a relative permittivity at 10 GHz of 6.8 or less.6. The glass plate according to claim 1 , wherein any two portions separated from each other by 40 mm or more have a difference in dielectric dissipation factor at 10 GHz of 0.0005 or less.7. The glass plate according to claim 1 , wherein any two portions separated from each other by 40 mm or more have a difference in relative permittivity at 10 GHz of 0.05 or less.8. The glass plate according to claim 1 , comprising from 30 to 85% of SiOas represented by mol % based on oxides.9. The glass plate according to claim 1 , comprising claim 1 , as represented by mol % based on oxides claim 1 ,{'sub': '2', 'SiO: from 57 to 70%,'}{'sub': 2', '3, 'AlO: from 5 to 15%,'}{'sub': 2', '3, 'BO: from ...

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Номер записи: 29
11-01-2018 дата публикации

GLASS SHEET

Номер: US20180009705A1
Автор: HATANO Maya, ISHIBASHI Hiroki, Nakagawa Koji, Nakano Atsushi, NIHEI Toshifumi, OTA Shinya, YAMASHITA Shuichi
Принадлежит: Asahi Glass Company, Limited

A glass sheet is a single glass sheet having a first surface and a second surface facing the first surface. The glass sheet has a curvature part curved in a first direction and a second direction orthogonal to the first direction. A radius of curvature in the first direction of the curvature part is 8,500 mm or less. At least a part of the first surface has been chemically strengthened in the curvature part. In the first direction within the chemically strengthened region in the curvature part, an Na amount in the first surface is smaller than the Na amount in the second surface. 1. A glass sheet , which is a single glass sheet having a first surface and a second surface facing the first surface , wherein:the glass sheet has a curvature part curved in a first direction and a second direction orthogonal to the first direction;a radius of curvature in the first direction of the curvature part is 8,500 mm or less;at least a part of the first surface has been chemically strengthened in the curvature part; andin the first direction within the chemically strengthened region in the curvature part, an Na amount in the first surface is smaller than the Na amount in the second surface.2. The glass sheet according to claim 1 , wherein in the first direction within the region in the curvature part claim 1 , a ratio of the Na amount in the first surface to the Na amount in the second surface is 0.936 or less.3. The glass sheet according to claim 1 , wherein the radius of curvature in the first direction of the curvature part is 7 claim 1 ,000 mm or less claim 1 , and in the first direction within the region in the curvature part claim 1 , a ratio of the Na amount in the first surface to the Na amount in the second surface is 0.925 or less.4. The glass sheet according to claim 2 , wherein in the first direction within the region in the curvature part claim 2 , the ratio of the Na amount in the first surface to the Na amount in the second surface is 0.825 or less.5. The glass ...

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Номер записи: 30
14-01-2021 дата публикации

Glass ceramic sintered body and wiring substrate

Номер: US20210009464A1
Автор: Shin Takane, Yasuharu Miyauchi, Yousuke Futamata
Принадлежит: TDK Corp

A glass ceramic sintered body having a small dielectric loss in a high frequency band of 10 GHz or higher and stable characteristics against temperature variation and a wiring substrate using the same are provided. The glass ceramic sintered body contains crystallized glass, an alumina filler, silica, and strontium titanate. The content of the crystallized glass is 50 mass % to 80 mass %, the content of the alumina filler is 15.6 mass % to 31.2 mass % in terms of Al2O3, the content of silica is 0.4 mass % to 4.8 mass % in terms of SiO2, and the content of the strontium titanate is 4 mass % to 14 mass % in terms of SrTiO3.

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Номер записи: 31
10-01-2019 дата публикации

INFRARED TRANSMISSION CHALCOGENIDE GLASSES

Номер: US20190010078A1
Автор: Carlie Nathan
Принадлежит: SCHOTT CORPORATION

A glass composition and a method for producing the glass composition having an improved infrared transmission are provided. The composition includes indium and or cadmium; germanium; phosphorus, arsenic, and/or antimony; silver; lead; and sulfur, selenium, and/or tellurium. The method is performed by melting a mixture for a time period of between about 5 to about 48 hours and mixing the mixture at a temperature range that is between about 600-1000° C. 1. A chalcogenide glass composition , the composition consisting essentially of , in percent by weight of the total weight of the composition:gallium;indium in an amount from about 2% to about 20%;germanium; andat least one chalcogen selected from the group consisting of: sulfur, selenium, and tellurium, wherein the at least one chalcogen is in an amount from about 30% to about 80%.2. The composition of claim 1 , wherein the chalcogen is sulfur.3. The composition of claim 1 , wherein the amount of germanium is from about 10% to about 30%.4. The composition of claim 1 , wherein the at least one chalcogen is in an amount from about 50% to about 80%.5. The composition of claim 1 , wherein the composition is prepared by mixing in a temperature range from about 850° C. to 1000° C.6. A chalcogenide glass composition claim 1 , the composition consisting essentially of claim 1 , in percent by weight of the total weight of the composition:indium;germanium in an amount from about 10% to about 30%;at least one alkali selected from the group consisting of: potassium, rubidium, or cesium;at least one chalcogen selected from the group consisting of: sulfur, selenium, and tellurium; andat least one halide selected from the group consisting of: chlorine, bromine, and iodine.7. The composition of claim 6 , wherein the at least one halide is in an amount from about 7% to about 25%.8. The composition of claim 6 , wherein the at least one halide is bromine.9. The composition of claim 6 , wherein the chalcogen is sulfur.10. The composition ...

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Номер записи: 32
10-01-2019 дата публикации

Fluorescent Glass For Light Emitting Diode And Manufacturing Method Thereof

Номер: US20190010079A1
Автор: Liao Yi-Yao, Lin Chun-Teng, Lu Chun-Yuan
Принадлежит:

The present disclosure is related to a fluorescent glass for a light emitting diode and a manufacturing method thereof. The fluorescent glass for the light emitting diode includes a glass powder and a fluorescent powder, wherein the glass powder and the fluorescent powder are mixed to form a fluorescent glass, the material for manufacturing the glass powder comprises silicon dioxide with 20 wt % to 37 wt %, diboron trioxide with 31 wt %-47 wt % and calcium oxide with 16 wt %˜35 wt %, and the material of the fluorescent powder is selected from one of Ce-YAG, LuAG, silicate, and nitrides/oxynitrides fluorescent powder. The fluorescent glass of the present disclosure is formed by mixing and sintering the glass powder and the fluorescent powder and has low sintering temperature, so as to avoid the deterioration of color of the fluorescent powder due to high temperature. Therefore, the fluorescent glass of the present disclosure has good transparency, and the light emitting diode applying this fluorescent glass has good lighting efficiency. 1. A fluorescent glass for a light emitting diode , comprising a glass powder and a fluorescent powder , wherein the glass powder and the fluorescent powder are mixed to form a fluorescent glass , the material for manufacturing the glass powder comprises silicon dioxide with 20 wt % to 37 wt % , diboron trioxide with 31 wt %˜47 wt % and calcium oxide with 16 wt %˜35 wt % , and the material of the fluorescent powder is selected from one of Ce-YAG , LuAG , silicate , and nitrides/oxynitrides fluorescent powder.2. The fluorescent glass for the light emitting diode as claimed in claim 1 , wherein the material for manufacturing the glass powder further comprises magnesium oxide or zinc oxide claim 1 , the weight percent of magnesium oxide or zinc oxide is between 0 wt % and 17 wt %.3. The fluorescent glass for the light emitting diode as claimed in claim 2 , wherein the material for manufacturing the glass powder further comprises aluminum ...

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Номер записи: 33
10-01-2019 дата публикации

COMPOSITION FOR FORMING SOLAR CELL ELECTRODE AND ELECTRODE PREPARED USING THE SAME

Номер: US20190010081A1
Автор: Heo Ryun Min, Kim Chul Kyu, Kim Ye Jin, Koo Young Kwon, LEE Ji Seon, LEE Jung Chul, Lee Sung Eun, Yoo Sang Hoon
Принадлежит:

A composition for solar cell electrodes includes a conductive powder, a glass frit, and an organic vehicle. The glass frit contains about 20 mol % to about 40 mol % of an alkali metal, about 20 mol % to about 30 mol % of zinc (Zn), and about 7 mol % to about 20 mol % of magnesium (Mg) in terms of oxide content. 1. A composition for solar cell electrodes , comprising:a conductive powder;a glass frit; andan organic vehicle,wherein the glass frit contains about 20 mol % to about 40 mol % of an alkali metal, about 20 mol % to about 30 mol % of zinc (Zn), and about 7 mol % to about 20 mol % of magnesium (Mg) in terms of oxide content.2. The composition according as claimed in claim 1 , wherein a molar ratio of the alkali metal to magnesium (Mg) ranges from about 1:1 to about 6:1 in terms of oxide content.3. The composition according as claimed in claim 1 , wherein the glass frit further contains tellurium (Te) and satisfies Equation 1:{'br': None, 'sub': Zn', 'AL', 'Te, 'About 0.4≤(M+M)/M≤about 4.0\u2003\u2003[Equation 1]'}{'sub': Zn', 'AL', 'Te, '(where Mdenotes mol % of zinc (Zn), Mdenotes mol % of the alkali metal, and Mdenotes mol % of tellurium (Te), as measured in terms of oxide content).'}4. The composition according as claimed in claim 1 , wherein the alkali metal includes at least one of lithium (Li) claim 1 , sodium (Na) claim 1 , and potassium (K).5. The composition according as claimed in claim 1 , wherein the glass frit includes at least one of a lead (Pb)-tellurium (Te)-alkali metal-zinc (Zn)-magnesium (Mg)-oxygen (O) glass frit claim 1 , a bismuth (Bi)-tellurium (Te)-alkali metal-zinc (Zn)-magnesium (Mg)-oxygen (O) glass frit claim 1 , and a lead (Pb)-bismuth (Bi)-tellurium (Te)-alkali metal-zinc (Zn)-magnesium (Mg)-oxygen (O) glass frit.6. The composition according as claimed in claim 1 , wherein the glass flit further contains boron (B).7. The composition according as claimed in claim 1 , comprising:about 67.5 wt % to about 96.5 wt % of the conductive ...

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Номер записи: 34
09-01-2020 дата публикации

Highly stable and chemically temperable glasses

Номер: US20200010354A1
Автор: Christian MIx, Michael Schwall, Peter Nass, Ulf Dahlmann, Ulrich Fotheringham
Принадлежит: SCHOTT AG

Glasses and glass products which combine the chemical temperability with very good alkali and acid resistance, hydrolytic resistance, as well as a desired coefficient of thermal expansion are provided. The glass has a composition characterized by the following constituent phases: a composition characterized by the following constituent phases: 20-60 mol % albite; 0-40 mol % silicon dioxide; 0-20 mol % orthoclase; 0-10 mol % wollastonite; 0-20 mol % enstatite; 0-20 mol % parakeldyshite; 0-20 mol % narsarsukite; 0-40 mol % disodium zinc silicate; 0-20 mol % cordierite; 0-10 mol % strontium silicate; and 0-10 mol % barium silicate.

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Номер записи: 35
09-01-2020 дата публикации

GLASSES WITH IMPROVED ION EXCHANGEABILITY

Номер: US20200010355A1
Автор: Berndhäuser Christoph, Fotheringham Ulrich, Groß Christoph, Hochrein Oliver, Mannstadt Wolfgang, Ritter Simone Monika, Wegener Holger
Принадлежит: SCHOTT AG

The present invention relates to glasses, such as e.g. thin or thinnest glasses, but also to glasses for the production of tubular glass, carpules and syringes as well as other pharmaceutical vessels. The glasses are characterized by a high chemical prestressability (tem-perability) with very well alkali, hydrolytic and/or acid resistance as well as an advantageous coefficient of thermal expansion. The glass has a composition characterized by the following constituent phases: 0-60 mol % reedmergnerite; 20-60 mol % albite; 0-30 mol % orthoclase; 0-20 mol % natrosilite; 0-20 mol % sodium metasilicate; 0-20 mol % parakeldyshite; 0-20 mol % narsarsukite; 0-20 mol % disodium zinc silicate; 0-21 mol % cordierite; and 0-20 mol % danburite. A quotient of a coefficient of thermal expansion of the glass multiplied by 1000 (in ppm/K) and the product of a pH value and a removal rate in alkaline environment (in mg/(dm3h)) according to ISO 695 is at least 9.0. 1. A glass , comprising:a composition characterized by the following constituent phases:0-60 mol % reedmergnerite;20-60 mol % albite;0-30 mol % orthoclase;0-20 mol % natrosilite;0-20 mol % sodium metasilicate;0-20 mol % parakeldyshite;0-20 mol % narsarsukite;0-20 mol % disodium zinc silicate;0-21 mol % cordierite; and{'sup': '2', '0-20 mol % danburite, wherein a quotient of a coefficient of thermal expansion of the glass multiplied by 1000 (in ppm/K) and the product of a pH value and a removal rate in alkaline environment (in mg/(dm3 h)) according to ISO 695 is at least 9.0.'}2. The glass of claim 1 , wherein a proportion of disodium zinc silicate is at most 19 mol %.3. The glass of claim 1 , wherein a proportion of cordierite is at least one of at most 20 mol % or at least 3 mol %.4. The glass of claim 1 , wherein a proportion of albite is at least one of at least 30 mol % or at most 55 mol %.5. The glass of claim 1 , wherein a proportion of orthoclase is at least one of at least 5 mol % or at most 25 mol %.6. The glass of ...

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Номер записи: 36
27-01-2022 дата публикации

CONDUCTIVE PASTE FOR SOLAR CELL ELECTRODE AND SOLAR CELL FABRICATED USING SAME

Номер: US20220029036A1
Автор: JANG Mun Seok, JUN Tae Hyun, KIM Chung Ho, Kim In Chul, KO Min Soo, NOH Hwa Young, PARK Kang Ju
Принадлежит:

Proposed is a conductive paste for a solar cell electrode. The conductive paste includes a metal powder, a glass frit, and an organic vehicle. The glass frit includes an alkali metal oxide, and the metal powder includes an alkali component. 1. A conductive paste for a solar cell electrode , the conductive paste comprisinga metal powder,a glass frit, andan organic vehicle,wherein the glass frit comprises an alkali metal oxide, andthe metal powder comprises an alkali component.2. The conductive paste of claim 1 , wherein the metal powder comprises the alkali component in an amount of 20 to 2000 ppm with respect to the total weight of the silver powder.3. The conductive paste of claim 1 , wherein the glass frit is configured such that the total molar ratio of the alkali metal oxide to the entire glass frit is 10 to 20 mol %.4. The conductive paste of claim 1 , wherein the alkali component included in the silver powder comprises at least one selected from the group consisting of lithium (Li) claim 1 , sodium (Na) claim 1 , and potassium (K).5. The conductive paste of claim 1 , wherein the metal powder comprises the alkali component in an amount of 50 to 500 ppm with respect to the total weight of the silver powder.6. The conductive paste of claim 1 , wherein the alkali metal oxide comprises at least one of lithium oxide (LiO) claim 1 , sodium oxide (NaO) claim 1 , and potassium oxide (KO).7. The conductive paste of claim 6 , wherein the alkali metal oxide is used by mixing at least two of the lithium oxide claim 6 , the sodium oxide claim 6 , and the potassium oxide.8. A solar cell comprising:a semiconductor substrate;a first conductivity type region formed on a front surface of the semiconductor substrate;a passivation film formed on the first conductivity type region and including an aluminum oxide film;a front electrode penetrating the passivation film and connected to the first conductivity type region; anda back electrode formed on a back surface of the ...

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Номер записи: 37
12-01-2017 дата публикации

THICK FILM RESISTOR AND PRODUCTION METHOD FOR SAME

Номер: US20170011825A1
Автор: MASHIMA Hiroshi, MOROFUJI Yukari
Принадлежит: SHOEI CHEMICAL INC.

An object of the present invention is to provide a thick film resistor excluding a toxic lead component from a conductive component and glass and having characteristics equivalent to or superior to conventional resistors in terms of, in a wide resistance range, resistance values, TCR characteristics, current noise characteristics, withstand voltage characteristics and the like. The present invention is a thick film resistor formed of a fired product of a resistive composition, wherein the thick film resistor contains ruthenium-based conductive particles containing ruthenium dioxide and a glass component being essentially free of a lead component and has a resistance value in the range of 100 Ω/□ to 10 MΩ/□ and a temperature coefficient of resistance within ±100 ppm/° C. 1. A thick film resistor comprising a fired product of a resistive composition , wherein the thick film resistor comprises ruthenium-based conductive particles containing ruthenium dioxide and a glass component being essentially free of a lead component; the glass component contains at least a first glass component and a second glass component having a glass transition point that is higher than the first glass component; and the thick film resistor has a sea-island structure in which the second glass component is scattered in a matrix of the first glass component so as to form islands , and has a resistance value in a range of 100 Ω/□ to 10 MΩ/□ and a temperature coefficient of resistance within ±100 ppm/° C.2. The thick film resistor according to claim 1 , wherein the thick film resistor has a resistance value in a range of 1 kΩ/□ to 10 MΩ/□.3. The thick film resistor according to claim 2 , wherein the thick film resistor has a resistance value in a range of 10 kΩ/□ to 10 MΩ/□.4. The thick film resistor according to claim 3 , wherein the thick film resistor has a resistance value in a range of 100 kΩ/□ to 10 MΩ/□.5. The thick film resistor according to claim 4 , wherein the thick film resistor has a ...

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Номер записи: 38
09-01-2020 дата публикации

Infrared-transmitting glass

Номер: US20200011729A1
Автор: Fumio Sato, Yoshimasa Matsushita
Принадлежит: Nippon Electric Glass Co Ltd

Provided is a novel infrared-transmitting glass that can be vitrified without containing any environmentally harmful compound and has high light transmissivity from visible range to a mid-infrared range of wavelengths of about 4 to about 8 μm. An infrared-transmitting glass containing, in % by mole, 50% or more TeO2, 0 to 45% (exclusive of 0%) ZnO, and 0 to 50% (exclusive of 0% and 50%) RO (where R is at least one selected from the group consisting of Ca, Sr, and Ba).

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Номер записи: 39
12-01-2017 дата публикации

METHOD OF PREPARING SOLID ELECTROLYTE COMPOSITION FOR LITHIUM SECONDARY BATTERY

Номер: US20170012318A1
Автор: GO Daeyeon, KIM Taeheung, Lim Hyungsik, SONG Jaeeun, YOON Duckki
Принадлежит:

Disclosed is a method of preparing a solid electrolyte composition for a lithium secondary battery which includes: (a) mixing materials including LiO, SiO, TiO, PO, BaO, CsO and VO; (b) melting the mixed materials; (c) rapidly cooling the molten materials at room temperature and compressing the molten materials using a preheated plate to form electrolyte glass having a predetermined thickness; (d) heating the electrolyte glass to eliminate stress at a predetermined temperature range; (e) heating the electrolyte glass to a higher temperature range higher than in the step of heating the electrolyte glass to eliminate stress to be crystallized; and (f) precisely adjusting a thickness of the electrolyte glass by lapping the electrolyte glass. 1. A method of preparing a solid electrolyte composition for a lithium secondary battery , comprising:{'sub': 2', '2', '2', '2', '5', '2', '2', '5, '(a) mixing materials including LiO, SiO, TiO, PO, BaO, CsO and VO;'}(b) melting the mixed materials;(c) rapidly cooling the molten materials at room temperature and compressing the molten materials using a preheated plate to form electrolyte glass;(d) heating the electrolyte glass to eliminate stress at 500 to 600° C.;(e) heating the electrolyte glass to a temperature range higher than in the step of heating the electrolyte glass to eliminate stress to be crystallized; and(f) precisely adjusting a thickness of the electrolyte glass by lapping the electrolyte glass.2. The method of claim 1 , wherein 5 to 8 wt % of LiO claim 1 , 2 to 5 wt % of SiO claim 1 , 30 to 35 wt % of TiO claim 1 , 56 to 60 wt % of PO claim 1 , 0.1 to 2 wt % of BaO claim 1 , 0.1 to 2 wt % of CsO and 0.5 to 2 wt % of VOare mixed in the step (a).3. The method of claim 1 , wherein the mixed materials are introduced into a platinum crucible and are heated at a rate of 10° C./min to become molten in an air atmosphere at a temperature of 1300 to 1450° C. in the step (b).4. The method of claim 1 , wherein the molten ...

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Номер записи: 40
19-01-2017 дата публикации

ASYMMETRICALLY STRUCTURED THIN GLASS SHEET THAT IS CHEMICALLY STRENGTHENED ON BOTH SURFACE SIDES, METHOD FOR ITS MANUFACTURE AS WELL AS USE OF SAME

Номер: US20170015584A1
Автор: Apitz Dirk, Brueckner Matthias, Joerdens Thomas, Krzyzak Marta, Walther Marten
Принадлежит: SCHOTT AG

A thin glass sheet includes a first and a second surface side, wherein the thin glass sheet is asymmetrically structured in that the two surface sides differ from one another, wherein both surface sides are chemically strengthened and wherein respectively a depth of layer exists of the alkali ions that are introduced through chemical strengthening, whereby the depth of layer of the first surface side (DoL) and the depth of layer of the second surface side (DoL) are coordinated with each other in such a way that they are equal or are adapted on both surface sides, and that on both surface sides respectively a coating consisting of one or several layers is provided, wherein the coating on the first surface side differs from the coating on the second surface side in at least one property or characteristic. 1. A thin glass sheet , comprising:{'sub': '1', 'a first surface side which is chemically strengthened, said first surface side having a first depth of layer of alkali ions (DoL) introduced through chemical strengthening;'}at least one layer of a first coating provided on said first surface side;{'sub': 2', '2', '1', '2', '1, 'a second surface side differing from said first surface side in at least one property or characteristic and which is chemically strengthened, said second surface side having a second depth of layer of alkali ions (DoL) introduced through chemical strengthening, said DoLand said DoLbeing coordinated with each other in such a way that DoLand DoLare equal or are adapted on both surface sides; and'}at least one layer of a second coating provided on said second surface side, said second coating differing from said first coating in at least one property or characteristic.2. The thin glass sheet according to claim 1 , wherein said at least one differing property or characteristic between said first coating and said second coating is at least one of a thickness claim 1 , a porosity claim 1 , a number of coating layers claim 1 , a structure claim 1 , a ...

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Номер записи: 41
19-01-2017 дата публикации

Luminescent Markings

Номер: US20170016188A1
Автор: David Langtry
Принадлежит: Patent Applied Technology

Reflective luminescent markings on a road or sign surface are formed by applying onto the surface a base material which is liquid in an initial state for application and sets or cures to form a solid layer after application where the base material contains a fine/medium filler material of glass ground from recycled materials in a rotary mill. Coarse material from the grinder is separated out and supplied as a separate material to be applied onto the surface of the layer of base material and fine ground glass. The base material is connected or impregnated with a luminescent material such as photo luminescent 2 4 6 trichlorophenyl in a binder such as polyurea.

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Номер записи: 42
18-01-2018 дата публикации

SULFIDE GLASS AND CRYSTALLINE SOLID ELECTROLYTE PRODUCTION METHOD, CRYSTALLINE SOLID ELECTROLYTE, SULFIDE GLASS AND SOLID-STATE BATTERY

Номер: US20180016185A1
Автор: MARUYAMA Junpei, Nakata Akiko
Принадлежит: IDEMITSU KOSAN CO., LTD.

A method for producing sulfide glass wherein phosphorus sulfide satisfying the following formula (1) is used as a raw material: 1. A method comprising producing sulfide glass from a raw material comprising phosphorus sulfide satisfying a formula (1):{'br': None, 'i': 'A/B≧', '100×37 \u2003\u2003(1)'}{'sup': 31', '31, 'wherein in the formula, A is peak areas of peaks that appear at peak positions in a range of 57.2 ppm or more and 58.3 ppm or less, and 63.0 ppm or more and 64.5 ppm or less in PNMR spectroscopy, and B is the total of peak areas of all peaks measured in PNMR spectroscopy.'}2. A method comprising producing sulfide glass from a raw material comprising phosphorus sulfide satisfying a formula (2):{'br': None, 'i': A+D', 'B≦, '37≦100×()/70 \u2003\u2003(2)'}{'sup': 31', '31', '31, 'wherein in the formula, A is peak areas of peaks that appear at peak positions in a range of 57.2 ppm or more and 58.3 ppm or less, and 63.0 ppm or more and 64.5 ppm or less in PNMR spectroscopy, D is peak areas of peaks that appear at peak positions in a range of 84.0 ppm or more and 86.0 ppm or less, and 110 ppm or more and 113 ppm or less in PNMR spectroscopy, and B is the total of peak areas of all peaks measured in PNMR spectroscopy.'}38-. (canceled)9. Sulfide glass satisfying a formula (9):{'br': None, 'i': Tc', 'Tc, '1+45≦2 \u2003\u2003(9)'}wherein in the formula, Tc1 is the temperature of an exothermic peak that appears for the first time when sulfide glass is subjected to differential thermogravimetry in a dry nitrogen atmosphere at a temperature-elevating rate of 10° C./min from 20° C. to 600° C., and Tc2 is the temperature of an exothermic peak that appears subsequent to the appearance of an exothermic peak of which the temperature is Tc1.1019-. (canceled)20. The method of claim 1 , wherein the phosphorus sulfide further satisfies a formula (2):{'br': None, 'i': A+D', 'B≦, '37≦100×()/70 \u2003\u2003(2)'}{'sup': 31', '31', '31, 'wherein in the formula, A is peak areas of ...

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Номер записи: 43
17-01-2019 дата публикации

GLASSES HAVING IMPROVED TOUGHNESS AND SCRATCH RESISTANCE

Номер: US20190016625A1
Автор: Dejneka Matthew John, Ellison Adam James, Gomez Sinue, Morena Robert Michael
Принадлежит:

A silicate glass that is tough and scratch resistant. The toughness is increased by minimizing the number of non-bridging oxygen atoms in the glass. In one embodiment, the silicate glass is an aluminoborosilicate glass in which −15 mol %≤(RO+R′O−AlO−ZrO)−BO≤4 mol %, where R is one of Li, Na, K, Rb, and Cs, and R′ is one of Mg, Ca, Sr, and Ba. 123-. (canceled)24. A silicate glass , the silicate glass being ion exchangeable and comprising:{'sub': '2', '62-70 mol % SiO;'}{'sub': 2', '3, '0-18 mol % AlO;'}{'sub': 2', '3, '>0-10 mol % BO;'}{'sub': '2', '>0-15 mol % LiO;'}{'sub': '2', '6-20 mol % NaO;'}{'sub': '2', '0-18 mol % KO;'}>0-17 mol % MgO;{'sub': '2', 'ZrO; and'}{'sub': '2', 'SnO,'}{'sub': 2', '2', '3', '2, 'wherein 10 mol %≤AlO+BO+ZrO≤30 mol %, and'}{'sub': '2', 'wherein 14 mol %≤RO+R′O≤25 mol %, where R is at least one of Li, Na, K, Rb, and Cs, and R′ is at least one of Mg, Ca, Sr, and Ba.'}25. The silicate glass according to claim 24 , wherein the silicate glass has a toughness in a range from about 0.7 MPa mup to about 1.2 MPa m.26. The silicate glass according to claim 25 , wherein the silicate glass has a brittleness of less than about 8.5 μm.27. The silicate glass according to claim 24 , wherein the silicate glass is ion exchanged and has a surface compressive stress of at least about 200 MPa and a surface compressive layer claim 24 , the surface compressive layer having a depth of at least about 30 μm.28. The silicate glass according to claim 24 , wherein the silicate glass has a liquidus viscosity of at least 100 kpoise.29. The silicate glass according to claim 24 , wherein the silicate glass is substantially free of at least one of antimony oxide and arsenic oxide.30. The silicate glass according to claim 24 , wherein the silicate glass forms a cover plate for a mobile electronic device claim 24 , wherein the cover plate has a thickness in a range from about 0.3 mm up to about 1.5 mm.31. The silicate glass according to claim 24 , wherein the silicate ...

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Номер записи: 44
17-01-2019 дата публикации

GLASS-BASED ARTICLES WITH IMPROVED STRESS PROFILES

Номер: US20190016627A1
Автор: LI Qiao, Pal Santona
Принадлежит:

Glass-based articles comprise: a glass-based substrate having opposing first and second surfaces defining a substrate thickness (t); a stress profile comprising: a compressive stress region extending from the first surface to a depth of compression (DOC), the DOC located at 0.04•t or deeper; and a central tension region. An alkali metal oxide is present in the central tension region. A first metal oxide whose metal has the same or smaller atomic radius as the metal of the alkali metal oxide, and a second metal oxide whose metal has a larger atomic radius than the metal of the alkali metal oxide are both present in independent concentrations that vary within at least a portion of the compressive stress region. The glass-based substrates are exposed to a multi-step ion exchange process including a first treatment of doping with ions smaller than the alkali metal oxide of the pre-fabricated glass-based substrate; and a second treatment of strengthening with larger ions to enable superior stress profile attributes. The first treatment may occur at temperatures within 300° C. of the strain point of the glass-based substrate. 1. A glass-based article comprising:a glass-based substrate having opposing first and second surfaces defining a substrate thickness (t); a compressive stress region extending from the first surface to a depth of compression (DOC), wherein the DOC is located at 0.04•t or deeper; and', 'a central tension region;, 'a stress profile comprisingan alkali metal oxide present in at least the central tension region, wherein the alkali metal oxide is not lithium oxide;a first metal oxide whose metal has the same or smaller atomic radius than the alkali metal of the alkali metal oxide, wherein a concentration of the first metal oxide varies within at least a portion of the compressive stress region; anda second metal oxide whose metal has a larger atomic radius than the alkali metal of the alkali metal oxide, wherein a concentration of the second metal oxide ...

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Номер записи: 45
21-01-2016 дата публикации

GLASS SHEET HAVING HIGH INFRARED RADIATION TRANSMISSION

Номер: US20160018919A1
Автор: Dogimont Audrey, LAMBRICHT Thomas
Принадлежит: AGC Glass Europe

The invention relates to a glass sheet having high infrared radiation transmission, intended, in particular, for use in a touch tablet, panel or screen. More specifically, the invention relates to a glass sheet having a composition comprising, concentrations expressed as a percentage of the total weight of the glass: 55-78% SiO2; 0-18% Al2O3; 0-18% B2O3; 5-20% Na2O; 0-15% CaO; 0-10% MgO; 0-10% K2O; 0-5% BaO; 0.002-0.06% total iron (expressed as Fe2O3), and selenium (expressed as Se) varying between 0.001 and 1%.

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Номер записи: 46
21-01-2016 дата публикации

GLASS SHEET HAVING HIGH INFRARED RADIATION TRANSMISSION

Номер: US20160018949A1
Автор: Dogimont Audrey, LAMBRICHT Thomas
Принадлежит: AGC Glass Europe

The invention relates to a glass sheet having high infrared radiation transmission, intended, in particular, for use in a touch tablet, panel or screen. More specifically, the invention relates to a glass sheet having a composition comprising, concentrations expressed as a percentage of the total weight of the glass: 55-78% SiO2; 0-18% Al2O3; 0-18% B2O3; 5-20% Na2O; 0-15% CaO; 0-10% MgO; 0-10% K2O; 0-5% BaO; 0.002-0.06% total iron (expressed as Fe2O3), and cobalt (expressed as CoO) varying between 0.001 and 1%.

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Номер записи: 47
16-01-2020 дата публикации

GLASS CERAMIC ARTICLES HAVING IMPROVED PROPERTIES AND METHODS FOR MAKING THE SAME

Номер: US20200017398A1
Автор: Click Carol Ann, Edmonston James Howard, Fu Qiang, Hall Jill Marie, Hubert Mathieu Gerard Jacques, Joshi Dhananjay, JR. John Robert, Kittleson Andrew Peter, Kroemer Katherine Weber, Moore Galan Gregory, Rai Rohit, Ridge John Richard, Saltzer, Smith Charlene Marie, Stapleton Erika Lynn, Trosa Matthew Daniel, Ukrainczyk Ljerka, Wilson Shelby Kerin, YANG Bin, Zheng Zheming
Принадлежит: CORNING INCORPORATED

A glass ceramic article including a lithium disilicate crystalline phase, a petalite crystalline phased, and a residual glass phase. The glass ceramic article has a warp (μm)<(3.65×10/μm×diagonal) where diagonal is a diagonal measurement of the glass ceramic article in μm, a stress of less than 30 nm of retardation per mm of glass ceramic article thickness, a haze (%)<0.0994t+0.12 where t is the thickness of the glass ceramic article in mm, and an optical transmission (%)>0.91×10of electromagnetic radiation wavelengths from 450 nm to 800 nm, where t is the thickness of the glass ceramic article in mm. 1. A glass ceramic article comprising:a lithium disilicate crystalline phase;a petalite crystalline phased; anda residual glass phase, whereinthe glass ceramic article comprises:{'sup': '−6', 'a warp (μm)<(3.65×10μm×diagonal) where diagonal is a diagonal measurement of the glass ceramic article in μm;'}a stress of less than 30 nm of retardation per mm of glass ceramic article thickness;a haze (%)<0.0994t+0.12 where t is the thickness of the glass ceramic article in mm; and{'sup': '(2-0.03t)', 'an optical transmission (%)>0.91×10of electromagnetic radiation wavelengths from 450 nm to 800 nm, where t is the thickness of the glass ceramic article in mm.'}2. The glass ceramic article of claim 1 , wherein the glass ceramic article has a fracture toughness in a range from 1.0 MPa√m to 2.0 MPa√m.3. The glass ceramic article of claim 1 , wherein the glass ceramic article has a hardness measured by a Vickers indenter at a 200 gram load of greater than 680 kgf.4. The glass ceramic article of claim 1 , wherein the glass ceramic article is strengthened and has compressive stress greater than 175 MPa.5. The glass ceramic article of claim 4 , wherein the glass ceramic article has a central tension greater than or equal to 80 MPa.6. The glass ceramic article of claim 4 , wherein the glass ceramic article has a depth of compression of 0*t to 0.3*t claim 4 , where t is thickness of the ...

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Номер записи: 48
21-01-2021 дата публикации

CHALCOGENIDE GLASS MATERIAL

Номер: US20210017066A1
Автор: MATSUSHITA Yoshimasa, Sato Fumio
Принадлежит:

Provided is a glass having excellent infrared transmittance and being suitable for use in infrared sensors. A chalcogenide glass material has an oxygen content of 100 ppm or less. 1. A chalcogenide glass material having an oxygen content of 100 ppm or less.2. The chalcogenide glass material according to claim 1 , containing claim 1 , in terms of % by mole claim 1 , over 0 to 100% Te+S+Se as a composition.3. The chalcogenide glass material according to claim 1 , containing claim 1 , in terms of % by mole claim 1 , 20 to 90% Te.4. The chalcogenide glass material according to claim 1 , containing claim 1 , in terms of % by mole claim 1 , over 0 to 50% Ge+Ga+Sb+As.5. The chalcogenide glass material according to claim 1 , containing claim 1 , in terms of % by mole claim 1 , 0 to 50% Ag.6. The chalcogenide glass material according to claim 1 , containing claim 1 , in terms of % by mole claim 1 , 0 to 50% Si.7. The chalcogenide glass material according to claim 1 , wherein the glass material is free from striae with a length of 500 μm or more.8. An optical element in which the chalcogenide glass material according to is used.9. An infrared sensor in which the optical element according to is used. The present invention relates to chalcogenide glass materials for use in infrared sensors, infrared cameras, and so on.Vehicle-mounted night vision devices, security systems, and the like include infrared sensors for use to detect living bodies at night. To sense infrared rays with wavelengths of about 8 to 14 μm emitted from living bodies, such an infrared sensor is provided, in front of the sensor part, with an optical element, such as a filter or a lens, capable of transmitting infrared rays in the above wavelength range.Examples of a material for the optical element as described above include Ge and ZnSe. These materials are crystalline bodies and therefore poor in processability, which makes them difficult to process into complicated shapes, such as an aspheric lens. For this ...

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Номер записи: 49
21-01-2021 дата публикации

CONDUCTIVE PASTE, METHOD, ELECTRODE AND SOLAR CELL

Номер: US20210017067A1
Автор: ARAPOV Kirill, CELA GREVEN Beatriz, CURRIE Edwin Peter Kennedy, KATZBACH Roland
Принадлежит:

A conductive paste for forming a conductive track or coating on a substrate, the paste comprising a solids portion dispersed in an organic vehicle, the solids portion comprising electrically conductive material and an inorganic particle mixture; wherein the inorganic particle mixture comprises particles of glass frit and substantially crystalline particles of one or more metal compounds; and wherein the glass frit comprises at least 90 mol % Te O. 1. A conductive paste for forming a conductive track or coating on a substrate , the paste comprising a solids portion dispersed in an organic vehicle , wherein the inorganic particle mixture comprises particles of glass frit and substantially crystalline particles of one or more metal compounds;', {'sub': '2', 'wherein the glass frit comprises greater than 90 mol % TeOand one or more of an alkali metal oxide, an alkaline earth metal oxide, an oxide of cerium, and an oxide of bismuth,'}, 'wherein the substantially crystalline particles of one or more metal compounds comprise one or more of a lithium compound, a sodium compound, a potassium compound, a barium compound, a cerium compound and a bismuth compound, and', 'wherein the conductive paste is lead-free., 'the solids portion comprising electrically conductive material and an inorganic particle mixture;'}2. A conductive paste according to wherein the glass frit comprises at least 91 mol % TeO claim 1 , preferably at least 92 mol % TeO claim 1 , more preferably at least 95 mol % TeO.3. (canceled)4. (canceled)5. A conductive paste according to wherein the glass frit is substantially free of silicon oxide.6. A conductive paste according to wherein the inorganic particle mixture comprises particles of glass frit in an amount of at least 25 wt. % claim 1 , at least 40 wt. % claim 1 , at least 45 wt. % claim 1 , or at least 50 wt. %.7. A conductive paste according to wherein the inorganic particle mixture comprises particles of glass frit in an amount of 75 wt. % or less ...

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Номер записи: 50
21-01-2021 дата публикации

Fusion-formable glass-based articles including a metal oxide concentration gradient

Номер: US20210017072A1
Автор: Charlene Marie Smith, Guangli Hu, Rostislav Vatchev Roussev, Steven Alvin Tietje, Timothy Michael Gross, Zhongzhi Tang
Принадлежит: Corning Inc

A glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than about 0.7·t to t, comprise a tangent with a slope having an absolute value greater than about 0.1 MPa/micrometer. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t) and a maximum central tension of less than about 71.5/√(t) (MPa). In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a point between the first surface and the second surface and increases from the point to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.

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Номер записи: 51
18-01-2018 дата публикации

POSITIVE ELECTRODE ACTIVE MATERIAL FOR SECONDARY BATTERY, AND SECONDARY BATTERY INCLUDING THE SAME

Номер: US20180019474A1
Автор: JUNG Wang Mo, Kang Seong Hoon, Lee Dae Jin
Принадлежит: LG CHEM, LTD.

The present invention provides a positive electrode active material for a lithium secondary battery which is capable of preventing the degeneration of a positive electrode active material and the generation of a gas during operating a battery due to humidity, by including a surface treatment layer of an amorphous glass including an alkali metal oxide and an alkaline earth metal oxide on the surface of a core including a lithium composite metal oxide and by decreasing humidity reactivity, and a secondary battery including the same. 1. A positive electrode active material for a lithium secondary battery , the positive electrode active material comprising:a core comprising a lithium composite metal oxide; anda surface treatment layer positioned on a surface of the core,wherein the surface treatment layer comprises an amorphous glass containing an alkali metal oxide and an alkaline earth metal oxide.2. The positive electrode active material for a lithium secondary battery of claim 1 , wherein the amorphous glass is an alkaline-earth aluminosilicate comprising the alkali metal oxide claim 1 , the alkaline earth metal oxide claim 1 , SiO claim 1 , and AlO.3. The positive electrode active material for a lithium secondary battery of claim 2 , wherein the alkaline-earth aluminosilicate comprises 1 to 30 parts by weight of the alkali metal oxide and 1 to 30 parts by weight of the alkaline earth metal oxide based on 100 parts by weight of a total amount of SiOand AlO.4. The positive electrode active material for a lithium secondary battery of claim 2 , wherein the alkaline-earth aluminosilicate comprises at least one selected from the group consisting of a SiO—AlO—NaO—CaO-based glass and a SiO—AlO—LiO—CaO-based glass.5. The positive electrode active material for a lithium secondary battery of claim 1 , wherein the surface treatment layer comprises the amorphous glass comprising the alkali metal oxide and the alkaline earth metal oxide claim 1 , the amorphous glass showing ...

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Номер записи: 52
17-01-2019 дата публикации

PROCESS, USE AND ARTICLE

Номер: US20190019595A1
Автор: Hoppe Alexander, SCHUMANS Maurice Theodoor Maria
Принадлежит:

A process for the production of an article of glass with an applied electrically conductive grid comprising: a) applying a conductive paste to a glass substrate; b) firing the paste to form the electrically conductive grid; and c) soldering an electrical connector to the electrically conductive grid via a lead-free solder; wherein the conductive paste comprises finely divided particles of a conductive metal, particles of glass frit, and an organic medium; and wherein the particles of the glass fit have a particle size Dof less than 4 microns. 2. The process as claimed in claim 1 , wherein the particles of the glass frit have a particle size Dof less than 3 microns claim 1 , preferably less than 2 microns.3. The process as claimed in claim 1 , wherein the glass frit comprises bismuth and/or zinc borosilicate compounds.4. The process as claimed in claim 1 , wherein said glass frit is present in an amount of 0.1-10% by weight of the total weight of said paste.5. The process as claimed in claim 1 , wherein said conductive metal is present in an amount of 50-90% by weight of the total weight of said paste.6. The process as claimed in claim 1 , wherein said conductive metal is silver.7. The process as claimed in claim 6 , wherein said silver has an average particle size of 0.1 to 15 microns.8. The process as claimed in claim 1 , wherein said organic medium comprises of ethyl cellulose claim 1 , terpineol claim 1 , and butyl carbitol.9. The process as claimed in claim 1 , wherein said organic medium is present in an amount of 5-50% by weight of the total weight of said paste.10. The process as claimed in claim 1 , wherein the paste further comprises a transition metal oxide in an amount of 3-15% by weight of the total weight of said paste.11. The process as claimed in wherein the lead-free solder comprises tin claim 1 , silver claim 1 , and copper.12. The process as claimed in claim 11 , wherein the lead-free solder further comprises nickel claim 11 , cobalt claim 11 , ...

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Номер записи: 53
17-04-2014 дата публикации

ION EXCHANGEABLE GLASS WITH HIGH DAMAGE RESISTANCE

Номер: US20140106172A1
Автор: Dejneka Matthew John, Ellison Adam James, Mauro John Christopher
Принадлежит: CORNING INCORPORATED

An ion exchangeable glass having a high degree of resistance to damage caused by abrasion, scratching, indentation, and the like. The glass comprises alumina, BO, and alkali metal oxides, and contains boron cations having three-fold coordination. The glass, when ion exchanged, has a Vickers crack initiation threshold of at least about 30 kilogram force. 1. A glass comprising:{'sub': '2', 'a. at least about 50 mol % SiO;'}{'sub': 2', '2', '2, 'b. at least about 10 mol % RO, wherein RO comprises NaO;'}{'sub': 2', '3', '2', '3', '2, 'c. AlO, wherein −0.5 mol %≦AlO(mol %)−RO(mol %)≦2 mol %; and'}{'sub': 2', '3', '2', '3', '2', '2', '3, 'd. BO, wherein BO(mol %)−(RO(mol %)−AlO(mol %))≧4.5 mol %, and wherein the glass is ion exchangeable.'}2. The glass of claim 1 , wherein the glass comprises: at least about 50 mol % SiO claim 1 , from about 12 mol % to about 22 mol % AlO; from about 4.5 mol % to about 10 mol % BO; from about 10 mol % to about 20 mol % NaO; from 0 mol % to about 5 mol % KO; at least about 0.1 mol % MgO claim 1 , ZnO claim 1 , or combinations thereof claim 1 , wherein 0 mol %≦MgO≦6 and 0≦ZnO≦6 mol %; and claim 1 , optionally claim 1 , at least one of CaO claim 1 , BaO claim 1 , and SrO claim 1 , wherein 0 mol %≦CaO+SrO+BaO≦2 mol %.3. The glass of claim 2 , wherein the glass comprises from about 60 to 66 mol % SiO.4. The glass of claim 1 , wherein the glass comprises at least about 0.1 mol % of at least one of MgO and ZnO.5. The glass of claim 1 , wherein the glass comprises greater than 4.5 mol % BOin which boron cations are three-fold coordinated.6. The glass of claim 1 , wherein the glass is ion exchanged and has a layer under a compressive stress of at least about 600 MPa claim 1 , the layer extending from a surface of the glass into the glass to a depth of layer of at least about 30 μm.7. The glass of claim 6 , wherein the compressive stress is at least about 800 MPa.8. The glass of claim 6 , wherein the glass has a Vickers crack initiation threshold ...

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Номер записи: 54
28-01-2016 дата публикации

GLASS SHEET HAVING HIGH INFRARED RADIATION TRANSMISSION

Номер: US20160023940A1
Автор: Dogimont Audrey, LAMBRICHT Thomas
Принадлежит: AGC Glass Europe

The invention relates to a glass sheet having high infrared radiation transmission, intended, in particular, for use in a touch tablet, panel or screen. More specifically, the invention relates to a glass sheet having a composition comprising, concentrations expressed as a percentage of the total weight of the glass: 55-78% SiO; 0-18% AlO; 0-18% BO; 5-20% NaO; 0-15% CaO; 0-10% MgO; 0-10% KO; 0-5% BaO; 0.002-0.06% total iron (expressed as Fe2O3), said composition also comprising at least one noble metal M selected from among silver, gold, iridium, palladium, platinum and rhodium at a concentration (expressed as M) varying between 0.001 and 1 wt.-% in relation to the total weight of the glass. 2. The glass sheet of claim 1 , wherein the composition comprises at least one noble metal M selected from the group consisting of silver claim 1 , gold claim 1 , iridium claim 1 , palladium claim 1 , platinum and rhodium in an amount (expressed in M form) ranging from 0.005 to 0.5% by weight relative to the total weight of the glass.3. The glass sheet of claim 1 , wherein the composition comprises at least one noble metal M selected from the group consisting of silver claim 1 , gold claim 1 , iridium claim 1 , palladium claim 1 , platinum and rhodium in an amount (expressed in M form) ranging from 0.001 to 0.1% by weight relative to the total weight of the glass.4. The glass sheet of claim 3 , wherein the composition comprises at least one noble metal M selected from the group consisting of silver claim 3 , gold claim 3 , iridium claim 3 , palladium claim 3 , platinum and rhodium in an amount (expressed in M form) ranging from 0.002 to 0.05% by weight relative to the total weight of the glass.5. The glass sheet of claim 1 , wherein the noble metal is platinum or rhodium.6. The glass sheet of claim 5 , wherein the noble metal is platinum.7. The glass sheet of claim 5 , wherein the noble metal is rhodium.8. The glass sheet of claim 1 , wherein the composition comprises a total ...

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Номер записи: 55
26-01-2017 дата публикации

GLASS ARTICLES EXHIBITING IMPROVED FRACTURE PERFORMANCE

Номер: US20170022092A1
Автор: DeMartino Steven Edward, Fabian Michelle Dawn, Kohli Jeffrey Todd, Lyon Jennifer Lynn, Smith Charlene Marie, Tang Zhongzhi
Принадлежит:

Embodiments of this disclosure pertain to a strengthened glass article including a first surface and a second surface opposing the first surface defining a thickness (t) of about less than about 1.1 mm, a compressive stress layer extending from the first surface to a depth of compression (DOC) of about 0.1·t or greater, such that when the glass article fracture, it breaks into a plurality of fragments having an aspect ratio of about 5 or less. In some embodiments, the glass article exhibits an equibiaxial flexural strength of about 20 kgf or greater, after being abraded with 90-grit SiC particles at a pressure of 25 psi for 5 seconds. Devices incorporating the glass articles described herein and methods for making the same are also disclosed. 1. A strengthened glass article comprising:a first surface and a second surface opposing the first surface defining a thickness (t) of about 1.1 mm or less;a compressive stress layer extending from the first surface to a depth of compression (DOC) of greater than about 0.11·t;wherein, after the glass article fractures according to a Frangibility Test, the glass article includes a plurality of fragments, wherein at least 90% of the plurality of fragments have an aspect ratio of about 5 or less.2. The strengthened glass article of claim 1 , wherein the glass article fractures into the plurality of fragments in 1 second or less claim 1 , as measured by the Frangibility Test.3. The strengthened glass article of claim 1 , wherein at least 80% of the plurality of fragments have a maximum dimension that is less than or equal to 3·t.4. The strengthened glass article of claim 1 , wherein at least 50% of plurality of fragments comprises an aspect ratio of 2 or less.5. The strengthened glass article of claim 1 , wherein at least 50% of the plurality of fragments comprises a volume of less than or equal to about 10 mm.6. The strengthened glass article of claim 1 , wherein the plurality of fragments comprises an ejected portion of fragments ...

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Номер записи: 56
26-01-2017 дата публикации

Glass articles exhibiting improved fracture performance

Номер: US20170022093A1
Автор: Charlene Marie Smith, Jeffrey Todd Kohli, Jennifer Lynn Lyon, Michelle Dawn Fabian, Steven Edward DeMartino, Zhongzhi Tang
Принадлежит: Corning Inc

Embodiments of this disclosure pertain to a strengthened glass article including a first surface and a second surface opposing the first surface defining a thickness (t) of about less than about 1.1 mm, a compressive stress layer extending from the first surface to a depth of compression (DOC) of about 0.1·t or greater, such that when the glass article fracture, it breaks into a plurality of fragments having an aspect ratio of about 5 or less. In some embodiments, the glass article exhibits an equibiaxial flexural strength of about 20 kgf or greater, after being abraded with 90-grit SiC particles at a pressure of 25 psi for 5 seconds. Devices incorporating the glass articles described herein and methods for making the same are also disclosed.

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Номер записи: 57
22-01-2015 дата публикации

ZIRCON COMPATIBLE GLASSES FOR DOWN DRAW

Номер: US20150024210A1
Автор: Dejneka Matthew John, Ellison Adam James, Hanson Benjamin Zain
Принадлежит:

A glass that is down-drawable and ion exchangeable. The glass has a temperature Twhich the viscosity is 35 kilopoise. Tis less than the breakdown temperature Tof zircon. 131-. (canceled)32. A glass comprising SiO , AlO , and NaO , wherein SiO+BO≧66 mol % , AlO≧7 mol % , BO≦7 mol % , NaO≧9 mol % , BO+NaO+KO+MgO+CaO≧18 mol % , and CaO≦2 mol % , wherein 610.6 mol %−41.0[AlO]+9.9[BO]−3.5[NaO]−20.2[KO]−25.6[MgO]+34.2[CaO]≧0 , where concentrations [AlO] , [BO] , [NaO] , [KO] , [MgO] , and [CaO] are expressed in mol %.33. The glass of claim 32 , wherein the glass is ion exchanged to form a compressive layer on at least one surface of the glass.34. The glass of claim 33 , wherein the ion exchanged glass has a compressive stress of at least 350 MPa and a compressive depth of layer of at least 20 microns.35. The glass of claim 32 , wherein the glass comprises: 61 mol %≦SiO≦75 mol %; 7 mol %≦AlO≦15 mol %; 0 mol %≦BO≦7 mol %; 9 mol %≦NaO≦21 mol %; 0 mol %≦KO≦4 mol %; 0 mol %≦MgO≦7 mol %; and 0 mol %≦CaO≦3 mol %.36. The glass of claim 32 , wherein the glass is down-drawable.37. The glass of claim 32 , wherein the glass is fusion drawn into a glass sheet.38. The glass of claim 37 , wherein the glass sheet has less than one inclusion of solid ZrOper pound of glass sheet.39. The glass of claim 32 , wherein BO+NaO+KO−AlO≧0 mol %.40. The glass of claim 32 , wherein the glass has a liquidus viscosity of greater than about 100 kpoise.41. The glass of claim 32 , wherein the glass has a 350 poise temperature Tof less than or equal to 1650° C.42. The glass of claim 32 , wherein the glass is formed into one of a cover plate claim 32 , a window claim 32 , a casing claim 32 , a display screen claim 32 , and a touch panel of an electronic device.43. The glass of claim 32 , wherein the glass has a temperature Twhich the glass has a viscosity of 35 kpoise and a zircon breakdown temperature Tat which zircon breaks down to form ZrOand SiO claim 32 , wherein Tis greater than T.44. A glass ...

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Номер записи: 58
25-01-2018 дата публикации

Ion exchangeable glass with high crack initiation threshold

Номер: US20180022637A1
Автор: Timothy Michael Gross
Принадлежит: Corning Inc

Alkali aluminosilicate glasses that are resistant to damage due to sharp impact and capable of fast ion exchange are provided. The glasses comprise at least 4 mol % P 2 O 5 and, when ion exchanged, have a Vickers indentation crack initiation load of at least about 7 kgf.

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Номер записи: 59
25-01-2018 дата публикации

ION EXCHANGEABLE LI-CONTAINING GLASS COMPOSITIONS FOR 3-D FORMING

Номер: US20180022638A1
Автор: Comte Marie Jacqueline Monique, Drake Melinda Ann, Geisinger Karen Leslie, Gomez Sinue, Morena Robert Michael, Smith Charlene Marie, Youngman Randall Eugene
Принадлежит:

According to one embodiment, a glass article may include SiO, AlO, LiO and NaO. The glass article may have a softening point less than or equal to about 810° C. The glass article may also have a high temperature CTE less than or equal to about 27×10/° C. The glass article may also be ion exchangeable such that the glass has a compressive stress greater than or equal to about 600 MPa and a depth of layer greater than or equal to about 25 μm after ion exchange in a salt bath comprising KNOat a temperature in a range from about 390° C. to about 450° C. for less than or equal to approximately 15 hours. 127-. (canceled)28. A glass article comprising:{'sub': '2', 'greater than or equal to 67 mol. % to about 71 mol. % SiO;'}{'sub': 2', '3, 'from about 7 mol. % to about 12 mol. % AlO;'}{'sub': '2', 'from about 1 mol. % to about 9 mol. % LiO;'}{'sub': '2', 'less than about 16 mol. % NaO;'}{'sub': '2', 'greater than 0 mol. % to about 5 mol. % KO; and'}from about 0.8 mol. % to about 10 mol. % of a divalent oxide, wherein the divalent oxide comprises greater than 0 mol. % to about 1 mol. % CaO and at least one of MgO and ZnO.29. The glass article of further comprising from about 0.5 mol. % to about 2 mol % ZrO.30. The glass article of claim 28 , wherein a concentration of KO is less than or equal to about 3.0 mol. %.31. The glass article of claim 28 , wherein a concentration of CaO is less than or equal to about 0.5 mol. %.32. The glass article of claim 28 , wherein the concentration of BOis less than or equal to 1.0 mol. %.33. The glass article of claim 28 , wherein the glass article is substantially free of BO.34. The glass article of claim 28 , wherein a sum of a concentration of AlO(mol. %) claim 28 , and a concentration of the divalent oxide (mol. %) is greater than about 10 mol %.35. The glass article of claim 28 , wherein a concentration of SiOis greater than or equal to 68 mol. %.36. The glass article of claim 28 , wherein the glass article is ion exchange strengthened. ...

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Номер записи: 60
10-02-2022 дата публикации

TEMPERED GLASS SHEET AND METHOD FOR MANUFACTURING SAME

Номер: US20220041493A1
Автор: ICHIMARU Tomonori, KINOSHITA Kiyotaka, NAGANO Yuta, Suzuki Ryota, YUKI Ken
Принадлежит:

The present invention provides a tempered glass sheet having a compressive stress layer in a surface thereof, the tempered glass sheet including as a glass composition, in terms of mol %, 50% to 80% of SiO, 8% to 25% of AlO, 0% to 10% of BO, 3% to 15% of LiO, 3% to 21% of NaO, 0% to 10% of KO, 0% to 10% of MgO, 0% to 10% of ZnO, and 0% to 15% of PO. 1. A tempered glass sheet having a compressive stress layer in a surface thereof ,{'sub': 2', '2', '3', '2', '3', '2', '2', '2', '2', '5, 'the tempered glass sheet comprising as a glass composition, in terms of mol %, 50% to 80% of SiO, 8% to 25% of AlO, 0% to 10% of BO, 3% to 15% of LiO, 3% to 21% of NaO, 0% to 10% of KO, 0% to 10% of MgO, 0% to 10% of ZnO, and 0% to 15% of PO.'}2. The tempered glass sheet according to claim 1 , wherein the tempered glass sheet satisfies the following relationship: a molar ratio ([NaO]−[LiO])/([AlO]+[BO]+[PO])≤0.29.3. The tempered glass sheet according to claim 1 , wherein the tempered glass sheet satisfies the following relationship: a molar ratio ([BO]+[NaO]−[PO])/([AlO]+[LiO])≥0.30.4. The tempered glass sheet according to claim 1 , wherein the tempered glass sheet comprises 12 mol % or more of ([LiO]+[NaO]+[KO]) claim 1 , and satisfies the following relationship: [SiO]+1.2×[PO]−3×[AlO]−2×[LiO]−1.5×[NaO]−[KO]−[BO]≥−22 mol %.5. The tempered glass sheet according to claim 1 , wherein the tempered glass sheet has a content of POof from 0.1 mol % to 2.3 mol %.6. The tempered glass sheet according to claim 1 , wherein the tempered glass sheet has a content of BOof from 0.1 mol % to 4 mol %.7. The tempered glass sheet according to claim 1 , wherein the compressive stress layer has a compressive stress value of from 200 MPa to 1 claim 1 ,000 MPa on an outermost surface.8. The tempered glass sheet according to claim 1 , wherein the compressive stress layer has a depth of layer of from 50 μm to 200 μm.9. The tempered glass sheet according to claim 1 , wherein the tempered glass sheet has a ...

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Номер записи: 61
23-01-2020 дата публикации

CONDUCTIVE PASTE FOR SOLAR CELL ELECTRODE AND SOLAR CELL MANUFACTURED USING SAME

Номер: US20200024180A1
Автор: JANG Mun Seok, JUN Tae Hyun, KIM Chung Ho, Kim In Chul, KO Min Soo, NOH Hwa Young
Принадлежит:

The present invention relates to a conductive paste for a solar cell electrode, including a metal powder, a glass frit and an organic vehicle, wherein the metal powder includes a metal powder having a sintering shrinkage rate of 15 to 30%, whereby the light-receiving area of the front electrode of a solar cell formed using the conductive paste including the metal powder having an increased sintering shrinkage rate can be enlarged and short-circuit current (Isc) can be increased, thus increasing the power generation efficiency of the solar cell. 1. A conductive paste for a solar cell electrode , comprising a metal powder , a glass frit , and an organic vehicle ,wherein the metal powder includes a metal powder having a shrinkage rate of 15 to 30%, measured as an area reduction rate after applying, drying and firing the paste including the metal powder, compared to before firing.2. The conductive paste of claim 1 , wherein the metal powder includes a first metal powder having a sintering shrinkage rate of 15 to 20%.3. The conductive paste of claim 1 , wherein the metal powder includes a second metal powder having a sintering shrinkage rate of 20 to 25%.4. The conductive paste of claim 1 , wherein the metal powder includes a third metal powder having a sintering shrinkage rate of 25 to 30%.5. The conductive paste of claim 1 , wherein the metal powder includes at least two metal powders selected from the group consisting of a first metal powder having a sintering shrinkage rate of 15 to 20% claim 1 , a second metal powder having a sintering shrinkage rate of 20 to 25% claim 1 , and a third metal powder having a sintering shrinkage rate of 25 to 30%.6. The conductive paste of claim 5 , wherein the metal powder is configured such that an amount of the metal powder having a relatively high shrinkage rate is greater than an amount of the metal powder having a relatively low shrinkage rate.7. The conductive paste of claim 1 , wherein the metal powder has an average particle ...

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Номер записи: 62
23-01-2020 дата публикации

PROTECTIVE GLASS FOR A CAPACITIVE TOUCH CONTROL SYSTEM

Номер: US20200024187A1
Автор: GONG Ruhua, HE Gen, Li Qing, Shengyin LI, ZHAN Guixin
Принадлежит:

This invention relates to a protective glass for a capacitive touch control system having a dielectric constant of 8.0-9.8 at room temperature and at an operating frequency of 1 kHz; and another protective glass for a capacitive touch control system, comprising a compressive stress layer of a certain depth formed on the surface of the glass through chemical strengthening treatment. High dielectric constant and high strength glass may be provided, which is applicable to protective glass for a capacitive touch control system and may have high light transmittance and create a good user experience of touch control. 1. A protective glass for a capacitive touch control system , having a dielectric constant of 8.0-9.8 , preferably 8.0-9.0 , at room temperature and at an operating frequency of 1 kHz.2. A protective glass for a capacitive touch control system , comprising a compressive stress layer of a certain depth formed on the surface of the glass through chemical strengthening treatment.3. The protective glass for a capacitive touch control system of claim 2 , wherein through first chemical strengthening treatment claim 2 , the surface of the glass obtains a compressive stress of 300-1100 MPa claim 2 , preferably 600-1100 MPa claim 2 , more preferably 650-1100 MPa claim 2 , and a depth of the compressive stress layer of 10-60 μm claim 2 , preferably 15-50 μm claim 2 , more preferably 20-45 μm; and through second or more chemical strengthening treatments claim 2 , the surface of the glass obtains a superposed compressive stress of 300-1100 MPa claim 2 , preferably 650-1100 MPa claim 2 , and a depth of the compressive stress layer of 10-90 μm claim 2 , preferably 20-80 μm.4. The protective glass for a capacitive touch control system of claim 3 , wherein the first chemical strengthening treatment is performed at the temperature of 380-500° C. for 2-10 hours.5. The protective glass for a capacitive touch control system of claim 3 , wherein the second chemical strengthening ...

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Номер записи: 63
25-01-2018 дата публикации

LITHIUM ION CONDUCTOR, SOLID ELECTROLYTE LAYER, ELECTRODE, BATTERY, AND ELECTRONIC DEVICE

Номер: US20180026300A1
Автор: FURUYA Tatsuya, Kishimoto Kenji, Shimizu Keisuke, SUDO Go, SUZUKI Masamitsu, Tamura Yasushi, YOSHIDA Yumiko
Принадлежит:

A lithium ion conductor includes a first lithium ion conductor that contains at least one selected from among oxide crystals and glass ceramics, and a second lithium ion conductor that has a sintering temperature of not more than 600° C. The lithium ion conductivity of the first lithium ion conductor is higher than the lithium ion conductivity of the second lithium ion conductor. 1. A lithium ion conductor comprising:a first lithium ion conductor that contains at least one selected from among oxide crystals and glass ceramics; anda second lithium ion conductor that has a sintering temperature of not more than 600° C.,wherein a lithium ion conductivity of the first lithium ion conductor is higher than a lithium ion conductivity of the second lithium ion conductor.2. The lithium ion conductor according to claim 1 , wherein the first lithium ion conductor and the second lithium ion conductor contain an oxide.3. The lithium ion conductor according to claim 1 , wherein a sintering temperature of the first lithium ion conductor exceeds 600° C.4. The lithium ion conductor according to claim 1 , wherein the second lithium ion conductor contains a glass.5. The lithium ion conductor according to claim 4 , wherein the glass contains at least one selected from among germanium claim 4 , silicon claim 4 , boron claim 4 , and phosphorus claim 4 , as well as lithium and oxygen.6. The lithium ion conductor according to claim 1 , wherein in a state where the second lithium ion conductor has been sintered claim 1 , the lithium ion conductivity of the lithium ion conductor is not less than 5×10S/cm.7. The lithium ion conductor according to claim 1 , wherein an average particle diameter of the first lithium ion conductor is not less than an average particle diameter of the second lithium ion conductor.8. The lithium ion conductor according to claim 1 , wherein a proportion by volume of the first lithium ion conductor is not less than a proportion by volume of the second lithium ion ...

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Номер записи: 64
10-02-2022 дата публикации

Surface treatment of a sulfide glass solid electrolyte layer

Номер: US20220045353A1
Автор: Alexei Petrov, Bruce D. Katz, Steven J. Visco, Vitaliy Nimon, Yevgeniy S. Nimon
Принадлежит: Polyplus Battery Co Inc

Chemically treating ionically conductive sulfide glass solid electrolyte separators or separator layers can improve performance. In particular, treatment involving chemically etching a surface or surface region of the sulfide glass separator to blunt, lessen or remove edge defects or surface flaws, and/or to enhance surface smoothness is cost effective, reliable and well suited for high production environments compared to physical methods of removing scratches or smoothing surfaces, such as mechanical grinding and polishing.

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Номер записи: 65
25-01-2018 дата публикации

CERAMIC SUBSTRATE

Номер: US20180027653A1
Автор: Ito Masanori, Katoh Tatsuya, KUTSUNA Masaki
Принадлежит:

A ceramic substrate includes a ceramic layer mainly formed of a glass ceramic and a conductor trace mainly formed of silver (Ag). In an adjacent region located adjacent to the conductor trace, the concentration of boron atoms (B) contained in the ceramic layer increases toward the conductor trace. 1. A ceramic substrate comprising a ceramic layer mainly formed of a glass ceramic and a conductor trace mainly formed of silver (Ag) , wherein in an adjacent region located adjacent to the conductor trace , the concentration of boron atoms (B) contained in the ceramic layer increases toward the conductor trace.2. The ceramic substrate according to claim 1 , wherein the adjacent region includes a region in which the concentration of boron atoms (B) is at least three times that in a central region of the ceramic layer centrally located in a thickness direction.3. The ceramic substrate according to claim 1 , wherein the conductor trace contains at least either of lanthanum atoms (La) and titanium atoms (Ti).4. The ceramic substrate according to claim 1 , wherein the ceramic layer contains borosilicate glass and alumina (AlO). The present invention relates to a ceramic substrate.There has been known a ceramic substrate having a ceramic layer mainly formed of a glass ceramic and a conductor trace containing silver (Ag) as a main component. Such a ceramic substrate is formed by applying a conductor paste which is the pre-firing form of the conductor trace to a green sheet which is the pre-firing form of the ceramic layer and then firing the green sheet carrying the conductor paste applied thereto. Such a ceramic substrate is also called a low temperature co-fired ceramic (LTCC) substrate.When the ceramic substrate is formed by firing, a silver component of the conductor paste diffuses into the ceramic layer. This may cause, for example, formation of voids in the ceramic layer, deformation of the ceramic layer, and change of the color of the ceramic layer. It is considered that ...

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Номер записи: 66
29-01-2015 дата публикации

LOW CTE, ION-EXCHANGEABLE GLASS COMPOSITIONS AND GLASS ARTICLES COMPRISING THE SAME

Номер: US20150030827A1
Автор: Gomez Sinue, Kiczenski Timothy James, Mauro John Christopher, Schaut Robert Anthony, Smedskjaer Morten Mattrup, Venkataraman Natesan
Принадлежит: One Incorporated

Glass compositions and glass articles comprising the glass compositions are disclosed. In one embodiment, a glass composition includes from about 65 mol. % to about 70 mol. % SiO2; from about 9 mol. % to about 14 mol. % AlO; and from about 0 mol. % to about 11 mol. % BOas glass network formers. The glass composition also includes from about 5 mol. % to less than 10 mol. % alkali oxide RO, wherein R is at least one of Li, Na, and K. The glass composition also includes from about 3 mol. % to about 11 mol. % of divalent oxide MO, wherein M is at least one of Mg, Ca, Ba, SrO and Zn. The glass composition has a coefficient of thermal expansion which is less than or equal to 55×10-/° C. and is amenable to strengthening by ion-exchange. The glass composition is well suited for use as the glass cladding layers of a laminated glass article. 1. A glass composition comprising:{'sub': '2', 'from about 65 mol. % to about 70 mol. % SiO;'}{'sub': 2', '3, 'from about 9 mol. % to about 14 mol. % AlO;'}{'sub': 2', '3, 'from about 0 mol. % to about 11 mol. % BO;'}{'sub': '2', 'from about 5 mol. % to less than 10 mol. % alkali oxide RO, wherein R is at least one of Li, Na, and K; and'}{'sup': '−7', 'sub': '3', 'from about 3 mol. % to about 11 mol. % of divalent oxide MO, wherein M is at least one of Mg, Ca, Ba, SrO and Zn, wherein an average coefficient of thermal expansion of a glass formed from the glass composition is less than or equal to 55×10/° C., a compressive stress in the glass composition is greater than or equal to 400 MPa following ion-exchange in a 100% KNOsalt bath at 410° C. for 8 hours, and a liquidus viscosity greater than or equal to 35 kPoise.'}2. The glass composition of claim 1 , wherein the glass composition comprises:{'sub': '2', 'from about 65 mol. % to about 68 mol. % SiO;'}{'sub': 2', '3, 'from about 10 mol. % to about 13 mol. % AlO;'}{'sub': 2', '3, 'from about 6 mol. % to about 9 mol. % BO;'}{'sub': '2', 'from about 6 mol. % to less than 9 mol. % alkali ...

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Номер записи: 67
29-01-2015 дата публикации

Composite Laminated Ceramic Electronic Component

Номер: US20150030830A1
Автор: Hiroshige ADACHI, Kazuhiro Kaneko, Sadaaki Sakamoto, Satoru Adachi, Seiji Fujita
Принадлежит: Murata Manufacturing Co Ltd

A composite laminated ceramic electronic component that includes co-fired low dielectric-constant ceramic layers and high dielectric-constant ceramic layers. The low dielectric-constant ceramic layers and the high dielectric-constant ceramic layers are each composed of a glass ceramic containing: a first ceramic composed of MgAl 2 O 4 and/or Mg 2 SiO 4 ; a second ceramic composed of BaO, RE 2 O 3 (where RE is a rare-earth element), and TiO 2 ; glass containing each of 44.0 to 69.0 weight % of RO (where R is an alkaline-earth metal), 14.2 to 30.0 weight % of SiO 2 , 10.0 to 20.0 weight % of B 2 O 3 , 0.5 to 4.0 weight % of Al 2 O 3 , 0.3 to 7.5 weight % of Li 2 O, and 0.1 to 5.5 weight % of MgO; and MnO. The content ratios of the glass, etc. are varied between the low dielectric-constant ceramic layers and the high dielectric-constant ceramic layers.

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Номер записи: 68
29-01-2015 дата публикации

Strengthened glass articles having improved survivability

Номер: US20150030834A1
Автор: Benjamin Allen Stevens, Brina Paul Strines, Jonathan David Pesansky, Kevin Barry Reiman, Laurence Ralph Morey
Принадлежит: Corning Inc

Embodiments are directed to strengthened glass articles comprising a thickness t≦1 mm (1000 μm), an inner region under a central tension CT (in MPa), and at least one compressive stress layer adjacent the inner region and extending within the strengthened glass article from a surface of the strengthened glass article to a depth of layer DOL (in μm), wherein the strengthened glass article is under a compressive stress at the surface CS s (in MPa), wherein the strengthened glass article is an alkali aluminosilicate glass article comprising 0-5 mol % Li 2 O, and at least 3 mol % Al 2 O 3 , and wherein the DOL≧70 μm, and a CS s /DOL ratio≧2.5 MPa/μm.

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Номер записи: 69
29-01-2015 дата публикации

TWO-STEP METHOD FOR STRENGTHENING GLASS

Номер: US20150030840A1
Автор: Gomez Sinue, Lamberson Lisa Ann, Morena Robert Michael
Принадлежит:

A method of strengthening an alkali aluminoborosilicate glass. A compressive layer extending from a surface of the glass to a depth of layer is formed by exchanging larger metal cations for smaller metal cations present in the glass. In a second step, metal cations in the glass are exchanged for larger metal cations to a second depth in the glass that is less than the depth of layer and increase the compressive stress of the compressive layer. Formation of the compressive layer and replacement of cations with larger cations can be achieved by a two-step ion exchange process. An alkali aluminoborosilicate glass having a compressive layer and a crack indentation threshold of at least 3000 gf is also provided. 1. An alkali aluminoborosilicate glass comprising lithium cations , sodium cations , and potassium cations , wherein the glass has a surface having a compressive layer extending from the surface to a depth of layer and is enriched in potassium cations to a second depth that is less than the depth of layer , and wherein the surface of the glass has a crack initiation layer threshold of at least 6000 gf upon indentation with a Vickers indenter.2. The glass of claim 1 , further comprising 50-70 mol % SiO; 5-15 mol % AlO; 5-20 mol % BO; 2-15 mol % LiO; 0-20 mol % NaO; and 0-10 mol % KO.3. The glass of claim 1 , wherein the surface has a compressive stress of at least 500 MPa claim 1 , and wherein the depth of layer is at least about 50 μm.4. The glass of claim 1 , wherein the depth of layer is in a range from about 70 μm up to about 290 μm.5. The glass of claim 1 , wherein the second depth is in a range from about 5 μm up to about 20 μm.6. The glass of claim 1 , wherein the alkali aluminoborosilicate glass further comprises at least one of: 0-10 mol % PO; 0-5 mol % MgO; 0-1 mol % CeO; and 0-1 mol % SnO.7. The glass of claim 1 , wherein the glass is a glass sheet having a thickness of up to 2 mm.8. The glass of claim 1 , glass has a crack initiation layer threshold of ...

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Номер записи: 70
02-02-2017 дата публикации

ANTIMICROBIAL AND STRENGTHENED-GLASS ARTICLES THROUGH PRESSURIZED ION EXCHANGE

Номер: US20170029325A1
Автор: Martin Arthur Winston, Truesdale Carlton Maurice
Принадлежит:

A method of treating a substrate in a pressure vessel that includes the steps: preparing an ion-exchange bath with a bath composition that comprises a polar solvent and a plurality of ion-exchanging ions in a vessel; submersing a substrate having an outer region containing a plurality of exchangeable ions in the bath; pressurizing the bath in the vessel to a predetermined pressure substantially above ambient pressure; heating the bath in the vessel to a predetermined temperature; and treating the substrate for a predetermined ion-exchange duration at the predetermined pressure and temperature such that a portion of the plurality of exchangeable ions is exchanged with a portion of the ion-exchanging ions. The substrate can consist essentially of a glass, glass-ceramic or ceramic substrate composition, and the predetermined ion-exchange duration, temperature and pressure can each be selected based at least in part on the substrate composition and the bath composition. 1. A method of treating a substrate in a pressure vessel , comprising:preparing a bath with a bath composition that comprises a polar solvent and a plurality of cations in a vessel;submersing a substrate in the bath;pressurizing the bath in the vessel to a predetermined pressure, wherein the predetermined pressure is substantially greater than ambient pressure; andexchanging or infusing a portion of the plurality of cations from the bath composition into an outer region of the substrate for a predetermined duration at the predetermined pressure, wherein the outer region extends from a first surface to a first selected depth in the substrate.2. The method according to claim 1 , wherein the substrate comprises a plurality of exchangeable cations that are exchanged with the portion of the plurality of cations from the bath composition.3. The method according to claim 2 , wherein the substrate comprises a glass substrate or glass-ceramic substrate.4. The method according to claim 1 , wherein the substrate ...

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Номер записи: 71
01-02-2018 дата публикации

GLASSES HAVING IMPROVED TOUGHNESS AND SCRATCH RESISTANCE

Номер: US20180029923A1
Автор: Dejneka Matthew John, Ellison Adam James, Gomez Sinue, Morena Robert Michael
Принадлежит:

A silicate glass that is tough and scratch resistant. The toughness is increased by minimizing the number of non-bridging oxygen atoms in the glass. In one embodiment, the silicate glass is an aluminoborosilicate glass in which −15 mol %≦(RO+R′O—AlO—ZrO)—BO≦4 mol %, where R is one of Li, Na, K, Rb, and Cs, and R′ is one of Mg, Ca, Sr, and Ba. 1. A silicate glass , the silicate glass being ion exchangeable and comprising:{'sub': '2', '62-70 mol. % SiO;'}{'sub': 2', '3, '>0-18 mol % AlO;'}{'sub': 2', '3, '>0-10 mol % BO;'}{'sub': '2', '0-15 mol % LiO;'}{'sub': '2', '6-20 mol % NaO;'}{'sub': '2', '0-18 mol % KO;'}>0-17 mol % MgO; and{'sub': '2', 'ZrO,'}{'sub': 2', '3', '2', '3', '2', '2', '2', '2', '3', '2', '2', '3, 'wherein 16 mol %≦AlO+BO+ZrO≦29 mol %; 14 mol %≦RO+≦25 mol %; and −15 mol %≦(RO+—AlO—ZrO)—BO≦4 mol %, where R is at least one of Li, Na, K, Rb, and Cs, and R′ is at least one of Mg, Ca, Sr, and Ba.'}2. The silicate glass according to claim 1 , wherein the silicate glass has a toughness in a range from about 0.7 MPaup to about 1.2 MPa.3. The silicate glass according to claim 2 , wherein the silicate glass has a brittleness of less than about 8.5 μm.4. The silicate glass according to claim 1 , wherein the silicate glass is ion exchanged and has a surface compressive stress of at least about 200 MPa and a surface compressive layer claim 1 , the surface compressive layer having a depth of at least about 30 μm.5. The silicate glass according to claim 1 , wherein the silicate glass has a liquidus viscosity of at least 100 kpoise.6. The silicate glass according to claim 1 , wherein the silicate glass is substantially free of at least one of lithium claim 1 , antimony oxide claim 1 , and arsenic oxide.7. The silicate glass according to claim 1 , wherein the silicate glass forms a cover plate for a mobile electronic device claim 1 , wherein the cover plate has a thickness in a range from about 0.3 mm up to about 1.5 mm.8. The silicate glass according to claim 1 , ...

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Номер записи: 72
05-02-2015 дата публикации

Glass core substrate and method for manufacturing the same

Номер: US20150034377A1
Автор: Tae Hong Min
Принадлежит: Samsung Electro Mechanics Co Ltd

Disclosed herein are a glass core substrate and a method for manufacturing the same. According to an embodiment of the present invention, there is provided the glass core substrate including: a glass core laminate including a glass layer and insulating layers which are stacked on upper and lower portions of the glass layer; a through hole formed by penetrating through the glass core laminate and provided with at least one crack which is formed at a penetrating inner wall by penetrating into the glass layer; and a conductive material filled in the through hole and the crack. Further, the method for manufacturing a glass core substrate is provided.

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Номер записи: 73
31-01-2019 дата публикации

CONDUCTIVE PASTE, METHOD, ELECTRODE AND SOLAR CELL

Номер: US20190031557A1
Автор: BOOTH Jonathan Charles Shepley, CELA GREVEN Beatriz, CURRIE Edwin Peter Kennedy, DROSTE Tobias, Johnson Simon
Принадлежит:

The present invention relates to a conductive paste for forming a conductive track on a substrate, the paste comprising a solids portion dispersed in an organic medium, the solids portion comprising an electrically conductive material, particles of a glass fit and particles of a tellurium compound. The invention further relates to methods for preparing such a paste, to a method of manufacturing an electrode on a surface of a solar cell, and to a solar cell having an electrode formed thereon. 1. A conductive paste for forming a conductive track on a substrate , the paste comprising a solids portion dispersed in an organic medium ,the solids portion comprising an electrically conductive material, particles of a bismuth-cerium, bismuth-molybdenum, bismuth-tungsten, or bismuth-alkali metal glass frit and particles of a tellurium compound, wherein the glass frit is substantially lead-free and wherein the solids portion comprises 85 to 99.9 wt % of electrically conductive material.2. The conductive paste according to claim 1 , wherein the content ratio of glass frit to tellurium compound is 4:1 to 11:9 w/w.3. The conductive paste according to claim 1 , wherein the glass frit contains less than 10 wt % of the tellurium compound.4. The conductive paste as claimed in wherein claim 3 , the glass frit is substantially tellurium-free.5. The conductive paste as claimed in wherein claim 3 , the glass frit includes less than 0.1 wt % TeO.6. The conductive paste according to claim 1 , wherein the glass frit includes less than 0.1 wt % PbO.7. The conductive paste according to claim 1 , wherein the glass frit is substantially boron-free.8. The conductive paste according to claim 1 , wherein the glass frit includes less than 0.1 wt % BO.9. The conductive paste according to claim 1 , wherein the D90 particle size of the glass frit particles is 2 μm or less claim 1 , and/or the D90 particle size of the tellurium compound particles is 2 μm or less.10. The conductive paste according to ...

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Номер записи: 74
04-02-2021 дата публикации

CHEMICALLY STRENGTHENED BIOACTIVE GLASS-CERAMICS

Номер: US20210030920A1
Автор: Deng Huayun, Fu Qiang, Mauro John Christopher
Принадлежит:

A chemically strengthened bioactive glass-ceramic composition as defined herein. Also disclosed are methods of making and using the disclosed compositions. 1. A glass-ceramic composition , comprising:a first crystalline phase and a second crystalline phase, in combination, comprise a source of:{'sub': '2', '50 to 75 wt % SiO,'}{'sub': 2', '3, '1 to 5 wt % AlO,'}{'sub': 2', '3, '0.1 to 10% BO,'}{'sub': '2', '5 to 20 wt % LiO,'}{'sub': '2', '0.5 to 5 wt % NaO,'}{'sub': '2', '0 to 4% KO,'}{'sub': 2', '5, '0.5 to 6 wt % PO'}{'sub': '2', '0.5 to 8% ZrO, and'}{'sup': '−', '0.1 to 1.0 wt % F, based on a 100 wt % total of the composition.'}2. The glass-ceramic composition of further comprising having composition particles having ion-exchanged surfaces having a reduced lithium ion (Li) concentration and having at least one of an elevated sodium ion (Na) surface concentration claim 1 , an elevated potassium ion (K) surface concentration claim 1 , or elevated concentrations of lithium ion (Li) and sodium ion (Na) on the surface.3. The glass-ceramic composition of wherein the source is:{'sub': '2', '50 to 70 wt % SiO,'}{'sub': 2', '3, '1 to 4 wt % AlO,'}{'sub': 2', '3, '0.1 to 4% BO,'}{'sub': '2', '6 to 18 wt % LiO,'}{'sub': '2', '1 to 4 wt % NaO,'}{'sub': '2', '0 to 3% KO,'}{'sub': 2', '5, '1 to 5 wt % PO'}{'sub': '2', '1 to 6% ZrO, and'}{'sup': '−', '0.1 to 1.0 wt % F, based on a 100 wt % total of the composition.'}4. The glass-ceramic composition of further comprising having composition particles having ion-exchanged surfaces having a reduced lithium ion (Li) concentration and having at least one of an elevated sodium (Na) concentration claim 3 , an elevated potassium (K) concentration claim 3 , or an elevated concentrations of lithium ion (Li) and sodium ion (Na).5. A glass-ceramic composition claim 3 , comprising:a first crystalline phase and a second crystalline phase, in combination, comprising:{'sub': '2', '55 to 65 wt % SiO,'}{'sub': 2', '3, '2 to 4 wt % AlO,'}{'sub': ...

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Номер записи: 75
30-01-2020 дата публикации

Method for achieving a stress profile in a glass

Номер: US20200031711A1
Автор: Douglas Clippinger Allen, Gaozhu Peng, Guangli Hu, Xiaoju GUO
Принадлежит: Corning Inc

A method for generating various stress profiles for chemically strengthened glass. An alkali aluminosilicate glass is brought into contact with an ion exchange media such as, for example, a molten salt bath containing an alkali metal cation that is larger than an alkali metal cation in the glass. The ion exchange is carried out at temperatures greater than about 420° C. and at least about 30° C. below the anneal point of the glass.

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Номер записи: 76
31-01-2019 дата публикации

Fluorescent member and light-emitting module

Номер: US20190032886A1
Автор: Hisayoshi Daicho, Yu Shinomiya
Принадлежит: Koito Manufacturing Co Ltd

A fluorescent member includes: a wavelength converter including an incidence part on which a light of a light source is incident and an output part from which a converted light subjected to wavelength conversion as a result of excitation by an incident light is output; and a reflecting part provided in at least a portion of a surface of the wavelength converter. The wavelength converter is comprised of a material whereby a degree of scattering of the light of the light source incident via the incidence part and traveling toward the output part is smaller than in the case of a polycrystalline material.

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Номер записи: 77
01-02-2018 дата публикации

COMPLIANT SOLID-STATE IONICALLY CONDUCTIVE COMPOSITE MATERIALS AND METHOD FOR MAKING SAME

Номер: US20180034061A1
Автор: Burdynska Joanna, Nasybulin Eduard, Rupert Benjamin, Teran Alexander, Uppal Simmi Kaur, Venugopal Saranya
Принадлежит:

Provided herein are ionically conductive solid-state compositions that include ionically conductive inorganic particles in a matrix of an organic material. The resulting composite material has high ionic conductivity and mechanical properties that facilitate processing. In particular embodiments, the ionically conductive solid-state compositions are compliant and may be cast as films. In some embodiments of the present invention, solid-state electrolytes including the ionically conductive solid-state compositions are provided. In some embodiments of the present invention, electrodes including the ionically conductive solid-state compositions are provided. The present invention further includes embodiments that are directed to methods of manufacturing the ionically conductive solid-state compositions and batteries incorporating the ionically conductive solid-state compositions. 140-. (canceled)41. A method of forming a solid-state composite comprising:mixing ionically conductive amorphous inorganic material with one or more organic components to form a composite, wherein the one or more organic components comprises a first component that is a non-ionically conductive polymer having a number average molecular weight of between 500 g/mol and 50,000 g/mol; andapplying external pressure to the composite, wherein applying external pressure increases the ionic conductivity of the composite by a factor of at least two.42. The method of claim 41 , further comprising releasing the applied pressure.43. The method of claim 42 , further comprising heating the composite during the application of external pressure to a temperature greater than 70° C. claim 42 , and cooling the composite after heating.44. The method of claim 43 , wherein an increase of at least a factor of two in ionic conductivity is maintained after releasing the applied pressure.45. The method of claim 41 , wherein the one or more organic components further comprises a binder claim 41 , wherein the binder is a ...

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Номер записи: 78
01-02-2018 дата публикации

Compliant solid-state ionically conductive composite electrolytes and materials

Номер: US20180034096A1
Автор: Alexander Teran, Benjamin Rupert, Eduard Nasybulin, Joanna Burdynska, Saranya Venugopal, Simmi Kaur Uppal
Принадлежит: Blue Current Inc

Provided herein are ionically conductive solid-state compositions that include ionically conductive inorganic particles in a matrix of an organic material. The resulting composite material has high ionic conductivity and mechanical properties that facilitate processing. In particular embodiments, the ionically conductive solid-state compositions are compliant and may be cast as films. In some embodiments of the present invention, solid-state electrolytes including the ionically conductive solid-state compositions are provided. In some embodiments of the present invention, electrodes including the ionically conductive solid-state compositions are provided. The present invention further includes embodiments that are directed to methods of manufacturing the ionically conductive solid-state compositions and batteries incorporating the ionically conductive solid-state compositions.

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Номер записи: 79
05-02-2015 дата публикации

HYBRID SODA-LIME SILICATE AND ALUMINOSILICATE GLASS ARTICLES

Номер: US20150037586A1
Автор: Gross Timothy Michael
Принадлежит:

A glass article is provided having from greater than or equal to about 40 mol % to less than or equal to about 68 mol % SiO, less than or equal to about 11 mol % AlO, an RO:R′O molar ratio of from greater than or equal to about 1:1 to less than or equal to about 2:1, and an MgO:CaO molar ratio of from greater than or equal to about 0.6:1 to less than or equal to about 1.8:1. The class article may also include a compressive stress layer on at least one surface thereof, the compressive stress layer having a compressive stress that is greater than or equal to about 800 MPa, and a depth that is greater than or equal to about 20 μm. 1. A glass article comprising:{'sub': '2', 'from greater than or equal to about 40 mol % to less than or equal to about 68 mol % SiO;'}{'sub': 2', '3, 'less than or equal to about 11 mol % AlO;'}{'sub': '2', 'an RO:R′O molar ratio of from greater than or equal to about 1:1 to less than or equal to about 2:1;'}an MgO:CaO molar ratio of from greater than or equal to about 0.6:1 to less than or equal to about 1.8:1; anda compressive stress layer on at least one surface thereof, the compressive stress layer having a compressive stress that is greater than or equal to about 800 MPa.2. The glass article of claim 1 , wherein a depth of the compressive stress layer is greater than or equal to about 20 μm.3. The glass article of claim 2 , wherein the depth of the compressive stress layer is less than or equal to about 80 μm.4. The glass article of claim 1 , wherein the glass article comprises from greater than or equal to about 4 mol % to less than or equal to about 9 mol % MgO.5. The glass article of claim 1 , wherein the glass article comprises from greater than or equal to about 57 mol % to less than or equal to about 65 mol % SiO.6. The glass article of claim 1 , wherein the glass article comprises from greater than or equal to about 2.5 mol % to less than or equal to about 8 mol % CaO.7. The glass article of claim 1 , wherein the glass article ...

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Номер записи: 80
05-02-2015 дата публикации

CHALCOGENIDE GLASS

Номер: US20150038314A1
Автор: Aitken Bruce Gardiner, Currie Stephen Charles, Youngman Randall Eugene
Принадлежит:

Boron-containing network sulfide glass which may be useful in IR transmitting applications, such as IR optics, laser or fiber amplifiers doped with rare earths with emission in the near IR, and methods of making the same. 1. A glass comprising in atomic percent:0-40 Ge;0-40 As, Sb, or As+Sb;0-15 Ga, In, or Ga+In;0-15 P;0-40 Te;greater than 0-25 B; and50-85 S, Se, or S+Se.2. The glass according to claim 1 , wherein the glass is substantially homogenous.3. The glass according to claim 1 , wherein the glass is substantially oxygen free.4. The glass according to claim 1 , further comprising 0-15 Tl claim 1 , Pb claim 1 , Bi claim 1 , Sn claim 1 , or combinations thereof.5. The glass according to claim 1 , further comprising 0-20 alkali metal claim 1 , alkaline earth metal claim 1 , rare earth metal claim 1 , transition metals claim 1 , or combinations thereof.6. The glass according to claim 1 , comprising 0-4 percent Ge.7. The glass according to claim 1 , comprising 10-15 percent Ge.8. The glass according to claim 1 , comprising 24-40 percent Ge.9. The glass according to claim 1 , comprising in atomic percent:greater than 0-40 Ge;0-40 As;0-15 Ga;0-15 P;0-40 Te;greater than 0-25 B; and55-75 S, Se, or S+Se.10. The glass according to claim 1 , comprising in atomic percent:0-40 Ge;greater than 0-40 As;0-15 Ga;0-15 P;0-40 Te;greater than 0-25 B; and55-75 S, Se, or S+Se.11. The glass according to claim 1 , comprising in atomic percent:0-40 Ge;0-40 As;greater than 0-15 Ga;0-15 P;0-40 Te;greater than 0-25 B; and55-75 S, Se, or S+Se.12. The glass according to claim 1 , comprising in atomic percent:0-40 Ge;0-40 As;0-15 Ga;greater than 0-15 P;0-40 Te;greater than 0-25 B; and55-75 S, Se, or S+Se.13. A method for making a glass claim 1 , the method comprising:providing a precursor glass or crystalline material comprising in atomic percent0-40 Ge;0-40 As, Sb, or As+Sb;0-15 Ga, In, or Ga+In;0-15 P;0-40 Te;greater than 0-25 B; and50-85 S, Se, or S+Secombining the precursor glass or ...

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Номер записи: 81
05-02-2015 дата публикации

METHOD FOR PRODUCING CHEMICALLY TEMPERED GLASS

Номер: US20150038315A1
Автор: Akiba Shusaku, Endo Jun, Ono Kazutaka, Sawamura Shigeki
Принадлежит: Asahi Glass Company, Limited

To provide a method for producing chemically tempered glass, whereby frequency of replacement of the molten salt can be reduced. A method for producing chemically tempered glass, which comprises repeating ion exchange treatment of immersing glass in a molten salt, wherein the glass comprises, as represented by mole percentage, from 61 to 77% of SiO, from 1 to 18% of AlO, from 3 to 15% of MgO, from 0 to 5% of CaO, from 0 to 4% of ZrO, from 8 to 18% of NaO and from 0 to 6% of KO; SiO+AlOis from 65 to 85%; MgO+CaO is from 3 to 15%; and R calculated by the following formula by using contents of the respective components, is at least 0.66: 1. (canceled)2. Glass for chemical tempering , which comprises , as represented by mole percentage based on the following oxides , from 63 to 73% of SiO , from 10.2 to 18% of AlO , from 0 to 15% of MgO , from 0 to 4% of ZrO , from 11 to 16% of NaO , from 0 to 1% of KO and at most 5.6% of BO , and does not contain CaO; the total content of SiOand AlOis from 65 to 85%; the total content of MgO and CaO is from 0 to 15% , and R′ calculated by the following formula by using contents of the respective components , is at least 0.66:{'br': None, 'sub': 2', '2', '3', '2', '2', '2', '2', '3, 'R′=0.029×SiO+0.021×AlO+0.016×MgO−0.004×CaO+0.016×ZrO+0.029×NaO+0×KO+0.028×BO+0.012×SrO+0.026×BaO−2.002'}3. The glass for chemical tempering according to claim 2 , wherein the content of BOis at most 4%.4. The glass for chemical tempering according to claim 2 , wherein the content of NaO is from 11 to 14%.5. The glass for chemical tempering according to claim 2 , wherein no KO is contained.6. The glass for chemical tempering according to claim 4 , wherein no KO is contained.7. The glass for chemical tempering according to claim 2 , wherein the total content of SiO claim 2 , AlO claim 2 , MgO claim 2 , CaO claim 2 , ZrO claim 2 , NaO claim 2 , KO claim 2 , BO claim 2 , SrO and BaO is at least 98.5%.8. The glass for chemical tempering according to claim 2 , ...

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Номер записи: 82
05-02-2015 дата публикации

Glass plate

Номер: US20150038316A1
Автор: Tomoyuki Kobayashi, Yuki Kondo, Yusuke Arai
Принадлежит: Asahi Glass Co Ltd

To provide a glass plate which can be made to have higher Te than conventional glass plates when its iron content is substantially the same as the conventional glass plates, to have substantially the same level of Te as conventional glass plates when its iron content is larger than the conventional glass plates, or to have very high Te when its iron content is smaller than conventional glass plates, and which presents good productivity. A glass plate which comprises, as represented by mol percentage based on oxides, SiO 2 : from 57 to 71%, Al 2 O 3 : from 0 to 6%, B 2 O 3 : from 0 to 5%, Na 2 O: from 10 to 16%, MgO: from 7.5 to 19.8%, and CaO: from 1.6 to 11%, provided that S-value represented by MgO+Al 2 O 3 +B 2 O 3 —Na 2 O (as represented by mol percentage) is from −10 to 10.5%, and the ratio of the content of MgO, as represented by mol percentage based on oxide, to the content of CaO, as represented by mol percentage based on oxide, ([MgO]/[CaO]), is from 0.8 to 10.

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Номер записи: 83
11-02-2016 дата публикации

CONDUCTIVE PASTE AND MULTILAYER CERAMIC ELECTRONIC COMPONENT

Номер: US20160039711A1
Автор: Miyazaki Tomochika
Принадлежит:

A conductive paste for forming external electrodes for a multilayer ceramic electronic component. The paste contains a glass composition containing (a) BaO, (b) at least one of SrO and CaO, (c) ZnO, (d) BO, and (e) at least one selected from the group consisting of SiO, AlO, and TiO, in which the total content percentage of BaO, SrO, and CaO is 30 mol % or more, the molar ratio represented by BO/(SiO+AlO+TiO) is 0.7 to 1.5, and the content percentage of ZnO is 0 to 5 mol %. 1. A conductive paste comprising:a glass composition that contains:(a) BaO;(b) at least one of SrO and CaO;(c) ZnO;{'sub': 2', '3, '(d) BO; and'}{'sub': 2', '2', '3', '2, '(e) at least one selected from the group consisting of SiO, AlO, and TiO, wherein'}a total content percentage of BaO, SrO, and CaO is 30 mol % or more with respect to a total amount of the glass composition in the conductive paste,{'sub': 2', '3', '2', '2', '3', '2, 'a molar ratio represented by BO/(SiO+AlO+TiO) is 0.7 to 1.5, and'}a content percentage of ZnO is 0 to 5 mol % with respect to the total amount of the glass composition in the conductive paste.2. The conductive paste according to claim 1 , wherein the content percentage of the ZnO is 0.3. The conductive paste according to claim 2 , wherein the molar ratio represented by BO/(SiO+AlO+TiO) is 0.7 to 1.0.4. The conductive paste according to claim 1 , wherein the molar ratio represented by BO/(SiO+AlO+TiO) is 0.7 to 1.0.5. The conductive paste according to claim 1 , wherein the glass composition contains 20 mol % or more of BO.6. The conductive paste according to claim 2 , wherein the glass composition contains 20 mol % or more of BO.7. The conductive paste according to claim 3 , wherein the glass composition contains 20 mol % or more of BO.8. The conductive paste according to claim 4 , wherein the glass composition contains 20 mol % or more of BO.9. The conductive paste according to claim 1 , further comprising a total of 1 mol % or less of one or more of LiO claim 1 , ...

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Номер записи: 84
09-02-2017 дата публикации

A THERMOCHROMIC GLASS MATERIAL AND A PRODUCTION METHOD THEREOF

Номер: US20170036946A1
Автор: AYDIN Suheyla, CELIKBILEK ERSUNDU Miray, ERSUNDU Ali Ercin
Принадлежит: ISTANBUL TEKNIK UNIVERSITESI

The present invention relates a thermochromic glass material comprising heavy metal oxide, alkali oxide, halide and at least one of other compounds supporting glass formation together with tellurium oxide (TeO); and a production method thereof comprising the steps of preparing the powder mixture comprising TeO(), melting the mixture by heating (), cooling the molten mixture by pouring into a mold and obtaining glass (), keeping the glass removed from the mold in a drying oven and cooling (). 111.-. (canceled)12. A thermochromic glass material comprising at least one of heavy metal oxide , alkali oxide , halide components together with tellurium oxide (TeO) in order to achieve glass formation; and TeOwhich is in ratio of 30-95% by mole and which enables transmittance value , absorption edge value and band gap energy and thus the color to continuously and reversibly change in the visible region depending on temperature , and allows electronic passage by behaving like an electrolyte as a result of being vitrified and shows semi-conductive feature.13. A thermochromic glass material according to claim 12 , wherein the material comprises at least one of WO claim 12 , LiO claim 12 , NaO claim 12 , KO claim 12 , ZnO claim 12 , CdO claim 12 , BO claim 12 , TiO claim 12 , CuO claim 12 , FeO claim 12 , VO claim 12 , PbO claim 12 , NbO claim 12 , MoO claim 12 , GeO claim 12 , PO claim 12 , AgO claim 12 , SbO claim 12 , PbF claim 12 , LiCl claim 12 , ZnClcompounds as well as TeO14. A thermochromic glass material according to claim 13 , wherein the material comprises 0-35% WO claim 13 , 0-45% LiO claim 13 , 0-40% NaO claim 13 , 0-30% KO claim 13 , 0-40% ZnO claim 13 , 0-15% CdO claim 13 , 0-27.5% BO claim 13 , 0-15% TiO claim 13 , 0-50% CuO claim 13 , 0-20% FeO claim 13 , 0-55% VO claim 13 , 0-20% PbO claim 13 , 0-25% NbO claim 13 , 0-55% MoO claim 13 , 0-30% GeO claim 13 , 0-25% PO claim 13 , 0-20% AgO claim 13 , 0-20% SbO claim 13 , 0-25% PbF claim 13 , 0-30% LiCl claim 13 , 0- ...

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Номер записи: 85
09-02-2017 дата публикации

STRENGTHENED GLASS WITH DEEP DEPTH OF COMPRESSION

Номер: US20170036952A1
Автор: Amin Jaymin, Egboiyi Benedict Osobomen, Pesansky Jonathan David, Reiman Kevin Barry, Roussev Rostislav Vatchev, Strines Brian Paul
Принадлежит:

Chemically strengthened glass articles having at least one deep compressive layer extending from a surface of the article to a depth of at least about 45 μm within the article are provided. In one embodiment, the compressive stress profile includes a single linear segment extending from the surface to the depth of compression DOC. Alternatively, the compressive stress profile includes two linear portions: the first portion extending from the surface to a relatively shallow depth and having a steep slope; and a second portion extending from the shallow depth to the depth of compression. The strengthened glass has a 60% survival rate when dropped from a height of 80 cm in an inverted ball drop test and an equibiaxial flexural strength of at least 10 kgf as determined by abraded ring-on-ring testing. Methods of achieving such stress profiles are also described. 130-. (canceled)31. A glass article having a thickness t , the glass article comprising: a. the compressive layer extends from the surface to a depth of compression DOC, wherein DOC≧0.1·t when t<0.5 mm and DOC≧50 μm when t≧0.5 mm, and wherein the compressive layer has a compressive stress profile; and', [{'sub': b', 'b', 'b', 'b, 'i. a first portion b extending from the surface to a depth dand having an average slope m, wherein 3 μm≦d≦15 μm and −40 MPa/μm≧m≧−200 MPa/μm;'}, {'sub': c', 'c', 'c, 'ii. a second portion c extending from a depth dto the DOC and having an average slope m, wherein −2 MPa/μm≧m≧−8 MPa/μm; and'}], 'b. the compressive stress profile comprises], 'a compressive layer having a compressive stress CS in a range from about 500 MPa up to about 1200 MPa at a surface of the glass article, wherein{'sub': b', 'c', 'b', 'c', 'c', 'b, 'iii. a transition region extending from dto dhaving a slope that transitions from slope mto slope m, wherein d−dis 8 μm or less.'}32. The glass article of claim 31 , wherein d-dis 7 μm or less.33. The glass article of claim 31 , wherein d-dis 5 μm or less.34. The glass ...

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Номер записи: 86
09-02-2017 дата публикации

STRENGTHENED GLASS WITH DEEP DEPTH OF COMPRESSION

Номер: US20170036953A1
Автор: Amin Jaymin, Egboiyi Benedict Osobomen, Pesansky Jonathan David, Reiman Kevin Barry, Roussev Rostislav Vatchev, Strines Brian Paul
Принадлежит:

Chemically strengthened glass articles having at least one deep compressive layer extending from a surface of the article to a depth of at least about 45 μm within the article are provided. In one embodiment, the compressive stress profile includes a single linear segment extending from the surface to the depth of compression DOC. Alternatively, the compressive stress profile includes two linear portions: the first portion extending from the surface to a relatively shallow depth and having a steep slope; and a second portion extending from the shallow depth to the depth of compression. The strengthened glass has a 60% survival rate when dropped from a height of 80 cm in an inverted ball drop test and an equibiaxial flexural strength of at least 10 kgf as determined by abraded ring-on-ring testing. Methods of achieving such stress profiles are also described. 112-. (canceled)13. A strengthened glass having a thickness t , the strengthened glass comprising:an inner region under a central tension CT; andat least one compressive stress layer under a compressive stress CS, the compressive stress layer extending from a surface of the glass to a depth of compression DOC, wherein DOC≧0.1·t when t<0.5 mm and DOC≧50 μm when t≧0.5 mm, and being adjacent to the inner region,wherein the strengthened glass has an equibiaxial flexural strength of at least about 10 kgf as determined by abraded ring-on-ring testing.14. The strengthened glass of claim 13 , wherein a CS at a surface of the glass is in a range from about 500 MPa up to about 1200 MPa and wherein the compressive layer has a compressive stress profile comprising:{'sub': b', 'b', 'b', 'b, 'a. a first portion b extending from the surface to a depth dand having a slope m, wherein 3 μm≦d≦15 μm and −40 MPa/μm≧m≧−200 MPa/μm;'}{'sub': c', 'c, 'b. a second portion c extending from a depth dto the DOC and having an average slope m, wherein −2 MPa/μm≧m≧−8 MPa/μm; and'}{'sub': b', 'c', 'b', 'c, 'c. a transition region extending from ...

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Номер записи: 87
09-02-2017 дата публикации

METHODS OF MAKING ANTIMICROBIAL GLASS ARTICLES

Номер: US20170036954A1
Автор: Fagan Sumalee Likitvanichkul, Kuksenkova Ekaterina Aleksandrovna, Pal Santona, Tetiker Mehmet Derya
Принадлежит:

Described herein are various methods and manufacturing methods for making antimicrobial and strengthened, antimicrobial glass articles and substrates. The methods described herein generally include contacting the article with a KNO-containing molten salt bath set at about 380 C to about 460 C for about 30 minutes to about 24 hours to form a compressive stress layer that extends inward from a surface of the glass substrate to a first depth; and contacting the article comprising the compressive stress layer with a AgNO-containing molten salt bath set at about 300° C. to about 400° C. for about 5 minutes to about 18 hours to form an antimicrobial region that extends inward from the surface of the glass substrate to a second depth. The methods also include poisoning at least the AgNO-containing molten salt bath and, in some cases, the KNO-containing molten salt bath. Poisoning components include Na and Li ions. 1. A method of making an antimicrobial glass article , the method comprising:providing a glass substrate;{'sub': 3', '3, 'contacting the glass substrate with a KNO-containing molten salt bath for about 30 minutes to about 24 hours to form a compressive stress layer, wherein the KNO-containing molten salt bath is set at a temperature of about 380° C. to about 460° C. and the compressive stress layer extends inward from a surface of the glass substrate to a first depth;'}{'sub': '3', 'providing an AgNO-containing molten salt bath set at a temperature of about 300° C. to about 400° C.;'}{'sub': '3', 'poisoning the AgNO-containing molten salt bath; and'}{'sub': '3', 'contacting the glass substrate comprising the compressive stress layer with the poisoned AgNO-containing molten salt bath for about 5 minutes to about 18 hours to form an antimicrobial region, wherein the antimicrobial region extends inward from the surface of the glass substrate to a second depth.'}2. The method of claim 1 , wherein the poisoning step is configured to minimize Ag consumption during the ...

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Номер записи: 88
08-02-2018 дата публикации

GLASS-COATED LIGHT-ACCUMULATING MATERIAL AND METHOD FOR PRODUCING GLASS-COATED LIGHT-ACCUMULATING MATERIAL

Номер: US20180037811A1
Автор: Kobayashi Yoshinao, NEMOTO Kunihiko
Принадлежит: KOA GLASS CO., LTD.

A glass-coated light-accumulating material having excellent water resistance and having excellent luminescence properties for a long time period, and an efficient method for producing such a glass-coated light-accumulating material are provided. 18-. (canceled)9. A glass-coated light-accumulating material which has a particulate shape , and which is uniformly mixed and dispersed into resins or the inorganic materials , comprising a metal aluminate salt as a light-accumulating material incorporated into a glass component including a zinc phosphate glass as a main component ,{'sub': 2', '5', '2, 'wherein the zinc phosphate glass includes PO, ZnO, and RO, wherein R═Na or K, as main components,'}{'sub': 2', '5', '2, 'the mixing composition of the zinc phosphate glass is such that the content of POhas a value within the range of 40% to 60% by weight, the content of ZnO has a value within the range of 25% to 39% by weight, and the content of RO has a value within the range of 3% to 15% by weight, with respect to the total amount,'}the melting point of the zinc phosphate glass is adjusted to a value within the range of 600° C. to 900° C.,{'sup': '2', 'the Vickers hardness is within the range of 10 to 500 kgf/mm, and'}the average particle size has a value within the range of 1 μm or more and below 500 μm.10. A glass-coated light-accumulating material which has a granular shape or a flat plate shape , comprising a metal aluminate salt as a light-accumulating material incorporated into a glass component including a zinc phosphate glass as a main component ,{'sub': 2', '5', '2, 'wherein the zinc phosphate glass includes PO, ZnO, and RO (wherein R═Na or K) as main components,'}{'sub': 2', '5', '2, 'the mixing composition of the zinc phosphate glass is such that the content of POhas a value within the range of 40% to 60% by weight, the content of ZnO has a value within the range of 25% to 39% by weight, and the content of RO has a value within the range of 3% to 15% by weight, ...

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Номер записи: 89
31-01-2019 дата публикации

HEATING ELEMENT STRUCTURE, METHOD OF FORMING THE SAME, AND HEATING DEVICE INCLUDING THE HEATING ELEMENT STRUCTURE

Номер: US20190037645A1
Автор: Bae Minjong, KIM Doyoon, Kim Hajin, KIM Jinhong, KIM Seyun, Koh Haengdeog, LEE Changsoo, MIZUSAKI Soichiro
Принадлежит:

A The heating element structure includes: a conductive metal substrate; a heating layer spaced apart from the conductive metal substrate and configured to generate heat in response to an electrical signal; electrodes in contact with the heating layer and configured to provide the electrical signal to the heating layer; and a first insulating layer on the conductive metal substrate, the first insulating layer comprising a first matrix material and a particle, wherein a difference between a coefficient of thermal expansion (CTE) of the first matrix material and a coefficient of thermal expansion of the particle is about 4×10per Kelvin or less. 1. A heating element structure comprising:a conductive metal substrate;a heating layer spaced apart from the conductive metal substrate and configured to generate heat in response to an electrical signal;electrodes in contact with the heating layer and configured to provide the electrical signal to the heating layer; anda first insulating layer on the conductive metal substrate, the first insulating layer comprising a first matrix material and a particle,{'sup': '−6', 'wherein a difference between a coefficient of thermal expansion of the first matrix material and a coefficient of thermal expansion of the particle is about 4×10per Kelvin or less.'}2. The heating element structure of claim 1 , wherein the first matrix material has a coefficient of thermal expansion of about 8×10per Kelvin to about 12×10per Kelvin.3. The heating element structure of claim 1 , wherein the particle has a coefficient of thermal expansion of about 7×10per Kelvin to about 13×10per Kelvin.4. The heating element structure of claim 3 , wherein the coefficient of thermal expansion of the particle is greater than the coefficient of thermal expansion of the matrix material.5. The heating element structure of claim 1 , wherein the difference between the coefficient of thermal expansion of the first matrix material and the coefficient of thermal expansion of ...

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Номер записи: 90
24-02-2022 дата публикации

Mixed silver powder and conductive paste comprising same

Номер: US20220055941A1
Автор: Chi Ho Yoon, Jin Ho Kwak, Jong Chan Lim, Moo Hyun LIM, Won Jun JO, Young Ho Lee
Принадлежит: Dae Joo Electronic Materials Co Ltd

A mixed silver powder and a conductive paste comprising the powder are disclosed. The mixed silver powder is obtained by mixing two or more spherical silver powders having different properties from each other. The mixed powder may minimize the disadvantages of the respective types of the two or more powders and maximize the advantages thereof, thereby improving the characteristics of products. In addition, by comprehensively controlling the particle size distribution of surface-treated mixed silver powder and the particle diameter and specific gravity of primary particles, a high-density conductor pattern, a precise line pattern, and the suppression of aggregation over time can be simultaneously achieved.

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Номер записи: 91
11-02-2016 дата публикации

SPARK PLUG WITH IMPROVED SEAL

Номер: US20160043531A1
Автор: FIRSTENBERG KEITH, JR. William J., Walker
Принадлежит:

An electrically conductive glass seal for providing a hermetic bond between an electrically conductive component and an insulator of a spark plug is provided. The glass seal is formed by mixing glass frits, binder, expansion agent, and electrically conductive metal particles. The glass frits can include silica (SiO), boron oxide (BO), aluminum oxide (AlO), bismuth oxide (BiO), and zinc oxide (ZnO); the binder can include sodium bentonite or magnesium aluminum silicate, polyethylene glycol (PEG), and dextrin; the expansion agent can include lithium carbonate; and the electrically conductive particles can include copper. The finished glass seal includes the glass in a total amount of 50.0 to 85.0 weight (wt. %), and electrically conductive metal particles in an amount of 15.0 to 50.0 wt. %, based on the total weight of the glass seal. 1. An electrically conductive glass seal for a spark plug , comprising:at least one glass in a total amount of 50.0 to 85.0 weight (wt. %), based on the total weight of said glass seal;electrically conductive metal particles in an amount of 15.0 to 50.0 wt. %, based on the total weight of said glass seal;wherein said glass seal includes gas-filled pores in an amount of 25.0 to 75.0 volume percent (vol. %), based on the total volume of said glass seal; andsaid glass seal is electrical conductive.2. The electrically conductive glass seal of claim 1 , wherein said glass includes silica (SiO) claim 1 , boron oxide (BO) claim 1 , aluminum oxide (AlO) claim 1 , bismuth oxide (BiO) claim 1 , and zinc oxide (ZnO); and said electrically conductive particles include copper.3. The electrically conductive glass seal of claim 1 , wherein said glass includes silica (SiO) in an amount of 35.0 to 40.0 wt. % claim 1 , boron oxide (BO) in an amount of 20.0 to 28.0 wt. % claim 1 , aluminum oxide (AlO) in an amount of 10.0 to 15.0 wt. % claim 1 , bismuth oxide (BiO) in an amount of 10.0 to 15.0 wt. % claim 1 , and zinc oxide (ZnO) in an amount of 3.0 to 5.0 ...

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Номер записи: 92
09-02-2017 дата публикации

PROCESS FOR PRODUCING CONDUCTIVE PASTES FOR FORMING SOLAR CELL ELECTRODES

Номер: US20170040472A1
Автор: Takahashi Tetsu
Принадлежит: NAMICS CORPORATION

A process for producing conductive pastes for forming solar cell electrodes, including a step of measuring binding energies of oxygen in a glass frit by X-ray photoelectron spectroscopy, a step of selecting a glass frit providing an X-ray photoelectron spectrum representing binding energies of oxygen in which the signal intensity of a peak with a peak top at a range from 529 eV to less than 531 eV has a proportion of 40% or more relative to the total of signal intensities from 526 eV to 536 eV, and a step of mixing together a conductive powder, the glass frit and an organic vehicle. 1. A process for producing conductive pastes for forming solar cell electrodes , comprising:a step of measuring binding energies of oxygen in a glass frit by X-ray photoelectron spectroscopy,a step of selecting a glass frit providing an X-ray photoelectron spectrum representing binding energies of oxygen in which the signal intensity of a peak with a peak top at a range from 529 eV to less than 531 eV has a proportion of 40% or more relative to the total of signal intensities from 526 eV to 536 eV, anda step of mixing together a conductive powder, the glass frit and an organic vehicle.2. The process according to claim 1 , wherein the glass frit comprises silicon dioxide.3. The process according to claim 1 , wherein the glass frit comprises at least one oxide selected from the group consisting of lead oxide and boron oxide.4. The process according to claim 1 , wherein the glass frit is in an amount of 1.5 to 10 parts by weight with respect to 100 parts by weight of the conductive powder.5. The process according to claim 1 , wherein the conductive powder is a silver powder.6. The conductive paste according to claim 1 , wherein the glass frit has particle sizes in a range from 0.5 to 5 μm.7. The conductive paste according to claim 1 , wherein the glass frit has a softening point of 400 to 600° C. This is a Divisional application of U.S. application Ser. No. 13/898,610, filed May 21, 2013, ...

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Номер записи: 93
07-02-2019 дата публикации

SELENIUM-FREE SUNGLASS MATERIAL WITH BROWN TINT

Номер: US20190039943A1
Автор: Baron Pierre-Jean, Brocheton Yves Andre Henri
Принадлежит:

UV- and IR-absorbing materials with brown tint for sunglasses are described. The sunglass materials are prepared from a base glass through a post-fabrication process that includes ion exchange with silver. The tint of the sunglass material can be adjusted by controlling the level of ion exchange of the base glass with silver by varying the conditions of ion exchange. A wide range of tint is possible, including multiple shades of brown tint. In a typical process, a base glass having strong absorption in the UV and IR is fabricated and the resulting glass is subjected to a post-fabrication silver ion exchange process to control tint. The post-fabrication silver ion exchange process permits control of tint while maintaining strong UV and IR absorption and adequate transmittance in the visible. 1. A method for processing a glass comprising:{'sub': 2', '3', '2, 'placing a first glass in an ion-exchange bath, said first glass comprising BOand SiO, said first glass lacking Se, said ion-exchange bath comprising a silver salt and introducing silver into said first glass to form a second glass.'}2. The method of claim 1 , wherein said silver salt has a concentration in the range from 0.01 wt % to 1.0 wt % in said ion-exchange bath.3. The method of claim 1 , wherein said silver salt is silver nitrate.4. The method of claim 1 , wherein said first glass has a first average percent transmittance (% T) claim 1 , for a thickness of 1.9 mm claim 1 , over the wavelength range from 780 nm-2000 nm and said second glass has a second average percent transmittance (% T) claim 1 , for a thickness of 1.9 mm claim 1 , over the wavelength range from 780 nm-2000 nm claim 1 , said second average percent transmittance (% T) being within the range from 50%-150% of said first average percent transmittance (% T).5. The method of claim 4 , wherein said first glass has a third average percent transmittance (% T) claim 4 , for a thickness of 1.9 mm claim 4 , over the wavelength range from 280 nm-400 ...

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Номер записи: 94
07-02-2019 дата публикации

METHOD FOR THE PREPARATION OF LITHIUM SILICATE GLASSES AND LITHIUM SILICATE GLASS CERAMICS

Номер: US20190039944A1
Автор: Bürke Harald, Höland Wolfram, Krolikowski Sebastian, Rampf Markus, Ritzberger Christian, Schweiger Marcel
Принадлежит:

The invention relates to a method for the preparation of a lithium silicate glass or a lithium silicate glass ceramic which comprise cerium ions and are suitable in particular for the preparation of dental restorations, the fluorescence properties of which largely correspond to those of natural teeth. 1. Method for the preparation of a lithium silicate glass , a lithium silicate glass with nuclei which are suitable for forming lithium metasilicate and/or lithium disilicate crystals , or a lithium silicate glass ceramic , which comprises a step in which a melt of a starting glass which comprises cerium ions is reacted with at least one reducing gas.2. Method according to claim 1 , wherein the gas comprises hydrogen or comprises hydrogen and nitrogen.3. Method according to claim 1 , in which the starting glass comprises up to 5.0 wt.-% alkaline earth metal oxide.4. Method according to claim 3 , wherein the alkaline earth metal oxide is CaO claim 3 , BaO claim 3 , MaO claim 3 , SrOor a mixture thereof.7. Method according to claim 1 , in which the starting glass furthermore comprises terbium ions.8. Method according to for the preparation of a lithium silicate glass with nuclei which are suitable for forming lithium metasilicate and/or lithium disilicate crystals.9. Method according to for the preparation of a lithium silicate glass ceramic which comprises lithium metasilicate as main crystal phase and/or comprises more than 10 vol.-% lithium metasilicate crystals.10. Method according to claim 9 , wherein the lithium metasilicate glass ceramic comprises more than 20 vol.-% lithium metasilicate crystals.11. Method according to for the preparation of a lithium silicate glass ceramic which comprises lithium disilicate as main crystal phase and/or comprises more than 10 vol.-% lithium disilicate crystals.12. Method according to claim 11 , wherein the lithium silicate glass ceramic comprises more than 20 vol.-% lithium disilicate crystals.13. Method according to claim 1 , in ...

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Номер записи: 95
07-02-2019 дата публикации

Method of Manufacture of Copper-doped Glasses

Номер: US20190039948A1
Автор: Huston Alan L., Justus Brian L., Marcheschi Barbara A.
Принадлежит: The Government of the United States of America, as represented by the Secretary of the Navy

A method of making a copper-doped glass comprising placing a target glass in a container, placing a target glass in a container, surrounding the target glass with a powder mixture comprised of fused silica (SiO) powder and copper sulfide (CuS) powder, such that both the target glass and the surrounding powder are contained in the container, and heating the container and the target glass and the surrounding powder mixture to a temperature of between 800° C. and 1150° C. 1. A method of making a copper-doped glass comprising the steps of:placing a target glass in a container;{'sub': 2', '2, 'surrounding the target glass with a powder mixture comprised of fused silica (SiO) powder and copper sulfide (CuS) powder, such that both the target glass and the surrounding powder are contained in the container; and'}heating the container and the target glass and the surrounding powder mixture to a temperature of between 800° C. and 1150° C.2. The method of making a copper-doped glass of wherein the powder mixture is comprised of a SiOpowder and Cus powder mixed according to the formula (SiO)(CuS) claim 1 , where 0.01 Подробнее

Номер записи: 96
24-02-2022 дата публикации

FILLING MATERIALS AND METHODS OF FILLING THROUGH HOLES OF A SUBSTRATE

Номер: US20220059436A1
Автор: KEUSSEYAN Roupen Leon, Mobley Tim
Принадлежит:

Pastes are disclosed that are configured to coat a passage of a substrate. When the paste is sintered, the paste becomes electrically conductive so as to transmit electrical signals from a first end of the passage to ta second end of the passage that is opposite the first end of the passage. The metallized paste contains a lead-free glass frit, and has a coefficient of thermal expansion sufficiently matched to the substrate so as to avoid cracking of the sintered paste, the substrate, or both, during sintering. 1. A glass substrate defining first and second external surfaces , the substrate comprising:a passage that extends from the first external surface to the second external surface, wherein the passage is defined by at least one side wall of the glass substrate;a lead-free electrically conductive material that extends along an entirety of the passage and is bonded to the at least one side wall; anda lead-free glass frit disposed in the passage.2. The glass substrate of claim 1 , wherein the lead-free electrically conductive material comprises a metal.3. The glass substrate of claim 2 , wherein the metal comprises silver or an oxide or alloy thereof claim 2 , copper or an oxide or alloy thereof claim 2 , or gold or an oxide or alloy thereof.4. The glass substrate of claim 1 , wherein the passage is a through-passage.5. The glass substrate of claim 4 , wherein the passage has a maximum cross-sectional dimension that is in a range from about 5 microns to about 3000 microns.6. The glass substrate of claim 4 , comprising quartz.7. The glass substrate of claim 5 , wherein the first and second external surfaces are opposite each other.8. A glass substrate defining first and second external surfaces claim 5 , the substrate comprising:a hole that extends from the first external surface to the second external surface, wherein the hole is defined by at least one side wall of the glass substrate;a lead-free metal plated in the hole; andan electrically nonconductive polymer ...

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Номер записи: 97
16-02-2017 дата публикации

GLASS

Номер: US20170044049A1
Автор: Akiba Shusaku, KITAOKA Kenji, YAMAZAKI Shuji
Принадлежит: Asahi Glass Company, Limited

A glass includes, as represented by mole percentage based on the following oxides, from 56 to 72% of SiO, from 3 to 20% of BO, from 8 to 20% of AlO, from 8 to 25% of NaO, from 0 to 5% of KO, from 0 to 15% of MgO, from 0 to 5% of CaO, from 0 to 3% of SrO, from 0 to 3% of BaO, and from 0.1 to 8% of ZrO. The glass contains substantially no LiO. 1. A glass comprising , as represented by mole percentage based on the following oxides , from 56 to 72% of SiO , from 3 to 20% of BO , from 8 to 20% of AlO , from 8 to 25% of NaO , from 0 to 5% of KO , from 0 to 15% of MgO , from 0 to 5% of CaO , from 0 to 3% of SrO , from 0 to 3% of BaO , and from 0.1 to 8% of ZrOand containing substantially no LiO.2. The glass according to claim 1 , wherein the following relationship using contents of respective components is satisfied: 0.05 Подробнее

Номер записи: 98
15-02-2018 дата публикации

Machinable and chemically toughenable glass ceramic

Номер: US20180044225A1
Автор: Chong Wang, Huiyan Fan, José ZIMMER, Junming Xue, Wenliang PING
Принадлежит: Schott Glass Technologies Suzhou Co Ltd

The present invention is directed to a kind of machinable glass ceramic which can be chemically toughened. The machinable and chemically toughenable glass ceramic, which comprises, as represented by weight percentage based on the following compositions, 25-75 wt % of SiO 2 , 6-30 wt % of Al 2 O 3 , 0.1-30 wt % of Na 2 O, 0-15 wt % of K 2 O, 0-30 wt % of B 2 O 3 , 4-35 wt % of MgO, 0-4 wt % of CaO, 1-20 wt % of F, 0-10 wt % of ZrO 2 , 0.1-10 wt % of P 2 O 5 , 0-1 wt % of CeO 2 and 0-1 wt % of SnO 2 , wherein P 2 O 5 +Na 2 O>3 wt %, and Al 2 O 3 +Na 2 O+P 2 O 5 >17 wt %. Mica crystalline phase can be formed in the glass ceramic and the glass ceramic can be chemically toughened by one step, two steps or multiple steps with depth of K-ion layer of at least 15 μm and surface compress stress of at least 300 MPa. The profile on depth of the ion exchange layer follows the complementary error function. Hardness can be improved by at least 20% after chemical toughening. The dimension deviation ratio is less than 0.06% by ion-exchanging.

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Номер записи: 99
15-02-2018 дата публикации

METHODS FOR REDUCING SURFACE DEFECTS

Номер: US20180044231A1
Автор: Amin Jaymin, Jin Yuhui, Smith Kristy Lynn
Принадлежит:

Methods for reducing a defective area in a strengthened substrate to produce a non-defective substrate are provided. The methods include contacting a strengthened defective substrate with a heated salt bath containing at least one monovalent salt, and removing the strengthened substrate from the bath. The strengthened substrate, before being contacted with the salt bath, is a defective substrate having at least one defective area and one or more non-defective area. Upon removal from the salt bath, at least one defective area has been reduced or substantially removed to produce a non-defective substrate. 1. A method for removing a defective area in a strengthened substrate comprising:heating a salt bath comprising at least one monovalent salt to a temperature of from greater than or equal to 95° C.;contacting at least a portion of a strengthened substrate with the salt bath, wherein, before the strengthened substrate is contacted with the salt bath, the strengthened substrate has one or more non-defective areas having an average concentration of total metal monovalent cations, and at least one defective area having an average concentration of total metal monovalent cations that deviates from the average concentration of the one or more non-defective areas by greater than or equal to 10 mol %;removing the at least a portion of the strengthened substrate from the salt bath, wherein, after removal, the at least one defective area has an average concentration of total metal monovalent cations that deviates from the an average concentration of total metal monovalent cations of the one or more non-defective areas by less than 10 mol %.2. The method of claim 1 , wherein the average concentration of the at least one defective area comprises greater than or equal to 60 mol % of a first metal monovalent cation before the strengthened substrate is contacted with the salt bath and after removing the at least a portion of the strengthened substrate from the salt bath claim 1 , ...

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Номер записи: 100