Multi-phase particulates, method of making, and composition containing same

Provided is a method of preparing a multi-phase particulate. The method includes: (1) blending together (a) a dispersed phase component of a metal, a metal oxide, an organometallic compound, salts thereof, and/or mixtures thereof, and (b) a bulk phase component of an inorganic material different from the dispersed phase component to form an admixture; and (2) dry-milling and/or compressing the admixture for a time and at a pressure sufficient to disperse the dispersed phase component in and bind the dispersed phase component to the bulk phase component, thereby forming a multi-phase particulate. Coating compositions including the multi-phase particulate also are provided.

Silica composite particles and method of preparing the same

Silica composite particles include silicon oxide and titanium in an amount of from 0.001% by weight to 10% by weight, wherein the silica composite particles have an average particle diameter of from 30 nm to 500 nm, a particle size distribution index of from 1.1 to 1.5, and an average degree of circularity of primary particles of from 0.5 to 0.85.

EFFECT PIGMENTS

The present invention relates to effect pigments which are based on flake-form substrates having a circular form factor of 1.2-2 and are coated with at least one high-refractive-index layer, and to the use thereof, inter alia in paints, coatings, printing inks, plastics and in cosmetic formulations. 1. An effect pigment comprising a flake-form substrate having a circular form factor of circumference/area standardized to a circle of 1.2-2 coated with at least one high-refractive-index layer having a refractive index of n≧1.8.2. The effect pigment according to claim 1 , wherein the substrate has a circular form factor of 1.2-1.8.3. The effect pigment according to claim 1 , wherein the substrate has a particle size of 5-60 μm.4. The effect pigment according to one or more of claim 1 , wherein the substrate has a thickness of 0.2-0.6 μm.5. The effect pigment according to one or more of claim 1 , wherein the flake-form substrate is synthetic mica flakes claim 1 , natural mica flakes claim 1 , SiOflakes claim 1 , AlOflakes claim 1 , glass flakes claim 1 , iron oxide flakes claim 1 , graphite flakes claim 1 , TiOflakes or mixtures thereof.6. The effect pigment according to claim 1 , wherein the flake-form substrate is a mica or glass flake.7. The effect pigment according to claim 1 , wherein the flake-form substrate is a natural mica flake.8. The effect pigment according to claim 1 , wherein the high-refractive-index layer is a compound that is at least one metal oxide claim 1 , metal sulfide claim 1 , iron titanate claim 1 , iron oxide hydrate claim 1 , titanium suboxide claim 1 , metal claim 1 , or mixtures or mixed phases of said compound.9. The effect pigment according to claim 1 , wherein the high-refractive-index layer comprises at least one compound that is TiO claim 1 , BiOCl claim 1 , CeO claim 1 , CrO claim 1 , CoO claim 1 , CoO claim 1 , FeO claim 1 , FeO claim 1 , FeOOH claim 1 , NiO claim 1 , SnO claim 1 , VO claim 1 , VO claim 1 , ZrO claim 1 , ZnO claim 1 , ...

Preparation method of carbon modified filler

A preparation method of carbon modified filler is provided. The method is: putting the fillers into the reaction zone of a reactor, starting the first heating-up to 400-500° C. under the protective atmosphere at first, then introducing hydrogen after the heating-up; starting the second heating-up to 600-1200° C. after introducing hydrogen and simultaneously introducing the mixture of hydrogen and carbon source gas, keeping at the terminal temperature for 0.1-5 hours, introducing nitrogen and stopping heating after the reaction, cooling, and then getting the carbon modified filler. The above method can obtain a friction material with good mechanical properties, excellent friction and wear performances, stable friction coefficient at high temperature, good braking force and no heat recession.

Weather-Resistant Pearlescent Pigments, Process for the Production and Use Thereof

The present invention relates to a weather-resistant pearlescent pigment which consists of a platelet-shaped substrate coated with one or more highly refractive metal oxides, the platelet-shaped substrate being selected from the group consisting of synthetic mica flakes, glass flakes, SiOflakes, AlOflakes, synthetic boehmite flakes, BiOCl flakes and mixtures thereof, and a top layer, wherein the top layer consists of the following layers: a) a cerium-containing layer, selected from the group consisting of cerium oxide, cerium hydroxide, hydrated cerium oxide, and mixtures thereof, the cerium-containing layer being applied directly to the highly refractive metal oxide layer, and b) an organic-chemical compatibilizing layer, which comprises the reaction products of oligomeric silanes, wherein the oligomeric silanes have one or more amino groups, the organic-chemical compatibilizing layer being applied directly to the cerium-containing layer a). 1. A weather-resistant pearlescent pigment which consists of a platelet-shaped substrate coated with one or more highly refractive metal oxides , the platelet-shaped substrate being selected from the group consisting of synthetic mica flakes , glass flakes , SiOflakes , AlOflakes , synthetic boehmite flakes , BiOCl flakes and mixtures thereof , and a top layer , wherein the top layer consists of the following layers:a) a cerium-containing layer selected from the group consisting of cerium oxide, cerium hydroxide, hydrated cerium oxide and mixtures thereof, the cerium-containing layer being applied directly to the highly refractive metal oxide layer, andb) an organic-chemical compatibilizing layer, which comprises the reaction product(s) of oligomeric silanes, wherein the oligomeric silanes have one or more amino groups, the organic-chemical compatibilizing layer being applied directly to the cerium-containing layer a).2. The weather-resistant pearlescent pigment according to claim 1 , wherein the platelet-shaped synthetic ...

METAL SILICATE NANOSHEETS, METHODS OF MAKING METAL SILICATE NANOSHEETS, AND METHODS OF USE

Embodiments of the present disclosure relate to the preparation of colloidal dispersions or suspensions of inorganic materials with nano-sized and nano-structured morphologies, preferably the nanosheet form, compositions produced by this method, and the like. 1. A composition , comprising:a metal silicate material having the dimensions of a nanosheet that is 1 to 10 monolayers thick and has one or two lateral dimensions of about 100 nm to 100 μm.2. The composition of claim 1 , wherein one layer of the metal silicate material has a thickness of about 1 to 3 nm.3. The composition of claim 1 , wherein the metal silicate pigment is selected from the group consisting of: an alkaline earth copper silicate and a gillespite-type series silicate.4. The composition of claim 3 , wherein the alkaline earth copper silicate is selected from the group consisting of: CaCuSiO claim 3 , SrCuSiO claim 3 , BaCuSiO claim 3 , and BaCuSiO.5. The composition of claim 3 , wherein the gillespite-type series silicate is defined by ABSiO claim 3 , wherein A is selected from Ca claim 3 , Ba claim 3 , and Sr claim 3 , and wherein B is selected from Cr and Fe.6. The composition of claim 1 , wherein the metal silicate material has the following formula: ACBDSiO claim 1 , where A=Ca claim 1 , Sr claim 1 , Ba; C=Zn claim 1 , Ti claim 1 , lanthanide element; 0≦x≦1; B=Cu claim 1 , Cr claim 1 , Fe; D=alkali metal; and 0≦y≦1.7. A method of making a metal silicate pigment claim 1 , comprising:delaminating bulk metal silicate to form a metal silicate material; andexfoliating the metal silicate material to form a metal silicate pigment having the dimensions of a nanosheet that is 1 to 10 monolayers thick and has one or two lateral dimensions of about 100 nm to 100 μm.8. The method of claim 7 , wherein delaminating includes mixing the bulk metal silicate with water at about 60 to 100° C. for about 1 to 10 days.9. The method of claim 7 , wherein exfoliating includes sonicating the metal silicate material in ...

AQUEOUS CORROSION RESISTANT COATINGS WITH SURFACE-HYDROPHOBIC INORGANIC PARTICLES

Aqueous coating compositions providing enhanced anticorrosive and water-resistant properties. The anticorrosive coating comprises water borne resin, surface-hydrophobic inorganic pigments, and/or surface-hydrophobic inorganic extenders. 1. A corrosion resistant coating comprising:a. a water borne resin;b. water; andc. one or more particles selected from the group comprising an inorganic particle, extender, and combination thereof; wherein the one or more particle comprises a hydrophobic coating selected from the group consisting of polyols, organosiloxanes, organosilanes, alkylcarboxylic acids, alkylsulfonates, organophosphates, organophosphonates, fluoropolymers and mixtures thereof.2. A corrosion resistant coating comprising:a. water borne resin;b. water;c. one or more particles selected from the group comprising an inorganic particle, extender, and combination thereof; wherein the one or more particle comprises a hydrophobic coating selected from the group consisting of polyols, organosiloxanes, organosilanes, alkylcarboxylic acids, alkylsulfonates, organophosphates, organophosphonates, fluoropolymers and mixtures thereof; andd. at least one solvent.3. The corrosion resistant coating of wherein the hydrophobic coating reduces corrosion and water penetration ability.4. The corrosion resistant coating of wherein the hydrophobic coating reduces corrosion and water penetration ability.5. The corrosion resistant coating of wherein the at least one solvent comprise a solvent having an octanol-water partition coefficient of 1 to 5.6. The corrosion resistant coating of wherein the at least one solvent is selected from the group consisting of ketones claim 2 , alcohols claim 2 , esters and ethers of alcohols claim 2 , aromatics claim 2 , glycol ethers and esters.7. The corrosion resistant coating of wherein the at least one solvent is selected from the group consisting of propylene glycol n-butyl ether claim 2 , dipropylene glycol n-butyl ether claim 2 , tripropylene ...

Iron Oxide-Coated Layered Silicate Pigment

The present invention provides an iron oxide-coated layered silicate pigment that has no interference color, strongly exhibits the color inherent in iron oxide, and is excellent in gloss. The pigment of the present invention is an iron oxide-coated layered silicate pigment comprising a layered-silicate plate particle as base, and an iron oxide coated on the plate particle; wherein the iron oxide does not coat the surface portion of the plate particle or the iron oxide is localized on the edge portion rather than the surface portion of the plate particle. As the iron oxide, at least one kind selected from black iron oxide (FeO) and red iron oxide (FeO) can be used preferably. As the layered silicate, a mica-group layered silicate can be used preferably. The iron oxide-coated layered silicate pigment of the present invention can be incorporated into cosmetic preferably. 114-. (canceled)15. An iron oxide-coated layered silicate pigment comprising: a layered-silicate plate particle as base , and an iron oxide coated on the plate particle;wherein the iron oxide does not coat the surface portion of the plate particle or the iron oxide thickness of the edge portion, which is the thickness of iron oxide coating layer parallel to the direction of the face of the base plate particle, is 1.5 times or more of the iron oxide thickness of the surface portion, which is the thickness of iron oxide coating layer parallel to the direction of the thickness of the base plate particle16. The iron oxide-coated layered silicate pigment of claim 15 , wherein the entire edge portion of the base plate particle is coated with the iron oxide.17. The iron oxide-coated layered silicate pigment of claim 15 , wherein the surface portion of the base plate particle is not coated with the iron oxide.18. The iron oxide-coated layered silicate pigment of claim 15 , wherein the part of the surface portion of the base plate particle is coated with the iron oxide.19. The iron oxide-coated layered silicate ...

Semiconductor particles, dispersion, film, optical filter, building member, and radiant cooling device

Provided are semiconductor particles including a Group 12-16 semiconductor including a Group 12 element and a Group 16 element, a Group 13-15 semiconductor including a Group 13 element and a Group 15 element, or a Group 14 semiconductor including a Group 14 element, the semiconductor particles having a plasma frequency of 1.7×1014 rad/s to 4.7×1014 rad/s and a maximum length of 1 nm to 2,000 nm; and a dispersion, a film, an optical filter, a building member, or a radiant cooling device, in all of which the semiconductor particles are used.

SUPERHYDROPHOBIC COATING AND PROCESS OF MAKING SAME

An improved superhydrophobic coating and a process of making it is provided herein. More particularly, a robust superhydrophobic coating is produced by using carbon dioxide to enhance the integration of a binder material into the superhydrophobic coating. The carbon dioxide may be used to infiltrate and fill the interstitial voids of a superhydrophobic material, such as diatomaceous earth. Consequently, occupying these voids in the superhydrophobic material effectively blocks other components (e.g., binders) from entering the voids. As a result, the coating formulations of the present invention are more robust and may strongly adhere to the substrates to which they are applied. 1. A process for enhancing integration of a binder material in a hydrophobic coating , the process comprising:placing diatomaceous earth into a vessel;introducing carbon dioxide into the vessel to at least partially infiltrate interstitial voids of the diatomaceous earth;adding a binder material to the vessel; andmixing the diatomaceous earth, the carbon dioxide, and the binder material to form the hydrophobic coating.2520. The process of claim 1 , wherein the hydrophobic coating comprises to weight percent of the binder material based on the total weight of the hydrophobic coating.3. The process of claim 1 , wherein the carbon dioxide comprises supercritical carbon dioxide.4. The process of claim 1 , wherein the diatomaceous earth comprises a superhydrophobic diatomaceous earth.5. The process of claim 1 , further comprising applying the hydrophobic coating onto a substrate to thereby form a coated substrate.6. The process of claim 1 , wherein the applying comprises spraying the hydrophobic coating onto the substrate claim 1 , wherein residual carbon dioxide in the vessel is used as a propellant for the spraying.7. A superhydrophobic coating claim 1 , the superhydrophobic coating comprising:(a) a superhydrophobic diatomaceous earth;(b) carbon dioxide; and(c) at least one binder.8. The ...

METHOD FOR MAKING FUNCTIONALIZED SILICA FOR RUBBER MASTERBATCH

A method for blending functionalized silica with styrene butadiene rubber or ethylene propylene diene monomer rubber can include silica and an organosilane chemically and covalently bound to a surface of the silica. The organosilane can be derived from an organic silane with a functional group. A silica rubber masterbatch for complexing with an emulsion styrene butadiene rubber latex, a synthetic polymer, a natural polymer, or combinations thereof can include the functionalized silica with the organosilane or a blend of organosilanes chemically and covalently bound to a surface of the silica. Each organosilane can have an average tetrameric structure having a T/Tratio of 0.3 to 0.9 or greater as measured by Si silicon cross polarization magic angle spinning nuclear magnetic resonance. 2. The method of claim 1 , wherein the functionalized silica comprises an organosilane attached to a surface of the silica.3. The method of claim 1 , wherein the silica has a specific surface area ranging from 100 m2/gm to 300 m2/gm claim 1 , as measured by the Brunauer-Emmett-Teller analysis.4. The method of claim 1 , wherein the silica is a fumed silica or a precipitated silica.5. The method of claim 1 , wherein X is a vinyl group and Y is an integer greater than zero.6. The method of claim 1 , wherein the Z1 claim 1 , Z2 claim 1 , and the Z3 are each independently selected from the following: a hydrogen claim 1 , a C1-C18 alkyl claim 1 , an aryl claim 1 , a cycloalkyl claim 1 , an aryl alkoxy claim 1 , and a halo-substituted alkyl claim 1 , and at least one of Z1 claim 1 , Z2 claim 1 , and the Z3 is an alkoxy claim 1 , a hydrogen claim 1 , a halogen claim 1 , or a hydroxyl.7. The method of claim 1 , comprising simultaneously adding a third silane coupling agent while the first and second silane coupling agents are added to the silica.8. The method of claim 7 , wherein the third silane coupling agent is an ethanol free silane.9. The method of claim 1 , wherein the first and second ...

Process to Co-Mill Waste Fiberglass With Post-Consumer Glass Into Powder

A method of making an alkali glass powder includes obtaining down chute waste fiberglass (DCWF) and post-consumer waste glass (PCWG), processing the DCWF into a DCWF particulate form, combining the DCWF and PCWG at a ratio of PCWG to DCWF, and co-grinding the combined DCWF particulate form and the PCWG into a DCWF-PCWG powder having an alkali content based on the ratio of PCWG to DCWF. 1. A method of making an alkali powder , the method comprising:providing clean and dry down chute waste fiberglass (DCWF) and clean and dry post-consumer waste glass (PCWG);processing the DCWF into particulate DCWF;providing the particulate DCWF and PCWG at a ratio of PCWG to DCWF; andco-grinding the combined particulate DCWF and the PCWG into a DCWF-PCWG powder having an alkali content based on the ratio.2. The method according to claim 1 , wherein:the DCWF includes at least one of loose strands of fiberglass and mats of stranded fiberglass.3. The method according to claim 1 , wherein:processing the DCWF includes at least one of cutting the DCWF into smaller strands and grinding the smaller strands into the particulate DCWF.4. The method according to claim 3 , wherein:cutting the DCWF into smaller strands includes cutting the DCWF strands into pieces of 55 microns to 6 inch long, and grinding the smaller strands into DCWF powder includes grinding the smaller strands into the particulate DCWF having a particle size not exceeding 20 mesh.5. The method according to claim 4 , wherein:cutting the DCWF includes (1) first cutting the DCWF along a first direction, and second cutting the DCWF along a second direction transverse to the first direction or (2) cutting the DCWF with a rotary blade cutter.6. The method according to claim 1 , wherein:providing PCWG includes obtaining PCWG having a particle size of less than 1.25 inch.7. The method according to claim 1 , further comprising:separating DCWF-PCWG powder having a particle size above a first threshold size from DCWF-PCWG powder particles ...

SILICON NANOPARTICLES AND METHODS FOR PREPARING SILICON NANOPARTICLES

Silicon nanoparticles and methods for preparation of silicon nanoparticles are provided. Embodiments include a method for grinding silicon. Methods include providing silicon material, providing a grinding liquid including a polar solvent, and grinding the silicon material in the presence of the grinding liquid to yield silicon nanoparticles. Grinding the silicon in the presence of the grinding liquid can chemically functionalize the silicon material as the nanoparticles are formed to provide stable chemically functionalized nanoparticles. 1. A composition comprising:silicon particles having a diameter of less than 200 nm, wherein a surface of the silicon particles includes bonded functional groups; anda porous three-dimensional network, wherein the silicon particles are dispersed throughout the porous three-dimensional network.2. The composition of claim 1 , wherein the porous three-dimensional network is a sol-gel solution.3. The composition of claim 2 , wherein the sol-gel solution comprises an aerogel precursor.4. The composition of claim 2 , wherein the sol-gel solution comprises a polyimide precursor.5. The composition according to claim 1 , wherein the porous three-dimensional network comprises an aerogel.6. The composition according to claim 1 , wherein the porous three-dimensional network comprises a carbon aerogel.7. The composition according to claim 1 , wherein the porous three-dimensional network comprises a polyimide-derived carbon aerogel.8. The composition according to claim 1 , wherein the functional groups on the surface of the silicon particles are bonded to carbon atoms within the porous three-dimensional network.9. The composition according to claim 1 , wherein the functional groups include at least one of —OH claim 1 , —COOH claim 1 , —C—O—C— claim 1 , —NH claim 1 , —NHR claim 1 , or combinations thereof.10. (canceled)11. The composition according to claim 1 , wherein the bonded functional groups is selected from the group consisting of ...

FILLER PIGMENTS

Filler pigments based on platelet-shaped substrates, which are coated with barium sulfate and at least two metal oxides and/or metal hydroxides are highly suitable as filler pigments especially for cosmetic formulations. 1. A filler pigment comprising a platelet-shaped substrate coated with barium sulfate and at least two metal oxides and/or metal hydroxides of the following layer structure:{'sub': 2', '2', '4, 'substrate+SnO+TiO+BaSO'}{'sub': 2', '2', '4, 'substrate+mixture of SnO+TiO+BaSO'}{'sub': 2', '2', '4', '2, 'substrate+mixture of SnO+TiO+BaSO+layer of SiOon top'}{'sub': 2', '2', '4, 'substrate+SiO+TiO+BaSO'}{'sub': 2', '2', '4, 'substrate+SiO+SnO+BaSO'}{'sub': 2', '2', '4, 'substrate+SnO+TiO+BaSO+Carmine red'}{'sub': 2', '2', '4, 'substrate+SnO+TiO+BaSO+Prussian Blue'}{'sub': 2', '4', '2, 'substrate+SnO+BaSO/TiO'}{'sub': 2', '2', '4', '2, 'substrate+SnO+TiO+BaSO+SiO'}{'sub': 4', '2', '2', '2, 'substrate+BaSO+SnO+TiO+SiO'}{'sub': 2', '3', '4', '2', '2, 'substrate+AlO+BaSO+SnO+SiO'}{'sub': 2', '3', '4', '2, 'substrate+ZnO+AlO+BaSO+SiO'}{'sub': 2', '3', '4', '2, 'substrate+AlO+BaSO+SnOor'}{'sub': 2', '3', '4, 'substrate+ZnO+AlO+BaSO.'}2. A filler pigment according to claim 1 , wherein the substrate is natural or synthetic mica claim 1 , doped or undoped AlOflakes claim 1 , doped or undoped SiOflakes claim 1 , talc claim 1 , kaolin claim 1 , or doped or undoped glass flakes or mixtures thereof.3. (canceled)4. The filler pigment according to claim 1 , wherein the substrate has an aspect ratio of 2 to 2000.5. The filler pigment according to claim 1 , containing an amount of barium sulfate of 5-200 wt.-% based on the substrate.6. (canceled)7. The filler pigment according to claim 1 , surface coated with a layer of SiO.8. (canceled)9. A process for the production of a filler pigment of claim 1 , comprising suspending the substrate in an aqueous solution claim 1 , adding the barium salt and at least two metal salt solutions at a pH which is suitable for hydrolysis ...

COMPOSITE PARTICLES INCLUDING A FLUOROPOLYMER, METHODS OF MAKING, AND ARTICLES INCLUDING THE SAME

A composite particle includes a discrete, hollow, ceramic spheroid and a fluoropolymer layer disposed thereon. The fluoropolymer is a homopolymer or copolymer of a perfluoroalkyl vinyl ether; a perfluoroalkoxy vinyl ether; at least one fluoroolefin independently represented by formula C(R)═CF—Rf, wherein Rf is fluorine or a perfluoroalkyl having from 1 to 8 carbon atoms and R is hydrogen, fluorine, or chlorine; or a combination thereof. Methods of making the composite particles, composite materials, and articles including them are also disclosed. 2. The composite particle of claim 1 , wherein the fluoropolymer is a copolymer of vinylidene fluoride and hexafluorpropylene; a copolymer of vinylidene fluoride claim 1 , hexafluorpropylene claim 1 , and tetrafluoroethylene; a copolymer of vinylidene fluoride claim 1 , hexafluorpropylene claim 1 , tetrafluoroethylene claim 1 , and perfluoromethylvinyl ether; a copolymer of vinylidene fluoride claim 1 , propylene claim 1 , and tetrafluoroethylene; a copolymer of vinylidene fluoride claim 1 , hexafluorpropylene claim 1 , tetrafluoroethylene claim 1 , perfluoromethylvinyl ether claim 1 , and ethylene; a copolymer of ethylene and tetrafluoroethylene; a copolymer of tetrafluoroethylene and hexafluoropropylene; or poly(vinylidene fluoride).3. The composite particle of claim 1 , wherein the fluoropolymer is a copolymer of vinylidene fluoride and hexafluorpropylene or a copolymer of vinylidene fluoride claim 1 , hexafluorpropylene claim 1 , and tetrafluoroethylene.4. The composite particle of claim 1 , wherein the fluoropolymer is not a homopolymer of tetrafluoroethylene.5. The composite particle of claim 1 , wherein the composite particle comprises at least 75 percent by weight of ceramic claim 1 , based on the total weight of the composite particle.6. The composite particle of claim 1 , wherein the composite particle comprises up to 25 percent by weight of the fluoropolymer claim 1 , based on the total weight of the composite ...

Method for manufacturing gas separation membrane

A method for producing a gas separation membrane, including the following steps: step(a): treating the surfaces of silica nanoparticles dispersed in a first solvent with a reactive functional group-containing compound, while nanoparticles are being dispersed in the solvent, to thereby prepare a first solvent dispersion of reactive functional group-modified silica nanoparticles; step(b): replacing the first solvent dispersion's dispersion medium of reactive functional group-modified silica nanoparticles prepared in step(a) with a second solvent without drying of dispersion medium, and then reacting functional group-modified silica nanoparticles with dendrimer-forming monomer or hyperbranched polymer-forming monomer in the second solvent's presence so that dendrimer or hyperbranched polymer is added to reactive functional group, to thereby prepare dendrimer- or hyperbranched polymer-bound silica nanoparticles; step(c): mixing dendrimer- or hyperbranched polymer-bound silica nanoparticles prepared in step(b) with a matrix resin; and step (d): applying mixture prepared in step(c) to a substrate, and then removing the solvent.

METHODS OF PRODUCING FUNCTIONALIZED POWDER PARTICLES

The present disclosure provides functionalized powder particles and methods of forming functionalized powder particles. The functionalization is acquired through the formation of primary and/or secondary structures on a powder particle. Functionalization can be controlled to bring about changes in a broad range of physical and/or chemical properties. 1128-. (canceled)129. A method of lysing a cell , the method comprising:(a) providing one or more crystalline, polycrystalline, semi-crystalline, or amorphous semiconductor or insulator powder particle having a diameter between 1 and 1,000 microns;(b) forming, on the one or more powder particle, a type of structure selected from the group consisting of pores, pits, craters, nanowires, cones, pinnacles, hoodoos, coral, cords, walls, fins, ridges, crags, pyramids, and inverted pyramids, thereby forming one or more functionalized powder particle, and(c) contacting a cell with said one or more functionalized powder particle, thereby lysing the cell.130. The method of claim 129 , wherein the type of structure is a submillistructure.131. The method of claim 129 , wherein the one or more powder particle provided in (a) is one or more crystalline or polycrystalline powder particle.132. The method of claim 129 , wherein said type of structure is selected from the group consisting of pinnacles claim 129 , hoodoos claim 129 , coral claim 129 , cords claim 129 , walls claim 129 , fins claim 129 , ridges claim 129 , crags claim 129 , and inverted pyramids.133. The method of claim 129 , wherein the one or more functionalized powder particle is an elemental or compound crystalline or polycrystalline semiconductor powder particle selected from group IVA elements claim 129 , groups IV-VI compounds claim 129 , groups II-IVB compounds claim 129 , groups I-VII compounds claim 129 , groups II-VI compounds claim 129 , groups III-V compounds claim 129 , groups IV-IV compounds claim 129 , transition metal oxides claim 129 , and compounds ...

Glass Composites for Tissue Augmentation, Biomedical and Cosmetic Applications

Compositions and methods for glass composites suitable for tissue augmentation, biomedical, and cosmetic applications are provided. The glass microsphere component of the composites are biologically inert, non-reactive and act as a nearly permanent tissue filler. One embodiment provides a tissue augmentation composite containing an effective amount of solid glass microspheres, hollow glass microspheres, porous wall hollow glass microspheres, or combinations thereof with a suitable biocompatible matrix to serve as a bulking agent when injected into a patient. The compositions can be used for soft or hard tissue augmentation as well as delivery of cargos on demand. 1. A composite material comprising:(a) 50% vol/vol or greater of long lasting silica-based glass microspheres, wherein the silica-based glass microspheres are selected from the group consisting of hollow glass microspheres, porous wall hollow glass microspheres, or a combination thereof; and(b) a biocompatible matrix,wherein the silica-based glass microspheres flow readily, and induce little or no inflammatory response when administered to the subject.2. (canceled)3. The composite material of claim 1 , wherein the glass microsphere components have a diameter of 10 mm to 100 μm.4. The composite material of claim 1 , where the matrix component comprises a gelling agent.5. The composite material of claim 1 , wherein the microsphere components are coated with a coating agent to provide controlled release of a substance loaded into the microspheres.6. The composite material of claim 1 , wherein the microsphere components are gated with a gating agent to provide controlled release of a substance loaded in the microspheres.7. The composite material of claim 6 , wherein the gating agent is a polymer.8. The composite material of claim 6 , wherein the gating agent is selected from the group consisting of dextran claim 6 , colloidal starch claim 6 , polymerized fibrin claim 6 , and a polyvinylpyrrolidone.9. The ...

FUNCTIONALIZED SILICON

The process of bi-functionalizing silicon nanoparticles and bi-functionalized silicon nanoparticles are described. The processes include applying shear forces to silicon metal in the presence of an alkane, thereby providing an alkyl-hydride-functionalized silicon nanoparticle, which is then treated with a reactant, e.g., a compound that reacts with the hydride functionality, to provide the bi-functionalized silicon nanoparticles. The resulting product can include a plurality of functionalities on a silicon nanoparticle derived from alkenes, alkynes, aldehydes, alcohols, thiols, amines, carboxylates, and/or carboxylic acids. 1. A process comprising:admixing a hydride-functionalized silicon nanoparticle with a reagent, the hydride-functionalized silicon nanoparticle having silicon-hydride features on a silicon surface;wherein the reagent reacts adds to the silicon surface.2. The process of claim 1 , wherein the hydride-functionalized silicon nanoparticle is an alky-hydride-functionalized silicon nanoparticle having hydride and alkyl surface features derived from an alkane.3. The process of claim 1 , wherein the hydride-functionalized silicon nanoparticle is an alky-hydride-functionalized silicon nanoparticle;the alky-hydride-functionalized silicon nanoparticle includes a silicon nanoparticulate having a composition of silicon or a silicon alloy, and having a plurality of surfaces, each surface comprising silicon atoms covalently affixed to hydride and alkyl or heteroalkyl functionalities derived from an alkane or heteroalkane.4. The process of claim 1 , wherein the reagent covalently binds to the silicon surface.5. The process of claim 1 , wherein the reagent is selected from an alkene claim 1 , an alkyne claim 1 , an aldehyde claim 1 , and a mixture thereof.6. The process of claim 5 , wherein the addition of the alkene yields an alkyl-functionality on the silicon nanoparticle.7. The process of claim 5 , wherein the addition of the alkyne yields an alkenyl- ...

Method for preparing a composition comprising functionalised silico/germano-metal particles and composition obtained

A method for preparing a composition includes silico/germano-metal particles functionalized by at least one organic group, which involves:—carrying out a hydrothermal treatment of a hydrogel precursor of the silico/germano-metal mineral particles, and—preparing a hydrogel including silico/germano-metal particles having at least one organic group by co-precipitation in an aqueous medium. A composition including functionalized silico/germano-metal mineral particles of which 1% to 75% of the silicon atoms and/or of the germanium atoms are covalently bonded to at least one organic group is also described.

INTERFERENCE PIGMENT, AND COSMETIC PREPARATION, COATING MATERIAL, INK, AND RESIN COMPOSITION EACH CONTAINING SAME

The present invention provides an interference pigment that develops interference colors even on light-colored bases. An interference pigment of the present invention includes: a flaky inorganic substrate a transparent metal layer that coats the inorganic substrate and a metal oxide layer that coats the metal layer 1. An interference pigment comprising:a flaky inorganic substrate;a transparent metal layer that coats the inorganic substrate; anda metal oxide layer that coats the metal layer.2. The interference pigment according to claim 1 , wherein claim 1 , when the metal oxide layer is referred to as a first metal oxide layer claim 1 , the interference pigment further comprises a second metal oxide layer that is formed between the inorganic substrate and the metal layer and that coats the inorganic substrate.3. The interference pigment according to claim 1 , wherein the inorganic substrate comprises at least one material selected from the group consisting of glass claim 1 , mica claim 1 , silica claim 1 , and alumina.4. The interference pigment according to claim 3 , wherein the material of the inorganic substrate is glass.5. The interference pigment according to claim 1 , wherein a metal in the metal layer is one kind metal or a metal alloy.6. The interference pigment according to claim 5 , wherein the metal is at least one selected from the group consisting of silver claim 5 , gold claim 5 , platinum claim 5 , and palladium.7. The interference pigment according to claim 5 , wherein the metal is at least one selected from the group consisting of silver and gold.8. The interference pigment according to claim 1 , wherein the metal layer has an average thickness of 5 nm or less.9. The interference pigment according to claim 1 , wherein the metal layer has an average thickness of 2 nm or less.10. The interference pigment according to claim 1 , wherein claim 1 , when the metal oxide layer that coats the metal layer is referred to as a first metal oxide layer claim 1 , ...

METHOD FOR PREPARING ORGANIC-INORGANIC HYBRID POROUS INSULATION COATING COMPOSITION

A method for preparing an organic-inorganic hybrid porous insulation coating composition includes steps of: adding sepiolite nanoparticles that have been surface-treated with silane or dimethyl ammonium chloride to a thermal-resistant resin solution; and stirring the thermal-resistant resolution solution containing the sepiolite nanoparticles at 3600 rpm or more for 30 minutes or more. The thermal-resistant resin solution includes at least one thermal-resistant resin selected from the group consisting of polyamide-imide, polyester, polyester-imide and polyamic acid. 1. A method for preparing an organic-inorganic hybrid porous insulation coating composition comprising steps of:adding sepiolite nanoparticles that have been surface-treated with silane or dimethyl ammonium chloride to a thermal-resistant resin solution; andstirring the thermal-resistant resolution solution containing the sepiolite nanoparticles at 3600 rpm or more for 30 minutes or more,wherein the thermal-resistant resin solution includes at least one thermal-resistant resin selected from the group consisting of polyamide-imide, polyester, polyester-imide and polyamic acid.2. The method of claim 1 , wherein the sepiolite nanoparticles are added in a content of 0.1 to 5 wt % claim 1 , based on a total weight of a solid included in the solution.3. The method of claim 1 , wherein the sepiolite nanoparticle has a specific surface area of 230 to 380 m/g.4. The method of claim 1 , wherein the sepiolite nanoparticle has a size of 50 to 500 nm.5. The method of claim 1 , wherein the thermal-resistant resin solution includes the thermal-resistant resin in a content of 15 to 45 wt % claim 1 , based on a total weight of the thermal-resistant resin solution.6. The method of claim 1 , wherein the thermal-resistant resin solution includes at least one organic solvent selected from the group consisting of N-methylpyrrolidone (NMP) claim 1 , dimethyl formamide (DMF) claim 1 , dimethylacetamide (DMAc) claim 1 , ...

SILICA PARTICLES AND METHOD FOR PRODUCING THE SAME

Silica particles includes a nitrogen-containing compound. The ratio of the integral C of a signal observed at a chemical shift of −50 ppm or more and −75 ppm or less in a Si solid-state nuclei magnetic resonance (NMR) spectrum of the silica particles, the Si solid-state NMR spectrum being obtained by cross polarization/magic angle spinning (CP/MAS), to the integral D of a signal observed at a chemical shift of −90 ppm or more and −120 ppm or less in the Si solid-state NMR spectrum, that is, C/D, is 0.10 or more and 0.75 or less. The amount X of the nitrogen-containing compound extracted from the silica particles with a mixed solution of ammonia and methanol is 0.1% by mass or more. The amount X of the nitrogen-containing compound extracted and the amount Y of the nitrogen-containing compound extracted from the silica particles with water satisfy Y/X<0.3. 1. Silica particles comprising:a nitrogen-containing compound,{'sup': 29', '29', '29, 'wherein a ratio of an integral C of a signal observed at a chemical shift of −50 ppm or more and −75 ppm or less in a Si solid-state nuclei magnetic resonance (NMR) spectrum of the silica particles, the Si solid-state NMR spectrum being obtained by cross polarization/magic angle spinning (CP/MAS), to an integral D of a signal observed at a chemical shift of −90 ppm or more and −120 ppm or less in the Si solid-state NMR spectrum, that is, C/D, is 0.10 or more and 0.75 or less, and'}wherein an amount X of the nitrogen-containing compound extracted from the silica particles with a mixed solution of ammonia and methanol is 0.1% by mass or more, and the amount X of the nitrogen-containing compound extracted and an amount Y of the nitrogen-containing compound extracted from the silica particles with water satisfy Y/X<0.3.2. The silica particles according to claim 1 ,the silica particles having a number average size of 10 nm or more and 200 nm or less.3. The silica particles according to claim 2 ,wherein the number average size is 10 nm ...

AQUEOUS CORROSION RESISTANT COATINGS WITH SURFACE-HYDROPHOBIC INORGANIC PARTICLES

Aqueous coating compositions providing enhanced anticorrosive and water-resistant properties. The anticorrosive coating comprises water borne resin, surface-hydrophobic inorganic pigments, and/or surface-hydrophobic inorganic extenders. 125.-. (canceled)26. A method of inhibiting corrosion of a substrate comprising the step of: i. a water borne resin;', 'ii. water;', 'iii. one or more particles selected from the group comprising an inorganic particle, extender, and combination thereof; wherein the one or more particle comprises a hydrophobic coating selected from the group consisting of polyols, organosiloxanes, organosilanes, alkylcarboxylic acids, alkylsulfonates, organophosphates, organophosphonates, fluoropolymers, and mixtures thereof;, 'a. providing a corrosion resistant coating comprisingb. applying the corrosion resistant coating to a surface of a substrate; andc. drying the corrosion resistant coating.27. A method of inhibiting corrosion of a substrate comprising the step of: i. a water borne resin;', 'ii. water;', 'iii. one or more particles selected from the group comprising an inorganic particle, extender, and combination thereof; wherein the one or more particle comprises a hydrophobic coating selected from the group consisting of polyols, organosiloxanes, organosilanes, alkylcarboxylic acids, alkylsulfonates, organophosphates, organophosphonates, fluoropolymers, and mixtures thereof;', 'iv. at least one solvent;, 'a. providing a corrosion resistant coating comprisingc. applying the corrosion resistant coating to a surface of a substrate; andd. drying the corrosion resistant coating.28. The method of inhibiting corrosion of claim 26 , wherein the substrate is metal.29. The method of inhibiting corrosion of claim 26 , wherein the substrate is steel.30. The method of inhibiting corrosion of claim 26 , wherein the substrate is concrete.31. The method of inhibiting corrosion of claim 26 , wherein the substrate is wood.32. The method of inhibiting corrosion ...

Process for manufacturing coated filler particles

The invention pertains to a process for manufacturing filler modified with functional particles in a high energy blending process through collisions of sufficient energy to bound, adhere, or otherwise associate the pigment particles to the filler.

METHODS OF MAKING HIGHLY PURIFIED DIATOMACEOUS EARTH WITH WIDE RANGE OF FILTRATION RATES

A highly purified diatomite composition may include greater than or equal to 90% silica, from about 0.5% to about 5% of a calcium-containing compound, and less than or equal to about 2% total of aluminum-containing oxides and iron-containing oxides. A method of making a highly purified diatomite composition may include providing a diatomite comprising at least 5% of a calcium-containing compound, calcining the diatomite, and acid washing the calcined diatomite. The calcined, acid-washed diatomite may include less than or equal to about 1% total of extractable aluminum-containing oxides and iron-containing oxides, and less than or equal to about 5% of the calcium-containing compound. The acid washing may include an acid selected from the group consisting of sulfuric acid (HSO), hydrochloric acid (HCl), and nitric acid (HNO). The method may not include a flotation step. 123-. (canceled)24. A method of making a highly purified diatomite composition , the method comprising:providing a diatomite comprising at least 5% of a calcium-containing compound;calcining the diatomite; andacid washing the diatomite,wherein the calcined, acid-washed diatomite comprises less than or equal to about 2% total of extractable aluminum-containing oxides and iron-containing oxides, and less than or equal to about 5% of the calcium-containing compound.25. The method of claim 24 , wherein the acid washing comprises washing the diatomite with at least one acid selected from the group consisting of sulfuric acid (HSO) claim 24 , hydrochloric acid (HCl) claim 24 , and nitric acid (HNO).26. The method of claim 24 , wherein the method does not include a flotation step.27. The method of claim 24 , wherein the calcining step occurs prior to the acid washing step.28. The method of claim 24 , wherein the acid washing step occurs prior to the calcining step.29. The method of claim 24 , wherein the calcined claim 24 , acid-washed diatomite comprises from about 1% to about 3% of the calcium-containing ...

BLACK CERAMIC ADDITIVES, PIGMENTS, AND FORMULATIONS

Ceramic black materials for use as, or in, colorants, inks, pigments, dyes, additives and formulations utilizing these black materials. Black ceramics having silicon, oxygen and carbon, and methods of making these ceramics; formulations utilizing these black ceramics; and devices, structures and apparatus that have or utilize these formulations. Plastics, paints, inks, coatings, formulations, liquids and adhesives containing ceramic black materials, preferably polymer derived black ceramic materials, and in particular polysilocarb polymer derived ceramic materials. 1. A coating formulation comprising: a first material and a second material; wherein the first material defines a first material weight percent of the coating formulation and the second material defines a second material weight percent of the coating formulation; wherein the second material is a black polymer derived ceramic material comprising silicon , oxygen and carbon having from about 30 weight % to about 60 weight % silicon , from about 5 weight % to about 40 weight % oxygen , and carbon; wherein about 20 weight % to about 80 weight % of the carbon is free carbon; and wherein the first material weight percent is larger than the second material weight percent.220-. (canceled)21. The coating formulation of claim 1 , wherein the first material comprises a system selected from the group of systems consisting of acrylics claim 1 , lacquers claim 1 , alkyds claim 1 , latex claim 1 , polyurethane claim 1 , phenolics claim 1 , epoxies and waterborne.22. The coating formulation of claim 1 , wherein the first material comprises a material selected from the group consisting of HDPE claim 1 , LDPE claim 1 , PP claim 1 , Acrylic claim 1 , Epoxy claim 1 , Linseed Oil claim 1 , PU claim 1 , PUR claim 1 , EPDM claim 1 , SBR claim 1 , PVC claim 1 , water based acrylic emulsions claim 1 , ABS claim 1 , SAN claim 1 , SEBS claim 1 , SBS claim 1 , PVDF claim 1 , PVDC claim 1 , PMMA claim 1 , PES claim 1 , PET claim 1 , ...

A METHOD OF INCREASING THE FILLER CONTENT IN PAPER OR PAPERBOARD

The invention relates to a method of making paper or paperboard comprising the steps of; a. providing a stock suspension; b. adding a mixture of alkali-metal silicate and precipitated calcium carbonate to said stock suspension; c. adding an acidic media to said stock suspension substantially directly before and/or after step (b) d. forming a web of the stock suspension obtained in step (d) e. drying said web. The addition of a mixture of alkali-metal silicate and PCC and of an acidic media to the stock suspension in accordance with the invention improves the bonding between the fibers and the filler (PCC), whereby problems related to dusting is decreased. Moreover, the method enables the addition of a higher amount of fillers to the paper without substantially affecting the strength. 1. A method of making paper or paper board comprising the steps of;a. providing a stock suspension;b. adding a mixture of alkali-metal silicate and precipitated calcium carbonate to said stock suspension;c. adding an acidic media to said stock suspension substantially directly before and/or after step b;d. forming a web of the stock suspension obtained in step (d); ande. drying said web2. The method according to claim 1 , wherein said alkali-metal silicate is sodium silicate and/or potassium silicate.3. The method according to claim 1 , wherein the acidic media is added to the stock suspension in step (c) substantially directly after step (b).4. The method according to claim 1 , wherein the acidic media comprises any one of mineral acids claim 1 , acidic metal salts and carbon dioxide.5. The method according to claim 4 , wherein the acidic media comprises an acidic salt.6. The method according to claim 1 , wherein cationic starch and/or cationic synthetic polymer is added to the stock suspension.7. The method according to claim 5 , wherein the acidic salt comprises ammonium sulfate claim 5 , aluminum sulfate claim 5 , polyaluminum nitrate claim 5 , polyaluminium chloride or combinations ...

FILLING MATERIAL, RESIN COMPOSITION, PACKAGE, LIGHT-EMITTING DEVICE, AND METHODS OF MANUFACTURING SAME

A filling material for a resin composition includes a base material and a coating material coating at least a portion of a surface of a particle of the base material. The base material comprises a first inorganic compound containing a Group II element. The coating material comprises a second inorganic compound containing the Group II element and is different from the first inorganic compound. A method of manufacturing the filling material is provided. A resin composition comprising the filling material, a package, a light-emitting device, and methods of manufacturing them are also provided. 1. A filling material comprising:a base material, wherein the base material comprises a first inorganic compound containing a Group II element, anda coating material coating at least a portion of a surface of a particle of the base material, wherein the coating material comprises a second inorganic compound containing the Group II element and is different from the first inorganic compound.2. The filling material of claim 1 , wherein the second inorganic compound is selected from the group consisting of a fluoride including the Group II element claim 1 , a phosphate including the Group II element claim 1 , and a sulfate including the Group II element.3. The filling material of claim 1 , wherein the base material and the coating material have an interface therebetween including at least a portion through which the base material and the coating material are continuously formed.4. The filling material of claim 1 , wherein the Group II element is Ca or Mg.5. The filling material of claim 1 , wherein the first inorganic compound is calcium silicate.6. The filling material of claim 1 , wherein the first inorganic compound is wollastonite.7. The filling material of claim 1 , wherein the base material is a fibrous material having an average fiber diameter of 0.1 μm to 15 μm claim 1 , an average fiber length of 1 μm to 100 μm claim 1 , and an average aspect ratio of 3 or more.8. The ...

SILANE-TREATED FORSTERITE FINE PARTICLES AND PRODUCTION METHOD THEREFOR, AND ORGANIC SOLVENT DISPERSION OF SILANE-TREATED FORSTERITE FINE PARTICLES AND PRODUCTION METHOD THEREFOR

The invention provides silane-treated forsterite microparticles having a specific surface area of 5 to 100 m/g, wherein 1 to 5 silyl groups are bound to 1 nmof the surface area thereof. 118-. (canceled)19. Silane-treated forsterite microparticles , the forsterite microparticles have a specific surface area of 5 to 100 m/g , and 1 to 5 silyl groups are bound to 1 nmof the surface area thereof.21. An organic solvent dispersion of silane-treated forsterite microparticles claim 19 , the dispersion comprises silane-treated forsterite microparticles as recited in claim 19 , and a dispersion medium containing an organic solvent.22. An organic solvent dispersion of silane-treated forsterite microparticles according to claim 21 , wherein the dispersion medium containing an organic solvent has a solubility parameter (SP) of 8 to 15.23. An organic solvent dispersion of silane-treated forsterite microparticles according to claim 21 , wherein the organic solvent is at least one member selected from the group consisting of methyl alcohol (SP=14.5) claim 21 , ethyl alcohol (SP=12.7) claim 21 , isopropyl alcohol (SP=11.5) claim 21 , dimethylformamide (SP=12.0) claim 21 , methylcellosolve (SP=11.4) claim 21 , ethylcellosolve (SP=9.9) claim 21 , butylcellosolve (SP=8.9) claim 21 , ethylene glycol (SP=14.6) claim 21 , propylene glycol monomethyl ether (SP=10.5) claim 21 , propylene glycol monomethyl ether acetate (SP=8.7) claim 21 , 1-pentanol (SP=11.0) claim 21 , methyl ethyl ketone (SP=9.3) claim 21 , methyl isobutyl ketone (SP=8.3) claim 21 , cyclohexanone (SP=9.8) claim 21 , ethyl acetate (SP=9.1) claim 21 , butyl acetate (SP=8.5) claim 21 , toluene (SP=8.9) claim 21 , methyl methacrylate (SP=9.9) claim 21 , pentaerythritol triacrylate (SP=10.0) claim 21 , dipentaerythritol hexaacrylate (SP=9.1) claim 21 , bisphenol A epoxy resin (SP=10.4) claim 21 , and bisphenol F epoxy resin (SP=10.8).24. An organic solvent dispersion of silane-treated forsterite microparticles according to ...

A Method for Forming a Titania-Coated Inorganic Particle

A method of forming a titania-coated inorganic particle comprising the steps of (a) stirring a mixture of a titania precursor such as a titanium alkoxide and an inorganic particle such as a hollow glass particles in an organic solvent such as an alcohol for more than 1 h to cause adsorption of the titania precursor on the surface of the inorganic particle; and (b) adding water dropwise to the mixture under stirring to convert the titania precursor to titania which then forms a coating on the inorganic particle. A method for forming a paint formulation, a titania-coated inorganic particle, a paint formulation comprising a titania-coated inorganic particle and use of a titania-coated inorganic particle in a paint formulation is also described. 123.-. (canceled)24. A method for forming a titania-coated inorganic particle comprising:a. stirring a mixture of a titania precursor and an inorganic particle in an organic solvent for a time period of more than 1 hour to cause adsorption of said titania precursor on the surface of said inorganic particle; andb. adding water to the mixture under stirring to convert said titania precursor to titania which then forms a coating on said inorganic particle.25. The method according to claim 24 , wherein in operation (a) claim 24 , said titania precursor and said inorganic particle are present at a ratio of titania precursor (molar) to inorganic particle (g) in the range from 8:1 to 18:1 (mmol/g).26. The method according to claim 24 , wherein in operation (b) claim 24 , said water and said titania precursor are present at a molar ratio of water to titania precursor in the range of 2:1 to 8:1.27. The method according to claim 24 , wherein said titania precursor is a titanium alkoxide.28. The method according to claim 27 , wherein said titanium alkoxide is a titanium C-alkoxide.29. The method according to claim 28 , wherein said titanium alkoxide is a C-alkoxide selected from the group consisting of titanium methoxide claim 28 , ...

Blends of microcrystalline and macrocrystalline talc for reinforcing polymers

A composition may include a first talc having a morphology index less than or equal to about 0.6 and a second talc having a morphology index greater than or equal to about 0.6. The first talc and the second talc may form a talc composition, and the talc composition may have a content ratio of the first talc to the second talc ranging from about 30:70 by weight to about 80:20 by weight. A polymer composition may include a polymer matrix and a filler composition. The filler composition may include a first talc having a morphology index less than or equal to about 0.8 and a second talc having a morphology index greater than or equal to about 0.8, The filler composition may have a content ratio of the first talc to the second talc ranging from about 30:70 by weight to about 80:20 by weight. The first talc may be a microcrystalline talc. The second talc may be a macrocrystalline talc.

MOLYBDENUM-SILICON CARBIDE COMPOSITE POWDER AND A FABRICATING METHOD THEREOF

Molybdenum-silicon carbide composite powder and a fabrication method thereof are provided. The molybdenum-silicon carbide composite powder includes a micro-scale silicon carbide powder and a plurality of submicron-scale molybdenum particles bonding on the surface of the silicon carbide powder.

DYE, FILLER MADE THEREFROM, COMPOSITIONS INCLUDING THE FILLER, AND METHOD OF DETERMINING DEGREE OF CURE OF SUCH COMPOSITIONS

A compound represented by formula: 2. The treated filler of claim 1 , wherein the inorganic filler comprises at least one of alumina claim 1 , tin oxides claim 1 , antimony oxides claim 1 , silica claim 1 , zirconia claim 1 , titania claim 1 , glass claim 1 , ceramics claim 1 , calcium carbonate claim 1 , or sodium metaborate.3. The treated filler of claim 1 , wherein the inorganic filler comprises at least one of calcium carbonate claim 1 , sodium metaborate claim 1 , or hollow glass elements.4. The treated filler of claim 1 , wherein W is a carboxylic acid group or —Si(Y)(Z) claim 1 , wherein x is 0 claim 1 , and wherein each Zis independently hydroxyl claim 1 , alkoxy claim 1 , —O— covalently bonded to the surface of the filler claim 1 , or —O bonded to another silicon atom to form a siloxane.5. The treated filler of claim 1 , wherein W is a sulfonic acid group claim 1 , a phosphonic acid group claim 1 , or carboxylic acid group.6. The treated filler of claim 1 , wherein X is alkylene that is optionally interrupted by at least one ether claim 1 , ester claim 1 , carbonate claim 1 , carbamate claim 1 , or arylene.7. The treated filler of claim 1 , wherein R is H.8. A composition comprising a curable polymeric resin and the treated filler of .9. The composition of claim 8 , further comprising a free radical initiator.10. The composition of claim 9 , wherein the free-radical initiator is an organic peroxide.11. The composition of claim 8 , wherein the curable polymeric resin is an unsaturated polyester resin.12. The composition or method of claim 8 , wherein the composition further comprises at least one of styrene monomer claim 8 , a substituted styrene monomer claim 8 , an acrylate monomer claim 8 , or a methacrylate monomer.13. A method for determining degree of cure of a curable polymeric resin claim 8 , the method comprising:{'claim-ref': {'@idref': 'CLM-00001', 'claim 1'}, 'providing a composition comprising a curable polymeric resin, a free-radical initiator, ...

HYDROPHILIZATION TREATMENT AGENT FOR ALUMINUM-CONTAINING METAL MATERIAL

Provided is a hydrophilization treatment agent for an aluminum-containing metal material, for forming a film that can provide excellent hydrophilicity and hydrophilic sustainability, as well as odor property to an aluminum-containing metal material for use in a heat exchanger or the like. 1. A hydrophilization treatment agent for an aluminum-containing metal material , the hydrophilization treatment agent containing: organic-inorganic composite particles obtained by combining one or more selected from water-soluble resins (A) having a hydroxyl group , one or more selected from poorly water-soluble inorganic oxides (B) , one or more selected from organoalkoxysilanes (C) , and a surfactant (D) such that (C)/{(B)+(D)} and (A)/{(B)+(C)+(D)} are respectively 0.001 to 1.0 and 0.1 to 5.0 in solid content ratio by weight; and water , wherein the organic-inorganic composite particles are 40 to 100 mass % based on total solid content by mass.2. The hydrophilization treatment agent according to claim 1 , wherein the water-soluble resins (A) having a hydroxyl group are constituents (a) claim 1 , which are polyvinyl alcohol and/or derivatives of polyvinyl alcohol claim 1 , with a saponification degree of 90 mol % or more.3. The hydrophilization treatment agent according to claim 1 , wherein the surfactant (D) has a surface tension of 15 to 65 mN/m (25° C. claim 1 , 0.1 mass % aqueous solution claim 1 , a wilhelmy method).4. The hydrophilization treatment agent according to claim 1 , wherein the surfactant (D) is a non-ionic surfactant.5. The hydrophilization treatment agent according to claim 1 , wherein a combination ratio of (D)/{(A)+(B)+(C)+(D)} is 0.0001 to 0.03 in solid content ratio by weight.6. The hydrophilization treatment agent according to claim 1 , wherein the combination ratio of (C)/{(B)+(D)} is 0.01 to 1.0 in solid content ratio by weight.7. The hydrophilization treatment agent according to claim 1 , wherein the water-soluble resins (A) having a hydroxyl group ...

GLITTER PIGMENT, PIGMENT-CONTAINING COMPOSITION, AND PIGMENT-CONTAINING PAINTED PRODUCT

The present invention provides a new glitter pigment suitable for providing high-brightness whitish reflected light. The glitter pigment according to the present invention includes: a flaky substrate and a silicon oxide layer and a titanium oxide layer formed in this order on the flaky substrate , wherein in the case where the flaky substrate is the glass flake, the glass flake has a thickness of 284 to 322 nm, the silicon oxide layer has a thickness of 89 to 109 nm, and the titanium oxide layer has a thickness of 51 to 86 nm. In the case where the flaky substrate is the alumina flake, the alumina flake has a thickness of 260 to 280 nm, the silicon oxide layer has a thickness of 79 to 102 nm, and the titanium oxide layer has a thickness of 47 to 87 nm. 18-. (canceled)9. A glitter pigment , comprising:a flaky substrate; anda silicon oxide layer and a titanium oxide layer formed in this order on the flaky substrate,whereinthe silicon oxide layer and the titanium oxide layer are formed on both a first principal surface and a second principal surface of the flaky substrate, the first principal surface and the second principal surface being opposite to each other,the titanium oxide layer, the silicon oxide layer, the flaky substrate, the silicon oxide layer, andthe titanium oxide layer which are arranged in this order along a thickness direction of the flaky substrate compose a five-layer optical interference system producing whitish reflected light,the flaky substrate is a glass flake,the glass flake has a thickness of 294 nm or more and 314 nm or less,the silicon oxide layer has a thickness of 92 nm or more and 102 nm or less,the titanium oxide layer has a thickness of 55.9 nm or more and 76 nm or less, andthe glitter pigment surrounded by air produces reflected light having absolute values of a* and b* that are each 20 or less and an L* value that is 72 or more as calculated by an optical simulation.10. The glitter pigment according to claim 9 , wherein the titanium ...

Method for preparing a composition comprising coloured silicate mineral particles and a composition comprising coloured silicate mineral particles

A method for preparing a composition including silicate mineral particles that have colouring properties in which a talcose composition, including phyllosilicate mineral particles chosen from the group formed: from the particles having the chemical formula: ((Si x Ge 1-x ) 4 M 3 O 10 (OH) 2 , the particles having at least one interlayer space and having the chemical formula: (Si x Ge 1-x ) 4 M 3-ε O 10 (OH) 2 , (M′ m+ ) ε′ .nH 2 O: —M having the formula Mg y(1) Co y(2) Zn y(3) Cu y(4) Mn y(5) Fe y(6) Ni y(7) Cry(8); —M′ m+ designating at least one interlayer cation, the silicate mineral particles having a thickness of less than 100 nm and of which the largest dimension is less than 10 μπι, is brought into contact with a dye solution, including dye cations, of at least one element chosen from the transition metals, the lanthanides and the actinides. The composition obtained by this method is also described.

METHOD FOR OBTAINING HIERARCHICALLY ORDERED INORGANIC PHOSPHATE STRUCTURES ON PHYLLOSILICATES

The present invention relates to a method for preparing hierarchically ordered structures of inorganic phosphate particles, homogeneously deposited on the surface of a phyllosilicate, which is characterized in that it comprises the following steps: a) obtaining an acid solution of precursor compounds of an inorganic phosphate; b) preparing a dispersion of particles of a phyllosilicate in aqueous medium and acidifying the phyllosilicate dispersion by adding at least one acid, thereby obtaining an acid dispersion; c) mixing the acid solution obtained in step a) with the dispersion obtained in step b); and d), with stirring, adding a base to the mixture obtained in step c) until the required pH value for precipitating the corresponding inorganic phosphate on the phyllosilicate particles has been achieved, resulting in a hierarchically ordered structure of homogeneously distributed submicrometric or nanometric inorganic phosphate particles supported on the phyllosilicate surface. 1. A method for preparing hierarchically ordered structures of inorganic phosphate particles , homogenously deposited on the surface of a phyllosilicate , wherein it comprises the following steps:a) obtaining an acid solution of precursor compounds of an inorganic phosphate,b) preparing a dispersion of particles of a phyllosilicate in aqueous medium and acidifying the phyllosilicate dispersion by adding at least one acid, thereby obtaining an acid dispersion,c) mixing the acid solution obtained in step a) with the dispersion obtained in step b)d) with stirring, adding a base to the mixture obtained in step c) until the pH value required for precipitating the corresponding inorganic phosphate on the phyllosilicate particles is achieved, resulting in a hierarchically ordered structure of homogenously distributed submicrometric or nanometric inorganic phosphate particles, supported on the phyllosilicate surface.2. The method according to claim 1 , wherein the acid solution of the precursor ...

FILLING MATERIAL, RESIN COMPOSITION, PACKAGE, AND LIGHT-EMITTING DEVICE

A filling material for a resin composition includes a base material and a coating material coating at least a portion of a surface of a particle of the base material. The base material comprises a first inorganic compound containing a Group II element. The coating material comprises a second inorganic compound containing the Group II element and is different from the first inorganic compound. A method of manufacturing the filling material is provided. A resin composition comprising the filling material, a package, a light-emitting device, and methods of manufacturing them are also provided. 1. A filling material comprising:a base material, wherein the base material comprises a first inorganic compound containing a Group II element, anda coating material coating at least a portion of a surface of a particle of the base material, wherein the coating material comprises a second inorganic compound containing the Group II element and is different from the first inorganic compound.2. The filling material of claim 1 , wherein the second inorganic compound is selected from the group consisting of a fluoride including the Group II element claim 1 , a phosphate including the Group II element claim 1 , and a sulfate including the Group II element.3. The filling material of claim 1 , wherein the base material and the coating material have an interface therebetween including at least a portion through which the base material and the coating material are continuously formed.4. The filling material of claim 1 , wherein the Group II element is Ca or Mg.5. The filling material of claim 1 , wherein the first inorganic compound is calcium silicate.6. The filling material of claim 1 , wherein the first inorganic compound is wollastonite.7. The filling material of claim 1 , wherein the base material is a fibrous material having an average fiber diameter of 0.1 μm to 15 μm claim 1 , an average fiber length of 1 μm to 100 μm claim 1 , and an average aspect ratio of 3 or more.8. The ...

Surface-modified inorganic substance, method for manufacturing surface-modified inorganic substance, method for modifying surface of inorganic substance with organic substance, heat dissipation material, thermally conductive material, and lubricant

The present invention provides a novel surface-modified inorganic substance obtained by modifying the surface of an inorganic nitride or an inorganic oxide with a boronic acid compound, and a heat dissipation material, a thermally conductive material, and a lubricant which use the surface-modified inorganic substance. The present invention also provides a method for manufacturing the surface-modified inorganic substance, and provides, as a novel method for modifying the surface of an inorganic substance selected from an inorganic oxide and an inorganic nitride with an organic substance, a method for modifying the surface of an inorganic nitride or an inorganic oxide with an organic substance that includes making a contact between the inorganic nitride or the inorganic oxide with a boronic acid compound.

Photoluminescent pigment; cosmetic, paint composition, and resin composition containing same; and bright pigment production method

A bright pigment of the present invention is a bright pigment including flaky particles and a metal oxide layer covering each surface of the flaky particles. The metal oxide layer has a thickness variation coefficient (standard deviation of thickness of the metal oxide layer/average thickness of the metal oxide layer) of 20% or less. The bright pigment preferably contains a sodium component, and the sodium component is Na 2 O. The content of Na 2 O in the flaky particles is 3% by mass or more and less than 9.5% by mass. The bright pigment preferably has a specific surface area of 5.0 m 2 /g or less.

Method, powder, film & lithium ion battery

Method for producing a powder of particles comprising a core region ( 26 ) and a shell region ( 28 ), said core region ( 26 ) comprising amorphous or microcrystalline Silicon and said core region ( 26 ) comprising a passivating material. The method comprises the steps of supplying a reactant gas ( 12 ) containing Silicon to a reaction chamber ( 16 ) of a reactor, and heating said reactant gas ( 12 ) to a temperature sufficient for thermal decomposition or reduction of the reactant gas ( 12 ) to take place inside the reaction chamber ( 16 ) to thereby produce nano- to micro-scale particles of amorphous or microcrystalline Silicon, and thereafter coating said particles with passivating material.

METHODS OF MAKING HIGHLY PURIFIED DIATOMACEOUS EARTH WITH WIDE RANGE OF FILTRATION RATES

A highly purified diatomite composition may include greater than or equal to 90% silica, from about 0.5% to about 5% of a calcium-containing compound, and less than or equal to about 2% total of aluminum-containing oxides and iron-containing oxides. A method of making a highly purified diatomite composition may include providing a diatomite comprising at least 5% of a calcium-containing compound, calcining the diatomite, and acid washing the calcined diatomite. The calcined, acid-washed diatomite may include less than or equal to about 1% total of extractable aluminum-containing oxides and iron-containing oxides, and less than or equal to about 5% of the calcium-containing compound. The acid washing may include an acid selected from the group consisting of sulfuric acid (HSO), hydrochloric acid (HCl), and nitric acid (HNO). The method may not include a flotation step. 1. A highly purified diatomite composition comprising:greater than or equal to 90% silica;from about 0.5% to about 5% of a calciurn-containing compound; andless than or equal to about 2% total of aluminum-containing oxides and iron-containing oxides.2. The diatomite composition of claim 1 , wherein the calcium-containing compound includes at least one of calcium oxide (CaO) and calcium carbonate (CaCO).3. The diatomite composition of claim 1 , wherein the diatomite composition comprises an acid-washed diatomite composition.4. The diatomite composition of claim 1 , wherein the diatomite composition comprises less than or equal to about 1% total of aluminum-containing oxides and iron-containing oxides.5. The diatomite composition of claim 1 , wherein the diatomite composition comprises from about 1% to about 2% of the calcium-containing compound.6. The diatomite composition of claim 1 , wherein the diatomite composition comprises greater than or equal to about 96% silica.7. The diatomite composition of claim 1 , wherein the diatomite composition comprises less than or equal to about 1 ppm acid-soluble ...

Coated silicon carbide particle powder

The present invention provides a means that can improve density and mechanical strength in a sintered body of a composition containing a sintering aid and a silicon carbide particle, and a molded article containing the sintered body. The present invention relates to a coated silicon carbide particle powder containing a silicon carbide particle, and a coating layer coating the silicon carbide particle, in which the coating layer contains an aluminum element, and the mass of the aluminum element per unit surface area of the silicon carbide particle is 0.5 mg/m 2 or more.

TALC PARTICULATE AND USES THEREOF

There is disclosed a talc particulate having a dof from about 0.5 to 5.0 μm and comprising less than about 500 ppm of particles having a particle size of equal to or greater than 45 μm and a shape factor equal to or greater than about 40. A process for making the talc particulate is also disclosed. The talc particulate may be used in polymer compositions as a filler from which polymer composites and articles may be formed. 1. A processed talc particulate having a dof from about 0.5 to 5.0 μm , having a shape factor equal to or greater than about 40 , and comprising less than about 500 ppm of particles having a particle size of equal to or greater than 45 μm.2. The talc particulate according to comprising less than about 250 ppm of particles having a particle size of equal to or greater than about 45 μm.3. The talc particulate according to having:a steepness of equal to or greater than about 30.0,a lamellarity index of from about 2.8 to about 45.0; ora shape factor equal to or greater than 70 and no greater than 150; anda d95 of from about 5.0 to about 15.0 μm.4. The talc particulate according to having a specific surface area (BET) of from about 10 m/g to about 20 m/g.5. The talc particulate according to which is surface treated with a surface treatment agent.6. A process for preparing a talc particulate having a dof from about 0.5 to 5.0 μm and a shape factor equal to or greater than 40 claim 4 , and comprising less than about 500 ppm of particles having a particle size of equal to or greater than 45 μm claim 4 , said process comprising:{'sub': 50', '95, '(a) delaminating a liquid suspension of a talc particulate having an initial particle size with a dof greater than about 5.0 μm and a dof at least about 20.0 μm to obtain a talc particulate having a particle size less than the initial particle size;'}{'sub': '95', '(b) treating the suspension to reduce or eliminate particles having a dof greater than about 15.0 μm; and'}{'sub': '50', '(c) at least partially drying ...

INORGANIC FILLER, INSULATION LAYER INCLUDING THE SAME, AND SUBSTRATE USING INSULATION LAYER

An inorganic filler including a closed pore having a content of 1 to 30 vol. %, an insulation layer including the same, and a substrate using the insulation layer. With the insulation layer using the inorganic filler prepared so as to include a closed pore corresponding to a change rate in volume, the closed pore may offset change in volume in the inorganic filler and release stress, thereby improving a coefficient of thermal expansion according to change in temperature of the insulation layer. 1. An inorganic filler comprising a closed pore having a content of 1 to 30 vol. %.2. The inorganic filler according to claim 1 , wherein an average particle size of the inorganic filler is 5 to 500 nm.3. The inorganic filler according to claim 1 , wherein the closed pore has a size of 0.2 to 20% based on the average particle size of the inorganic filler.4. The inorganic filler according to claim 1 , wherein the inorganic filler is at least one selected from a group consisting of SiO claim 1 , AlO claim 1 , ZrO claim 1 , ZnO claim 1 , BaO claim 1 , CaO claim 1 , MgO claim 1 , and SrO.5. The inorganic filler according to claim 1 , wherein the inorganic filler is surface-treated with a silane coupling agent.6. An insulation layer comprising the inorganic filler according to .7. The insulation layer according to claim 6 , wherein the inorganic filler is included in the insulation layer by 30 to 70 vol. %.8. A substrate comprising the insulation layer according to .9. The substrate according to claim 8 , wherein the insulation layer has a thickness of 20 μm or less. This application claims the benefit under 35 U.S.C. Section 119 of Korean Patent Application Serial No. 10-2013-0073014, entitled “Inorganic Filler, Insulation Layer Including the Same, and Substrate Using the Insulation Layer” filed on Jun. 25, 2013, which is hereby incorporated by reference in its entirety into this application.1. Technical Field The present invention relates to an inorganic filler, an insulation ...

Talc composition

An electrically conducting talc composition may include synthetic talc particulate coated with an electrically conducting coating agent, wherein the coating agent may include carbon nanotubes or an electrically conductive polymeric material, such as a nanocarbon material, such as, for example, carbon nanotubes. A method of making an electrically conducting talc composition may include forming electrically conducting coating agent on or about particles of the talc particle.

Color-Bleed Resistant Silica and Silicate Pigments and Methods of Making Same

Color-bleed resistant pigment particles containing an anionic dye, a quaternary ammonium compound, and a silica and/or silicate material having a negative zeta potential are disclosed. Related methods of making these colored pigment particles also are provided. 1. Colored pigment particles comprising:(i) a silica and/or silicate material having a negative zeta potential;(ii) an anionic dye; and(iii) a quaternary ammonium compound; wherein:a ratio of the quaternary ammonium compound to the silica and/or silicate material is in a range from about 1% to about 400% of the amount, by weight, of the quaternary ammonium compound sufficient to achieve a zero mV zeta potential of a 1 wt. % mixture of the dry silica and/or silicate material in deionized water; anda weight ratio of the anionic dye is in a range from about 0.01:1 to about 0.72:1, based on the weight of the quaternary ammonium compound.2. The pigment particles of claim 1 , wherein:the ratio of the quaternary ammonium compound to the silica and/or silicate material is in a range from about 50% to about 300% of the amount, by weight, of the quaternary ammonium compound sufficient to achieve a zero mV zeta potential of a 1 wt. % mixture of the dry silica and/or silicate material in deionized water; andthe weight ratio of the anionic dye is in a range from about 0.02:1 to about 0.24:1, based on the weight of the quaternary ammonium compound.3. The pigment particles of claim 1 , wherein:the colored pigment particles are characterized by a pH in a range from about 5 to about 9;the ratio of the quaternary ammonium compound to the silica and/or silicate material is in a range from about 75% to about 200% of the amount, by weight, of the quaternary ammonium compound sufficient to achieve a zero mV zeta potential of a 1 wt. % mixture of the dry silica and/or silicate material in deionized water; andthe weight ratio of the anionic dye is in a range from about 0.02:1 to about 0.18:1, based on the weight of the quaternary ...

High Temperature Boron Black Ceramic Additives, Pigments, and Formulations

High temperature boron-PDC (polymer derived ceramic) black materials for use as, or in, colorants, inks, pigments, dyes, additives and formulations utilizing these black materials. Boron-PDC materials having boron, silicon, oxygen and carbon, and methods of making these ceramics; formulations utilizing these black ceramics; and devices, structures and apparatus that have or utilize these formulations. Plastics, paints, inks, coatings, formulations, liquids and adhesives containing ceramic black materials, preferably polymer derived boron containing black ceramic materials, and in particular boron-SiOC derived ceramic materials. 1. A high temperature black ceramic pigment comprising:a. a ceramic matrix, the matrix consisting essentially of: silicon, oxygen, carbon and boron;b. wherein the ceramic pigment has a black color defining a degree of blackness;c. whereby when the pigment is exposed to a temperature of 1,000° F. for a period of 20 hours the degree of blackness does not change.2. The pigment of claim 1 , wherein the matrix is free from boric acid.3. The pigment of claim 1 , wherein the matrix is free from boron oxide.4. The pigment of claim 1 , wherein the matrix consists of silicon carbon oxygen and boron.5. A high temperature black ceramic pigment comprising:a. a ceramic matrix, the matrix comprising: silicon, oxygen, carbon and boron; and being free from boron oxide;b. wherein the ceramic pigment has a black color defining a degree of blackness;c. whereby when the pigment is exposed to a temperature of 1,000° F. for a period of 20 hours the degree of blackness does not change.6. A high temperature black ceramic pigment comprising:a. a ceramic matrix, the matrix comprising: silicon, oxygen, carbon and boron; and being free from boric acid;b. wherein the ceramic pigment has a black color defining a degree of blackness;c. whereby when the pigment is exposed to a temperature of 1,000° F. for a period of 20 hours the degree of blackness does not change.7. The ...

TALC COMPOSITION AND USES THEREOF

A surface treated high aspect ratio talc may be surface treated with a surface treatment agent including a polymeric species including one or more ether linkages. Functional compositions including a surface treated high aspect ratio talc may be polymer compositions. A process for preparing a surface treated high aspect ratio talc may include mixing the high aspect ratio talc and surface treatment agent. A process for preparing a polymer composition may include combining a high aspect ratio talc with a polymer in an amount of at least about 30% by weight, based on the total weight of the polymer composition. 115-. (canceled)16. A surface treated high aspect ratio talc (HART) , wherein HART is surface treated with a surface treatment agent comprising a polymeric species comprising one or more ether linkages.17. The surface treated HART according to claim 16 , wherein the HART has a lamellarity index of at least about 3.0.18. The surface treated HART according to claim 16 , wherein the HART has a dof from about 1 to about 4 μm.19. The surface treated HART according to claim 16 , wherein the polymeric species comprising one or more ether linkages is a polyether or derivative thereof.20. The surface treated HART according to claim 16 , wherein the surface treated HART comprises from about 0.1 to about 10% by weight surface treatment agent claim 16 , based on the weight of talc.21. A process for preparing a surface treated high aspect ratio talc (HART) claim 16 , the method comprising mixing the HART and surface treatment agent as defined in to obtain the surface treated HART.22. A functional composition comprising the surface treated HART according to .23. The functional composition according to claim 22 , wherein the functional composition is a polymer composition.24. The polymer composition according to claim 23 , wherein the polymer is selected from polypropylene claim 23 , polyethylene claim 23 , a propylene-ethylene copolymer claim 23 , or combinations thereof.25. ...

PEARLESCENT PIGMENT FOR SECURITY PURPOSES INCLUDING ORGANIC OR INORGANIC FLUORESCENT MATERIAL

A pearlescent pigment for security purposes according to an embodiment of the present invention includes a single or a plurality of coating layers containing a metal oxide and an organic or inorganic fluorescent material. Since the pearlescent pigment for security purposes according to the present disclosure includes a fluorescent layer containing the organic or inorganic fluorescent material, it can be used as a pigment for security purposes due to its optical characteristics and can also provide effects such as magnetism, high color intensity, multiple colors, etc. Also, since the pearlescent pigment for security purposes has aesthetic benefit and security characteristic at the same time, it is economical, easy to use and applicable in various industries. 1. A pearlescent pigment , comprising:a flake substrate;a coating layer formed on the flake substrate, the coating layer comprising a metal oxide; anda fluorescent layer formed on the coating layer, the fluorescent layer comprising a fluorescent material.2. The pearlescent pigment of claim 1 , wherein a metal of the metal oxide is selected from the group consisting of silicon (Si) claim 1 , titanium (Ti) claim 1 , zirconium (Zr) claim 1 , antimony (Sb) claim 1 , zinc (Zn) claim 1 , tin (Sn) claim 1 , iron (Fe) claim 1 , magnesium (Mg) claim 1 , manganese (Mn) claim 1 , aluminum (Al) claim 1 , cobalt (Co) claim 1 , barium (Ba) and a combination thereof.3. The pearlescent pigment of claim 1 , wherein the metal oxide is FeO.4. The pearlescent pigment of claim 1 , wherein the coating layer comprises:{'sub': 2', '3, 'a first coating layer comprising FeO;'}{'sub': '2', 'a second coating layer formed on the first coating layer, the second coating layer comprising MgO.SiO; and'}{'sub': 2', '3, 'a third coating layer formed on the surface of the second coating layer, the third coating layer comprising FeO.'}5. The pearlescent pigment of claim 1 , wherein the coating layer comprises:{'sub': '2', 'a first coating layer ...

Modified oxidic nano-particle with hydrophobic inclusions, method for the production and use of said particle

Additive for the stabilization of silicon particles in aqueous media

Es wird eine Zusammensetzung zur Stabilisierung von Siliziumpartikeln in einem wäßrigen Medium bereitgestellt, wobei die Zusammensetzung eine organische Säure mit 1–8 Kohlenstoffatomen, einen sekundären aliphatischen Monoalkohol mit 3–8 Kohlenstoffatomen oder einen tertiären aliphatischen Monoalkohol mit 4–8 Kohlenstoffatomen und einen aliphatischen Alkohol mit 2 oder mehr Hydroxygruppen und mit 2–8 Kohlenstoffatomen umfaßt. Ferner wird die Verwendung dieser Zusammensetzung als Additiv in einem Siliziumpartikel enthaltenden, wäßrigen Medium und ein Verfahren zur Stabilisierung von Siliziumpartikeln in wäßrigen Medien bereitgestellt. There is provided a composition for stabilizing silicon particles in an aqueous medium, the composition comprising an organic acid having 1-8 carbon atoms, a secondary aliphatic monoalcohol having 3-8 carbon atoms or a tertiary aliphatic monoalcohol having 4-8 carbon atoms and an aliphatic alcohol having 2 or more hydroxy groups and having 2-8 carbon atoms. Further provided is the use of this composition as an additive in an aqueous medium containing silicon particles and a method of stabilizing silicon particles in aqueous media.

Composition for stabilizing silicon particles in aqueous media and their use

Zusammensetzung zur Stabilisierung von Siliziumpartikeln in einem wäßrigen Medium, bestehend aus a) 0,5–25 Gew.-% einer Carbonsäure mit 1-8 Kohlenstoffatomen, b) 0,1–10 Gew.-% eines primären aliphatischen Monoalkohols mit 1-8 Kohlenstoffatomen, c) 0,1–10 Gew.-% eines sekundären aliphatischen Monoalkohols mit 3-8 Kohlenstoffatomen oder eines tertiären aliphatischen Monoalkohols mit 4-8 Kohlenstoffatomen, d) 0,5–30 Gew.-% eines aliphatischen Alkohols mit 2 oder mehr Hydroxygruppen und 2-8 Kohlenstoffatomen und e) dem Rest Wasser. A composition for stabilizing silicon particles in an aqueous medium, consisting of a) 0.5-25% by weight of a carboxylic acid having 1-8 carbon atoms, b) 0.1-10% by weight of a primary aliphatic monoalcohol having 1-8 C) 0.1-10% by weight of a secondary aliphatic monoalcohol having 3-8 carbon atoms or a tertiary aliphatic monoalcohol having 4-8 carbon atoms, d) 0.5-30% by weight of an aliphatic alcohol having 2 or more hydroxy groups and 2-8 carbon atoms and e) the remainder water.

Suspension of nanoparticles and method for making the same

A stable suspension of ethylpolysilicate nanoparticles having a size of between about 5 nm and 120 nm are in water and stabilized with between about 0.05 and 5 weight percent tetraalkylammonium hydroxide. The particles are between about 95% and 99.5% hydrolyzed and have superior removal rates when used in chemical mechanical polishing. A process for making ethylpolysilicate nanoparticles includes the step of adding reverse osmosis water and 25% tetramethylammonium hydroxide and ammonium hydroxide to a reactor, agitating the mixture and heating the mixture to about 80° C. Tetraethylalkoxy silane is added to the mixture and the mixture stirred and hydrolyzed. Ethanol is then removed. The mixture was then subjected to a vacuum to remove additional distillate. The material left in the reactor was then transferred to a plastic drum.

Stannous compatible silica

Silica particles having a BET surface area from 0.1 to 7m 2 /g, a pack density from 35 to 55 lb/ft 3 , an Einlehner abrasion value from 8 to 25 mg lost/100,000 revolutions, a total mercury intrusion pore volume from 0.7 to 1.2cc/g,and a stannous compatibility from 70 to 99%, are disclosed, as well as methods for making these silica particles.

一种表面改性的SiC纳米线及其制备方法与应用

本发明公开了一种表面改性的SiC纳米线及其制备方法与应用，所述方法为：将SiC纳米线放置到管式烧结炉或可以气氛保护的加热装置中，通入氧气和氮气混合气流，然后启动加热，由室温加热至700～1400℃，控制加热速率为5～20℃/min，保温时间为30～120min，即可得到表面改性后的SiC纳米线。表面改性后的SiC纳米线为核壳结构的一维纳米材料，芯部为SiC，外层为SiO 2 ，SiO 2 紧密包覆在SiC外面形成致密的包覆层，SiO 2 包覆层为非晶态，界面处的结合为原子尺度的紧密结合，外部的SiO 2 包覆层厚度可以控制为2nm~500nm。本发明解决了现有碳化硅纳米线在使用过程中的活性低、难分散、易氧化、界面结合差等问题，具有制备工艺简单、节能环保、易控制、成本低、产率高的优点。

炭化ケイ素粉末及びその製造方法

【課題】平均粒子径が小さく且つ粒子径分布の幅が狭い炭化ケイ素粉末を提供する。【解決手段】炭化ケイ素粉末は、結晶形がα型である炭化ケイ素の粉末であって、平均粒子径が３００ｎｍ以下である。そして、この炭化ケイ素粉末は、体積基準の積算粒子径分布において小粒径側からの積算粒子体積が全粒子体積の１０％となる粒子径Ｄ１０と、体積基準の積算粒子径分布において小粒径側からの積算粒子体積が全粒子体積の９０％となる粒子径Ｄ９０との比Ｄ９０／Ｄ１０が４以下である。【選択図】なし

Low refractive index particles

Low refractive index particles

This invention relates to porous organosilica nanoparticles having a BET surface area of at least 400m 2 /g and/or a pore volume of at least 0.7cm 3 /g, wherein the nanoparticles have a mean pore diameter of l-50nm, a mean diameter in the range 1-100nm and wherein the pores of the nanoparticles are randomly oriented. This invention also relates to solutions, dispersions, powders, compressed pellets and coatings comprising a plurality of the porous organosilica nanoparticles, as well as to methods for preparing the porous organosilica nanoparticles.

Weathering-resistant pearl-lustre pigments, process for producing same and use

Dye, filler made therefrom, compositions including the filler, and method of determining degree of cure of such compositions

A compound represented by formula (I): and a treated filler having the compound on at least a portion of its surface. R is hydrogen or alkyl. X is alkylene, arylalkylene, or alkylarylene, each optionally interrupted by at least one of an ether, thioether, amine, amide, ester, thioester, carbonate, thiocarbonate, carbamate, thiocarbamate, urea, or thiourea, with alkylene optionally interrupted by arylene. W is hydroxyl, a sulfonic acid group, a phosphonic acid group, carboxylic acid group, —NHR 1 , epoxy, or —Si(Y) x (Z) 3-x . Y is alkyl, aryl, arylalkylenyl, or alkylarylenyl. Z is halide, hydroxyl, alkoxy aryloxy, acyloxy, polyalkyleneoxy, —O— covalently bonded to the surface of the filler, or —O bonded to another silicon atom, and x is 0 or 1. A composition including the treated filler, a method of making the treated filler, and a method of determining the degree of cure of a curable polymeric resin are also disclosed.

Aqueous dispersions and method for the production thereof

A stable aqueous dispersion, comprising a latex, an inorganic pigment and a dispersing agent dispersed in water, wherein at least 50 wt-% of the latex is adsorbed onto the inorganic particles and at least 20 wt-% of the dispersing agent is adsorbed onto the latex. It can be produced by admixing the latex with an anionic dispersing agent having a charge density of at least 14.1 meq/g to form a modified latex, admixing the inorganic pigment with the modified latex in aqueous phase to form a pigment-latex slurry, and subjecting the pigment-latex slurry to intensive mixing to form a dispersion. The novel dispersions can be used in the paper and pulp industry and in the paint industry.

METHOD FOR MANUFACTURING SUBSTRATE PIGMENTS

Thickener based on at least one synthetic layered silicate

Produit a base de particules lamellaires minerales et organiques, comportant un pigment melanique, son procede de preparation et son utilisation en cosmetique.

L'invention est relative à un produit sous forme de poudre constitué de particules à structure lamellaire, organiques ou minérales, ayant une dimension inférieure à 50 microns et comportant au moins un pigment mélanique synthétique, formé in situ par oxydation d'un composé indolique, et à son utilisation pour la protection de l'épiderme humain, dans les produits de maquillage et pour la coloration des cheveux.

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First tin compatible silica

一种利用不同极性处理剂改性的填料组合物、制备方法和应用

本发明提供了利用不同极性处理剂改性的填料组合物、制备方法和应用，先通过在无机填料微粉表面包覆高极性处理剂和低极性处理剂得到一种利用不同极性处理剂改性的填料组合物，并进一步将该填料组合物分散于有机溶剂中得到浆料，该浆料可以添加至不同极性混合树脂体系中制成树脂组合物。由于无机填料微粉表面利用极性差异较大的两种处理剂进行包覆处理，使其兼具极性与低极性两部分，再将处理后的粉体与溶剂混合、分散，制备成均匀稳定的浆料，浆料具有良好的分散性和流动性，添加至不同极性混合树脂体系后，相容性和流动性都非常好。

PROCESS FOR PRODUCTION OF SODIUM SOIL AND SULFITE WITH SODIUM SULFATE

processo para produção de siuca e sulfito de sódio com sulfato de sódio. a presente invenção refere-se a um processo para produção de sílica e sulfito de sódio com sulfato de sódio, onde uma mistura de areia de quartzo, sulfato de sódio e carbono á reagida para produzir silicato de sódio sólido e dlóxldo de enxofre; o dito silicato de sódio sólido é dissolvido em água e então filtrado para obter uma solução de silicato de sódio: a dita solução de silicato de sódio é coiocada em contato com o dlóxldo de enxofre para produzir sílica precipitada e solução de sulfito de sódio; a resultante mistura é filtrada; a torta de filtro é acidulada e então segue através de filtração, lavagem e secagem para obtenção de sílica; e o filtrado é concentrado e seco para obter sulfito de sódio. o processo da presente invenção tem grande vaior devido suas etapas simples, baixo custo de produção e redução de problemas ambientais. process for the production of suca and sodium sulfite with sodium sulfate. The present invention relates to a process for producing sodium silica and sodium sulfate with sodium sulfate, wherein a mixture of quartz sand, sodium sulfate and carbon is reacted to produce solid sodium silicate and sulfur dioxide; said solid sodium silicate is dissolved in water and then filtered to obtain a sodium silicate solution: said sodium silicate solution is contacted with sulfur dioxide to produce precipitated silica and sodium sulfite solution; the resulting mixture is filtered; the filter cake is acidulated and then followed by filtration, washing and drying to obtain silica; and the filtrate is concentrated and dried to obtain sodium sulfite. The process of the present invention has great advantage due to its simple steps, low production cost and reduction of environmental problems.

一种超疏水性白炭黑的制备方法

本发明公开一种超疏水性白炭黑的制备方法，包含以下步骤:1)将硅烷偶联剂、有机溶剂和水按体积比例为1︰(1～8)︰(1～2)进行混合，得硅烷偶联剂改性液；2)向白炭黑悬浮液中添加步骤1)硅烷偶联剂改性液，于50～90℃下，搅拌0.5～24h；再添加非离子型表面活性剂和含氟高分子聚合物，于40～95℃下，搅拌0.5～20h，得复合改性白炭黑悬浮液；3)将步骤2)复合改性白炭黑悬浮液过滤、干燥、粉碎，得超疏水性白炭黑。本发明对白炭黑进行复合改性，含氟高分子聚合物具有低的表面能，与硅烷偶联剂通过共价键的形式牢固的结合在一起，制成的改性白炭黑的疏水性能很好，在橡胶、轮胎的应用中表现出良好的相容性与分散性，提高了产品的加工性能与力学性能。

Silicon dioxide particles compatible with stannous(ii) compounds

FIELD: chemistry. SUBSTANCE: invention relates to silica materials for use as a component of products for dental hygiene. Silicon dioxide particles have a BET surface (specific surface determined according to the Brunauer-Emmett-Teller method by nitrogen adsorption) within the range of 0.1 to 7 m 2 /g; tapped density within the range of 0.561 to 0.881 g/cm 3 ; abrasiveness on the Einlechner scale within the range of 8 to 25 mg loss/100,000 rotations measured using an AT-1000 Einlechner abrasion test unit and a brass wire sieve of a fourdrinier paper machine; the total pore volume determined using mercury porosimetry within the range of 0.7 to 1.2 cm 3 /g; and compatibility with a tin(II) compound within the range of 70 to 99% measured after centrifugation at 12,000 rpm for 10 minutes using an optical emission spectrometer with inductively coupled plasma. Described is a method for synthesis of the particles. EFFECT: said particles have improved compatibility with a tin(II) compound, including tin(II) fluoride, for improving the total effectiveness of the tin(II) compound in a composition for teeth hygiene. 13 cl, 14 dwg, 9 tbl, 43 ex РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (13) 2 749 786 C2 (51) МПК C01B 33/193 (2006.01) C09C 1/28 (2006.01) C08K 3/36 (2006.01) A61K 8/02 (2006.01) A61K 8/25 (2006.01) A61Q 11/00 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ОПИСАНИЕ ИЗОБРЕТЕНИЯ К ПАТЕНТУ (52) СПК C01B 33/193 (2021.01); C09C 1/28 (2021.01); C08K 3/36 (2021.01); A61K 8/0279 (2021.01); A61K 8/25 (2021.01); A61Q 11/00 (2021.01); C01P 2002/02 (2021.01); C01P 2004/03 (2021.01); C01P 2004/32 (2021.01); C01P 2004/51 (2021.01); C01P 2006/11 (2021.01); C01P 2006/12 (2021.01); C01P 2006/14 (2021.01); C01P 2006/17 (2021.01); C01P 2006/19 (2021.01); C01P 2006/21 (2021.01) 2019121717, 01.12.2017 (24) Дата начала отсчета срока действия патента: 01.12.2017 16.06.2021 Приоритет(ы): (30) Конвенционный приоритет: (73) Патентообладатель(и): ЭВОНИК ОПЕРЕЙШНС ГМБХ (DE) 19.12 ...

Осажденный кремнезем, используемый в качестве упрочняющего материала для эластомеров, и способ его получения

Изобретение относится к новому осажденному кремнезему, применяемому в качестве упрочняющего материала для эластомеров, а также к способу его получения. Сущность способа заключается во взаимодействии силиката с подкисляющим агентом с получением суспензии осажденного кремнезема с последующим разделением и сушкой этой суспензии, в которой осаждение осуществляют следующим образом: готовят исходную шихту, содержащую, по меньшей мере, часть общего количества силиката, необходимого для реакции, и, по меньшей мере, один электролит, где концентрация силиката (в расчете на SiO 2 ) составляет 55-60 г/л, добавляют к шихте подкисляющий агент до достижения значения рН реакционной среды от 7 до 8,5, добавляют к реакционной среде подкисляющий агент и, в случае необходимости, одновременно добавляют оставшееся количество силиката, отделяют путем фильтрации, промывки и прессования, путем введения воздуха под давлением ниже 4,5 бар в течение 20-40 с., сушат путем распыления суспензии, в которой содержится менее 17 мас.% сухого материала. Сущность нового осажденного кремнезема заключается в том, что он имеет следующие характеристики: удельная поверхность ВЕТ от 185 до 250 м 2 /г, удельная поверхность СТАВ от 180 до 240 м 2 /г, такое распределение пор, при котором объем пор V2, образуемый порами с диаметром от 175 до 275 , составляет менее 50% от объема V1, образуемого порами с диаметром, меньшим или равным 400 , объем пор (V d1 ), образуемый порами с диаметром менее 1 мкм, более 1,65 см 3 /г, показатель зернистости 70 - 100 процентное содержание мелочи (τ f ) после ультразвуковой дезагломерации, по меньшей мере, 50%. Полученный продукт обладает достаточной способностью диспергироваться в эластомерах и хорошими упрочняющими свойствами. 2 с. и 22 з.п. ф-лы, 4 табл. ССОО ЬсС ПЧ с» (19) РОССИЙСКОЕ АГЕНТСТВО ПО ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ ВИ” 2 170 212 5 МК’ С 01 В 33/193 (13) С2 (12) ОПИСАНИЕ ИЗОБРЕТЕНИЯ К ПАТЕНТУ РОССИЙСКОЙ ФЕДЕРАЦИИ (21), (22) Заявка: 99103625/12, 15.05.1998 (24) Дата ...

一种高分散纳米二氧化硅的表面改性方法

本发明涉及一种高分散纳米二氧化硅的表面改性方法，包括以下步骤：1)将一定量的纳米二氧化硅配制成以乙醇为溶剂的纳米二氧化硅悬浮液，并将配制好的悬浮液在超声清洗器中超声分散；2)超声结束后测试悬浮液的PH值，并采用酸调节悬浮液的PH为4～5；3)将一定量的硅烷偶联剂加入到调节PH后的悬浮液中，并水浴加热搅拌均匀，得到混合液；4)将混合液抽滤并用酒精洗涤，将得到的固体物质放入真空恒温干燥箱中干燥，即得到了改性后的纳米二氧化硅粉末。该方法工艺简单、易于操作、成本低、绿色环保，得到的改性的纳米二氧化硅分散性及稳定性好，克服了纳米二氧化硅易团聚的问题，使得其在高性能混凝土性能调控方面具有巨大的应用潜力。

Способ получения двуокиси кремния и сульфита натрия с использованием сульфата натрия

1. Способ получения двуокиси кремния и сульфита натрия с использованием сульфата натрия, отличающийся тем, что: ! кварцевый песок, сульфат натрия и углерод смешивают в массовом соотношении 118,3-147,9:100:4-12, а затем помещают в печь и нагревают до температуры 1200-1500°С для получения твердого силиката натрия и двуокиси серы; ! названный твердый силикат натрия растворяют в воде в массовом соотношении 100:180-488 и фильтруют для получения раствора силиката натрия; ! в названный раствор силиката натрия вводят двуокись серы, предпочтительно, полученную в процессе получения твердого силиката натрия, при мольном соотношении 1:1 и осуществляют реакцию при 70-100°С в течение 1-4 ч; ! полученную смесь фильтруют; ! получают двуокись кремния и сульфит натрия после следующих стадий: ! (1) осадок подкисляют до pH 3,5-6,0 с последующей фильтрацией, промывкой и сушкой для получения двуокиси кремния; ! (2) фильтрат концентрируют и сушат для получения сульфита натрия. ! 2. Способ получения двуокиси кремния и сульфита натрия по п.1, отличающийся тем, что названной печью является термоизолированная печь с подковообразным пламенем. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 2007 148 703 (13) A (51) МПК C01B 33/113 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ЗАЯВКА НА ИЗОБРЕТЕНИЕ (21), (22) Заявка: 2007148703/15, 06.06.2006 (71) Заявитель(и): Дегусса Веллинк Зилика (Нанпинг) Ко. Лимитед (CN) (30) Конвенционный приоритет: 08.06.2005 CN 200510200314.7 (43) Дата публикации заявки: 20.07.2009 Бюл. № 20 (72) Автор(ы): ЛУ Юаньян (CN) (86) Заявка PCT: CN 2006/001226 (06.06.2006) R U (54) СПОСОБ ПОЛУЧЕНИЯ ДВУОКИСИ КРЕМНИЯ И СУЛЬФИТА НАТРИЯ С ИСПОЛЬЗОВАНИЕМ СУЛЬФАТА НАТРИЯ (57) Формула изобретения 1. Способ получения двуокиси кремния и сульфита натрия с использованием сульфата натрия, отличающийся тем, что: кварцевый песок, сульфат натрия и углерод смешивают в массовом соотношении 118,3-147,9:100:4-12, а затем помещают в печь и нагревают до ...

Интерференционные пигменты на основе оксидов кремния

ÐÎÑÑÈÉÑÊÀß ÔÅÄÅÐÀÖÈß (19) RU (11) 2005 115 065 (13) A (51) ÌÏÊ C09C 1/00 (2006.01) ÔÅÄÅÐÀËÜÍÀß ÑËÓÆÁÀ ÏÎ ÈÍÒÅËËÅÊÒÓÀËÜÍÎÉ ÑÎÁÑÒÂÅÍÍÎÑÒÈ, ÏÀÒÅÍÒÀÌ È ÒÎÂÀÐÍÛÌ ÇÍÀÊÀÌ (12) ÇÀßÂÊÀ ÍÀ ÈÇÎÁÐÅÒÅÍÈÅ (21), (22) Çà âêà: 2005115065/15, 07.10.2003 (71) Çà âèòåëü(è): ÖÈÁÀ ÑÏÅØÈÀËÒÈ ÊÅÌÈÊÝËÇ ÕÎËÄÈÍà ÈÍÊ. (CH) (30) Ïðèîðèòåò: 16.10.2002 EP 02405887.7 21.11.2002 EP 02406009.7 (43) Äàòà ïóáëèêàöèè çà âêè: 10.02.2006 Áþë. ¹ 4 (87) Ïóáëèêàöè PCT: WO 2004/035693 (29.04.2004) Àäðåñ äë ïåðåïèñêè: 101000, Ìîñêâà, Ì.Çëàòîóñòèíñêèé ïåð., 10, êâ.15, "ÅÂÐÎÌÀÐÊÏÀÒ", ïàò.ïîâ. È.À.Âåñåëèöêîé, ðåã. ¹ 11 R U Ôîðìóëà èçîáðåòåíè 1. Ïèãìåíò, ÷àñòèöû êîòîðîãî îáû÷íî îáëàäàþò äëèíîé, ðàâíîé îò 2 ìêì äî 5 ìì, øèðèíîé, ðàâíîé îò 2 ìêì äî 2 ìì è òîëùèíîé, ðàâíîé îò 20 íì äî 2 ìêì, è îòíîøåíèåì äëèíû ê òîëùèíå, ðàâíûì íå ìåíåå 2:1, â êîòîðîì ÷àñòèöû ñîäåðæàò äðî èç SiOy, â êîòîðîì 0,70≤y≤1,95, ïðåäïî÷òèòåëüíî 1,1≤y≤1,8, îáëàäàþùåå äâóì â îñíîâíîì ïàðàëëåëüíûìè ñòîðîíàìè, ðàññòî íèå ìåæäó ýòèìè ñòîðîíàìè âë åòñ ñàìîé êîðîòêîé îñüþ äðà, âêëþ÷àþùèé (à) ìàòåðèàë, ïðåäïî÷òèòåëüíî îêñèä ìåòàëëà, îáëàäàþùèé áîëüøèì ïîêàçàòåëåì ïðåëîìëåíè . 2. Ïèãìåíò, ÷àñòèöû êîòîðîãî îáû÷íî îáëàäàþò äëèíîé, ðàâíîé îò 2 ìêì äî 5 ìì, øèðèíîé, ðàâíîé îò 2 ìêì äî 2 ìì è òîëùèíîé, ðàâíîé îò 20 íì äî 2 ìêì, è îòíîøåíèåì äëèíû ê òîëùèíå, ðàâíûì íå ìåíåå 2:1, â êîòîðîì ÷àñòèöû ñîäåðæàò äðî èç SiOy, â êîòîðîì 0,70≤y≤1,95, ïðåäïî÷òèòåëüíî 1,1≤y≤1,8, îáëàäàþùåå äâóì â îñíîâíîì ïàðàëëåëüíûìè ñòîðîíàìè, ðàññòî íèå ìåæäó ýòèìè ñòîðîíàìè âë åòñ ñàìîé êîðîòêîé îñüþ äðà, âêëþ÷àþùèé (à) òîíêèé ïîëóïðîçðà÷íûé ñëîé ìåòàëëà. 3. Ïèãìåíò ïî ï.1, â êîòîðîì ïèãìåíò äîïîëíèòåëüíî âêëþ÷àåò (á) îêñèä ìåòàëëà, îáëàäàþùèé áîëüøèì ïîêàçàòåëåì ïðåëîìëåíè , â êîòîðîì ðàçíîñòü ïîêàçàòåëåé ïðåëîìëåíè ñîñòàâë åò íå ìåíåå 0,1. 4. Ïèãìåíò ïî ï.1 èëè 3, â êîòîðîì îêñèä ìåòàëëà, îáëàäàþùèé áîëüøèì ïîêàçàòåëåì ïðåëîìëåíè , ïðåäñòàâë åò ñîáîé TiO2, ZrO2, Fe2Î3, Fe3O4, Cr2O3, ZnO èëè ñìåñü ýòèõ îêñèäîâ èëè òèòàíàò æåëåçà, ãèäðàò îêñèäà æåëåçà, ñóáîêñèä òèòàíà èëè ñìåñü ...

Способ получения двуокиси кремния и сульфита натрия с использованием сульфата натрия

1. Способ получения двуокиси кремния и сульфита натрия с использованием сульфата натрия, характеризующийся тем, что: ! кварцевый песок, сульфат натрия и углерод смешивают в массовом соотношении 118,3-147,9:100:4-12, а затем помещают в печь и нагревают при температуре 1200-1500°С для получения твердого силиката натрия и двуокиси серы; ! указанный твердый силикат натрия и двуокись серы используют для получения двуокиси кремния и сульфита натрия на следующих стадиях: ! (1) указанный твердый силикат натрия растворяют в воде в массовом соотношении 100:180-488 и фильтруют для получения раствора силиката натрия; в названный раствор силиката натрия добавляют бисульфит натрия с концентрацией 1-40% в мольном отношении бисульфита натрия к силикату натрия 2:1 и смесь подвергают реакции при температуре 70-95°С в течение 1-4 ч для получения осажденной двуокиси кремния и раствора сульфита натрия, а полученную смесь фильтруют; ! (2) одну часть фильтрата, полученного в конце стадии (1), приводят в контакт с двуокисью серы, полученной в процессе получения силиката натрия, при температуре от 20 до 50°С для образования бисульфита натрия, который повторно используют для реакции на стадии (1); ! (3) значение pH отжатого на фильтре осадка, полученного в конце стадии (1), доводят до 3,5-6 с последующей фильтрацией, промывкой и сушкой для получения двуокиси кремния; а ! (4) другую часть фильтрата, полученного в конце стадии (1), концентрируют и сушат для получения твердого сульфита натрия. ! 2. Способ получения двуокиси кремния и сульфита натрия по п.1, характеризующийся тем, что указанной печью является термоизолированная печь с подковообразным пламенем. РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 2007 148 741 (13) A (51) МПК C01B 33/113 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ЗАЯВКА НА ИЗОБРЕТЕНИЕ (71) Заявитель(и): Дегусса Веллинк Зилика (Нанпинг) Ко. Лимитед (CN) (21), (22) Заявка: 2007148741/15, 06.06.2006 (30) Конвенционный приоритет: 08. ...

减缓粉体在端羟基聚合物中沉降速率的颗粒表面处理方法

本发明公开了一种减缓粉体在端羟基聚合物中沉降速率的颗粒表面处理方法，包括以下步骤：配制多酚羟基化合物水溶液；配制三氯化铁水溶液；搅拌包覆：先将粉体加入到多酚羟基化合物水溶液中快速搅拌，然后加入三氯化铁水溶液，继续搅拌，得到混合溶液；或，先将粉体加入至三氯化铁水溶液中快速搅拌，然后加入多酚羟基化合物水溶液，继续搅拌，得到混合溶液；逐步滴入碱性水溶液，调节混合溶液的pH值至7～14；用水洗涤、过滤、分离出粉体颗粒并进行干燥，得到表面处理后的粉体。本方法选用多酚羟基化合物和三氯化铁对粉体表面进行处理，处理方法简单，包覆处理时间短，试剂环保无毒，减缓了粉体在端羟基聚合物中的沉降速率。

染料、由其制备的填料、包括填料的组合物以及确定此类组合物的固化度的方法

一种由式(I)表示的化合物和经处理的填料，该经处理的填料在其表面的至少一部分上具有所述化合物。R为氢或烷基。X为亚烷基、芳基亚烷基或烷基亚芳基，各自任选地插入有醚、硫醚、胺、酰胺、酯、硫酯、碳酸酯、硫代碳酸酯、氨基甲酸酯、硫代氨基甲酸酯、脲或硫脲中的至少一种，其中亚烷基任选地插入有亚芳基。W为羟基、磺酸基团、膦酸基团、羧酸基团、‑NHR 1 、环氧基或‑Si(Y) x (Z) 3‑x 。Y为烷基、芳基、芳基亚烷基或烷基亚芳基。Z为卤化物、羟基、烷氧基、芳氧基、酰氧基、聚亚烷氧基、共价键合到填料的表面的‑O‑，或键合到另一个硅原子的‑O，并且x为0或1。本发明还公开了包括经处理的填料的组合物，制备经处理的填料的方法，以及确定可固化聚合物树脂的固化度的方法。

Macroporous microspheroids and a process for their manufacture

Disclosed herein is a powder of discrete, macroporous, microspheroids, each having an average diameter in the range of 2 to 50 microns and each composed of a plurality of large colloidal particles joined and cemented together at their points of contact by 1 to 10% by weight of nonporous, amorphous silica. These microspheroids have a high degree of mechanical stability and a surface area between about 80 and 110% of that of the large colloidal particles. Also disclosed is a process for the manufacture of this powder.

Process for manufacture of macroporous microspheroids

Disclosed herein is a powder of discrete, macroporous, microspheroids, each having an average diameter in the range of 2 to 50 microns and each composed of a plurality of large colloidal particles joined and cemented together at their points of contact by 1 to 10% by weight of non-porous, amorphous silica. These microspheroids have a high degree of mechanical stability and a surface area between about 80 and 110% of that of the large colloidal particles. Also disclosed is a process for the manufacture of this powder.

α-氧化铝薄片

本发明涉及具有限定的厚度和粒径分布的氧化铝薄片，以及它们在清漆、油漆、汽车涂料、印刷油墨、母料、塑料和化妆品制剂中及作为效果颜料的基材的用途。

核壳二氧化硅粒子及用于减少恶臭的用途

本发明涉及核壳二氧化硅粒子，其中每个核壳二氧化硅粒子包含二氧化硅核，并且所述二氧化硅核的表面被金属硅酸盐蚀刻，所述核壳二氧化硅粒子是通过以下步骤制备：i)将一定量在水中的二氧化硅粒子与一定量的碱混合以产生核壳二氧化硅粒子，其中所述碱包含一价金属离子，每个核壳二氧化硅粒子包含二氧化硅核，并且所述二氧化硅核的表面被一价金属离子的硅酸盐蚀刻；及ii)使在步骤i)中形成的核壳二氧化硅粒子与包含第二金属离子的金属盐反应以形成在二氧化硅核表面上包含第二金属离子硅酸盐的核壳二氧化硅粒子。

Rubber composition, crosslinked rubber composition and tire

The present invention provides a rubber composition that can offer excellent abrasion resistance when applied to a tire member such as a tread, without deteriorating rolling resistance. To solve the problem, a rubber composition according to the present invention contains a rubber component, hydrous silicate, and a surfactant, in which the hydrous silicate is modified by the surfactant before being kneaded with the rubber component.

Способ получения двуокиси кремния, сульфита натрия и бисульфита натрия с использованием сульфата натрия

1. Способ получения двуокиси кремния, сульфита натрия и бисульфита натрия с сульфатом натрия, отличающийся тем, что смешивают кварцевый песок, сульфат натрия и углерод и подают в печь для взаимодействия, а полученные твердый силикат натрия и двуокись серы используют для получения двуокиси кремния, сульфита натрия и бисульфита натрия на следующих стадиях: ! (1) для получения двуокиси кремния: названный твердый силикат натрия растворяют в воде в массовом соотношении 100:180-488 и фильтруют для получения раствора силиката натрия; полученный раствор силиката натрия подвергают взаимодействию с 98%-ной серной кислотой в массовом соотношении 13-19:1 при температуре 70-100°С в течение 1-4 ч для получения осажденной двуокиси кремния и раствора сульфата натрия; а осажденную двуокись кремния фильтруют, промывают, разжижают и сушат для получения двуокиси кремния, ! (2) для получения сульфита натрия: соду растворяют в растворе бисульфита натрия в мольном отношении соды к бисульфиту натрия 1:1 для образования раствора сульфита натрия; одну часть названного раствора сульфита натрия концентрируют и сушат для получения сухого сульфита натрия; а другую его часть подвергают взаимодействию с двуокисью серы в мольном соотношении 1:1 при температуре 20-50°С для получения раствора бисульфита натрия, который может быть использован повторно для получения сульфита натрия, ! (3) для получения бисульфита натрия: соду растворяют в растворе бисульфита натрия в мольном отношении соды к бисульфиту натрия 1:1 с последующим взаимодействием с двуокисью серы, полученной в процессе получения силиката натрия при температуре 20-50°С, для получения пересыщенного рас� РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) 2008 100 098 (13) A (51) МПК C01B 33/113 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ, ПАТЕНТАМ И ТОВАРНЫМ ЗНАКАМ (12) ЗАЯВКА НА ИЗОБРЕТЕНИЕ (71) Заявитель(и): Дегусса Веллинк Зилика (Нанпинг) Ко. Лимитед (CN) (21), (22) Заявка: 2008100098/15, 06.06.2006 (30) Конвенционный приоритет: 10.06. ...

有机硅烷改性的聚硅氧烷及其在表面改性中的用途

本发明涉及下式的有机硅烷改性的聚硅氧烷： 其中x、y、z、p、R 1 、R 2 、R 3 、R 4 、R 5 、R 6 、R 7 、R 8 、R 9 和R 10 如说明书中所述定义。另外本发明还涉及该有机改性的聚硅氧烷在表面涂覆中的用途及其制备。

Method for processing sphene concentrate

FIELD: technological processes.SUBSTANCE: invention can be used in the production of sorbents for the purification of liquid effluents from heavy metals and radionuclides, filler for paint and varnish and building materials. Method for processing sphene concentrate includes its grinding and decomposition by dilute sulfuric acid upon heating with transfer of titanium into the solution, and calcium and silicon into a solid residue. Titanium-containing solution is separated from the silicon-silicon residue, which is treated to form a filler. Salting out reagent is introduced into the titanium-containing solution in the form of sulfuric acid until a concentration of 850–950 g/l of HSOand heated to boiling. Resulting sulfuric acid liquid phase is sent to the decomposition of the concentrate. Titanium solid phase is treated with phosphoric acid at a concentration of 20–50 % HPOat a mass ratio PO:TiO, equal to 2–3.5:1. Resulting suspension is filtered with separation into a phosphate filtrate and a titanium phosphate precipitate, which is washed with water and dried. Phosphoric acid filtrate is used in the treatment of titanium solid phase.EFFECT: invention makes it possible to increase the ecological compatibility, to increase the sorption capacity of titanium phosphate, effectively.3 cl, 4 ex РОССИЙСКАЯ ФЕДЕРАЦИЯ ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) (19) RU (11) (13) 2 665 759 C1 (51) МПК C01G 23/00 (2006.01) C22B 3/08 (2006.01) C22B 34/12 (2006.01) C01B 25/37 (2006.01) C09C 1/02 (2006.01) C09C 1/28 (2006.01) B01J 20/02 (2006.01) ОПИСАНИЕ ИЗОБРЕТЕНИЯ К ПАТЕНТУ (52) СПК C01G 23/00 (2018.05); C22B 3/08 (2018.05); C22B 34/1213 (2018.05); C22B 34/124 (2018.05); C01B 25/372 (2018.05); C09C 1/02 (2018.05); C09C 1/28 (2018.05); B01J 20/0211 (2018.05); B01J 20/0292 (2018.05) (21)(22) Заявка: 2017145831, 25.12.2017 25.12.2017 Дата регистрации: Приоритет(ы): (22) Дата подачи заявки: 25.12.2017 (45) Опубликовано: 04.09.2018 Бюл. № 25 2 6 6 5 7 5 9 R U (54) ...

α-Alumina Flakes

본 발명은 정해진 두께 및 입자 크기 분포를 갖는 알루미나 플레이크, 및 바니쉬, 페인트, 자동차용 코팅, 인쇄용 잉크, 마스터뱃치, 플라스틱 및 화장품 제형에 있어서의, 및 효과 안료용 기재로서의 그의 용도에 관한 것이다. The present invention relates to alumina flakes having a defined thickness and particle size distribution and to their use in varnishes, paints, automotive coatings, printing inks, masterbatches, plastics and cosmetic formulations, and as substrates for effect pigments.

α-Alumina Flakes

본 발명은 정해진 두께 및 입자 크기 분포를 갖는 알루미나 플레이크 및 바니쉬, 페인트, 자동차용 코팅, 인쇄용 잉크, 마스터뱃치, 플라스틱 및 화장품 제형에 있어서의, 및 효과 안료용 기재로서의 그의 용도에 관한 것이다. The present invention relates to alumina flakes having a defined thickness and particle size distribution and to their use in varnishes, paints, automotive coatings, printing inks, masterbatches, plastics and cosmetic formulations, and as substrates for effect pigments.

Polymer encapsulation of high aspect ratio materials and methods of making same

Embodiments of this invention comprise a pigment comprising one or more substantially spherical-shaped beads, wherein each substantially spherical-shaped bead comprises one or more high aspect ratio particles encapsulated within an encapsulating material. Embodiments also comprise a resinous composition comprising said pigment. Yet further embodiments comprise a method of preparing said pigment via suspension polymerization. The substantially spherical-shaped beads of this invention may be used to produce resinous compositions having a flowline-free colored, sparkling and/or metallescent appearance.

Polymer Encapsulation of High Aspect Ratio Materials and Methods of Making Same

A pigment contains one or more substantially spherical-shaped beads. Each substantially spherical-shaped bead includes one or more high aspect ratio particles encapsulated within an encapsulating material. Resinous compositions containing this pigment and a plastic, for example a polycarbonate, have a flowline-free colored, sparkling and/or metallescent appearance.

Polymer encapsulation of high aspect ratio materials and methods of making same

A pigment contains one or more substantially spherical-shaped beads. Each substantially spherical-shaped bead includes one or more high aspect ratio particles encapsulated within an encapsulating material. Resinous compositions containing this pigment and a plastic, for example a polycarbonate, have a flowline-free colored, sparkling and/or metallescent appearance.

Methods for encapsulation of materials and methods for making resinous compositions and articles comprising the same

An embodiment of a method of encapsulation of a material comprises dispersing high aspect ratio particles in a monomer and/or a polymer to form a suspension mixture, adding the suspension mixture to an aqueous mixture to form an aqueous reaction mixture, heating and mixing the aqueous reaction mixture to encourage the formation of substantially spherical-shaped beads, quenching the aqueous reaction mixture after the substantially spherical-shaped beads are formed, and collecting the substantially spherical-shaped beads.

Polymer encapsulation of high aspect ratio materials and methods of making same

A pigment contains one or more substantially spherical-shaped beads. Each substantially spherical-shaped bead includes one or more high aspect ratio particles encapsulated within an encapsulating material. Resinous compositions containing this pigment and a plastic, for example a polycarbonate, have a flowline-free colored, sparkling and/or metallescent appearance.

Polymer encapsulation of high aspect ratio materials and methods of making same

Embodiments of this invention comprise a pigment comprising one or more substantially spherical-shaped beads, wherein each substantially spherical-shaped bead comprises one or more high aspect ratio particles encapsulated within an encapsulating material. Embodiments also comprise a resinous composition comprising said pigment. Yet further embodiments comprise a method of preparing said pigment via suspension polymerization.

一种雪地轮胎用改性白炭黑及其制备方法

本发明涉及改性白炭黑技术领域，公开了一种雪地轮胎用改性白炭黑及其制备方法，首先将硅酸钠水溶液，蒸馏水以及AEO‑9均匀混合，得到底液，然后另取硅酸钠水溶液和浓硫酸滴加入底液中获得白炭黑合成液，然后另取浓硫酸加入白炭黑合成液中，获得酸性白炭黑浆液，之后将硼酸酯偶联剂与另取的蒸馏水以及AEO‑9混合，搅拌，乳化得到改性剂乳液；最后将改性剂乳液，木质纤维素短纤维同时加入到酸性白炭黑浆液中，获得改性白炭黑浆液并将改性白炭黑浆液过滤、洗涤、干燥，获得雪地轮胎用改性白炭黑，利用该雪地轮胎用改性白炭黑制备成雪地轮胎后，该雪地轮胎能够保持更好的柔软性和更高的抓地力，适用于低温环境。

α-Alumina Flakes

본 발명은 정해진 두께 및 입자 크기 분포를 갖는 알루미나 플레이크, 및 바니쉬, 페인트, 자동차용 코팅, 인쇄용 잉크, 마스터뱃치, 플라스틱 및 화장품 제형에 있어서의, 및 효과 안료용 기재로서의 그의 용도에 관한 것이다. The present invention relates to alumina flakes having a defined thickness and particle size distribution and to their use in varnishes, paints, automotive coatings, printing inks, masterbatches, plastics and cosmetic formulations, and as substrates for effect pigments.

Patent RU2019121717A3

РОССИЙСКАЯ ФЕДЕРАЦИЯ (19) RU (11) (13) 2019 121 717 A (51) МПК C01B 33/18 (2006.01) ФЕДЕРАЛЬНАЯ СЛУЖБА ПО ИНТЕЛЛЕКТУАЛЬНОЙ СОБСТВЕННОСТИ (12) ЗАЯВКА НА ИЗОБРЕТЕНИЕ (21)(22) Заявка: 2019121717, 01.12.2017 (71) Заявитель(и): ЭВОНИК ОПЕРЕЙШНС ГМБХ (DE) Приоритет(ы): (30) Конвенционный приоритет: 19.12.2016 US 62/435,921; 22.05.2017 US 62/509,276 (85) Дата начала рассмотрения заявки PCT на национальной фазе: 19.07.2019 EP 2017/081091 (01.12.2017) (87) Публикация заявки PCT: WO 2018/114280 (28.06.2018) A Адрес для переписки: 105082, Москва, пер. Спартаковский, 2, стр. 1, секция 1, этаж 3, ЕВРОМАРКПАТ R U (57) Формула изобретения 1. Частицы диоксида кремния, отличающиеся: (i) БЭТ-поверхностью (удельная поверхность, определяемая по методике БрунауэраЭммета-Теллера по адсорбции азота), находящейся в диапазоне от примерно 0,1 до примерно 7 м2/г; (ii) насыпной плотностью после уплотнения, находящейся в диапазоне от примерно 35 до примерно 55 фунт/фут3; (iii) показателем абразивности по Айнлехнеру, находящимся в диапазоне от примерно 8 до примерно 25 мг потерь/100000 оборотов; (iv) определенным с помощью ртутной порометрии полным объемом пор, находящимся в диапазоне от примерно 0,7 до примерно 1,2 см3/г; и (v) совместимостью с соединением олова(II), находящейся в диапазоне от примерно 70 до примерно 99%. 2. Частицы диоксида кремния по п. 1, где частицы диоксида кремния отличаются БЭТ-поверхностью, находящейся в диапазоне от примерно 1,5 до примерно 7 м2/г. 3. Частицы диоксида кремния по любому из пп. 1-2, где частицы диоксида кремния отличаются насыпной плотностью после уплотнения, находящейся в диапазоне от Стр.: 1 A 2 0 1 9 1 2 1 7 1 7 (54) ЧАСТИЦЫ ДИОКСИДА КРЕМНИЯ, СОВМЕСТИМЫЕ С СОЕДИНЕНИЕМ ДВУХВАЛЕНТНОГО ОЛОВА(II) 2 0 1 9 1 2 1 7 1 7 (86) Заявка PCT: R U (43) Дата публикации заявки: 19.01.2021 Бюл. № 2 (72) Автор(ы): ГАЛЛИС Карл У. (US), ХАГАР Уильям Дж. (US), НАССИВЕРА Терри У. (US), ДОЛАН Лоуренс Эдвард (US), МИДХА Санджив (US), ШНАЙДЕРМАН Эва (US) примерно 40 до ...

Oligomer-grafted nanofillers and advanced composite materials

Organized clay complex, method for producing the same, and resin complex containing organized clay complex

Disclosed is a method for producing an organized clay complex, wherein a step for cation exchanging an interlayer metal cation of a layered clay mineral to an organic onium ion by swelling the layered clay mineral with water or an aqueous solvent and then adding and mixing thereinto an emulsion which is obtained in advance by emulsifying a curable resin composition with use of an organic onium salt or with use of an organic onium salt and a nonionic surfactant, and a step for introducing the curable resin composition into the interlayer of the layered clay mineral are performed simultaneously. Also disclosed is an organized clay complex obtained by the method. Further disclosed is a resin molded body obtained by molding/curing such an organized clay complex. In this organized clay complex, the compound introduced into the interlayer of the layered clay mineral does not affect the physical properties of the base into which the organized clay is dispersed. Consequently, this organized clay complex has an expanded interlayer distance, while exhibiting good dispersibility.