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Небесная энциклопедия

Космические корабли и станции, автоматические КА и методы их проектирования, бортовые комплексы управления, системы и средства жизнеобеспечения, особенности технологии производства ракетно-космических систем

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Мониторинг СМИ

Мониторинг СМИ и социальных сетей. Сканирование интернета, новостных сайтов, специализированных контентных площадок на базе мессенджеров. Гибкие настройки фильтров и первоначальных источников.

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Поддерживает ввод нескольких поисковых фраз (по одной на строку). При поиске обеспечивает поддержку морфологии русского и английского языка
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Применить Всего найдено 5994. Отображено 100.
08-03-2012 дата публикации

Method for making single-phase anatase titanium oxide

Номер: US20120058887A1
Принадлежит: Hong Kong Polytechnic University HKPU

This invention relates to methods of making single phase nanocrystalline titanium dioxide. It is hereby provided a method for preparing single-phase anatase type titanium dioxide photocatalyst having a particle size of nano level at near room temperatures without the need for a sintering process at high temperatures.

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17-05-2012 дата публикации

Photocatalytic Nanocomposite Material

Номер: US20120122668A1
Принадлежит: Arcelik AS

The present invention relates to a photocatalytic nanocomposite material, wherein the realization of the optimal wavelength for optical activation is controlled and accordingly is designed to work together with a LED operating at the wavelength for yielding the maximum efficiency.

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24-05-2012 дата публикации

Black composite particle, black resin composition, color filter substrate and liquid crystal display

Номер: US20120128898A1
Принадлежит: TORAY INDUSTRIES INC

Disclosed are black composite particles having a high light-shielding performance suitable as a black component such as a black matrix in a color filter. Further disclosed is a black resin composition from which a black matrix having a high light-shielding performance can be formed. The black composite particles are represented by the composition formula: TiNxOy.zX (wherein X is a metal atom such as silver; x is a number greater than 0 and less than 2; y is a number not less than 0 and less than 2; and z is a number greater than 0 and less than 10). The black resin composition comprises at least a light shielding agent, a resin, and a solvent and comprises the black composite particles as the light shielding agent.

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31-05-2012 дата публикации

Dispersion Liquid of Core-Shell Type Composite Oxide Fine Particles, Process for Producing the Dispersion Liquid, and Coating Composition Containing the Fine Particles

Номер: US20120132108A1
Принадлежит: JGC Catalysts and Chemicals Ltd

Core-shell type composite oxide fine particles are described in which the core particles are oxide fine particles or composite oxide fine particles that do not contain silicon and/or aluminum as main components, and the surface of the core particles is covered with a shell including a composite oxide that contains silicon and aluminum as main components, the shell containing silicon and aluminum in a weight ratio in terms of oxides, SiO 2 /Al 2 O 3 , in the range of 2.0 to 30.0. A dispersion liquid of the core-shell type composite oxide fine particles exhibits very high stability.

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14-06-2012 дата публикации

Surface modified pigment

Номер: US20120148648A1
Принадлежит: Kobo Products Inc

A composition comprising a pigment particle that is coated with a cationic material and isopropyl titanium triisostearate. The pigment particle can be included in a cleansing composition for deposition on a surface, such as skin.

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19-07-2012 дата публикации

Cosmetic pigments, their production method, and cosmetics containing the cosmetic pigments

Номер: US20120183592A1
Принадлежит: Daito Kasei Kogyo Co Ltd, Toyobo Co Ltd

To provide cosmetic pigments that are human-body friendly with good skin adhesion and that provide good feeling, their production method, and cosmetics containing such cosmetic pigments which provide fresh and enriched feeling accordingly. Pigment surfaces are coated with mannosylerythritol lipid, which is glucolipids, consisting of mannose, sugar alcohol and a fatty acid as shown in the general expression (1) below: (Note: In the general expression, R 1 and R 2 denote aliphatic acyl group with carbon numbers 6 through 20, which can be either same or different. R 3 and R 4 denote hydrogen or acetyl group, which can be either same or different. n denotes an integer in the range of 2 to 4.)

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01-11-2012 дата публикации

Titanium Oxide Spacing by SIP

Номер: US20120277346A1
Принадлежит: Behr Process Corp

A method of making a titanium oxide-containing coating composition comprises attaching an initiator to a pretreated titanium oxide to form an initiator/pretreated titanium oxide complex. The pretreated titanium oxide includes a plurality of pretreated titanium oxide particles which are titanium oxide particles that are pretreated with at least one metal oxide. The initiator/pretreated titanium oxide complex is contacted with a polymerizable unsaturated monomer such that a polymeric encapsulate forms on the initiator/pretreated titanium oxide particles to form polymeric encapsulated titanium oxide particles.

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08-11-2012 дата публикации

Stable Sub-Micron Titania Sols

Номер: US20120283092A1
Автор: David M. Chapman
Принадлежит: Millennium Inorganic Chemicals Inc

The present invention is directed to compositions and processes for the production of stable, alkaline, high solids, low viscosity, low surface tension, low flammability, sub-micron titania sols that have minimal offensive odor and methods of their use. Compositions of the present invention include, for example, mixtures of strong and weak organic bases used as dispersants to stabilize the titania sols. The dispersant mixtures have been found to result in relatively high titania solids content, low surface tension, low viscosity suspensions that are low in flammability. Sols produced according to the present invention can be used, for example, in catalytic applications such as catalyst supports for diesel emission control, or in pollutant photocatalyst applications in which it is desirable to have the titania in sol form.

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29-11-2012 дата публикации

Method for preparing organic-inorganic composite materials

Номер: US20120302682A1
Принадлежит: NANJING TECH UNIVERSITY

A method for preparing organic-inorganic composite materials is provided. It is a dispersion method that the inorganic phase is introduced into the polymer matrix uniformly. The core-shell structure, in which the inorganic materials are core and the organic materials are shell, is formed by first wrapping the inorganic materials with the organic materials in the same reactor. Therefore, the match between the polarity of inorganic phase and the polarity of polymer phase is increased.

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03-01-2013 дата публикации

Organic/inorganic composite filler and manufacturing method therefor

Номер: US20130005846A1
Принадлежит: Tokuyama Dental Corp

Disclosed is an organic/inorganic composite filler that contains: inorganic agglomerated particles comprising agglomerations of inorganic primary particles having a mean diameter between 10 and 1000 nm; an organic resin phase that covers the surface of each inorganic primary particle and binds the inorganic primary particles to each other; and intra-agglomerate voids, formed between the organic resin phase covering the surface of each inorganic primary particle, with a pore volume (here, “pore” refers to holes with diameters between 1 and 500 nm) between 0.01 and 0.30 cm 3 /g as measured by mercury intrusion porosimetry. Also disclosed is a method for manufacturing the above organic/inorganic composite filler.

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21-03-2013 дата публикации

Multi-phase particulates, method of making, and composition containing same

Номер: US20130071682A1
Принадлежит: PPG Industries Ohio Inc

Provided is a method of preparing a multi-phase particulate. The method includes: (1) blending together (a) a dispersed phase component of a metal, a metal oxide, an organometallic compound, salts thereof, and/or mixtures thereof, and (b) a bulk phase component of an inorganic material different from the dispersed phase component to form an admixture; and (2) dry-milling and/or compressing the admixture for a time and at a pressure sufficient to disperse the dispersed phase component in and bind the dispersed phase component to the bulk phase component, thereby forming a multi-phase particulate. Coating compositions including the multi-phase particulate also are provided.

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04-04-2013 дата публикации

Microspheres and photoprotective personal care composition comprising same

Номер: US20130084318A1
Принадлежит: Conopco Inc

The invention relates to photoprotective cosmetic compositions comprising microspheres and a process to prepare them. In particular, the invention is especially effective in protecting the skin against visible solar radiation while ensuring a highly acceptable even skin tone and appearance. The present inventors have developed a microsphere with hollow interior and shell of a material having a specific optical property and specific thickness and coated with another material having a different specific optical property, a combination of which gives the microsphere surprising benefits both in terms of protection from the harmful sun rays while giving a pleasing skin appearance when these microspheres are incorporated in topical compositions.

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11-04-2013 дата публикации

Water swellable polymer materials

Номер: US20130087736A1
Принадлежит: UNIVERSITY OF SYDNEY

The invention provides a method of preparing an aqueous dispersion of polymer encapsulated particulate material, the method comprising: providing a dispersion of the particulate material in a continuous aqueous phase, the dispersion comprising RAFT agent as a stabiliser for the particulate material; and polymerising ethylenically unsaturated monomer under the control of the RAFT agent to form polymer at the surface of the dispersed particulate material, thereby providing the aqueous dispersion of polymer encapsulated particulate material; wherein polymerisation of the ethylenically unsaturated monomer comprises: (a) polymerising a monomer composition that includes ionisable ethylenically unsaturated monomer so as to form a base responsive water swellable RAFT polymer layer that encapsulates the particulate material; and (b) polymerising a monomer composition that includes non-ionisable ethylenically unsaturated monomer so as to form an extensible, water and base permeable RAFT polymer layer that encapsulates the base responsive water swellable RAFT polymer layer.

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30-05-2013 дата публикации

PROCESS OF MAKING A WATER DISPERSIBLE TITANIUM DIOXIDE PIGMENT USEFUL IN PAPER LAMINATES

Номер: US20130133552A1
Принадлежит: E I DU PONT DE NEMOURS AND COMPANY

The present invention relates to a process for making a titanium dioxide pigment having consisting of titanium dioxide and single layer of inorganic surface treatment consisting of aluminum phosphate wherein the pigment is characterized by and isoelectric point which is greater than pH 6 and a negative zeta potential of at a pH of 7.5 or more. 114-. (canceled)15. A process for making a water dispersible titanium dioxide slurry comprising:(a) mixing dry titanium dioxide pigment with water to form a first mixture having a pigment concentration of from about 14 to 40 weight percent based on the weight of the first mixture then adjusting the pH of this first mixture to about 7 with aqueous sodium hydroxide;(b) heating the first mixture of step a) to a temperature of about 40 C to form a heated first mixture;(c) adding to the heated first mixture about 0.15 to 0.65 moles of a phosphoric acid per kilogram of dry titanium dioxide pigment and a sodium aluminate aqueous solution to form a second mixture comprising aluminum phosphate, wherein the phosphoric acid and the sodium aluminate aqueous solutions are added to the heated first mixture at a rate such that the pH of the second mixture is maintained at about 5 to 8 and the second mixture is substantially free of zirconia and/or silica;(d) curing the second mixture for about 10 to 30 minutes to form a cured mixture;(e) filtering the cured mixture and recovering, washing, drying, and fluid energy milling a treated titanium dioxide pigment comprising aluminum phosphate;(f) blending the treated titanium dioxide pigment comprising aluminum phosphate with water to form a third mixture;(g) adjusting the pH of the third mixture to form a slurry wherein the slurry comprises 70 to 80 percent by weight of the treated titanium dioxide pigment based on the weight of the slurry.16. The process of wherein in step (c) the addition of the sodium aluminate aqueous solution is such that the ratio of the moles of a phosphorous to the moles ...

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13-06-2013 дата публикации

Corrosion inhibiting pigments and methods for preparing the same

Номер: US20130145957A1

A pigment includes reservoirs of encapsulated corrosion inhibitors and/or biocides for active corrosion and/or antifouling protection of metallic and polymeric products and structures, wherein the reservoirs have average dimensions of 10-50000 nm and comprise a porous surface/interface, a porous or empty interior and stimuli-sensitive stoppers that release an encapsulated inhibitor or biocide outside the reservoir upon action of a stimulus selected from the group consisting of an external electromagnetic field, changes in local pH, ionic strength and ambient temperature, wherein the stimuli-sensitive stoppers result from a chemical or physical interaction between encapsulated corrosion inhibitor and/or biocide or encapsulated solvent/dispersing agent and an additional external compound and prevent release of an encapsulated inhibitor or biocide towards an exterior of the reservoir in the absence of the stimulus.

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13-06-2013 дата публикации

Bioactive compositions from theacea plants and processes for their production and use

Номер: US20130146481A1
Автор: Michael Koganov
Принадлежит: AKZO NOBEL SURFACE CHEMISTRY LLC

The present invention relates to isolated bioactive compositions containing bioactive fractions derived from Theacea plants. The present invention also relates to bioactive topical formulations containing the bioactive compositions. The present invention further relates to methods of using the bioactive compositions of the present invention, including, for example, methods for inhibiting inflammatory activity in skin tissue of a mammal, for protecting skin tissue of a mammal from ultraviolet light-induced damage, and for normalizing skin disorders in skin tissue of a mammal. The present invention also relates to methods for isolating bioactive fractions derived from cell juice or a cell walls component a Theacea plant.

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13-06-2013 дата публикации

FIVE-LAYERED PIGMENTS

Номер: US20130149363A1
Принадлежит: Merck Patent GmBH

The present invention relates to five-layered pigments based on multicoated platelet-shaped substrates which comprise a layer sequence comprising 2. The five-layered pigment according to claim 1 , wherein the platelet-shaped substrate is natural or synthetic mica claim 1 , glass claim 1 , or AlO claim 1 , SiOor TiOplatelets.3. The five-layered pigment according to claim 1 , wherein layer (C) is SiO claim 1 , AlO claim 1 , AlO(OH) claim 1 , BO claim 1 , MgF claim 1 , MgSiOor a mixture thereof.4. The five-layered pigment according to claim 1 , having an outer protective layer (F) increasing light claim 1 , temperature and weather stability.5. A process for the preparation of a five-layered pigment according to claim 1 , comprising coating the substrates by a wet-chemical method with hydrolytic decomposition of metal salts in aqueous medium.6. In a paint claim 1 , coating claim 1 , powder coating claim 1 , printing ink claim 1 , security printing ink claim 1 , plastic claim 1 , ceramic material claim 1 , glass claim 1 , dopants for laser marking of paper or plastic claim 1 , cosmetic formulation claim 1 , pigment preparation or dry pigment preparation comprising a luster or effect pigment claim 1 , the improvement wherein the luster or effect pigment is a five-layered pigment according to .7. A pigment preparation comprising at least one binder claim 1 , and at least one five-layered pigment according to .8. A Pigment preparation according to claim 7 , which is a dry preparation.9. The dry preparation according to claim 8 , comprising from 0 to 8% by weight of water and/or a solvent or solvent mixture.10. The dry preparation according to claim 8 , in the form of pellets claim 8 , granules claim 8 , chips or briquettes.11. A hydrophilic claim 1 , hydrophobic or lipophilic cosmetic formulation comprising at least one five-layered pigment according to .12. In a nail varnish claim 1 , lipstick claim 1 , compact powder claim 1 , gel claim 1 , lotion claim 1 , soap or ...

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01-08-2013 дата публикации

Filler composition and method of producing composite materials

Номер: US20130192778A1

A modified filler composition for use in composites, such as paper and paper board, which is produced by reacting a filler material with a binder and a reactant material. Also, a method to produce composites, such as paper and paperboard, produced containing the modified filler composition is disclosed.

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01-08-2013 дата публикации

Electrophoretic dispersion

Номер: US20130193385A1
Автор: Haiyan Gu, Hui Du, Yu Li
Принадлежит: Sipix Imaging Inc

The present invention is directed to an electrophoretic dispersion comprising charged pigment particles dispersed in a solvent or solvent mixture, wherein the pigment particles have an average aggregation size more than 2 times their primary size. The electrophoretic dispersion of the present invention is capable of improving image bistability through adjusting the aggregation size of the charged pigment particles.

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22-08-2013 дата публикации

Encapsulated cross-linked pigment dispersions

Номер: US20130214197A1
Автор: Harry Joseph Spinelli
Принадлежит: EI Du Pont de Nemours and Co

The present disclosure provides pigment dispersions containing a dispersant, and a pigment coated by a polymer that is cross-linked with a crosslinker. The polymer swells in an application medium resulting in improved, stability for the pigment dispersions.

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29-08-2013 дата публикации

Preparation method of carbon modified filler

Номер: US20130221266A1
Принадлежит: Individual

A preparation method of carbon modified filler is provided. The method is: putting the fillers into the reaction zone of a reactor, starting the first heating-up to 400-500° C. under the protective atmosphere at first, then introducing hydrogen after the heating-up; starting the second heating-up to 600-1200° C. after introducing hydrogen and simultaneously introducing the mixture of hydrogen and carbon source gas, keeping at the terminal temperature for 0.1-5 hours, introducing nitrogen and stopping heating after the reaction, cooling, and then getting the carbon modified filler. The above method can obtain a friction material with good mechanical properties, excellent friction and wear performances, stable friction coefficient at high temperature, good braking force and no heat recession.

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26-09-2013 дата публикации

Methods Of Modifying Metal-Oxide Nanoparticles

Номер: US20130253161A1
Принадлежит:

Methods employing acidic and basic catalysts are disclosed, and generally entail hydrolysis and condensation reactions of silicon based components. The methods are useful for forming siloxane-modified metal-oxide nanoparticles, such as modified ZrOnanoparticles. The siloxane-modified metal-oxide nanoparticles, and products including the siloxane-modified metal-oxide nanoparticles, can be used to form various products, such as lenses or encapsulants for making various devices, such as, but not limited to, light emitting diodes (LEDs). 2. The method as set forth in claim 1 , wherein the metal-oxide nanoparticles:{'sub': 2', '2, 'i) are ZrOnanoparticles or TiOnanoparticles;'}{'b': '50', 'ii) have a mean particle diameter (D) of from 1 to 100 nm; or'}iii) both i) and ii).3. (canceled)4. The method as set forth in claim 1 , wherein the alkoxysilane is MePhSi(OMe)or PhSi(OMe) claim 1 , where Ph is a phenyl group and Me is a methyl group.5. The method as set forth in claim 1 , wherein the organosiloxane is (ViMeSi)O claim 1 , where Vi is a vinyl group and Me is a methyl group.6. The method as set forth in claim 1 , wherein the silane is ViMeSiCl claim 1 , where Vi is a vinyl group and Me is a methyl group.7. The method as set forth in claim 1 , further comprising the step of removing water from the intermediate composition after step II) for inducing step III).8. The method as set forth in claim 1 , wherein the intermediate composition includes methanol claim 1 , and further comprising the step of removing at least a portion of the methanol from the intermediate composition prior to step III).9. The method as set forth in claim 1 , further comprising the step of applying heat for a period of time during at least one of steps II) and III).10. The method as set forth in claim 1 , wherein at least one of steps II) and III) is conducted in the presence of a solvent different than the water (d).11. The method as set forth in claim 1 , wherein the siloxane-modified metal-oxide ...

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02-01-2014 дата публикации

Method for the Surface Treatment of Inorganic Pigment Particles

Номер: US20140000483A1
Принадлежит: Kronos International, Inc.

The invention relates to a method for the surface treatment of inorganic pigment particles with agglomerates of fine primary particles or single crystals of inorganic compounds, particularly of oxides or sulphates. The method is characterized in that the inorganic compounds are first precipitated from an aqueous solution under suitable pH conditions in a separate vessel in the form of fluffily structured agglomerates and/or single crystals. The precipitation product is subsequently added to an aqueous suspension of inorganic pigment particles. The method is particularly suitable for the surface treatment of titanium dioxide particles, in order to achieve high hiding power or high opacity when used in emulsion paints or laminates. 1. A method for the surface treatment of inorganic pigment particles , comprising the steps of:a) Providing an aqueous suspension of inorganic pigment particles;b) Precipitating one or more inorganic compounds from a second aqueous solution in a separate vessel to form a precipitation product, where the precipitation product consists of agglomerates of fine primary particles and/or of single crystals;c) Adding the precipitation product to the aqueous suspension of inorganic pigment particles.2. The method of wherein the inorganic pigment particles are titanium dioxide particles.3. The method of wherein the precipitation product has a fluffy agglomerate structure.4. The method of wherein the precipitated inorganic compounds are selected from the group consisting of oxides claim 1 , sulphates and mixtures thereof.5. The method of wherein the precipitated inorganic compounds are selected from the group comprising oxides of silicon claim 4 , aluminum claim 4 , zirconium or titanium claim 4 , and mixtures thereof.6. The method of wherein the precipitated claim 1 , fine primary particles are predominantly crystalline.7. The method of wherein the inorganic pigment particles have previously been surface-treated.8. The method of further comprising ...

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02-01-2014 дата публикации

Composite Pigments Comprising Titanium Dioxide and Carbonate and Method for Producing

Номер: US20140000484A1
Принадлежит:

The invention relates to the manufacture of pigment-containing composite pigment particles containing titanium dioxide pigment particles and at least one inorganic and/or organic filler as extender, as well as calcium carbonate that is precipitated in the process, and their use for improving the pigment light-scattering efficiency in coatings, plastics and laminates. The extender is preferably selected from Ca-, Ca—Mg- and Mg-carbonates, natural and synthetic silicon dioxide and oxides and are manufactured in a combined process of precipitation and dispersion. Depending on the combination selected, the use of composite pigment particles according to the invention permits pigment savings with little or no loss of optical properties. Alternatively, if the pigment content remains unchanged, it is possible to achieve better values, e.g. for tinting strength. Particularly, a part or the whole TiOquantity in the user system can be replaced by the composite pigment particles according to the invention. 1. A composite pigment , comprising:titanium dioxide particles;at least one inorganic and/or organic extender;calcium carbonate in a quantity of less than 30% by weight, referred to composite pigment; andwherein the calcium carbonate is at least partially precipitated in situ.2. The composite pigment of claim 1 , wherein the titanium dioxide particles are surface-treated particles.3. The composite pigment of claim 1 , wherein the titanium dioxide particles are untreated titanium dioxide pigment particles.4. The composite pigment of claim 1 , wherein the inorganic extender is selected from the group consisting of calcium carbonate claim 1 , calcium-magnesium carbonates claim 1 , magnesium carbonates claim 1 , sulphates claim 1 , natural phosphates claim 1 , oxides claim 1 , hydroxides claim 1 , silicon oxide claim 1 , silicates claim 1 , alumosilicates claim 1 , perlite claim 1 , glass powder claim 1 , and mixtures thereof.5. The composite pigment of claim 4 , wherein the ...

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13-02-2014 дата публикации

Pigment paint for an exterior material having good weather resistance and method for manufacturing same

Номер: US20140041551A1
Принадлежит: Cqv Co ltd

The present invention relates to a pigment paint for an exterior material and to a method for manufacturing the same. The pigment paint comprises: a flake matrix, a first metal oxide layer coated on the upper portion of the transparent matrix, an oxide layer containing MgO—SiO 2 coated on the upper portion of the first metal oxide layer, and a second metal oxide layer coated on the upper portion of the oxide layer. In order to ensure humidity resistance and weather resistance required for a lustrous pigment paint for exterior materials, a cerium layer and an aluminum oxide layer are further coated. Properties such as high luminance, high chromaticity, and high gloss, which could not be achieved using conventional techniques, can be achieved and a pigment paint having a multi-colored pearl luster can be provided.

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13-03-2014 дата публикации

Infrared-Reflecting Pigment Based on Titanium Dioxide, and a Method for Its Manufacture

Номер: US20140073729A1
Принадлежит: Kronos International, Inc.

The invention relates to rutile titanium dioxide pigment particles that are capable of reflecting infrared radiation to a high degree and also display pigmenting properties, as well as a method for their manufacture. The particles have a mean particle size of 0.4 to 1.0 μm and are doped with zinc and potassium, but not with aluminium. Preferably, the particles have a compact particle form with a preferred height:width ratio of 1.5:1. The particles are preferably manufactured by the familiar sulphate process for manufacturing titanium dioxide, and are optionally subjected to inorganic and/or organic post-treatment following calcining. Preferably, the rutile titanium dioxide particles are suitable for manufacturing heat-insulating paints, coatings or plastics as well as for instance plasters or paving stones. 1. Infrared-reflecting pigment comprising rutile titanium dioxide particles having a particle size din the range of from about 0.4 to about 1 μm and wherein the particles are doped with zinc and potassium and not doped with aluminium.2. The particles of claim 1 , wherein the particles contain from about 0.1 to about 0.8 weight percent zinc calculated as ZnO and based on the weight of titanium dioxide in the particles.3. The particles of claim 2 , wherein the particles contain from about 0.2 to about 0.4 weight percent zinc calculated as ZnO and based on the weight of titanium dioxide in the particles.4. The particles of claim 3 , wherein the particles contain from about 0.2 to about 0.25 weight percent zinc calculated as ZnO and based on the weight of titanium dioxide in the particles.5. The particles of claim 2 , wherein the particles contain from about 0.1 to about 0.4 weight percent potassium calculated as KO and based on the weight of titanium dioxide in the particles.6. The particles of wherein the titanium dioxide particles have a maximum height:width ratio of about 1.5:1.7. The particles of claim 1 , wherein the particles contain from about 0.1 to about 0. ...

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20-03-2014 дата публикации

Electroconductive particles

Номер: US20140077136A1
Принадлежит: Mitsui Mining and Smelting Co Ltd

An electroconductive particle having a core particle and a tin oxide-containing coating layer on the core particle. The tin oxide of the coating layer has a crystallite size of 70 to 200 Å. The electroconductive particle preferably has a ratio of R 3 to R 1 of 1 to 250, wherein R 1 and R 3 are respective surface resistivities of electroconductive films formed of a coating composition containing the electroconductive particle and prepared by 1-hour dispersing and 3-hour dispersing, respectively. The coating layer preferably comprises dopant element-free, electroconductive tin oxide.

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27-03-2014 дата публикации

Hydrophilic treated pigments dispersible in a cosmetic composition

Номер: US20140086861A1
Принадлежит: Sensient Cosmetic Technologies SAS

The invention relates to a pigment composition comprising: a pigment, an additive of the following formula (I): to a method for preparation thereof, and to the cosmetic uses thereof.

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01-01-2015 дата публикации

SURFACE COATED PIGMENT PARTICLES

Номер: US20150000565A1
Принадлежит:

Disclosed is a method of surface coating pigment particles, comprising treating uncoated titanium dioxide particles with a reaction product of a silicon oxide with an alkaline earth metal salt to form a coating comprising an oxide of silicon and the alkaline earth metal. The particles may also be treated with aluminum compounds to produce an aluminum oxide in the coating. 1. Pigment particles coated at least in part with a coating comprising a reaction product of reactants comprising an oxide of silicon and a salt of an alkaline earth metal.2. The pigment particles of claim 1 , wherein the pigment particles are uncoated prior to being at least partially coated with the coating.3. The pigment particles of claim 2 , wherein the pigment comprises titanium dioxide.4. The pigment particles of claim 3 , wherein the alkaline earth metal comprises calcium and/or magnesium.5. The pigment particles of claim 3 , wherein the coating further comprises an aluminum compound.6. The pigment particles of claim 5 , wherein the aluminum compound is present at least in an outermost portion of the coating.7. The pigment particles of claim 6 , further comprising an organic compound covering at least a portion of the coating.8. The pigment particles of wherein the alkaline earth metal compound comprises 0.3-2.0 wt. % of the total weight of the pigment particles calculated as an oxide of the alkaline earth metal.9. The pigment particles of claim 3 , wherein the silicon oxide comprises 0.1-1.5 wt. % of the total weight of the pigment particles calculated as SiO.10. The pigment particles of claim 5 , wherein the aluminum compound comprises 0.5-3.0 wt. % of the total weight of the pigment particles calculated as AlO.11. The pigment particles of claim 3 , wherein the uncoated titanium dioxide particles are produced by a sulfate process.12. A method of preparing pigment particles comprising treating uncoated pigment particles with a silicon compound and an alkaline earth metal compound to form ...

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02-01-2020 дата публикации

SMALL PARTICLE COMPOSITIONS AND ASSOCIATED METHODS

Номер: US20200001303A1
Автор: Dobbs Robert J.
Принадлежит: Primet Precision Materials, Inc.

Milling methods that use grinding media particles formed of a ceramic material having an interlamellar spacing of less than 1250 nm. 1. Grinding media comprising:grinding media particles formed of a ceramic material, the ceramic material having an interlamellar spacing of less than 1250 nm.2. Grinding media comprising:grinding media particles comprising a core material and a coating formed on the core material, the coating including a plurality of layers, at least one of the layers having a thickness of less than 100 nanometers.3. The grinding media of claim 2 , wherein at least one of the layers has a thickness of less than 10 nanometers.4. The grinding media of claim 2 , wherein multiple layers have a thickness of less than 10 nanometers.5. The grinding media of claim 2 , wherein the coating includes at least 10 layers.6. The grinding media of claim 2 , wherein a first layer comprises zirconium and a second layer claim 2 , formed on the first layer claim 2 , comprises aluminum.7. The grinding media of claim 2 , wherein the particles have an average size of less than 150 micron.8. The grinding media of claim 2 , wherein the core material has a density of greater than 5 grams/cubic centimeter.9. Grinding media comprising:grinding media particles formed of a nanocrystalline composite comprising a plurality of nanoparticles dispersed in a matrix material.10. The grinding media of claim 9 , wherein the nanoparticles have an average particle size of less than 10 nanometers.11. The grinding media of claim 12 , wherein the nanoparticles comprise a transition metal nitride.12. The grinding media of claim 12 , wherein the matrix material comprises a nitride.13. A method comprising:milling inorganic feed particles using grinding media to produce an inorganic milled particle composition having an average particle size of less than 100 nm and a contamination level of less than 500 ppm, the feed particles having an average particle size of greater than 10 times the average ...

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05-01-2017 дата публикации

SURFACE TREATMENT OF PARTICLES AND THEIR USE

Номер: US20170002181A1
Принадлежит: EVONIK DEGUSSA GmbH

Surface treatment of titanium dioxide, barium sulfate, zinc sulfide, and/or lithopone particles, and mixtures of said particles with specific alkoxylated siloxanes for the improvement of dispersion in plastics. 2. The particle as claimed in claim 1 , wherein{'sup': 1', '3, 'sub': 2', 'p', 'x', 'y', 'z, 'Ridentically or differently is —(CH)—O-EO—PO—BO—R,'}{'sup': '1', 'with the proviso that in Rthe total number of carbon atoms and oxygen atoms is at least 70,'}EO is oxyethylene,PO is oxypropylene,BO is oxybutylene,x is from 0 to 20,y is from 5 to 100,z is from 0 to 20,p is from 2 to 4.3. The particle as claimed in claim 1 , wherein a numeric ratio of a to b is from 8:1 to 18:1.4. The particle as claimed in claim 2 , index wherein x is between 0.05 and 1.2 times a sum of y and z.5. The particle as claimed in claim 2 , whereinR is methyl,A is from 80 to 95,B is from 5 to 8,{'sup': '3', 'Ris hydrogen,'}x is from 3 to 5,y is from 10 to 25,z is 0.6. The particle as claimed in claim 1 , which is a surface-treated is TiOparticle.7. The particle as claimed in claim 1 , which has a dust value of at most 80 mg per 100 g of surface-treated particles.9. A process for producing a polymer composition claim 1 , comprising mixing the particle of with a polymer.10. The process as claimed in claim 9 , wherein the polymer composition is processed to give a plastic molding or a plastic film.11. A composition claim 1 , comprising a polymer claim 1 , which comprises a particle as claimed in .12. The composition as claimed in claim 11 , wherein the polymer is a thermoset or thermoplastic.13. The composition as claimed in claim 11 , which is a masterbatch claim 11 , a plastic molding claim 11 , or a plastic film.14. The particle of claim 2 , which is a surface-treated TiOparticle.15. The particle of claim 1 , whereinZ is a branched alkylene moiety or an unbranched alkylene moiety comprising 3 carbon atoms,m is 3,n is 1 or 2,o is 0,a is from 30 to 170, andb is from 2 to 30,where 0.05 to 1% ...

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04-01-2018 дата публикации

AQUEOUS CORROSION RESISTANT COATINGS WITH SURFACE-HYDROPHOBIC INORGANIC PARTICLES

Номер: US20180002532A1
Принадлежит:

Aqueous coating compositions providing enhanced anticorrosive and water-resistant properties. The anticorrosive coating comprises water borne resin, surface-hydrophobic inorganic pigments, and/or surface-hydrophobic inorganic extenders. 1. A corrosion resistant coating comprising:a. a water borne resin;b. water; andc. one or more particles selected from the group comprising an inorganic particle, extender, and combination thereof; wherein the one or more particle comprises a hydrophobic coating selected from the group consisting of polyols, organosiloxanes, organosilanes, alkylcarboxylic acids, alkylsulfonates, organophosphates, organophosphonates, fluoropolymers and mixtures thereof.2. A corrosion resistant coating comprising:a. water borne resin;b. water;c. one or more particles selected from the group comprising an inorganic particle, extender, and combination thereof; wherein the one or more particle comprises a hydrophobic coating selected from the group consisting of polyols, organosiloxanes, organosilanes, alkylcarboxylic acids, alkylsulfonates, organophosphates, organophosphonates, fluoropolymers and mixtures thereof; andd. at least one solvent.3. The corrosion resistant coating of wherein the hydrophobic coating reduces corrosion and water penetration ability.4. The corrosion resistant coating of wherein the hydrophobic coating reduces corrosion and water penetration ability.5. The corrosion resistant coating of wherein the at least one solvent comprise a solvent having an octanol-water partition coefficient of 1 to 5.6. The corrosion resistant coating of wherein the at least one solvent is selected from the group consisting of ketones claim 2 , alcohols claim 2 , esters and ethers of alcohols claim 2 , aromatics claim 2 , glycol ethers and esters.7. The corrosion resistant coating of wherein the at least one solvent is selected from the group consisting of propylene glycol n-butyl ether claim 2 , dipropylene glycol n-butyl ether claim 2 , tripropylene ...

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03-01-2019 дата публикации

ELECTROSTATIC INK COMPOSITION

Номер: US20190002721A1
Автор: Masoud Emad
Принадлежит:

There is provided an electrostatic ink composition comprising chargeable particles comprising white pigment particles having a basic species on their surface; and a charge director; wherein the white pigment particles are present in an amount of at least 75 wt % based on the total weight of the non-volatile solids in the electrostatic ink composition. A method of manufacturing an electrostatic ink composition and a printed medium are also described. 1. An electrostatic ink composition comprising:a) chargeable particles comprising white pigment particles having a basic species on their surface; and 'wherein the white pigment particles are present in an amount of at least 75 wt % based on the total weight of the non-volatile solids in the electrostatic ink composition.', 'b) a charge director;'}2. The electrostatic ink composition according to claim 1 , further comprising a liquid carrier.3. The electrostatic ink composition according to claim 1 , further comprising a thermoplastic resin.4. The electrostatic ink composition according to claim 1 , further comprising a dispersant.5. The electrostatic ink composition according to claim 1 , wherein the basic species on the surface of the white pigment particles is an inorganic species.6. The electrostatic ink composition according to claim 1 , wherein the white pigment particles comprise a first metal oxide and wherein the species on the surface comprises a second metal oxide.7. The electrostatic ink composition of claim 1 , wherein the white pigment particles comprise TiOparticles and wherein the species on the surface comprises alumina and/or zirconia.8. The electrostatic ink composition according to claim 5 , wherein the white pigment particles are also surface treated with an organic species selected from silicones and siloxanes.9. The electrostatic ink composition according to claim 1 , wherein the white pigment is present in an amount of at least 85 wt % based on the total weight of the non-volatile solids in the ...

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01-01-2015 дата публикации

Rare earth metal compounds, methods of making, and methods of using the same

Номер: US20150004086A1
Принадлежит: Spectrum Pharmaceuticals Inc

Rare earth metal compounds, particularly lanthanum, cerium, and yttrium, are formed as porous particles and are effective in binding metals, metal ions, and phosphate. A method of making the particles and a method of using the particles is disclosed. The particles may be used in the gastrointestinal tract or the bloodstream to remove phosphate or to treat hyperphosphatemia in mammals. The particles may also be used to remove metals from fluids such as water.

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04-01-2018 дата публикации

PLASMONIC METAL NITRIDE AND TRANSPARENT CONDUCTIVE OXIDE NANOSTRUCTURES FOR PLASMON ASSISTED CATALYSIS

Номер: US20180003865A1
Принадлежит: PURDUE RESEARCH FOUNDATION

A nanostructured material system for efficient collection of photo-excited carriers is provided. They system comprises a plurality of plasmonic metal nitride core material elements coupled to a plurality of semiconductor material elements. The plasmonic nanostructured elements form ohmic junctions at the surface of the semiconductor material or at close proximity with the semiconductor material elements. A nanostructured material system for efficient collection of photo-excited carriers is also provided, comprising a plurality of plasmonic transparent conducting oxide core material elements coupled to a plurality of semiconductor material elements. The field enhancement, local temperature increase and energized hot carriers produced by nanostructures of these plasmonic material systems play enabling roles in various chemical processes. They induce, enhance, or mediate catalytic activities in the neighborhood when excited near the resonance frequencies. 1. A nanostructured material system for efficient collection of photo-excited carriers , comprising:a plurality of plasmonic metal nitride core material elements coupled to a corresponding plurality of semiconductor material elements.2. The system of claim 1 , wherein the plasmonic nanostructured elements form ohmic junctions at the surface of the semiconductor material elements or at close proximity with the semiconductor material elements.3. The system of claim 1 , wherein the plasmonic metal nitride core material is titanium nitride (TiN).4. The system of claim 3 , wherein the semiconductor is titanium dioxide (TiO) or TiON claim 3 , where 01.7. The system of claim 6 , wherein the semiconductor material elements comprise tantalum pentoxide (TaO).8. The system of claim 5 , ...

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14-01-2021 дата публикации

COMPOSITE OXIDE POWDER AND METHOD FOR PRODUCTION THEREOF

Номер: US20210009432A1
Принадлежит:

Composite oxide fine particles are produced by sol-gel method under conditions in which coarse particles and aggregated particles are unlikely to be generated, and the composite oxide fine particles are further wet-filtered using a filter to remove the coarse particles and the aggregated particles. Then, a salt is added to a dispersion of the composite oxide fine particles to produce weak aggregates of the composite oxide fine particles in the dispersion. A solid content is separated from the dispersion of the composite oxide fine particles containing the aggregates, and then dried. The solid content is easily made finer because no firm aggregates are generated during the drying. That is, composite oxide fine particles containing no coarse particles and aggregated particles are obtained. Use of a known cracking means can further reduce the amount of coarse particles. 17-. (canceled)8. A silica-based composite oxide powder comprising:a composite oxide of silicon and at least one metal selected from the group consisting of titanium and zirconium, the silica-based composite oxide powder having a volume-based cumulative 50% diameter measured by a laser diffraction scattering method in a range of 0.05 μm to 2.0 μm, and a coefficient of variation of 40% or less, whereinin a 5 mass % dispersion of the silica-based composite oxide powder obtained by ultrasonic irradiation (at an output of 40 W for 10 minutes), a content of particles having a particle diameter of 5 μm or more in a particle size distribution obtained by a Coulter counter method is 10 ppm or less on a number basis.9. The silica-based composite oxide powder of claim 8 , whereina content of particles having a particle diameter of 3 μm or more in the particle size distribution obtained by the Coulter counter method is 10 ppm or less on a number basis.10. A surface-treated silica-based composite oxide powder claim 8 , obtained by surface-treating the silica-based composite oxide powder of with a silylating agent ...

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10-01-2019 дата публикации

TITANIUM DIOXIDE PIGMENT AND MANUFACTURING METHOD

Номер: US20190010287A1
Принадлежит:

A titanium dioxide pigment composition comprising a plurality of titanium dioxide particles and a polymer that is associated with the titanium dioxide particles and becomes associated with latex particles in an aqueous based coating formulation to inhibit agglomeration of the titanium dioxide particles while the coating formulation dries is provided. The polymer comprises a water soluble polymer backbone, at least one functional group that is attached to the polymer backbone and has an affinity for titanium dioxide, and at least one hydrophobic functional group that is attached to the polymer backbone and has an affinity for latex. Also provided is a method of manufacturing a titanium dioxide pigment composition. 1. A titanium dioxide pigment composition , comprising:a plurality of titanium dioxide particles; a water soluble polymer backbone having a longitudinal axis, a first point and a second point, wherein said water soluble polymer backbone is a polyoxyalkylene polymer or copolymer;', 'at least one functional group that is attached to said first point of said polymer backbone, has an affinity for titanium dioxide, and is formed by the reaction of said polymer backbone with a compound having an amino group, a carboxylic acid group, or a hydroxyl group, said compound having an amino group, a carboxylic acid group, or a hydroxyl group being selected from the group of a urea, imidazole, an amide, an amino alcohol, an amino acid, an amine, a carboxylic acid, a hydroxyl acid, a polyol, a silane capable of being covalently bonded to titanium dioxide, and a borate capable of being covalently bonded to titanium dioxide; and', 'at least one hydrophobic functional group that is attached to said second point of said polymer backbone, has an affinity for latex, and is selected from the group of a super hydrophobic functional group, and a functional group formed by the reaction of said polymer backbone with an aliphatic compound, an aromatic compound, or an aliphatic- ...

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09-01-2020 дата публикации

ORGANICALLY MODIFIED FINE PARTICLES

Номер: US20200010685A1
Автор: Ajiri Tadafumi
Принадлежит:

A technique for bonding an organic group with the surface of fine particles such as nanoparticles through strong linkage is provided, whereas such fine particles are attracting attention as materials essential for development of high-tech products because of various unique excellent characteristics and functions thereof. Organically modified metal oxide fine particles can be obtained by adapting high-temperature, high-pressure water as a reaction field to bond an organic matter with the surface of metal oxide fine particles through strong linkage. The use of the same condition enables not only the formation of metal oxide fine particles but also the organic modification of the formed fine particles. The resulting organically modified metal oxide fine particles exhibit excellent properties, characteristics and functions. 1. A process for producing organically modified metal oxide nanoparticles , which comprises:producing metal oxide nanoparticles in the coexistence of an organic modifying agent in a supercritical or subcritical hydrothermal synthesis reaction field, thereby forming organically modified metal oxide nanoparticleswherein an optionally substituted or unsubstituted hydrocarbon group is bonded to the surface of each nanoparticle through a linkage selected from the group consisting of a covalent bond, an ether bond, an ester bond, a bond through an N atom, a bond through an S atom, a metal-C— bond, a metal-C═ bond, and a metal-(C═O)— bond.2. The process according to claim 1 , wherein the hydrothermal synthesis reaction field is under supercritical or subcritical water conditions.3. The process according to claim 1 , wherein the hydrothermal synthesis reaction field is under water conditions at the critical pressure or a pressure above the critical point and/or at the critical temperature or a temperature above the critical point.4. The process according to claim 1 , wherein said organically modified metal oxide nanoparticles are formed in a reaction field ...

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09-01-2020 дата публикации

ORGANICALLY MODIFIED FINE PARTICLES

Номер: US20200010686A1
Автор: Ajiri Tadafumi
Принадлежит:

A technique for bonding an organic group with the surface of fine particles such as nanoparticles through strong linkage is provided, whereas such fine particles are attracting attention as materials essential for development of high-tech products because of various unique excellent characteristics and functions thereof. Organically modified metal oxide fine particles can be obtained by adapting high-temperature, high-pressure water as a reaction field to bond an organic matter with the surface of metal oxide fine particles through strong linkage. The use of the same condition enables not only the formation of metal oxide fine particles but also the organic modification of the formed fine particles. The resulting organically modified metal oxide fine particles exhibit excellent properties, characteristics and functions. 1. A process for producing organically modified metal oxide nanoparticles , which comprises:subjecting a metallic compound to a hydrothermal reaction in a reaction field of high-temperature, high-pressure water to form metal oxide nanoparticles; andreacting an organic modifying agent with the surface of the resulting metal oxide nanoparticle to form organically modified metal oxide nanoparticleswherein an optionally substituted or unsubstituted hydrocarbon group is bonded to the surface of each nanoparticle through a linkage selected from the group consisting of a covalent bond, an ether bond, an ester bond, a bond through an N atom, a bond through an S atom, a metal-C— bond, a metal-C═ bond, and a metal-(C═O)— bond.2. The process according to claim 1 , wherein the high-temperature claim 1 , high-pressure water is water under supercritical or subcritical conditions.3. The process according to claim 1 , wherein the high-temperature claim 1 , high-pressure water is water under conditions at the critical pressure or a pressure above the critical point and/or at the critical temperature or a temperature above the critical point.4. The process according ...

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19-01-2017 дата публикации

Preparation method of fluorine-doped lamellar black titanium dioxide nano material

Номер: US20170014811A1
Принадлежит: NORTH CHINA ELECTRIC POWER UNIVERSITY

The method for preparing fluorine-doped lamellar black TiO 2 nanomaterials includes mixing a solution of tetra-n-butyl titanate, n-propanol and hydrofluoric acid together, and then stir the solutions for a period of time. The solution is transferred into an autoclave and reacts at a certain temperature for a period of time. The sample obtained by the reaction is washed and dried. Then, the sample is heated in a protective atmosphere for a period of time so as to produce the fluorine-doped lamellar black TiO 2 nanomaterials. This fluorine-doped lamellar black TiO 2 owns superior optical absorption and electron transport performances.

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19-01-2017 дата публикации

COMPOSITIONS AND PROCESSES FOR IMPROVING PROPERTIES OF FILLERS

Номер: US20170015832A1
Принадлежит: NOVOZYMES A/S

The present invention relates to processes for modifying a filler material comprising treating the filler material with a composition comprising a xyloglucan endotransglycosylase and (a) a polymeric xyloglucan and a functionalized xyloglucan oligomer comprising a chemical group; (b) a polymeric xyloglucan functionalized with a chemical group and a functionalized xyloglucan oligomer comprising a chemical group; (c) a polymeric xyloglucan functionalized with a chemical group and a xyloglucan oligomer; (d) a polymeric xyloglucan and a xyloglucan oligomer; (e) a a polymeric xyloglucan functionalized with a chemical group; (f) a polymeric xyloglucan; (g) a functionalized xyloglucan oligomer comprising a chemical group; or (h) a xyloglucan oligomer; or a composition of (a-h) without a xyloglucan endotransglycosylase, wherein the modified filler material possesses an improved property compared to the unmodified filler material. The present invention also relates to modified filler materials and modified filler materials obtained by such processes. 1. A process for modifying a filler material comprising treating a suspension of the filler material with a composition selected from the group consisting of (a) a composition comprising a xyloglucan endotransglycosylase , a polymeric xyloglucan , and a functionalized xyloglucan oligomer comprising a chemical group; (b) a composition comprising a xyloglucan endotransglycosylase , a polymeric xyloglucan functionalized with a chemical group , and a functionalized xyloglucan oligomer comprising a chemical group; (c) a composition comprising a xyloglucan endotransglycosylase , a polymeric xyloglucan functionalized with a chemical group , and a xyloglucan oligomer; (d) a composition comprising a xyloglucan endotransglycosylase , a polymeric xyloglucan , and a xyloglucan oligomer; (e) a composition comprising a xyloglucan endotransglycosylase and a polymeric xyloglucan functionalized with a chemical group; (f) a composition comprising ...

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19-01-2017 дата публикации

Tailored dispersion and formation of integrated particle systems via ph responsive groups

Номер: US20170015847A1
Принадлежит: Chemours Co TT LLC

This invention provides methods and technology related to increased hiding power of a coating through mediating the interaction of the pigment with other system components including but not limited to other pigment particles, latex paint particles, latex binding particles, and organic or inorganic hollow particles. Organization and spacing are tailored via pH sensitive functionalities hosted on ligands or polymeric spacers that are located at/within the surface of one of the components.

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17-04-2014 дата публикации

TREATED INORGANIC PARTICLE

Номер: US20140102333A1
Автор: Musick Charles David
Принадлежит: E I DU PONT DE NEMOURS AND COMPANY

The disclosure provides a treated inorganic particle, in particular a titanium dioxide particle, having reduced photoactivity, lower acid solubility and improved anti-microbial properties comprising: an inorganic core particle, in particular a titanium dioxide particle; a first treatment of silica, wherein the silica is added in a single step; and a second treatment comprising co-precipitated zinc oxide and alumina. These particles have reduced photoactivity, lower acid solubility and improved anti-microbial properties. 1. A treated inorganic particle having reduced photoactivity and improved anti-microbial properties comprising:(a) an inorganic core particle;(b) a first treatment of silicon compound, wherein the silicon compound is added in a single step; and(c) a second treatment comprising co-precipitated zinc oxide and alumina.2. The treated inorganic particle of wherein the inorganic core particle is titanium dioxide.3. The treated inorganic particle of wherein the silicon compound is silica claim 2 , zinc silicate or borosilicate4. The treated inorganic particle of wherein the silicon compound is silica.5. The treated inorganic particle of wherein the silica is pyrogenically added silica.6. (canceled)7. The treated inorganic particle of wherein the silicon compound is present in the amount of about 0.5 to about 20% by weight claim 1 , based on the total weight of the inorganic core particle.8. The treated inorganic particle of wherein the silicon compound is present in the amount of about 1 to about 7% by weight claim 7 , based on the total weight of the inorganic core particle.9. The treated inorganic particle of wherein the alumina is present in the amount of about 0.05% to 20% by weight calculated as Al2O3 and based on the total weight of the inorganic core particle.10. (canceled)11. The treated inorganic particle of wherein the alumina is present in the amount of about 1% to about 5% by weight calculated as AlOand based on the total weight of the inorganic ...

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16-01-2020 дата публикации

ORGANICALLY MODIFIED FINE PARTICLES

Номер: US20200017691A1
Автор: Ajiri Tadafumi
Принадлежит:

A technique for bonding an organic group with the surface of fine particles such as nanoparticles through strong linkage is provided, whereas such fine particles are attracting attention as materials essential for development of high-tech products because of various unique excellent characteristics and functions thereof. Organically modified metal oxide fine particles can be obtained by adapting high-temperature, high-pressure water as a reaction field to bond an organic matter with the surface of metal oxide fine particles through strong linkage. The use of the same condition enables not only the formation of metal oxide fine particles but also the organic modification of the formed fine particles. The resulting organically modified metal oxide fine particles exhibit excellent properties, characteristics and functions. 1. A process for producing organically modified metal oxide nanoparticles , which comprises:reacting an organic modifying agent with the surface of a metal oxide nanoparticle in a reaction field of high-temperature, high-pressure water to form organically modified metal oxide nanoparticleswherein an optionally substituted or unsubstituted hydrocarbon group is bonded to the surface of each nanoparticle through a linkage selected from the group consisting of a covalent bond, an ether bond, an ester bond, a bond through an N atom, a bond through an S atom, a metal-C— bond, a metal-C═ bond, and a metal-(C═O)— bond.2. The process according to claim 1 , wherein the high-temperature claim 1 , high-pressure water is water under supercritical or subcritical conditions.3. The process according to claim 1 , wherein the high-temperature claim 1 , high-pressure water is water under conditions at the critical pressure or a pressure above the critical point and/or at the critical temperature or a temperature above the critical point.4. The process according to claim 1 , wherein said organically modified metal oxide nanoparticles are formed in a reaction field where ...

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21-01-2021 дата публикации

COMPOSITE PARTICLES AND METHOD FOR PRODUCING COMPOSITE PARTICLES

Номер: US20210017391A1
Принадлежит:

Provided are: composite particles having excellent oxidation resistance; and a method for producing composite particles. The composite particles are obtained by forming a composite of TiN and at least one of Al, Cr, and Nb. In the method for producing composite particles, a titanium powder and a powder of at least one of Al, Cr, and Nb are used as raw material powders and composite particles are produced using a gas phase method. 1. Composite particles in which TiN is combined with at least one of Al , Cr and Nb.2. The composite particles according to claim 1 , wherein when the TiN is combined with the Al claim 1 , a content of the Al is 0.1 to 20 mass %.3. The composite particles according to claim 1 , wherein when the TiN is combined with the Cr claim 1 , a content of the Cr is 0.1 to 20 mass %.4. The composite particles according to claim 1 , wherein when the TiN is combined with the Nb claim 1 , a content of the Nb is 0.1 to 20 mass %.5. A method of producing composite particles in which TiN is combined with at least one of Al claim 1 , Cr and Nb claim 1 , wherein the composite particles are produced using powder of titanium and powder of at least one of Al claim 1 , Cr and Nb as feedstock by means of a gas-phase process.6. The method of producing composite particles according to claim 5 , wherein the gas-phase process is a thermal plasma process claim 5 , a flame process claim 5 , an arc plasma process claim 5 , a microwave heating process or a pulsed wire process.7. The method of producing composite particles according to claim 6 , wherein the thermal plasma process involves a step of supplying carrier gas having the feedstock dispersed therein to a thermal plasma flame and a step of supplying cooling gas to a terminating portion of the thermal plasma flame to thereby produce the composite particles.8. The method of producing composite particles according to claim 7 , wherein the thermal plasma flame is derived from at least one of argon gas and nitrogen gas. ...

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10-02-2022 дата публикации

Titanium dioxide dispersion

Номер: US20220040069A1
Принадлежит: Croda International PLC

The invention provides a dispersion of precursor titanium dioxide particles having an intensity mean peak value particle size, measured by DLS, or a number mean peak value particle size, measured by DLS, in the range from 0.2 to 2.0 μm within a dispersing medium, wherein the particle size distribution of the titanium dioxide particles in dispersion is narrower than the particle size distribution of the precursor titanium dioxide particles. There is also provided the use of the dispersion of titanium dioxide particles to attenuate infrared radiation, particularly in a cosmetic composition, more particularly a cosmetic composition to provide protection against IR radiation, more particularly IRA radiation. There is also provided a personal care composition comprising the titanium dioxide dispersion.

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26-01-2017 дата публикации

Aqueous Dispersion of Hydrophobically Modified Pigment Particles

Номер: US20170022384A1
Принадлежит:

The present invention relates to a composition comprising a) a stable aqueous dispersion of inorganic pigment particles hydrophobically modified with covalently bonded polysiloxane or silyl groups; and b) a polymeric anionic dispersant; wherein the hydrophobically modified inorganic pigment particles have an average particle size in the range of from 200 nm to 10 μm, and the solids content of the hydrophobically modified inorganic pigment particles is from 10 to 80 weight percent, based on the weight of inorganic pigment particles and water. The composition of the present invention provides a way to improve water resistance in coatings formulations. 1. A composition comprising a) a stable aqueous dispersion of inorganic pigment particles hydrophobically modified with covalently bonded polysiloxane or silyl groups; and b) a polymeric anionic dispersant; wherein the hydrophobically modified inorganic pigment particles have an average particle size in the range of from 200 nm to 10 μm , and the solids content of the hydrophobically modified inorganic pigment particles is from 10 to 80 weight percent , based on the weight of inorganic pigment particles and water;{'sup': 1', '1', '1, 'sub': 3', '1', '18', '1', '18', '1', '18', '1', '18, 'wherein the silyl groups are represented by —Si(R); wherein each Ris independently C-Calkyl, C-Calkoxy, OH, phenyl, phenoxy, or a bond connecting the Si atom to which it is attached to the surface of an inorganic pigment particle, with the proviso that at least one Ris a C-Calkyl, C-Calkyoxy, phenyl, or phenoxy group; and'}wherein the inorganic pigment particles comprise oxides of titanium, aluminum, silicon, iron, calcium, magnesium, zirconium, or zinc.2. The composition of wherein the inorganic pigment particles are hydrophobically modified with —Si(R)3 groups claim 1 , wherein the inorganic pigment particles are TiO claim 1 , ZnO claim 1 , AlO claim 1 , CaCO claim 1 , FeO claim 1 , SiO claim 1 , or talc.3. The composition of wherein ...

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25-01-2018 дата публикации

COATED PRODUCT

Номер: US20180022924A1
Принадлежит: HUNTSMAN P&A UK LIMITED

A coated particulate inorganic material includes a particulate inorganic material selected from at least one of titanium dioxide and a doped titanium dioxide, and a coating. The particulate inorganic material has an average crystal size of 0.4-2 μm. The coating includes a first and second layer. The first layer includes an inorganic oxide and/or an inorganic phosphate. The second layer is alumina. The first layer is from 0.1 to 2.2% w/w based on a total weight of the first layer with respect to a total weight of the particulate inorganic material. The second layer is 0.1 to 3.5% w/w based on a total weight of the second layer with respect to the total weight of the particulate inorganic material. The coating is from 0.2 to 4.5% w/w based on the total weight of the first and second layer with respect to the total weight of the particulate inorganic material. 120-. (canceled)21: A coated particulate inorganic material comprising:a particulate inorganic material selected from at least one of titanium dioxide and a doped titanium dioxide, the particulate inorganic material having an average crystal size of from 0.4 μm to 2 μm; anda coating on the particulate inorganic material, the coating comprising a first layer and a second layer, [ group 4 (IVB) and group 12 (IIB) transition metals selected from Ti, Zr and Zn;', 'group 13 to group 15 (IIIA-VA) p-block elements selected from Si, P and Sn; and', 'lanthanides; and, 'each of the at least one inorganic oxide being independently selected from an oxide of, group 1 (IA) alkali metals and group 2 (IIA) alkaline earth metals selected from H, Li, Na, K, Rb, Be, Mg, Ca and Sr;', 'group 3 (IIIA) and group 4 (IVB) transition metals selected from Sc, Y, Ti and Zr; and', 'group 13 to group 15 (IIIA-VA) p-block elements selected from Al, Ga, In, Tl, Ge, Sn and Pb; and, 'each of the at least one inorganic phosphate being independently selected from a phosphate of], 'the first layer comprising at least one of at least one inorganic ...

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26-01-2017 дата публикации

POROUS PLATE-SHAPED FILLER, HEAT INSULATION FILM, AND METHOD FOR PRODUCING POROUS PLATE-SHAPED FILLER

Номер: US20170023168A1
Принадлежит: NGK Insulators, Ltd.

A porous plate-shaped filler is a plate shape having an aspect ratio of 3 or more, and has a minimum length of 0.1 to 50 μm and a porosity of 20 to 90%. Furthermore, the porous plate-shaped filler includes plate-shaped pores having an aspect ratio of 1.5 or more. Consequently, in the porous plate-shaped filler, a thermal conductivity is low. The heat insulation film includes the porous plate-shaped filler, whereby a heat insulation effect of the heat insulation film can improve. 1. A porous plate-shaped filler which is a plate shape having an aspect ratio of 3 or more , has a minimum length of 0.1 to 50 μM and a porosity of 20 to 90% , andincludes plate-shaped pores having an aspect ratio of 1.5 or more.2. The porous plate-shaped filler according to claim 1 ,wherein in a cross section in a direction of the minimum length of the porous plate-shaped filler, an average of angles between directions of minimum lengths of the pores and the direction of the minimum length of the porous plate-shaped filler is 45° or less.3. The porous plate-shaped filler according to claim 1 ,wherein a thermal conductivity in the direction of the minimum length of the porous plate-shaped filler is 1 W/(m·K) or less.4. A heat insulation film which includes the porous plate-shaped filler according to .5. The heat insulation film according to claim 4 ,wherein the thermal conductivity in a thickness direction is 1.5 W/(m·K) or less.6. A method for producing the porous plate-shaped filler according to claim 1 , which comprises: preparing a slurry including a plate-shaped pore former having an aspect ratio of 1.5 or more; and firing the pore former to produce the porous plate-shaped filler including the plate-shaped pores having an aspect ratio of 1.5 or more.7. The method for producing the porous plate-shaped filler according to claim 6 ,wherein a viscosity of the slurry is from 100 to 90000 cps. The present invention relates to a porous plate-shaped filler to form a heat insulation film in ...

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23-01-2020 дата публикации

HEAT-RESISTANT MILLABLE SILICONE RUBBER COMPOSITION

Номер: US20200024452A1
Принадлежит: SHIN-ETSU CHEMICAL CO., LTD.

Provided is a millable silicone rubber composition capable of yielding a silicone rubber (cured product) superior in heat resistance. The composition contains: 1. A heat-resistant millable silicone rubber composition comprising:(A) 100 parts by mass of an organopolysiloxane having at least two silicon atom-bonded alkenyl groups in one molecule, and having an average polymerization degree of not lower than 100;{'sup': '2', '(B) 5 to 100 parts by mass of a reinforcing silica having a specific surface area of not smaller than 50 m/g;'}(C) 0.01 to 10 parts by mass of a titanium oxide doped with a transition metal oxide of 0.01 to 5% by mass;(D) 0.01 to 10 parts by mass of a cerium oxide and/or a cerium hydroxide; and(E) 0.01 to 10 parts by mass of a curing agent.2. The heat-resistant millable silicone rubber composition according to claim 1 , wherein a content of the transition metal oxide in the silicone rubber composition is 0.001 to 0.1% by mass.3. The heat-resistant millable silicone rubber composition according to or claim 1 , wherein the transition metal oxide is an iron oxide.4. The heat-resistant millable silicone rubber composition according to claim 1 , further comprising a dispersant for filler claim 1 , as a component (F).5. The heat-resistant millable silicone rubber composition according to claim 1 , wherein the component (E) is an organic peroxide.6. The heat-resistant millable silicone rubber composition according to claim 1 , wherein the component (E) is composed of an organohydrogenpolysiloxane and a platinum group metal catalyst.7. A cured product of the heat-resistant millable silicone rubber composition according to . The present invention relates to a millable silicone rubber composition capable of yielding a silicone rubber with a favorable heat resistance.Silicone rubbers are widely used in various fields such as the fields of electric equipment, automobile, architecture, medical procedure and food, due to the fact that they have properties such ...

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04-02-2016 дата публикации

TITANIUM OXIDE AEROGEL COMPOSITES

Номер: US20160030908A1
Принадлежит:

The invention relates to titanium oxide aerogels, in particular to titanium oxide binary or ternary (e.g. titanium oxide-carbon) aerogel monoliths possessing ordered meso- and macroporosity. The porous scaffold can be made with or without addition of binders and/or surfactants. The aerogel obtained by this method has a specific surface area greater than 60 m2/g and porosity larger than 60%. The surface area ranges from 60 to 300 m2/g. The porosity can reach as high as 99.6%. The size of the titanium oxide crystals are between 5 nm and 100 nm. The aerogel contains 100% titanium oxide. The composite (binary or ternary) aerogel can be prepared by adding at least 10% carbon in the form of (carbon nanotubes, carbon nanofibers, carbon microfibers, exfoliated graphene, cellulose fibers, polymer fibers, metallic and metal oxide nano and microfibers etc.). The aerogel can be prepared with a predeterminable shape. It can be shaped in a mold having a shape of a cylinder, cube, sheet or sphere. The aerogel can be also transformed into a supported or self-standing film with a thickness. The material can be used as a self-cleaning filter e.g. in a solar-thermal water and air purification system, in mesoscopic solar cells e.g. dye sensitized solar cells, multifunctional filler in polymer composites, in ceramics, in metals, thermoelectric material to convert (waste) heat into electricity, heat insulation material and electrode material in lithium ion batteries and supercapacitors. 1. Titanium oxide aerogel made of at least 90% titanium oxide and showing a porosity of at least 90%.2. Aerogel according to with a porosity between 90% and 99.6%.3. Aerogel according to made of 100% of titanium oxide.4. Aerogel according to made of at least 90% titanium oxide claim 1 , showing a porosity of at least 60% claim 1 , having a specific surface area greater than 60 m/g and a porosity greater than 60% claim 1 , said aerogel being obtained according to a process including a step where a ...

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01-02-2018 дата публикации

METHOD FOR PRODUCING ORGANIC SOLVENT DISPERSION OF TITANIUM OXIDE PARTICLES

Номер: US20180029897A1
Принадлежит: SAKAI CHEMICAL INDUSTRY CO., LTD.

The invention provides a method for producing an organic solvent dispersion of titanium oxide particles in an organic solvent except methanol and ethanol, comprising: 2. The method for producing an organic solvent dispersion of titanium oxide particles according to claim 1 , wherein the titanium oxide particles are surface-treated with 1-40 parts by weight of the silane coupling agent and 1-80 parts by weight of 12-hydroxystearic acid each in relation to 100 parts by weight of the titanium oxide particles.3. The method for producing an organic solvent dispersion of titanium oxide particles according to claim 1 , wherein the organic solvent is at least one selected from the group consisting of methyl isobutyl ketone claim 1 , methyl ethyl ketone claim 1 , butanol claim 1 , propanol claim 1 , diacetone alcohol claim 1 , propylene glycol monomethyl ether claim 1 , toluene claim 1 , dimethylsulfoxide claim 1 , N claim 1 ,N-dimethylacetamide claim 1 , N claim 1 ,N claim 1 ,2-trimethylpropionamide claim 1 , γ-butyrolactone claim 1 , and butyl acetate.4. The method for producing an organic solvent dispersion of titanium oxide particles according to claim 1 , wherein the alcohol dispersion of titanium oxide particles has a content of 10% by weight or more claim 1 , a transmittance of 40% or more at a wavelength of 500 nm claim 1 , and a transmittance of 80% or more at a wavelength of 800 nm claim 1 , wherein the titanium oxide particles have a D50 in a range of 1 to 20 nm.5. The method for producing an organic solvent dispersion of titanium oxide particles according to claim 1 , wherein the alcohol dispersion of titanium oxide particles is surface-treated with the surface treating agent in the presence of an organic solvent other than the alcohol solvent.6. The method for producing an organic solvent dispersion of titanium oxide particles according to claim 1 , wherein the alcohol dispersion of titanium oxide particles used in the surface treating process is such that it is ...

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01-02-2018 дата публикации

ORGANIC SOLVENT DISPERSION OF TITANIUM OXIDE PARTICLES AND METHOD FOR PRODUCING SAME

Номер: US20180030305A1
Принадлежит: SAKAI CHEMICAL INDUSTRY CO., LTD.

The invention provides an organic solvent dispersion of titanium oxide particles in a content of 10% by weight or more in an organic solvent except methanol and ethanol, 2. The organic solvent dispersion of titanium oxide in an organic solvent according to claim 1 , in which the titanium oxide particles are surface-treated with 1-40 parts by weight of the silane coupling agent and 1-80 parts by weight of 12-hydroxystearic acid each in relation to 100 parts by weight of the titanium oxide particles.3. The organic solvent dispersion of titanium oxide in an organic solvent according to claim 1 , in which the organic solvent is at least one selected from methyl isobutyl ketone claim 1 , methyl ethyl ketone claim 1 , diacetone alcohol claim 1 , butanol claim 1 , propanol claim 1 , propylene glycol monomethyl ether claim 1 , toluene claim 1 , dimethylsulfoxide claim 1 , N claim 1 ,N-dimethylacetamide claim 1 , N claim 1 ,N claim 1 ,2-trimethylpropionamide claim 1 , y-butyrolactone claim 1 , and butyl acetate.4. The organic solvent dispersion of titanium oxide in an organic solvent according to claim 2 , in which the organic solvent is at least one selected from methyl isobutyl ketone claim 2 , methyl ethyl ketone claim 2 , diacetone alcohol claim 2 , butanol claim 2 , propanol claim 2 , propylene glycol monomethyl ether claim 2 , toluene claim 2 , dimethylsulfoxide claim 2 , N claim 2 ,N-dimethylacetamide claim 2 , N claim 2 ,N claim 2 ,2-trimethylpropionamide claim 2 , γ- butyrolactone claim 2 , and butyl acetate. The invention relates to a dispersion of titanium oxide particles in an organic solvent, i.e., an organic dispersion of titanium oxide particles, and a method for producing the same. The invention relates more particularly to an organic solvent dispersion of titanium oxide particles which contains titanium oxide particles in a high content, has a low viscosity, and is also superior in stability and transparency, and a method for producing the same. Because the ...

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30-01-2020 дата публикации

Colored Composite Material

Номер: US20200031719A1
Принадлежит: HUBLOT SA, GENÈVE

A solid composite material combining: 1. A solid composite material combining:an inorganic pigment in the form of discrete particles each comprising a colored core and a coating surrounding the core, said coating being adapted to allow light to pass through; anda matrix based on metalloid or metal oxide, said matrix being adapted to allow light to pass through.2. The solid composite material according to claim 1 , wherein all the inorganic pigment particles have an identical coating.3. A solid composite material according to claim 1 , wherein the inorganic pigment comprises a mixture of particles respectively having cores at least two different types claim 1 , in particular of different colors.4. The solid composite material according to claim 1 , wherein the inorganic pigment represents a volume fraction comprised between 2% and 50% of said composite material.5. The solid composite material according to claim 1 , wherein the core of at least one particle of the inorganic pigment is based on cobalt aluminate CoAl2O4.6. The solid composite material according to claim 1 , wherein the core of at least one particle of the inorganic pigment is an oxide comprising at least one element selected from: iron claim 1 , chromium claim 1 , aluminum claim 1 , titanium claim 1 , silicon claim 1 , zinc claim 1 , nickel claim 1 , cobalt claim 1 , cadmium claim 1 , copper claim 1 , vanadium claim 1 , bismuth claim 1 , niobium claim 1 , and manganese.7. The solid composite material according to claim 1 , wherein the coating of at least one particle of the inorganic pigment is fabricated from a material selected from: mica claim 1 , alumina claim 1 , zirconia claim 1 , and titanium dioxide.8. The solid composite material according to claim 1 , wherein the particles of inorganic pigment have an average diameter comprised between 0.2 μm and 10 μm.9. The solid composite material according to claim 1 , wherein the particles of inorganic pigment have an average diameter comprised between 0. ...

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11-02-2016 дата публикации

USE OF A POLYMERIC EMULSION FOR THE SURFACE TREATMENT OF PARTICLES OF MINERAL MATTER

Номер: US20160040014A1
Принадлежит:

The present invention relates to the use of a new polymeric aqueous emulsion for surface treating particles of mineral matter. 1: A method for surface treating particles of mineral matter comprising contacting said particles with a polymeric aqueous emulsion obtained by polymerization of:i) at least some acrylic acid and/or methacrylic acid monomers,ii) at least some alkyl acrylate and/or alkyl methacrylate monomers,iii) at least some monomers having at least one hydrophobic group, said hydrophobic group of these monomers comprising between 6 and 100 carbon atoms,in the presence, during said polymerization, of: {'br': None, 'sub': 3', '6', '2', 'n, 'RO—(CHO)—H\u2003\u2003(I)'}, 'iv) at least one polyglycerol of formulain which:R represents hydrogen, a carbon group comprising between 8 to 22 carbon atoms, or an ester group functionalized by a carbon group comprising between 8 to 22 carbon atoms, andn represents an integer or decimal number greater than 1, andv) at least one anionic surfactant agent.2: The method according to claim 1 , wherein the monomer iii) has a formula (II):{'br': None, 'R′-A-R″\u2003\u2003(II)'} A represents a polymeric chain composed of:', {'sub': 2', '1', '1, 'm alkylene oxide units of formula —CHCHRO— where Rrepresents an alkyl group comprising from 1 to 4 carbons, and m is from 0 to 150,'}, {'sub': 2', '2', '2, 'p alkylene oxide units of formula —CHCHRO— where Rrepresents an alkyl group comprising from 1 to 4 carbons, and p is from 0 to 150,'}, 'n ethylene oxide units where n is from 0 to 150,, 'in which{'sub': 2', '1', '2', '2, 'claim-text': R′ represents a radical containing a polymerizable unsaturated function selected from the group consisting of acrylic esters, methacrylic esters, maleic esters, itaconic esters, crotonic esters, acrylurethane, methacrylurethane, α-α′-dimethyl-isopropenyl-benzylurethane, allylurethane, allyl ethers, vinyl ethers, amides and imides; and', 'R″ represents a linear, branched or ramified hydrocarbon chain ...

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24-02-2022 дата публикации

CARBON-COATED PARTICLES

Номер: US20220056241A1
Принадлежит:

Core particles produced in situ or introduced as preformed core particles are coated with a layer of carbon. Non-carbon as well as some carbon-based core materials can be utilized. The resulting carbon coated particles can find applications in rubber products, for instance as reinforcement for tire components. 148-. (canceled)49. A rubber composition or a rubber article comprising carbon-coated particles , wherein the carbon coated particles comprise a non-carbon core , a reclaimed pyrolysis carbon core , or a plasma CB core coated by a carbon layer.50. The rubber composition or the rubber article of claim 49 , wherein the non-carbon core is formed from a material selected from the group consisting of precipitated silica claim 49 , fumed silica claim 49 , surface modified silica and any combination thereof.51. The rubber composition or the rubber article of claim 49 , wherein the non-carbon core is formed from nanoparticles of clay claim 49 , rice husk silica claim 49 , calcium carbonate and any combination thereof.52. The rubber composition or the rubber article of claim 49 , wherein the carbon layer is from about 0.5 nm to about 20 nm thick.53. The rubber composition or the rubber article of claim 49 , wherein the carbon layer is amorphous carbon.54. The rubber composition or the rubber article of claim 49 , wherein the non-carbon core claim 49 , the reclaimed pyrolysis carbon core claim 49 , or the plasma CB core has aciniform microstructure.55. The rubber composition or the rubber article of claim 49 , wherein the carbon-coated particles have a STSA within the range of from about 5 to about 275 m/g; and a COAN within the range of from about 40 to about 150 cc/100 g.56. The rubber composition or the rubber article of claim 49 , wherein the carbon-coated particles have a STSA within the range of from about 30 to about 250 m/g; and a COAN within the range of from about 55 to about 110 cc/100 g.57. The rubber composition or the rubber article of claim 49 , wherein ...

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18-02-2021 дата публикации

FLAKY TITANATE AND METHOD FOR PRODUCTION THEREOF, AND USE THEREOF

Номер: US20210047517A1
Автор: UESUSUKI Yusuke
Принадлежит: ISHIHARA SANGYO KAISHA, LTD.

Provided is a flaky titanate that exhibits a high weathering resistance while at the same time having the ability to endow a coating film with a silky feeling having a shading feeling and a strong luster feeling, and a method for the production thereof suitable at least for inexpensive industrial production. The flaky titanate contains a basic organic compound wherein the content of basic functional groups thereof is not more than 2.4%, and provides a coating film having a goniospectrophotometric color measured value ΔL* of at least 150. The method for producing a flaky titanate contains a step of classifying a flaking titanate having a basic organic compound at the surface and/or in interlayer position, to bring (D90−D10)/D50 in the volume based particle size distribution to 1.5 or less. 1. A flaky titanate according to claim 2 , wherein the flaky titanate has a goniospectrophotometric color measured value ΔL*of 150 or more in the form of a paint film.2. A flaky titanate comprising a basic organic compound claim 2 ,wherein the basic organic compound has a basic functional group content of 2.4% or less, and{'sub': '2', 'wherein the flaky titanate has a goniospectrophotometric color measured value ΔL*of 60 or more in the form of a paint film.'}3. A flaky titanate having (D90−D10)/D50 of 1.5 or less in a volume particle size distribution measured by a laser diffraction/scattering method claim 2 ,wherein the D10, D50, and D90 express a cumulative 10% particle size, a median size, and a cumulative 90% particle size, respectively.4. A method for producing a flaky titanate according to claim 3 , comprising a step of classifying a flaky titanate having a basic organic compound between layers and/or on a surface thereof claim 3 , thereby adjusting (D90−D10)/D50 in a volume particle size distribution to be 1.5 or less.5. A method for producing a flaky titanate according to claim 3 , comprising a step of performing delamination between layers of a layered titanate with a ...

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01-05-2014 дата публикации

Treated inorganic pigments having reduced photoactivity and improved anti-microbial properties and their use in polymer compositions

Номер: US20140121314A1
Автор: Charles David Musick
Принадлежит: EI Du Pont de Nemours and Co

The disclosure provides a polymer composition comprising a treated inorganic particle having improved photostability and improved anti-microbial properties, wherein the treated inorganic particle comprises: a inorganic core particle; a first treatment of a silicon compound, wherein the silicon compound is added in a single step; and a second treatment comprising a co-precipitated zinc oxide and alumina.

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03-03-2022 дата публикации

Titanium oxide powder and method for manufacturing same

Номер: US20220064016A1
Принадлежит: Tayca Corp

In producing titanium oxide containing rutile-type crystals by adding hydrochloric acid to an aqueous dispersion of an alkali metal titanate, sulfurous acid, disulfurous acid, sulfuric acid or a salt thereof is added. Thus, there is provided a titanium oxide powder which is doped with bivalent sulfur atoms (S 2− ) and in which a ratio (I A /I R ) of a peak intensity (I A ) of anatase-type crystals to a peak intensity (I R ) of rutile-type crystals as measured by X-ray diffractometry is 0.1 or less. Moreover, a cosmetic is provided by dispersing the titanium oxide powder in a dispersion medium. Thus, bluish color derived from Rayleigh scattering is negated, providing a dispersion, particularly a cosmetic, with excellent transparency and color tone.

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14-02-2019 дата публикации

INKJET RECORDING METHOD AND INKJET RECORDING APPARATUS

Номер: US20190048216A1
Принадлежит: RICOH COMPANY, LTD.

Provided is an ink containing at least: an inorganic pigment having a surface hydrophobicity; resin particles; and water. 113-. (canceled)14. An inkjet recording method for recording an image by using ink , on a non-porous substrate , comprising:(a) applying a white ink comprising an inorganic white pigment having a surface hydrophobicity, resin particles, and water, to the non-porous substrate, to form a white layer formed on said non-porous substrate, the non-porous substrate having been selected from the group consisting of polyvinyl chloride film, polyethylene terephthalate (PET) film, polycarbonate film, polyethylene film, acrylic film, polypropylene film, polyimide film, and polystyrene film; and(b) forming an image over the white layer formed by the white ink, by applying an ink of another color onto the white layer.15. The inkjet recording method according to claim 14 , further comprising:(c) heating the image at from 50° C. to 200° C. at the same time as or before forming the image.16. The inkjet recording method according to claim 14 , wherein surface hydrophobicity of the inorganic white pigment in the white ink applied in (a) is obtained by treating the inorganic white pigment with a surface treatment using hydrophobic silicone.17. The inkjet recording method according to claim 14 , wherein surface hydrophobicity of the inorganic white pigment in the white ink applied in (a) is obtained by treating the inorganic white pigment with a surface treatment using an alkyl.18. The inkjet recording method according to claim 14 ,wherein the resin particles in the white ink include at least one kind selected from the group consisting of styrene acrylic resin particles, acrylic silicone resin particles, polyurethane resin particles, and acrylic urethane resin particles.19. The inkjet recording method according to claim 14 , wherein the resin particles in the white ink include anionic self-emulsifying polyurethane resin particles.20. The inkjet recording method ...

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25-02-2021 дата публикации

MULTILAYER AND FLEXIBLE CAPACITORS WITH METAL-ION DOPED TIO2 COLOSSAL PERMITTIVITY MATERIAL/POLYMER COMPOSITES

Номер: US20210054168A1
Автор: HAO Jianhua, TSE Mei-Yan
Принадлежит: The Hong Kong Polytechnic University

Disclosed is polymer-ceramic composite material with colossal permittivity, comprising polymer matrix and ceramic powders embedded in the polymer matrix, wherein a part of the polymer matrix is exposed and adsorbed to the surface of the ceramic powders, and the polymer is electrically insulating. This invention simultaneously achieves large dielectric constant, negligible dielectric loss and high energy density in flexible composite capacitors based on metal-ion co-doped colossal permittivity materials. The host oxides used in this CP system is friendly to the environment, non-toxic and abundant. Additionally, the process developed is relatively simple, low cost and suitable for mass production-scale. Therefore, these composite capacitors have great technological potential for many applications. Compared to the conventional ceramic materials, composites of this invention are lightweight, scalable and easily fabricated into complex shapes towards miniaturization of the compact systems. The additional flexibility feature also possesses broad application prospects in modern electronic and energy storage devices. 1. A polymer-ceramic composite material with colossal permittivity , comprising polymer matrix and ceramic powders embedded in the polymer matrix , wherein a part of the polymer matrix is exposed and adsorbed to the surface of the ceramic powders , and the polymer is electrically insulating.2. The polymer-ceramic composite material according to claim 1 , wherein the ceramic powders comprise or essentially consisting of metal-ion doped TiOceramic powders.3. The polymer-ceramic composite material according to claim 1 , wherein the polymer is a fluoropolymer.4. The polymer-ceramic composite material according to claim 1 , which is in the form of a flexible sheet with one or more layers claim 1 , such as 1 claim 1 , 2 claim 1 , 3 claim 1 , 4 claim 1 , 5 claim 1 , 6 claim 1 , 7 claim 1 , 8 claim 1 , 9 claim 1 , 10 layers or more.5. The polymer-ceramic composite ...

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22-02-2018 дата публикации

PROCESS FOR PRODUCTION OF TITANIUM DIOXIDE (Ti02) NANOPARTICLES WITH DESIRED RATIO OF ANATASE AND RUTILE

Номер: US20180050922A1
Принадлежит:

The present invention relates to a process for the production of titanium dioxide (TiO) nanoparticles with desired ratio of anatase phase and rutile phase, the method comprising (a) reacting titanium trichloride (TiCl) solution with a flower extract (b) drying the reaction mixture obtained in step (a) at high temperature to powder form and (c) calcination of the powder obtained in step (b) at high temperatures. 1. A process for the production of titanium dioxide (TiO) nanoparticles with desired ratio of anatase phase and rutile phase , the method comprising{'sub': '3', '(a) reacting titanium trichloride (TiCl) solution with a flower extract'}(b) drying the reaction mixture obtained in step (a) at high temperature to powder form and(c) calcination of the powder obtained in step (b) at high temperatures.2. The process according to claim 1 , wherein the process comprises doping TiOnanoparticles with water soluble metal precursor.3. The process according to wherein step (a) comprises reacting titanium trichloride (TiCl) solution and a water soluble metal precursor with a flower extract.4. The process according to claim 3 , wherein the water soluble metal precursor is a water soluble metal precursor of a metal selected from the group consisting of Ag claim 3 , Ni claim 3 , Zn claim 3 , Cr claim 3 , Ge claim 3 , Mo claim 3 , Ru claim 3 , Rh claim 3 , Sn claim 3 , W claim 3 , Sr claim 3 , Al claim 3 , Si claim 3 , Mn claim 3 , Fe claim 3 , Au claim 3 , Pt claim 3 , Co claim 3 , V claim 3 , Cu and Pd.5. The process according to claim 3 , wherein the water soluble metal precursor is present in an amount of 1 to 30% by weight.6. The process according to claim 1 , wherein TiClin step (a) is 0.1%-30% aqueous solution of TiCl.7Peltophorum pterocarpum. The process according to wherein the flower extract is flower extract.8. The process according to claim 1 , wherein the flower extract is prepared by heating the flowers in double distilled deionized water at a temperature of 40° C ...

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13-02-2020 дата публикации

BURNERS FOR CONVERSION OF METHANE TO OLEFINS, AROMATICS, AND NANOPARTICLES

Номер: US20200049346A1
Принадлежит:

Embodiments of the present disclosure describe burner () configurations used in an industrial process to convert methane to olefins, aromatics, and nanoparticles/nanomaterials. Both a vitiated coflow burner and piloted turbulent burner with inhomogeneous inlets are disclosed. 1. A method of controlling secondary reactions of a burner of combustion products using injected methane , the method comprising:establishing a jet flame in coaxial flow of hot combustion products from a premixed vitiated coflow of gas passing through a porous plate or catalytic monolith, said jet flame established by gas exiting from a central tube;providing a tube positioner to translate the tip of the central tube to an offset height relative to the porous plate or catalytic monolith; andcontrolling the tube positioner to vary the offset height of the central tube tip in a dynamic manner based on chemical inputs, with said controlling resulting in different secondary reactions of combustion products from the burner.2. The method of claim 1 , wherein the central tube is a blunt-tipped tube and the gas exiting the central tube is methane.3. The method of claim 1 , wherein the coflow gas is a combination of methane and oxygen.4. The method of claim 1 , wherein offset height of the central tube tip is controlled to provide both a methane/oxygen combustion process and subsequent pyrolysis of methane to form olefins claim 1 , aromatics or nanoparticles.5. A method of controlling secondary reactions of a burner of combustion products using injected methane claim 1 , the method comprising:establishing a jet flame in coaxial flow of hot combustion products from gas passing through a porous plate or catalytic monolith, with said jet flame established by a piloted turbulent burner with inhomogeneous inlets and defining three concentric tubes;providing a tube positioner to translate an innermost one of the three concentric tubs to different positions relative to an intermediate tube; andcontrolling the ...

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26-02-2015 дата публикации

Titanium dioxide nano particle modified by surface stabilizer, titanium dioxide nano ink comprising the same, solar cell employing the same, and producing method of the same

Номер: US20150056745A1
Автор: Ki Chun Lee, Yong Jun Jang
Принадлежит: Hyundai Motor Co

Disclosed are a titanium dioxide nano ink having such a strong dispersibility as to be applicable by inkjet printing and having adequate viscosity without requiring printing several times, and a titanium dioxide nano particle modified by a surface stabilizer included therein. Inkjet printing of the titanium dioxide nano ink enables printing of a minute electrode. In addition, efficiency of a solar cell may be maximized since occurrence of pattern cracking is minimized.

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04-03-2021 дата публикации

A METHOD OF FORMING CONFORMABLE NANOSCALE COATINGS ON SUBSTRATES

Номер: US20210061662A1
Принадлежит:

A method is disclosed for forming nanoscale coatings on a solid substrate surface. In certain embodiments, the method includes the following steps: contacting a substrate with a first liquid organic solvent; adding a liquid agent to the first liquid organic solvent to form a liquid agent film on a surface of the substrate; and adding the nanocoating precursor in the first liquid organic solvent to react the nanocoating precursor with the liquid agent to form the nanocoating on the surface of the substrate. 1. A method of forming a nanocoating on a substrate comprising:contacting a substrate with a first liquid organic solvent;adding a liquid agent to the first liquid organic solvent to form a liquid agent film on a surface of the substrate; andadding a nanocoating precursor in the first liquid organic solvent, wherein the nanocoating precursor reacts with the liquid agent film to form the nanocoating on the surface of the substrate.2. The method of claim 1 , wherein the affinity or attraction between the liquid agent and the substrate is higher relative to the affinity or attraction between the liquid agent and the first liquid organic solvent.3. The method of claim 2 , wherein the liquid agent has a low solubility in the first liquid organic solvent.4. The method of claim 3 , wherein the step of adding the nanocoating precursor in the first liquid organic solvent comprises dissolving the nanocoating precursor in the first liquid organic solvent.5. The method of claim 3 , wherein prior to adding the nanocoating precursor into the first liquid organic solvent claim 3 , the nanocoating precursor is dissolved in a second liquid organic solvent claim 3 , and wherein the step of adding the nanocoating precursor in the first liquid organic solvent further comprises adding the combination of the nanocoating precursor and the second liquid organic solvent.6. The method of claim 5 , wherein the contacting step comprises dispersing the substrate in the first liquid organic ...

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04-03-2021 дата публикации

TITANIUM OXIDE POWDER, AND DISPERSION LIQUID AND COSMETIC USING SAID POWDER

Номер: US20210061669A1
Принадлежит: Sumitomo Osaka Cement Co., Ltd.

The titanium oxide powder of the present invention is a titanium oxide powder which has a BET specific surface area of 5 m/g or more and 15 m/g or less, and contains octahedral-shaped particles, wherein each octahedral-shaped particle thereof has line segments each of which connects two apexes which face each other and has a maximum value of the line segments, an average value of the maximum values is 300 nm or higher and 1000 nm or lower, and a value (D90/D10) is 1 or higher and 3 or lower, wherein the value is obtained by dividing a value (D90), which corresponds to 90% in a cumulative number percentage of the maximum values of line segments each of which connects two apexes which face each other, by a value (D10) which corresponds to 10% in the cumulative number percentage. 1. A titanium oxide powder , which has a BET specific surface area of 5 m/g or more and 15 m/g or less , and contains octahedral-shaped particles , whereineach octahedral-shaped particle thereof has line segments each of which connects two apexes which face each other and has a maximum value of the line segments,an average value of the maximum values is 300 nm or higher and 1,000 nm or lower, anda value (D90/D10) is 1 or higher and 3 or lower, wherein the value is obtained by dividing a value (D90), which corresponds to 90% in a cumulative number percentage of the maximum values of line segments each of which connects two apexes which face each other, by a value (D10) which corresponds to 10% in the cumulative number percentage.2. The titanium oxide powder according to claim 1 ,wherein a value (average value of the maximum values/BET-converted average particle diameter), which is obtained by dividing the average value of the maximum values of the line segments by an average particle diameter converted from the BET specific surface area, is 0.5 or higher and 2.5 or lower.3. The titanium oxide powder according to claim 1 ,wherein a content of the octahedral-shaped particles in the titanium oxide ...

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20-02-2020 дата публикации

HOLLOW STRUCTURE PARTICLES, METHOD FOR PRODUCING SAME AND WHITE INK

Номер: US20200056060A1
Принадлежит:

Hollow structure particles which contain titanium oxide and silica, in which the crystal type of the titanium oxide is rutile type; a method for producing the hollow structure particles; a white ink which contains these hollow structure particles as a coloring agent; use of the white ink in inkjet recording; and an inkjet recording method which uses the white ink. 1. A hollow structure particle comprising titanium oxide and silica , wherein the crystal form of the titanium oxide is rutile.2. The hollow structure particle according to claim 1 , wherein a primary particle diameter B is 10 nm to 1 claim 1 ,000 nm.3. The hollow structure particle according to claim 1 , wherein a ratio of inner diameter A of a hollow structure to the primary particle diameter B claim 1 , A/B claim 1 , is 0.3 to 0.95.4. The hollow structure particle according to claim 1 , further comprising an element other than titanium oxide and silica.5. A method of producing a hollow structure particle claim 1 , comprising:forming a shell containing a titanium oxide precursor on a surface of a template particle, which becomes a core, to obtain a first core/shell particle;applying a silica precursor to a surface of the first core/shell particle to obtain a second core/shell particle;removing the template particle from the second core/shell particle to obtain a shell particle; and{'claim-ref': {'@idref': 'CLM-00001', 'claim 1'}, 'firing the shell particle to obtain the hollow structure particle according to .'}6. A method of producing a hollow structure particle claim 1 , comprising:forming a shell containing a titanium oxide precursor on a surface of a template particle which becomes a core, to obtain a first core/shell particle,applying a silica precursor to the surface of the first core/shell particle to obtain a second core/shell particle, and{'claim-ref': {'@idref': 'CLM-00001', 'claim 1'}, 'firing the second core/shell particle to remove the template particle to obtain the hollow structure ...

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09-03-2017 дата публикации

Method for treating the surface of particles, the thus obtained particles and use thereof

Номер: US20170066924A1
Принадлежит: Huntsman P&A Germany GmbH

A method for producing surface-treated particles includes surface treatment of titanium dioxide, barium sulfate, zinc sulfide or lithopone particles, and to mixtures of the particles with alkoxylated siloxanes and phthalate-free plasticizers for improving dispersion in plastics. 2. The particles according to claim 1 , wherein in formula (I):{'sup': '1', 'Ris a polyether group of formula (II), in which'}Z is equal to an unbranched alkylene group having 2 to 4 carbon atoms,o is 0,x is 0 to 20,y is 5 to 100,z is 0 to 20.3. The particles according to claim 1 , wherein the numerical ratio of index a to index b in formula (I) is equal to 8 to 18.4. The particles according to claim 2 , wherein the index x is between 0.05 and 1.2 times the sum of indices y+z.5. The particles according to claim 2 , wherein:R is equal to methyl,{'sup': '3', 'Ris hydrogen,'}a is 80 to 95,b is 5 to 8,x is 3 to 5,y is 10 to 25,z is 0.6. The particles according to claim 1 , wherein the particles are TiO.7. The particles according to claim 1 , having a dust value of at most 30 mg per 100 g of surface-treated particles.8. The particles according to claim 1 , wherein the at least one phthalate-free plasticiser is selected from the group consisting of{'sub': 3', '2, 'esters of aliphatic hydrocarbons having 6 to 21 carbon atoms with at least one acid group selected from the group consisting of a carboxyl group, sulfonyl group —SOH, and sulfinyl group —SOH, with a monovalent or polyvalent aliphatic alcohol having 6 to 20 carbon atoms or a monovalent or bivalent aromatic alcohol, and'}esters of aromatic 1,4-(para)dicarboxylic acids or aromatic tricarboxylic acids with a monovalent or polyvalent aliphatic alcohol having 6 to 20 carbon atoms.11. The method for producing surface-treated particles from TiO claim 9 , BaSO claim 9 , ZnS or lithopone according to claim 9 , wherein the at least one phthalate-free plasticiser is selected from the group consisting of{'sub': 3', '2, 'esters of aliphatic ...

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12-03-2015 дата публикации

Metal Oxide Particles with Uniform Multilayer Polymer Coatings

Номер: US20150073134A1

The present invention is a multilayered composite comprising porous metal oxide particles that are covalently bonded by way of inorganic ether groups to one or more sites of a first polyhydroxyl-functionalized polymer. This first polymer is in turn covalently bonded by way of inorganic ether groups to one or more sites of a second polyhydroxyl-functionalized polymer. The multilayered composites can be prepared by contacting porous inorganic-oxide particles with a sufficient amount of OH-reactive crosslinking agent to form metal oxide particles imbibed with the crosslinking agent, and then contacting the inorganic-oxide particles with a solution of polyhydroxyl-functionalized polymer under reactive conditions.

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15-03-2018 дата публикации

HOLLOW NANOPARTICLES WITH HYBRID DOUBLE LAYERS

Номер: US20180071225A1
Автор: JOHN Vijay, McPherson Gary

The present invention discloses the morphology of hollow, double-shelled submicrometer particles generated through a rapid aerosol-based process. The inner shell is an essentially hydrophobic carbon layer of nanoscale dimension (5-20 nm), and the outer shell is a hydrophilic silica layer of approximately 5-40 nm, with the shell thickness being a function of the particle size. The particles are synthesized by exploiting concepts of salt bridging to lock in a surfactant (CTAB) and carbon precursors together with iron species in the interior of a droplet. This deliberate negation of surfactant templating allows a silica shell to form extremely rapidly, sealing in the organic species in the particle interior. Subsequent pyrolysis results in a buildup of internal pressure, forcing carbonaceous species against the silica wall to form an inner shell of carbon. The incorporation of magnetic iron oxide into the shells opens up applications in external stimuli-responsive nanomaterials. 1182-. (canceled)183. A method of forming a plurality of particles , each particle having a hollow core , a layer surrounding the hollow core , wherein the layer comprises a species derived from an organic precursor from the group consisting of monosaccharides and polysaccharides , a shell surrounding the layer , wherein the shell comprises a ceramic , and a plurality of metal oxide nanoparticles located within the shell or between the shell and layer , comprising the steps of:a) providing a solution comprising a ceramic precursor, an organic precursor from the group consisting of monosaccharides and polysaccharides, a metal salt, and a templating surfactant;b) atomizing the solution into aerosol droplets;c) heating the aerosol droplets to form a plurality of particles, each particle having a shell comprising a ceramic derived from the ceramic precursor and a core containing the organic precursor, metal salt, and templating surfactant; andd) conducting pyrolysis of the plurality of particles, ...

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15-03-2018 дата публикации

WHITE PIGMENT DISPERSIONS

Номер: US20180072585A1
Принадлежит:

A method for manufacturing low effective density TiOincludes providing a template having a surface. The template surface is coated with a titanium-containing compound that can be reduced to TiOat high temperature. The template is removed, thereby forming porous TiOparticles. The effective density of the porous TiOparticles is less than 4. 1. A method for manufacturing low effective density TiO , comprising:providing a template having a surface;{'sub': '2', 'coating the template surface with a titanium-containing compound that can be reduced to TiOat high temperature; and'}{'sub': '2', 'removing the template, thereby forming porous TiOparticles;'}{'sub': '2', 'wherein the effective density of the porous TiOparticles is less than 4.'}2. The method of wherein the titanium-containing compound is selected from the group consisting of titanium oxysulfate claim 1 , titanium diisopropoxide bis(acetylacetonate) claim 1 , titanium(IV) ethoxide claim 1 , and tetrakis(diethylamido)titanium(IV).3. The method of claim 1 , further comprising:forming the template comprising a polymer emulsion with carboxylate groups;coating the template surface with the titanium-containing compound; and{'sub': '2', 'removing the polymer template, thereby forming the porous TiOparticles.'}4. The method of claim 1 , further comprising:providing a bubble nucleating agent;{'sub': '2', 'combining the titanium-containing compound with the bubble nucleation agent and stirring to form the template, which comprises oxygen bubbles, coated with TiO(OH);'}removing water; and{'sub': '2', 'removing the oxygen bubble template, thereby forming the porous TiOparticles.'}5. The method of wherein the bubble nucleating agent comprises a mixture of hydrogen peroxide claim 4 , urea claim 4 , and water.6. The method of wherein the effective density of TiOis within a range of about 2.5 to 3.8.7. The method of wherein the template is removed by calcining at a temperature of at least 500° C. for a period of time of at least ...

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15-03-2018 дата публикации

A low sheen paint composition with effective opacity

Номер: US20180072911A1

The present invention provides an aqueous paint composition comprising by dry weight based on total dry weight of the pigment composition, from 11% to 35% of a polymeric duller of (co)polymeric particles having an average diameter of from 1 to 20 μm, and from 25% to 70% of titanium dioxide particles; wherein from 50% to 100% of the titanium dioxide particles are encapsulated by polymer shell of (co)polymeric particles.

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24-03-2022 дата публикации

Conductive particle and manufacturing method thereof, adhesive and application thereof

Номер: US20220089917A1
Автор: Chongwei TANG, Yuming XIA
Принадлежит: HKC Co Ltd

The disclosure relates to a conductive particle and a manufacturing method thereof, an adhesive and an application thereof. The conductive particle includes a core, a conductive carbon layer and a conductive polymer layer. The conductive carbon layer covers the core, and the conductive polymer layer is provided on the conductive carbon layer. The conductivity of the conductive particle is higher.

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16-03-2017 дата публикации

INORGANIC PIGMENTS SURFACE TREATED WITH POLYOL ESTERS

Номер: US20170073523A1
Принадлежит:

A treated, particulate inorganic pigment is provided. The treated, particulate inorganic pigment comprises a plurality of pigment particles, and a polyol ester deposited on the surfaces of the pigment particles. A method of forming a treated, particulate inorganic pigment and a polymer composition are also provided. 1. A treated , particulate inorganic pigment , comprising:a plurality of pigment particles; anda polyol ester deposited on the surfaces of said pigment particles.2. The treated claim 1 , particulate inorganic pigment of claim 1 , wherein said pigment particles are formed of a pigment selected from the group consisting of titanium dioxide claim 1 , basic carbonate white lead claim 1 , basic sulfate white lead claim 1 , basic silicate white lead claim 1 , zinc sulfide claim 1 , composite pigments of zinc sulfide and barium sulfate claim 1 , zinc oxide claim 1 , antimony oxide claim 1 , iron oxide claim 1 , lead oxide claim 1 , aluminum oxide claim 1 , silicon dioxide claim 1 , chromium oxide claim 1 , zirconium oxide claim 1 , calcium carbonate claim 1 , calcium sulfate claim 1 , china clay claim 1 , kaolin clay claim 1 , mica claim 1 , diatomaceous earth claim 1 , cadmium sulfide claim 1 , cadmium selenide claim 1 , lead chromate claim 1 , zinc chromate claim 1 , nickel titanate claim 1 , and mixtures thereof.3. The treated claim 2 , particulate inorganic pigment of claim 2 , wherein said pigment particles are formed of titanium dioxide.4. The treated claim 1 , particulate inorganic pigment of claim 1 , further comprising at least one inorganic coating selected from the group consisting of metal oxide coatings claim 1 , metal hydroxide coatings claim 1 , and mixtures claim 1 , said coating being deposited on the surfaces of said pigment particles.5. The treated claim 1 , particulate inorganic pigment of claim 1 , wherein said polyol ester is formed by reacting at least one fatty acid with a polyhydric alcohol.6. The treated claim 5 , particulate inorganic ...

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19-03-2015 дата публикации

Method for making titanium dioxide pigment grind dispersion and paint

Номер: US20150080521A1
Принадлежит: Valspar Sourcing Inc

Titanium dioxide may be more efficiently used in a coating composition containing a composite pigment particle-forming polymer if during composite formation, the polymer is initially present in a low concentration and the titanium dioxide particles and newly-formed composite particles are dispersed in a waterborne emulsion polymer that does not form such a composite. A pigment grind dispersion of titanium dioxide pigment-polymer composite particles may be made by mixing titanium dioxide particles with the waterborne emulsion polymer. The composite-forming polymer is then added to the waterborne emulsion polymer, or is added independently and concurrently with the titanium dioxide particles. The resulting titanium dioxide pigment-polymer composite particles provide improved coating composition opacity compared to a coating composition that does not contain such composite particles. The coating compositions can contain reduced titanium dioxide amounts and less than a saturation level of the composite-forming polymer.

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14-03-2019 дата публикации

Porous Metal Oxide Microspheres

Номер: US20190076809A1
Принадлежит: BASF Corp, BASF SE, Harvard College

Porous metal oxide microspheres are prepared via a process comprising forming a liquid dispersion of polymer nanoparticles and a metal oxide; forming liquid droplets of the dispersion; drying the droplets to provide polymer template microspheres comprising polymer nanospheres; and removing the polymer nanospheres from the template microspheres to provide the porous metal oxide microspheres. The porous microspheres exhibit saturated colors and are suitable as colorants for a variety of end-uses.

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23-03-2017 дата публикации

Coated Titanium Dioxide Dispersions

Номер: US20170081521A1
Принадлежит:

The invention provides a method for preparing a titanium dioxide product, comprising the steps of: 4. The method of claim 2 , wherein the titanium dioxide product is not dried before the step of placing the titanium dioxide product within a packaging container.5. The method of claim 1 , wherein the coating agent is selected from AlO claim 1 , SiO claim 1 , ZrO claim 1 , CeO claim 1 , PO claim 1 , sodium silicate claim 1 , potassium silicate claim 1 , sodium aluminate claim 1 , aluminum chloride claim 1 , aluminum sulphate claim 1 , silicic acid claim 1 , and mixtures thereof.6. The method of claim 5 , wherein the coating agent is selected from SiO claim 5 , PO claim 5 , sodium silicate claim 5 , potassium silicate claim 5 , sodium aluminate claim 5 , silicic acid claim 5 , and mixtures thereof.7. The method of claim 1 , wherein the coating is a dense silica coating or comprises a dense silica coating.8. The method of claim 1 , wherein the coating is achieved whilst maintaining the colloidal stability of the titanium dioxide particles within the dispersion by control of one or more of the following factors:(a) reducing the electrolyte concentration in the dispersion before or during the coating step;(b) reducing the level of soluble salt that is added during the coating step;(c) adding a steric stabilizer before or during the coating step;(d) adjusting the pH of the dispersion away the iso-electric point of the titanium dioxide before or during the coating step;(e) adjusting the iso-electric point of the titanium dioxide away from the pH of the dispersion, by the addition of a dispersant before or during the coating step.9. The method of claim 8 , wherein at least one of factors (a)-(c) is controlled.10. The method of claim 9 , wherein at least factor (a) is controlled.11. The method of claim 10 , wherein the electrolyte concentration in the dispersion is reduced during at least one of (i) before the coating step (ii) during the coating step by the use of ...

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05-05-2022 дата публикации

METAL OXIDE PARTICLES CONTAINING TITANIUM OXIDE COATED WITH SILICON DIOXIDE-STANNIC OXIDE COMPLEX OXIDE

Номер: US20220135814A1
Принадлежит: NISSAN CHEMICAL INDUSTRIES, LTD.

A substrate is coated with a transparent coating film using a coating liquid for forming a transparent coating film including metal oxide particles and a matrix formation component. The metal oxide particles each include a metal oxide particle containing titanium oxide coated with silicon dioxide-stannic oxide complex oxide, including a titanium oxide-containing core particle; and a coating layer with which the titanium oxide-containing core particle is coated and that is made of silicon dioxide-stannic oxide complex oxide colloidal particles having a mass ratio of silicon dioxide/stannic oxide of 0.1 to 5.0, where one or more intermediate thin film layers that are made of any one of an oxide; a complex oxide of at least one element selected from Si, Al, Sn, Zr, Zn, Sb, Nb, Ta, and W; and a mixture of the oxide and the complex oxide are interposed between the core particle and the coating layer.

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19-03-2020 дата публикации

SURFACE MODIFIED PIGMENT

Номер: US20200087161A1
Принадлежит:

A composition comprising a pigment particle that is coated with a cationic material and isopropyl titanium triisostearate. The pigment particle can be included in a cleansing composition for deposition on a surface, such as skin. 114-. (canceled)15. A method for preparing a body wash , shower gel , liquid hand soap or bar soap composition comprising a pigment particle pre-coated with a cationic material and isopropyl titanium triisostearate , the method comprising the steps of: (i) dissolving the cationic material in water in a vessel to form a mixture;', '(ii) adding the pigment particle to the mixture in step (i);', '(iii) drying the mixture from step (ii);', '(iv) cooling the dried mixture;', '(v) sieving the mixture from step (iv) to remove agglomerate thereby producing a sieved powder;', '(vi) adding to the sieved powder a solution of isopropyl titanium triisostearate dissolved in a solvent;', '(vii) mixing or blending the solution from step (vi), and', '(viii) drying the mixed or blended solution to produce the coated pigment particle; and, '(a) preparing a pigment particle coated with a cationic material and isopropyl titanium triisostearate, by(b) combining the coated pigment particle with one or more components of the body wash, shower gel, liquid hand soap or bar soap selected from anionic surfactants, amphoteric surfactants, nonionic surfactants, suspending agents, oil and petrolatum.16. The method of claim 19 , wherein the dissolving in step (i) is accomplished with heating.17. The method of claim 19 , wherein the drying in step (iii) is performed by heating.18. The method of claim 21 , wherein the heating is at approximately 105° C. for approximately 3 hours.19. The method of claim 19 , wherein step (iv) further comprises gently chopping the dried mixture.20. The method of claim 19 , wherein the sieving in step (v) comprises sieving with a No. 40 sieve.21. The method of claim 19 , wherein the solvent in step (vi) is ISOPAR C solvent claim 19 , added in ...

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19-03-2020 дата публикации

Method for Producing Dispersion of Iron-Containing Rutile Titanium Oxide Fine Particles, Iron-Containing Rutile Titanium Oxide Fine Particles, and Use Thereof

Номер: US20200087162A1
Принадлежит:

Provided are titanium oxide fine particles which are excellent in transparency and are less photocatalytically active while maintaining a high refractive index, a dispersion of such fine particles, and a method for producing such a dispersion. The method for producing a dispersion of iron-containing rutile titanium oxide fine particles including a step (1) of neutralizing an aqueous metal mineral acid salt solution containing Ti and Fe in FeO/(TiO+FeO)=0.001 to 0.010 to form an iron-containing hydrous titanic acid; a step (2) of adding an aqueous hydrogen peroxide solution to form an aqueous solution of iron-containing peroxotitanic acid having an average particle size of 15 to 50 nm; a step (3) of adding a tin compound so as to satisfy TiO/SnO=6 to 16; a step (4) of adding a sol of silica-based fine particles which contain Si and a metal element M in SiO/MO=99.9/0.1 to 80/20, the addition being made so as to satisfy SiO/(oxides of the other elements)=0.08 to 0.22; and a step (5) of hydrothermally treating the solution obtained in the step (4). 1. A method for producing a dispersion of iron-containing rutile titanium oxide fine particles , comprising:{'sub': 2', '3', '2', '2', '3, 'a step (1) of neutralizing an aqueous metal mineral acid salt solution containing Ti and Fe as metals to form an iron-containing hydrous titanic acid, the masses of the metals in the aqueous solution in terms of oxide being such that mass of FeO/(total mass of TiOand FeO)=0.001 to 0.010;'}a step (2) of adding an aqueous hydrogen peroxide solution to the iron-containing hydrous titanic acid obtained in the step (1) to form an aqueous solution of iron-containing peroxotitanic acid having an average particle size of 15 to 50 nm;{'sub': 2', '2, 'a step (3) of adding a tin compound to the aqueous solution of iron-containing peroxotitanic acid obtained in the step (2) in such an amount that the masses of Sn and Ti in the aqueous solution in terms of oxide satisfy mass of TiO/mass of SnO=6 to 16 ...

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28-03-2019 дата публикации

THERMAL RESISTANT TITANIUM DIOXIDE PARTICLES AND THE FORMATION OF COOL ARTICLES

Номер: US20190094426A1
Автор: CONNOLLY, JR. J. DON
Принадлежит:

The present disclosure relates to titanium dioxide particles designed to enhance reflection of both IR and visible wavelengths, or energy, and their use in forming cool, fully opaque polymeric articles prepared by melt processible resin. Such articles, made from melt processible thermoplastic and/or thermoset resin have enhanced outdoor utility because they inhibit damage caused by the sun as a result of the article including titanium dioxide particles of the present invention exhibiting low photo-activity properties. 1. Thermal resistant , low photo-activity , titanium dioxide particles comprising:a) a TiO2 particle comprising a surface having a median particle size between 0.30 μm and 0.38 μm;b) a silica coating;c) an alumina coating having an interior and exterior surface; andd) an organic coating,wherein the silica coating is located between the surface of the TiO2 particle and the interior surface of the alumina coating and the organic coating is located on the exterior surface of the alumina coating.2. The composition of wherein the TiO2 particle further comprises a rutile crystalline form.3. The composition of wherein the organic coating is selected from the group of organic compounds selected from the group consisting of an organosiloxane claim 1 , organosilane claim 1 , alkyl carboxylic acid claim 1 , alkyl sulfonate claim 1 , organophosphate claim 1 , orgaonophosphonate claim 1 , and a combination thereof.4. The composition of wherein the organic coating is polydimethyl siloxane.5. The composition of claim 1 , wherein the median particle size is in the range of 0.32 and 0.36.6. The composition of claim 1 , wherein the median particle size is in the range of 0.32 μm and 0.35 μm.7. The composition of wherein the silica coating is in the range of 1.0 to 5.0 wt. % of the total particle weight. This application is a divisional application of U.S. Ser. No. 15/078,125 filed Mar. 23, 2016, which claims the benefit of priority of U.S. Provisional Application No. 62 ...

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26-06-2014 дата публикации

Method for manufacturing fatty acid metal salt particle, and fatty acid metal salt particle

Номер: US20140178813A1
Принадлежит: Fuji Xerox Co Ltd

A method for manufacturing a fatty acid metal salt particle includes forming a coating layer including a fatty acid metal salt on a surface of a core material particle in supercritical carbon dioxide.

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26-03-2020 дата публикации

Laminate Pigment with Spacing Properties and High UV-Greying Stability

Номер: US20200095427A1
Принадлежит: Kronos International, Inc.

The invention relates to a titanium dioxide particle with high opacity and UV-greying resistance comprising two silica coats and at least one alumina coat, to a method for the obtaining the same, and to the use of said particle in a method for obtaining a decorative paper laminate or a décor foil. The present invention further pertains a decorative paper laminate or a décor foil containing said coated titanium dioxide particle. 1. A method for obtaining coated titanium dioxide particles , comprising the steps of:(i) providing an aqueous suspension of uncoated titanium dioxide particles;(ii) adding phosphoric acid to the suspension to adjust the pH of the suspension to a value of no more than about 2;(iii) adding a first alkaline silicon dioxide precursor to the suspension, wherein after the addition the suspension has a pH value of from about 7 to about 8 and the silicon dioxide precursor formed a first silica coat on the particles;(iv) adding an acid to the suspension to adjust the pH of the suspension to a value of from about 2 to about 3;(v) adding a second alkaline silicon dioxide precursor to the suspension, wherein after the addition the suspension has a pH value of from about 4 to about 5 and the second alkaline silicon dioxide precursor formed a second silica coat on the first silica coat; and(vi) applying at least one aluminum oxide coat onto the second silica coat.2. The method of claim 1 , wherein an acidic aluminum oxide precursor is added to the suspension in step (vi) to form the at least one aluminum oxide coat.3. The method of claim 2 , wherein the acidic aluminum oxide precursor is selected from the group consisting of aluminum sulfate claim 2 , aluminum nitrate claim 2 , aluminum chloride claim 2 , and combinations thereof.4. The method of claim 3 , wherein the acidic aluminum oxide precursor is aluminum sulfate.5. The method of claim 2 , wherein after the addition of at least one aluminum oxide coat the suspension has a pH value of from about 1 to ...

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26-03-2020 дата публикации

SILICONE RESIN REFLECTIVE SUBSTRATE, MANUFACTURING METHOD FOR SAME, AND BASE MATERIAL COMPOSITION USED IN REFLECTIVE SUBSTRATE

Номер: US20200095430A1
Принадлежит: ASAHI RUBBER INC.

A versatile silicone resin reflective substrate which exhibits high reflectance of high luminance light from an LED light source over a wide wavelength from short wavelengths of approximately 340-500 nm, which include wavelengths from 380-400 nm near lower limit of the visible region, to longer wavelength in the infra-red region. The silicone resin reflective substrate has a reflective layer which contains a white inorganic filler powder dispersed in a three-dimensional cross linked silicone resin, the inorganic filler powder having a high reflective index than the silicone resin. The reflective layer is formed on a support body as a film, a solid, or a sheet. The silicone resin reflective substrate can be easily formed as a wiring substrate, a packaging case or the like, and can be manufactured at low cost and a high rate of production. 1. A silicone resin reflective substrate made from a base material composition , which has a plasticity to be cured for the reflective substrate so that a white inorganic filler powder is incorporated into a 3-dimensionally cross-linked silicone resin ,the base material composition containing:base materials including a polymerisable silicone resin, and{'sub': 2', '3', '2', '2, 'claim-text': the base material composition is a liquid-like base material, and the base material composition of the liquid-like base material has a viscosity of 0.5-500 Pa·s, or', 'the base material composition is a grease-like, a plastic-like or a millable-type base material composition, and the base material composition of the grease-like, the plastic-like or the millable-type base material composition has a plasticity number of 100-500 mm/100., 'the white inorganic filler powder including titanium oxide surface-treated with Al, AlO, ZnO, ZrO, SiOand/or a silane coupling agent, which has a higher refractive index than that of the 3-dimensionally cross-linked silicone resin; wherein'}2. The silicone resin reflective substrate according to claim 1 , wherein ...

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12-04-2018 дата публикации

WHITE INKS

Номер: US20180100078A1

The present disclosure provides an example of a white ink. The ink includes an aqueous ink vehicle and from 5 wt % to 60 wt % of a white flocculated colorant mass. The white flocculated colorant mass can include white metal oxide pigment having an average particulate size from 100 nm to 2,000 nm, silica coated on the white metal oxide pigment to form a silica-coated pigment, and a polymeric dispersant associated with a surface of the silica-coated pigment. 1. A white ink , comprising:an aqueous ink vehicle; white metal oxide pigment having an average particulate size from 100 nm to 2,000 nm,', 'silica coated on the white metal oxide pigment forming a silica-coated pigment, wherein the white metal oxide pigment content to silica content is from 100:3.5 to 5:1 by weight, and', 'a polymeric dispersant associated with a surface of the silica-coated pigment., 'from 5 wt % to 60 wt % of a white flocculated colorant mass, comprising2. The white ink of claim 1 , further comprising alumina also coated on the white metal oxide pigment.3. The white ink of claim 2 , wherein the white metal oxide pigment content to total silica and alumina content is from 50:3 to 4:1 by weight.4. The white ink of claim 1 , wherein the white ink comprises from 5 wt % to 50 wt % the white metal oxide pigment claim 1 , from 0.175 wt % to 10 wt % silica claim 1 , and from 0.005 wt % to 5 wt % polymeric dispersant.5. The white ink of claim 1 , wherein the white metal oxide pigment includes titanium dioxide particulates claim 1 , zinc oxide particulates claim 1 , zirconium oxide particulates claim 1 , or combinations thereof.6. The white ink of claim 1 , wherein the white ink further comprises latex particulates having a glass transition temperature from −20° C. to 130° C.7. The white ink of claim 1 , wherein the polymeric dispersant includes a short-chain anionic dispersant having an acid number higher than 100 mg KOH/g based on dry polymer weight claim 1 , or a non-ionic or predominantly non-ionic ...

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23-04-2015 дата публикации

Process for preparing powder with enhanced bulk handling property

Номер: US20150110710A1
Принадлежит: Chemours Co TT LLC

The present invention relates to a process for manufacturing low-dusting, smoothly-discharging, easily dispersible, powders such as pigmentary titanium dioxide that resist compaction, aging, lumping, and/or caking. Particularly, the present invention relates to a process for treating powders such as pigmentary titanium dioxide with ammonia or a similarly basic substance prior to or during agglomeration to produce a powder with improved bulk handling properties.

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02-06-2022 дата публикации

PARTICLES WITH COLOR EFFECT AND COMPOSITIONS INCLUDING THE SAME

Номер: US20220169860A1
Принадлежит:

A particle is provided that includes a first material and a second material, arranged to provide a Fano resonance effect, for example in the visible portion of electromagnetic spectrum. The first and second materials may be substantially clear in the visible portion of the electromagnetic spectrum. The first material may include an inorganic material, such as SiO, TiO, HfO, ZrO, diamond, or a combination thereof. The second material may include a polymer. The first material has a first refractive index and the second material has a second refractive index, where the first refractive index and second refractive index have a difference of 0.5 or greater, and 1.0 or less. The first material may form a core and the second material may form a shell surrounding the core. Alternatively, the first and second materials may form a Janus particle, an asymmetric dimer, or an aggregate. 1. A particle comprising a first material and a second material , arranged to provide a Fano resonance effect in visible portion of electromagnetic spectrum.2. The particle of claim 1 , wherein the first and second materials are substantially clear in the visible portion of the electromagnetic spectrum.3. The particle of claim 1 , wherein the particle is substantially clear in IR portion of the electromagnetic spectrum or emits only in a wavelength range of 8 μm to 13 μm and is substantially clear in other parts of the IR portion.4. The particle of claim 1 , wherein the first material comprises an inorganic material comprising SiO claim 1 , TiO claim 1 , HfO claim 1 , ZrO claim 1 , diamond claim 1 , or a combination thereof.5. The particle of claim 1 , wherein the second material comprises a polymer claim 1 , wherein the polymer comprises a polyacrylate claim 1 , polymethylmethacrylate claim 1 , polymethylacrylate claim 1 , polydimethylsiloxane claim 1 , poly(1 claim 1 ,1 claim 1 ,1 claim 1 ,3 claim 1 ,3 claim 1 ,3-hexafluoroisopropyl acrylate) claim 1 , poly(2 claim 1 ,2 claim 1 ,2- ...

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21-04-2016 дата публикации

INORGANIC RED PIGMENT

Номер: US20160108247A1
Принадлежит:

An inorganic red pigment is provided which pigment comprises titanium oxide, tin oxide, zinc oxide, and tungsten oxide, wherein the molar ratios of the oxides correspond to a composition of formula 115.-. (canceled)18) The pigment according to claim 17 , wherein 1.1≦a≦2.4; 0.5≦b≦1.5; 0.4≦c≦1.1; 0.1≦d≦0.6; and 0≦e≦0.3.19) The pigment according to claim 17 , wherein EOis an oxide of K claim 17 , Mg claim 17 , Ca claim 17 , Sr claim 17 , Ba claim 17 , Al claim 17 , Si claim 17 , Bi claim 17 , V claim 17 , Nb claim 17 , Ta claim 17 , Mn or a combination thereof.20) The pigment according to claim 16 , wherein ZnO is partially replaced by ZnS and the molar ratio of ZnO to ZnS is in the range of from 1.25:0.05 to 1.0:0.3.21) The pigment according to claim 16 , wherein the pigment comprises a sulfide of Sn claim 16 , Ca claim 16 , Ba or Mn.22) The pigment according to claim 17 , wherein 0.4≦c≦0.7 and 0.01≦e≦0.3.23) The pigment according to claim 16 , wherein 0.1≦d≦0.5.24) The pigment according to claim 16 , wherein the molar ratio of SnO:SnOin SnOis of from 0.75:0.25 to 0.98:0.02.25) The pigment according to claim 16 , wherein the molar ratio of SnO:SnOin SnOis of from 0.8:0.2 to 0.9:0.1.26) The pigment according to claim 16 , wherein the pigment is coated with at least one layer.27) The pigment according to claim 26 , wherein the said at least one layer is an inorganic layer.28) A process for producing the pigment as defined in claim 16 , which process comprises{'sub': 2', '3', 'y', 'z', 'y', 'z, 'a) mixing TiO, ZnO, SnO, WO, or a precursor compound thereof, and optionally at least one compound selected from EO, SnS, ZnS or ES, or a precursor compound thereof as a dry powder to form a powder mixture;'}b) calcining the powder mixture at a temperature of from 600 to 950° C. to form a furnace clinker;c) grinding the furnace clinker to form pigment particles; andd) optionally coating the pigment particles with at least one layer.29) The process according to claim 28 , wherein ...

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19-04-2018 дата публикации

WHITE INKS

Номер: US20180105714A1

The present disclosure provides an example where a white ink can include an aqueous ink vehicle and from 5 wt % to 60 wt % of a white flocculated colorant mass. The white flocculated colorant mass can include white metal oxide pigment, an alumina coating, and polymeric dispersant associated with a surface of the alumina-coated pigment. The white metal oxide pigment can have an average particulate size from 100 nm to 2,000 nm. The alumina coating on the white metal oxide pigment can form an alumina-coated pigment where the alumina coating is predominantly alumina, and the white metal oxide pigment content to alumina content can be from 99:1 to 9:1 by weight. 1. A white ink , comprising:an aqueous ink vehicle; white metal oxide pigment having an average particulate size from 100 nm to 2,000 nm,', 'an alumina coating on the white metal oxide pigment forming an alumina-coated pigment, wherein the alumina coating is predominantly alumina, and wherein the white metal oxide pigment content to alumina content is from 99:1 to 9:1 by weight, and', 'a polymeric dispersant associated with a surface of the alumina-coated pigment., 'from 5 wt % to 60 wt % of a white flocculated colorant mass, comprising2. The white ink of claim 1 , wherein the white metal oxide pigment content to alumina content is from 49:1 to 47:3 by weight.3. The white ink of claim 1 , wherein the alumina coating further comprises silica.4. The white ink of claim 1 , wherein the white ink comprises 5 wt % to 50 wt % white metal oxide pigment claim 1 , 0.05 wt % to 10 wt % alumina in the alumina coating claim 1 , and 0.005 wt % to 5 wt % polymeric dispersant.5. The white ink of claim 1 , wherein the white metal oxide pigment includes titanium dioxide particulates claim 1 , zinc oxide particulates claim 1 , zirconium oxide particulates claim 1 , or combinations thereof.6. The white ink of claim 1 , wherein the white ink further comprises latex particulates having a glass transition temperature from −20° C. to ...

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02-04-2020 дата публикации

2-DIMENSIONAL MXENE PARTICLE SURFACE-MODIFIED WITH FUNCTIONAL GROUP CONTAINING SATURATED OR UNSATURATED HYDROCARBON, PREPARATION METHOD THEREOF AND USE THEREOF

Номер: US20200102444A1
Принадлежит:

The present invention relates to a 2-dimensional MXene particle surface-modified with a functional group comprising a saturated or unsaturated hydrocarbon, a preparation method thereof, and a use thereof (e.g., a conductive film). 1. A passivated 2-dimensional MXene particle , comprising:a 2-dimensional MXene particle surface-modified with a functional group comprising a saturated or unsaturated hydrocarbon; andan organic protective film formed on the surface of the surface-modified 2-dimensional MXene particle.2. The 2-dimensional MXene particle of claim 1 , wherein the functional group is capable of forming an ionic or a covalent bond between a MXene surface and a surface-modifying precursor comprising the saturated or unsaturated hydrocarbon dispersed in an organic phase.3. The 2-dimensional MXene particle of claim 1 , wherein the functional group is selected from the group consisting of a phosphonate claim 1 , an amine claim 1 , and a silane.4. The 2-dimensional MXene particle of claim 1 , wherein the 2-dimensional MXene particle surface-modified with the functional group comprising the saturated or unsaturated hydrocarbon is dispersed in an organic solvent forming a protective film.5. The 2-dimensional MXene particle of claim 1 , wherein the 2-dimensional MXene particle surface-modified with the functional group comprising the saturated or unsaturated hydrocarbon is covered with an organic polymer forming a protective film or dispersed in an organic polymer.7. The 2-dimensional MXene particle of claim 1 , wherein the 2-dimensional MXene particle claim 1 , as a subject of surface modification claim 1 , is a 2-dimensional transition metal carbide claim 1 , nitride claim 1 , or combination thereof comprising at least one layer wherein a crystal cell having Empirical Formula 1 or 2 is formed in a 2-dimensional array:{'br': None, 'sub': n+1', 'n, 'MX\u2003\u2003[Empirical Formula 1]'}wherein, each X is located within an octahedral array,M is a metal selected from ...

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27-04-2017 дата публикации

RED AND RED-SHADE VIOLET INORGANIC OXIDE MATERIALS CONTAINING COBALT

Номер: US20170114224A1
Принадлежит:

The current technology is directed to red and red-shade violet pigments with an hexagonal ABOstructure of the form Y(In, M)Oin which M is substituted for In in the trigonal bipyramidal B site of the ABOstructure, and where M is a mixture containing Co and charge compensating ions, or M is a mixture containing Co and charge compensating ions, as well as other aliovalent and isovalent ions. 1. An ABOmaterial having a formula A(M ,M′)Owherein A is Y, La, Sc, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, or mixtures thereof;wherein M=Al, Ga, In, Cr, Fe, Ni, B, Mn, or mixtures thereof;{'sub': A', 'B, 'wherein M′ is a mixture of Mand Mcations;'}{'sub': 'A', 'wherein M=Co, Zn, Mg, Ca, Sr, Ba, Cu, Ni, or mixtures thereof;'}{'sub': 'B', 'wherein M=Ti, Zr, Sn, Si, V, Sb, Nb, Mo, W, Ta, Bi or mixtures thereof;'}{'sub': 'A', 'wherein at least one of Mis Co;'}wherein cations are present in proportions close to those for making an electrically neutral hexagonal oxide.2. The material of wherein the formulas are selected from:{'sub': 1−x', '0.5', '0.5', 'x', '3, 'YIn(CoTi)O'}{'sub': 1−x', '0.5', '0.5', '3, 'YIn((Co,Zn)Ti)xO'}{'sub': 1−x', '0.5', '0.5', 'x', '3, 'Y(In, Mn)(CoTi)O'}{'sub': 1−x', '0.5', '0.5', 'x', '3, 'Y(In, Mn)((Co,Zn)Ti)O'}wherein 0 Подробнее

27-04-2017 дата публикации

SILICONE RESIN REFLECTIVE SUBSTRATE, MANUFACTURING METHOD FOR SAME, AND BASE MATERIAL COMPOSITION USED IN REFLECTIVE SUBSTRATE

Номер: US20170114226A1
Принадлежит: ASAHI RUBBER INC.

A versatile silicone resin reflective substrate which exhibits high reflectance of high luminance light from an LED light source over a wide wavelength from short wavelengths of approximately 340-500 nm, which include wavelengths from 380-400 nm near lower limit of the visible region, to longer wavelength in the infra-red region. The silicone resin reflective substrate has a reflective layer which contains a white inorganic filler powder dispersed in a three-dimensional cross linked silicone resin, the inorganic filler powder having a high reflective index than the silicone resin. The reflective layer is formed on a support body as a film, a solid, or a sheet. The silicone resin reflective substrate can be easily formed as a wiring substrate, a packaging case or the like, and can be manufactured at low cost and a high rate of production. 1. A base material composition which is usable for forming a silicone resin reflective substrate , and the base material composition is a liquid-like base material , or a grease-like , a plastic-like or a millable-type base material composition having a plasticity to be cured for the reflective substrate so that the white inorganic filler powder is incorporated into a 3-dimensionally cross-linked silicone resin , containing:base materials of a polymerisable silicone resin, and{'sub': 2', '3', '2', '2, 'the white inorganic filler powder including titanium oxide surface-treated with Al, AlO, ZnO, ZrO, SiOand/or a silane coupling agent, which has a higher refractive index than that of the 3-dimensionally cross-linked silicone resin.'}2. The base material composition according to claim 1 , wherein the base material composition contains a reaction inhibitor which is deactivated or vaporized when heated.3. The base material composition according to claim 1 , wherein the base material composition contains an organic solvent and/or a reactive diluent for adjusting viscosity.4. The base material composition according to claim 1 , wherein the ...

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13-05-2021 дата публикации

BLACK TITANIUM DIOXIDE LiDAR REFLECTING PARTICLES AND VEHICLES COMPRISING THE SAME

Номер: US20210139713A1

Black titanium dioxide has a crystalline titanium dioxide core and an amorphous titanium dioxide shell that encompasses the crystalline titanium dioxide core. The black titanium dioxide has a reflectivity of electromagnetic radiation in the visible spectrum that is less than or equal to 15% and a reflectivity for near-IR and LiDAR electromagnetic radiation that is greater than or equal to 10%. The black titanium dioxide has a band gap from greater than or equal to 1.0 eV to less than or equal to 2.0 eV. 1. Black titanium dioxide comprising:a crystalline titanium dioxide core; andan amorphous titanium dioxide shell that encompasses the crystalline titanium dioxide core, whereinthe black titanium dioxide has a reflectivity of electromagnetic radiation in the visible spectrum that is less than or equal to 15% and a reflectivity for near-IR and LiDAR electromagnetic radiation that is greater than or equal to 10%.2. The black titanium dioxide of claim 1 , wherein the black titanium dioxide has a reflectivity of electromagnetic radiation in the visible spectrum that is less than or equal to 5%.3. The black titanium dioxide of claim 1 , wherein the black titanium dioxide has a reflectivity for near-IR and LiDAR electromagnetic radiation that is greater than or equal to 20%.4. The black titanium dioxide of claim 1 , wherein the black titanium dioxide has a reflectivity for electromagnetic radiation in the visible spectrum that is from greater than or equal to 0.5% to less than or equal to 5%.5. The black titanium dioxide of claim 1 , wherein the black titanium dioxide has a reflectivity for near-IR and LiDAR electromagnetic radiation that is from greater than or equal to 15% to less than or equal to 65%.6. The black titanium dioxide of claim 1 , wherein the black titanium dioxide has a band gap from greater than or equal to 1.0 eV to less than or equal to 2.0 eV.7. The black titanium dioxide of claim 1 , wherein the black titanium dioxide has a band gap from greater than or ...

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07-05-2015 дата публикации

Titania fine-particle composite and compositions containing the titania fine-particle composite

Номер: US20150125501A1
Автор: Eiji Takahashi
Принадлежит: Pola Chemical Industries Inc

Provided are a novel titania fine-particle composite which has high transparency, high stability, and high ultraviolet-absorbing power and excellent redispersibility, and skin-care external preparations which contain the titania fine-particle composite and exert high ultraviolet protective effect. The titania fine-particle composite can be produced by adding one or more selected from among carboxylic acids and carboxylic acid derivatives represented by general formula (1), and polymers containing the carboxylic acids or carboxylic acid derivatives as a constituent monomer to an aqueous acid dispersion of titania fine particles, and neutralizing the resulting dispersion with an alkali to form a titania fine-particle composite composed of titania fine particles functioning as cores and the carboxylic monomer or polymer deposited on the surface of the cores. In the titania fine-particle composite, titania fine particles functioning as cores have a high degree of crystallization and the intermolecular interaction between titania fine particles and the carboxylic monomer or polymer is strong. Therefore, the titania fine-particle composite can be uniformly dispersed in a dispersion medium to attain high transparency and high stability. Further, skin-care external preparations which exert high ultraviolet protective effect can be produced by adding the titania fine-particle composite.

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05-05-2016 дата публикации

TITANIUM DIOXIDE PIGMENT AND MANUFACTURING METHOD

Номер: US20160122472A1
Принадлежит:

A novel polymer comprising a water soluble polymer backbone, at least one functional group attached to the polymer backbone and having an affinity for titanium dioxide, and at least one hydrophobic functional group attached to the polymer backbone and having an affinity for latex is provided. A titanium dioxide pigment composition is provided including the novel polymer is also provided. Also provided is a method of manufacturing a titanium dioxide pigment composition that includes the novel polymer. 1. A polymer , comprising:a water soluble polymer backbone;at least one functional group attached to said polymer backbone and having an affinity for titanium dioxide; andat least one hydrophobic functional group attached to said polymer backbone and having an affinity for latex.2. The polymer of claim 1 , wherein said functional group attached to said polymer backbone and having an affinity for titanium dioxide is a nitrogen containing functional group.3. The polymer of claim 2 , wherein said functional group attached to said polymer backbone and having an affinity for titanium dioxide is formed by the reaction of said polymer backbone with a compound selected from the group consisting of amines claim 2 , amino acids claim 2 , amides claim 2 , ureas claim 2 , urethane claim 2 , ureido claim 2 , biuret and imidazole.4. The polymer of claim 3 , wherein said functional group attached to said polymer backbone and having an affinity for titanium dioxide is formed by the reaction of said polymer backbone with a compound selected from the group consisting of amides claim 3 , ureas claim 3 , and imidazole.5. The polymer of claim 2 , wherein said functional group attached to said polymer backbone and having an affinity for titanium dioxide further comprises a hydroxyl group.6. The polymer of claim 5 , wherein said functional group attached to said polymer backbone and having an affinity for titanium dioxide is formed by the reaction of said polymer backbone with an amino ...

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05-05-2016 дата публикации

PIGMENTS BASED ON LiSbO3 AND LiNbO3 RELATED STRUCTURES

Номер: US20160122548A1
Автор: Yuhasz William M.
Принадлежит:

The present invention involves pigments derived from compounds with the LiSbO-type or LiNbO-type structures. These compounds possess the following formulations MMZ, MMMMZ, MMMZ, MMMMZ, MMMZ, MMMZ, or a combination thereof. The cation Mrepresents an element with a valence of +1 or a mixture thereof, the cation Mrepresents an element with a valence of +2 or a mixture thereof, the cation Mrepresents an element with a valence of +3 or a mixture thereof, the cation Mrepresents an element with a valence of +4 or a mixture thereof, the cation Mrepresents an element with a valence of +5 or a mixture thereof, and the cation Mrepresents an element with a valence of +6 or a mixture thereof. The cation M is selected from H, Li, Na, K, Rb, Cs, Mg, Ca, Sr, Ba, Sc, Y, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W, Mn, Fe, Ru, Co, Ni, Cu, Ag, Zn, B, Al, Ga, In, Si, Ge, Sn, P, Sb, or Te. The anion Z is selected from N, O, S, Se, Cl, F, hydroxide ion or a mixture thereof. Along with the elements mentioned above vacancies may also reside on the M or Z sites of the above formulations such that the structural type is retained. The above formula may also include M dopant additions below 20 atomic %, where the dopant is selected from H, Li, Na, K, Rb, Cs, Mg, Ca, Sr, Ba, Sc, Y, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W, Mn, Fe, Ru, Co, Ni, Cu, Ag, Zn, B, Al, Ga, In, Si, Ge, Sn, P, Sb, Bi, Te, or mixtures thereof. 1. A pigment comprising a compound with a LiSbO-type or a LiNbO-type structure , and having a chemical formula selected from the following:{'br': None, 'sup': 1', '5, 'sub': '3', 'MMZ, where M is a dopant at a level between 0.1 and 20 atomic %'}{'br': None, 'sup': 1', '2', '4', '5, 'sub': '6', 'MMMMZ,'}{'br': None, 'sup': 1', '3', '5, 'sub': 2', '6, 'MMMZ,'}{'br': None, 'sup': 1', '2', '3', '6, 'sub': '6', 'MMMMZ,'}{'br': None, 'sup': 1', '4', '6, 'sub': 2', '6, 'MMMZ,'}{'br': None, 'sup': 1 ...

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04-05-2017 дата публикации

Matting Agent and Method for Obtaining the Same

Номер: US20170121551A1
Принадлежит:

The invention relates to a matting agent comprising agglomerates of pigment particles, to a method for the preparation of such matting agents, and to coating formulations containing the matting agents disclosed herein. The present invention further relates to pigmented mat surfaces, and to the use of agglomerates of pigment particles for matting pigmented coatings. 1. A matting agent useful for preparing pigmented mat surfaces comprising pigment particles wherein such pigment particles are preset in agglomerates having an average agglomerate size d50 of from about 2 to about 200 μm and a specific surface (BET) area of from about 5 to about 50 m/g.2. The matting agent of claim 1 , wherein the agglomerates have an average agglomerate size of from about 2 to about 100 μm.3. The matting agent of claim 2 , wherein the agglomerates have an average agglomerate size of from about 2 to about 50 μm4. The matting agent of claim 3 , wherein the agglomerates have an average agglomerate size of from about 2 to about 20 μm5. The matting agent of claim 1 , wherein agglomerates have a specific surface (BET) of from 10 to 30 m/g.6. The matting agent of claim 5 , wherein agglomerates have a specific surface (BET) of from 11 to 25 m/g.7. The matting agent of claim 6 , wherein agglomerates have a specific surface (BET) of from 13 to 20 m/g.8. The matting agent of claim 1 , wherein the agglomerates have an oil absorption value as measured according to DIN ISO 787 Part 5 of about 15 to about 25 g/100 g.9. The matting agent of claim 8 , wherein the agglomerates have an oil absorption value as measured according to DIN ISO 787 Part 5 of about 17 to about 22 g/100 g.10. The matting agent of claim 1 , where the pigment particles have an average particle size d50 of from about 200 to about 500 nm.11. The matting agent of claim 1 , wherein the pigment particles are a metal salt.12. The matting agent of claim 11 , wherein the metal salt is a metal oxide.13. The matting agent of claim 12 , ...

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25-08-2022 дата публикации

Solid composition

Номер: US20220267210A1
Принадлежит: Sumitomo Chemical Co Ltd

A solid composition contains a first material and a powder and satisfies requirements 1 and 2. Requirement 1: |dA(T)/dT| satisfies 10 ppm/° C. or more at least at −200° C. to 1,200° C. A is (an a-axis lattice constant of a crystal in the powder)/(a c-axis lattice constant of a crystal in the powder), obtained from X-ray diffractometry of the powder. Requirement 2: C is 0.04 or more. C is (a log differential pore volume when a pore diameter of the solid composition is B in a pore distribution curve of the solid composition)/(a log differential pore volume corresponding to a maximum peak intensity in the pore distribution curve of the solid composition). B is (a pore diameter giving a maximum peak intensity in the pore distribution curve of the solid composition)/2. The pore distribution curve of the solid composition shows a relationship between the pore diameter and the log differential pore volume.

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25-08-2022 дата публикации

POWDER AND SOLID COMPOSITION

Номер: US20220267605A1
Принадлежит:

This powder satisfies requirements 1 and 2. 1. Powder that satisfies the following requirements 1 and 2:requirement 1: |dA(T)/dT| satisfies 10 ppm/° C. or more at at least one temperature T1 in a range of −200° C. to 1200° C.where A is (a-axis (shorter axis) lattice constant of a crystal in the powder)/(c-axis (longer axis) lattice constant of the crystal in the powder), and each of the lattice constants is obtained by X-ray diffractometry of the powder; andrequirement 2: a particle diameter D50 at a cumulative frequency of 50%, a particle diameter D10 at a cumulative frequency of 10%, and a particle diameter D90 at a cumulative frequency of 90% in a volume-based cumulative particle diameter distribution curve obtained by a laser diffraction scattering method satisfy the following conditions (I) and (II):(I) a ratio of D10 to D50 (D10/D50) is 0.05 or more and 0.45 or less, and(II) D90 is 0.5 um or more and 70 um or less.2. The powder according to claim 1 , wherein the powder is metal oxide powder.3. The powder according to claim 2 , wherein the metal oxide powder is metal oxide powder containing a metal having d electrons.4. The powder according to claim 2 , wherein the metal oxide powder is titanium-containing metal oxide powder.5. The powder according to claim 4 , wherein the titanium-containing metal oxide powder is TiO(x=1.30 to 1.66) powder.6. The powder according to claim 1 , wherein the D50 is 0.5 μm or more and 60 μm or less.7. A solid composition comprising the powder according to and a first material.8. The solid composition according to claim 7 , wherein the first material is at least one compound selected from the group consisting of resins claim 7 , alkali metal silicates claim 7 , ceramics claim 7 , and metals. The present invention relates to powder and a solid composition.Conventionally, it has been known to add a solid material having a negative linear thermal expansion coefficient to a solid material having a positive linear thermal expansion ...

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25-08-2022 дата публикации

COMPLEX FUNCTIONAL PIGMENT AND MANUFACTURING METHOD THEREOF

Номер: US20220267606A1

The complex functional pigment according to the present invention can effectively functionalize paints while minimizing the content of pigment added to a paint composition, that is, the solid content of a paint composition, for functionalization such as heat insulation, sound insulation, beautification, weather resistance, durability, chemical resistance, antibiotic properties, surface hydrophilization/hydrophobicity and the like, and even when added in a high content in the paint composition, it has an effect of excellent dispersibility. In addition, since the color realization area of a coating film is wide, various colors can be implemented, and it also has an effect that it is easy to adjust to the desired color. 1. A complex functional pigment , comprising a titanium oxide aerogel having a BET specific surface area of 50 to 2 ,000 m/g and absorption in the visible region , and doped with one or two or more metals selected from the group consisting of noble metals and transition metals.2. The complex functional pigment of claim 1 , wherein the noble metal and the transition metal are one or two or more metals selected from the group consisting of Au claim 1 , Ag claim 1 , Pt claim 1 , Pd claim 1 , Rh claim 1 , Cu claim 1 , Fe claim 1 , Mg claim 1 , V claim 1 , Cr claim 1 , Sr and Nb.3. The complex functional pigment of claim 1 , wherein Ti claim 1 , noble metal and transition metal included in the aerogel have single-phase elemental uniformity.4. The complex functional pigment of claim 3 , wherein the aerogel is manufactured by gelation of titania sol with a metal precursor comprising one or two or more metals selected from the group consisting of noble metals and transition metals.5. The complex functional pigment of claim 1 , wherein the titanium oxide aerogel has mesopores and macropores.6. The complex functional pigment of claim 1 , wherein the titanium oxide aerogel has absorption characteristics in the entire wavelength range of 400 nm to 800 nm in the ...

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