10-03-2022 дата публикации
Номер: US20220073751A1
Принадлежит:
The invention relates to a method for preparing an at least partially exfoliated clay. The present invention further relates to an at least partially exfoliated clay obtainable by such a method and to a suspension comprising such a clay, as well to the use of such an at least partially exfoliated clay and of a suspension comprising such an at least partially exfoliated clay. Furthermore, the present invention is also directed to a polymeric composition comprising an at least partially exfoliated clay and/or a suspension comprising an at least partially exfoliated clay. 1. A method for preparing an at least partially exfoliated clay , comprising the steps of:(1) providing a clay;(2) providing an exfoliating agent, comprising a partial ester of poly(alkylene oxide) (meth)acrylate, a cyclic carbonate and water,wherein the water is present in an amount of 10% by volume or less based on the volume of the exfoliating agent;(3) mixing the clay and the exfoliating agent; and(4) obtaining the at least partially exfoliated clay.2. The method according to claim 1 , wherein the clay is a natural or synthetic layered silicate mineral.3. The method according to claim 1 , wherein the clay is selected from the group consisting of smectite claim 1 , montmorillonite claim 1 , saponite claim 1 , beidellite claim 1 , montmorillonite claim 1 , hectorite claim 1 , stevensite claim 1 , vermiculite claim 1 , kaolinite claim 1 , hallosite claim 1 , magadiite claim 1 , fluorohectorite claim 1 , and combinations thereof.4. The method according to claim 1 , wherein the partial ester of poly(alkylene oxide) (meth)acrylate is represented by:{'br': None, 'sub': ['2', '2', '2', 'a', '2', 'b', '2', 'c', '2', 'd', 'y'], 'sup': ['1', '2', '3', '4', '5'], '#text': '(CH═CR—CO—(CHRCHO)—(CHRCHO))dx-L-((CHRCHO)—(CHRCHO)—OH)'}{'claim-text': [{'sup': ['1', '2', '5'], 'sub': '1-6', '#text': 'Ris hydrogen or methyl, Rto Rare each independently hydrogen or Calkyl,'}, {'sub': ['1-12', '3-12', '1-12'], '#text': ...
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