23-06-2023 дата публикации
Номер: CN116284106A
Принадлежит:
The preparation method comprises the following steps: adding n-dodecanethiol and liquid dibutyltin dichloride into a reaction kettle in proportion, starting to stir, and heating to 35-45 DEG C; then dropwise adding alkali liquor, controlling the reaction temperature to be 50-100 DEG C, stopping dropwise adding the alkali liquor when the pH value of the reaction feed liquid reaches 6.0-9.0, and continuously maintaining the reaction for 2-4 hours; and standing for phase splitting, directly carrying out reduced pressure distillation on the upper organic phase to remove water, and filtering to obtain the didodecylsulfanyl dibutyltin. The one-step method is adopted for direct synthesis, no solvent is added for extracting the product, no water washing desalination is carried out on the product, the method has the advantages of being safe in process, simple in equipment, small in wastewater generation amount, high in direct yield of the product, stable in product quality and the like, and the ...
Подробнее