07-04-2023 дата публикации
Номер: CN115932101A
Принадлежит:
The invention belongs to the technical field of oil product component detection, and particularly relates to a method for rapidly detecting the content of 1, 3-diglyceride in grease by using citric acid. The method mainly comprises the following steps: (1) drawing a standard curve; (2) weighing a grease sample, adding reaction reagents citric acid and concentrated sulfuric acid, carrying out a stirring reaction under a heating condition, centrifuging after the reaction is completed, taking a precipitate part, and weighing the mass of the precipitate; and (3) substituting into a standard curve for calculation to obtain the content of 1, 3-diglyceride. The detection method has good linear correlation when the concentration range of the 1, 3-diglyceride is 0-80 g/100 g, and the lowest detection limit of the 1, 3-diglyceride in the grease is 23.1 g/100 g. According to the method, high-end instruments and equipment and professional technicians are not needed, the operation is simple, the cost ...
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