14-07-2023 дата публикации
Номер: CN116425196A
Принадлежит:
The invention relates to the field of inorganic materials, in particular to a preparation method of high-purity antimony trioxide, which comprises the following steps: oxidizing high-antimony lead anode slime, heating at a certain vacuum degree, collecting condensed volatile matters to obtain an antimony trioxide crude product, mixing the antimony trioxide crude product with ethylene glycol, stirring, heating, reacting, carrying out reduced pressure distillation, carrying out hot filtration on the residual reaction liquid, cooling and crystallizing to obtain the antimony trioxide. The preparation method comprises the following steps: performing suction filtration, washing crystals with ethanol, drying to obtain ethylene glycol antimony, adding the ethylene glycol antimony into the ethanol, performing ultrasonic dispersion, dropwise adding an acid solution into the dispersion liquid, performing water bath reaction on the obtained mixed solution for 40-80 minutes, standing at room temperature ...
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