02-06-2023 дата публикации
Номер: CN116199632A
Принадлежит:
The invention discloses a method and a device for preparing prochloraz by adopting a micro-flow field reaction technology, and the preparation method comprises the following steps: dissolving 2, 4, 6-trichlorophenol by using liquid caustic soda, respectively pumping the dissolved 2, 4, 6-trichlorophenol and excessive 1, 2-dichloroethane into a micro-flow field reactor for reaction to obtain 2, 4, 6-trichlorophenoxyethyl chloride, and adding 1, 2-dichloroethane into the micro-flow field reactor for reaction to obtain 2, 4, 6-trichlorophenoxyethyl chloride; the preparation method comprises the following steps: carrying out liquid separation, distillation and refining on 2, 4, 6-trichlorophenoxyethyl chloride and n-propylamine in a micro-channel reactor to obtain N-(2, 4, 6-trichlorophenoxyethyl) propylamine, carrying out reaction on the N-(2, 4, 6-trichlorophenoxyethyl) propylamine and triphosgene in the presence of triethylamine in a micro-flow field dynamic reactor to generate acyl chloride ...
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