23-06-2023 дата публикации
Номер: CN116283692A
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The invention discloses a preparation method of sodium cresyl reductive acid. The preparation method comprises the following steps: step 1, preparing raw materials; 2, purifying the raw materials; step 3, preparing a sodium cresol solution; step 4, carrying out reaction treatment; and step 5, screening treatment. Nitrogen is used in cooperation with the kneading machine with an air temperature control circulation system, inert gas protection can be provided for the reaction of a sodium cresylate solution and carbon disulfide, and due to the characteristic that nitrogen is not prone to reacting with other substances, cresyl reducing acid sodium and active gas in air can be prevented from being subjected to a chemical reaction, so that the purity of the product is improved. By means of the inert performance of the nitrogen, the cresol-based reducing acid sodium has the advantages of being stable in property, convenient to transport and use and low in price, the problems that the collecting ...
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