05-09-2002 дата публикации
Номер: US20020123578A1
Process for the introduction of liquid into a continuous process for the gas-phase polymerisation of an olefin monomer and one or more other alpha-olefins in a fluidised-bed reactor, characterised in that the liquid is introduced by means of at least one nozzle comprising a feed pipe ( 1 ) and a sleeve ( 2 ) sliding inside and at the end of the said pipe, the position of the said sleeve along the feed pipe being determined by the pressure of the feed liquid ( 3 ) and the return force of a preloaded spring ( 4 ) the said spring having one end fixed to the sleeve and the other end to the feed pipe, the sleeve being provided with one or more recesses ( 10 ) along its surface for sliding with the feed pipe, the said recesses emerging in a groove ( 11 ) around the circumference of the sleeve and below a circular stop ( 8 ) integral with the same sleeve, the said stop resting, when the nozzle is not in use, on a rim ( 9 ) of the end of the feed pipe, the said rim and the circular stop of the sleeve each being provided with a bearing surface ( 12, 13 ), the contact area of which being minimised in order to allow good sealing.
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