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Применить Всего найдено 7. Отображено 7.
21-07-2010 дата публикации

Method for preparing basic bluestone by utilizing PCB ammonium persulfate-H2SO4 micro-etched waste liquid

Номер: CN0101780972A
Принадлежит:

The invention discloses a method for preparing basic bluestone by utilizing PCB ammonium persulfate-H2SO4 micro-etched waste liquid. The method comprises the following steps of: (1) preheating ammonium persulfate-H2SO4 micro-etched waste liquid and basic solution to the temperature of between 50 and 100 DEG C respectively, and adding the preheated micro-etched waste liquid into a neutralizing reaction kettle with a stirring device; (2) gradually adding the basic solution into the micro-etched waste liquid with the stirring for neutralization reaction, and controlling the pH value in the neutralizing reaction kettle to be between 8.0 and 13.0; (3) after filtering precipitate, adding dispersant into filtrate; (4) transferring the filtrate of which the pH value is regulated to an ammonia evaporation reaction kettle for atmospheric distillation to ensure that ammonia escapes from the reaction kettle till the pH value is reduced to be between 7.5 and 8.5, and completing ammonia evaporation; ...

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21-07-2010 дата публикации

Application of strong acid weak base salt or strong base weak acid salt in serving as anti-caking agent of type B basic copper chloride

Номер: CN0101780971A
Принадлежит:

The invention discloses application of a strong acid weak base salt or a strong base weak acid salt in serving as an anti-caking agent of type B basic copper chloride. The invention discovers that: the type B basic copper chloride reacts with the strong acid weak base salt or the strong base weak acid salt under a condition of sufficient stirring when the strong acid weak base salt or the strong base weak acid salt is added into the type B basic copper chloride, the crystalline structure of the type B basic copper chloride tends to be stable and cannot be agglomerated again, and the defect that the agglomeration of the type B basic copper chloride influences the use is overcome. The strong acid weak base salt or the strong base weak acid salt is added into the type B basic copper chlorideto ensure that the type B basic copper chloride has better stability, can be stored for a long time without agglomeration. The type B basic copper chloride added with the strong acid weak base salt or the ...

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02-04-2014 дата публикации

Producing method for producing electroplating grade copper sulfate with acid copper-bearing waste etching liquid

Номер: CN103693673A
Принадлежит:

The invention discloses a producing method for producing electroplating grade copper sulfate with acid copper-bearing waste etching liquid. The method comprises the steps of allowing clear water, or a copper oxide production mother solution, or a copper sulfate production mother solution to react with the acid copper-bearing waste etching liquid and mixed alkaline liquid to produce high-purity copper oxide, controlling the temperature of a reaction system to be 70-90 DEG C, and a pH (potential of hydrogen) value to be 8.5-9, adding prepared high-purity copper oxide and concentrated sulfuric acid into the clear water or an electroplating grade copper sulfate production mother solution, controlling the reaction pH value to be 0.1-3, and obtaining electroplating grade copper sulfate, wherein the mixed alkaline liquid is mixed by strong alkali and weak acid salt and strong alkali at a mass ratio of 1:6-1:8. The producing method is simple in technology and low in cost, a product reaches an electroplating ...

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14-07-2010 дата публикации

Application of sinkaline used as B type alkali copper chloride anticaking agent

Номер: CN0101773218A
Принадлежит:

The invention discloses an application of sinkaline used as a B type alkali copper chloride anticaking agent. The invention discovers that B type alkali copper chloride reacts with the sinkaline under the condition of sufficient stirring by adding the sinkaline to the B type alkali copper chloride, and the crystalline structure of the B type alkali copper chloride tends to be stable so that the B type alkali copper chloride does not cake any more and the defect of use influence of the B type alkali copper chloride due to caking is overcome. By adding the sinkaline to the B type alkali copper chloride, the B type alkali copper chloride has better stability and can be stored for a long time without caking; and the B type alkali copper chloride in which the sinkaline is added can be used as an animal feed additive.

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02-04-2014 дата публикации

Method for preparing electroplating grade copper sulfate pentahydrate by copper-bearing acid waste liquid without containing ammonia nitrogen

Номер: CN103693672A
Принадлежит:

The invention discloses a method for preparing electroplating grade copper sulfate pentahydrate by copper-bearing acid waste liquid without containing ammonia nitrogen; copper-bearing acid waste liquid and carbonate solution are added in clear water or alkali copper carbonate preparation mother liquor for stirring under the conditions of 6.0-9.0 of pH value and 50-100 DEG C of temperature to synthesize wet crystal alkali type copper carbonate; the alkali type copper carbonate is added in the clear water or electroplating grade copper sulfate preparation mother liquor, then is added in concentrated sulfuric acid for preparing the electroplating grade copper sulfate pentahydrate under the condition of 0.5-3.0 of pH value; the content of CuSO4.5H2O in the electroplating grade copper sulfate pentahydrate is higher than 98%, and the content of chloride is lower than 0.01%.

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29-02-2012 дата публикации

Method for preparing basic bluestone by utilizing PCB ammonium persulfate-H2SO4 micro-etched waste liquid

Номер: CN0101780972B
Принадлежит:

The invention discloses a method for preparing basic bluestone by utilizing PCB ammonium persulfate-H2SO4 micro-etched waste liquid. The method comprises the following steps of: (1) preheating ammonium persulfate-H2SO4 micro-etched waste liquid and basic solution to the temperature of between 50 and 100 DEG C respectively, and adding the preheated micro-etched waste liquid into a neutralizing reaction kettle with a stirring device; (2) gradually adding the basic solution into the micro-etched waste liquid with the stirring for neutralization reaction, and controlling the pH value in the neutralizing reaction kettle to be between 8.0 and 13.0; (3) after filtering precipitate, adding dispersant into filtrate; (4) transferring the filtrate of which the pH value is regulated to an ammonia evaporation reaction kettle for atmospheric distillation to ensure that ammonia escapes from the reaction kettle till the pH value is reduced to be between 7.5 and 8.5, and completing ammonia evaporation; ...

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01-02-2012 дата публикации

Recycling system for tail gas generated in process of utilizing etching waste liquid to produce copper chloride and copper sulfate

Номер: CN0202129012U

The utility model discloses a recycling system for tail gas generated in the process of utilizing etching waste liquid to produce copper chloride and copper sulfate, which comprises a negative pressure pumping device, a tail gas condensation device, a venturi absorber and a water cycling tank. The negative pressure pumping device is connected with the tail gas condensation device, and the tail gas condensation device is connected with the venturi absorber and a pump respectively through a three-way valve. The other end of the pump is connected with the water cycling tank, the venturi absorber is also connected with the water cycling tank, and the top end of the water cycling tank is connected with a water seal pipe. The recycling system for tail gas generated in the process of utilizing etching waste liquid to produce copper chloride and copper sulfate realizes zero emission of tail gas and stops secondary pollution caused by waste gas in production by adding a high-efficient water cycling ...

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