11-08-2023 дата публикации
Номер: CN116574114A
Принадлежит:
The invention discloses a preparation method of lithium alkylide in the technical field of lithium alkylide preparation, and the preparation method of lithium alkylide comprises the following steps: S1, under the protection of inert gas, putting metal lithium particles and a solvent into a washing kettle, stirring and washing the metal lithium particles, and removing a protective oil layer of the metal lithium particles; s2, taking out the washed metal lithium particles, putting the metal lithium particles into a synthesis kettle under the protection of inert gas, heating, and maintaining for a certain time to ensure that the metal lithium particles are molten into a liquid state; s3, a hydrocarbon solvent is put into the synthesis kettle, and the hydrocarbon solvent and the metal lithium liquid are stirred, mixed and synthesized; s4, after the synthetic reaction is completed, the materials are pressed into a settling tank through argon, standing is conducted, and after lithium slag in ...
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