04-06-2014 дата публикации
Номер: CN103834849A
Принадлежит:
The invention provides a FeV45N10 ferric vanadium nitrate product prepared through combustion synthesis and a production method thereof. The FeV45N10 ferric vanadium nitrate product comprises the following components in percentage by mass: 43.0-47.0 percent of V, 9.0-13.0 percent of N and the balance of Fe and less impurities. According to the production method, single FeV50 is used as a raw material and is crushed, wherein the crushed FeV50 with a grain size of 40-100 mu accounts for 26-36 percent, the crushed FeV50 with a grain size of 100-200 mu accounts for 27-36 percent, and the crushed FeV50 with a grain size of more than 200 mu accounts for 32-44 percent. A nitridation synthesis process comprises the following steps: adding the uniformly-mixed ferric vanadium synthetic material powder into a graphite crucible, then placing the graphite crucible in a high pressure synthetic furnace, introducing a high-purity nitrogen with the pressure of 7-12 MPa after a furnace door is closed, and ...
Подробнее