01-10-2014 дата публикации
Номер: CN104072341A
Принадлежит:
The invention belongs to the fields of fine chemicals and chemical production and discloses a method for finely purifying 2, 5-ditert-butylhydroquinone. The method comprises the concrete steps of adding a crude product of 2, 5-ditert-butylhydroquinone into tertiary butanol, and dissolving through heating to obtain a mixed solution; then, cooling the mixed solution, and standing for crystallizing to obtain a 2, 5-ditert-butylhydroquinone crystal; filtering the obtained 2, 5-ditert-butylhydroquinone crystal, and drying to obtain refined 2, 5-ditert-butylhydroquinone. Through utilizing the characteristic that the solubility of 2, 5-ditert-butylhydroquinone in tertiary butanol is relatively high in variation difference with temperature, the method provided by the invention can be used for controlling the crystallization speed and the crystallization degree, remarkably improving the product quality and increasing the yield and the crystallization efficiency so as to be suitable for industrial ...
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