18-09-2013 дата публикации
Номер: CN103305174A
Принадлежит:
The invention relates to a preparation method of a light/humidity dual-curing polyurethane hot melt adhesive. The preparation method comprises the following steps of: introducing N2 into an HDI (hexamethylene diisocyanate) tripolymer, removing water vapor, carrying out a protective reaction, respectively adding a polymerization inhibitor and a catalyst and dropwisely adding HEA (hydroxyethyl acrylate); after dropwisely adding and reacting, adding polyisocyanate, and stirring uniformly to obtain 3HDI-HEA/polyisocyanate; heating and fusing polyalcohol and stirring for dehydration; adding the 3HDI-HEA/polyisocyanate and the catalyst; discharging after reacting, packaging the sample with an aluminum foil bag for standby application to obtain a light/humidity dual-curing polyurethane hot melt adhesive prepolymer; melting the prepolymer, and adding a photoinitiator, a polymerization inhibitor, a plasticizer and the catalyst, stirring uniformly in a molten state, rising the temperature and removing ...
Подробнее