10-04-2014 дата публикации
Номер: US20140097088A1
The disclosed embodiments relate to methods and apparatus for immersing a substrate in electrolyte in an electroplating cell under sub-atmospheric conditions to reduce or eliminate the formation/trapping of bubbles as the substrate is immersed. Various electrolyte recirculation loops are disclosed to provide electrolyte to the plating cell. The recirculation loops may include pumps, degassers, sensors, valves, etc. The disclosed embodiments allow a substrate to be immersed quickly, greatly reducing the issues related to bubble formation and uneven plating times during electroplating. 1. A method of electroplating metal onto a substrate , comprising:flowing electrolyte through a plating recirculation loop comprising an electrolyte reservoir, a pump, an electroplating cell, and a degasser that degasses the electrolyte prior to its introduction to the electroplating cell;immersing the substrate in electrolyte in an electroplating cell, wherein the pressure in the electroplating cell during immersion is about 100 Torr or less;electroplating material onto the substrate; andremoving the substrate from electrolyte.2. The method of claim 1 , wherein the pressure in the electroplating cell during immersion is at least about 20 Torr.3. The method of claim 1 , wherein immersing the substrate in electrolyte occurs over a period of about 225 ms or less claim 1 , and wherein the substrate has a diameter of about 150 mm or greater.4. The method of claim 3 , wherein immersing the substrate in electrolyte occurs over a period of about 50 ms or less claim 3 , and wherein the substrate has a diameter of about 150 mm or greater.5. The method of claim 1 , wherein immersing the substrate in electrolyte occurs over a period having a first duration claim 1 , and electroplating material to fill a feature on the substrate occurs over a period having a second duration claim 1 , and wherein the first duration is about 10% or less of the second duration.6. The method of claim 5 , wherein the ...
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