07-07-2023 дата публикации
Номер: CN116396185A
Принадлежит:
The invention belongs to the field of synthesis of diazo compounds, and discloses a preparation method of an N-allyl aryl hydrazine compound. According to the invention, an aryl hydrazine compound and an allyl acetate compound are used as initial raw materials, and a two-molecule carbon-nitrogen coupling reaction is realized through a simple thermal reaction to construct the N-allyl aryl hydrazine compound. The new synthesis method provided by the invention does not need to use extra oxidizing agents and additives, the raw materials are simple and easy to obtain, the reaction route is short, the experimental operation is convenient, the production cost is low, the reaction conditions are not harsh, and the prepared target product is easy to purify, good in yield and high in product purity; the method is a brand-new synthesis method which is more economical, more environment-friendly and simpler and milder in reaction condition, and is more suitable for being applied to industrial organic ...
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