28-09-2011 дата публикации
Номер: CN0102198958A
Принадлежит:
The invention relates to a preparation method for high-purity molybdenum trioxide used for a hydrofining catalyst of petroleum, and the method comprises the following steps: carrying out box drying on ammonium tetramolybdate at the temperature of 75-85 DEG C for 18-20 hours, and placing in a sealed packaging bag for 7-10 days; screening dried ammonium tetramolybdate with a 40-mesh screen, and acquiring a screen undersize material; analyzing the contents of molybdenum and impurities in ammonium tetramolybdate used for preparing the high-purity molybdenum trioxide; conveying the treated ammonium tetramolybdate to the furnace end of a rotary tube electric furnace using a screw feeder, and dividing the rotary tube electric furnace into five zones, wherein the temperatures of the five zones are 470+/-5 DEG C, 490+/-5 DEG C, 510+/-5 DEG C, 490+/-5 DEG C, and 470+/-5 DEG C respectively; baking while controlling the rotation speed of the screw feeder at 20-23 Hz and the rotation speed of the rotary ...
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