06-03-2013 дата публикации
Номер: CN102952303A
Автор:
Liang Tao,
Wei Xuling,
Liu Baoyong,
Cong Rixin,
Wu Jiang,
Wei Yuli,
Gong Guangbi,
Zheng Jucheng,
Dai Zuhong,
Xu Dianhong,
Ai Chunjin,
Zhu Jing
Принадлежит:
A preparation method of an environmentally-friendly powdery chloroprene rubber having the characteristics of quick dissolving and high bonding comprises the following steps: 1, adding water and starch into a reaction bottle, reacting at 25-40DEG C, alternatively adding an alkaline solution and a diacid in a dropwise manner, adjusting the pH value to 7-8 when the pH value slowly changes, and carrying out heat insulation to prepare modified starch; 2, adding a polychloroprene latex, water, the modified starch, isoprene, a molecular weight adjusting agent, an initiator and an activator into a polymerization kettle, carrying out a graft polymerization reaction at 25-50DEG C, and adding a terminator when the polymerization conversion rate is 65-75% to prepare a grafted latex; and 3, adding the grafted latex into a condensation kettle, adding an isolation agent, a flocculating agent and a condensation agent, stirring, heating, slaking, dehydrating, and drying to obtain the environmentally-friendly ...
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