04-04-2023 дата публикации
Номер: CN115894291A
Принадлежит:
The invention relates to a preparation method of alpha-cyhalothrin, which comprises the following steps: adding sodium cyanide and a phase transfer catalyst into a three-neck bottle, and stirring at room temperature until the sodium cyanide and the phase transfer catalyst are completely dissolved; the preparation method comprises the following steps: dissolving ether aldehyde and a chiral catalyst in methylbenzene, adding into a reaction flask, stirring for 1 hour at the temperature of 0-minus 5 DEG C, and reacting to generate S-cyano-3-phenoxy benzyl alcohol; the method comprises the following steps: adding a solvent into a reaction kettle, dropwise adding cis-Z kung-fu refined acyl chloride, after dropwise adding, carrying out heat preservation stirring at 0-5 DEG C for 3-4 hours, and removing the solvent to obtain yellow oily liquid, namely optically active alpha-cyhalothrin crude oil with the content of 95% or above; the method comprises the following steps: adding a solvent and alpha-cyhalothrin ...
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