08-10-2020 дата публикации
Номер: US20200315924A1
Принадлежит:
The present disclosure provides an inorganic dental filler including a surface treated with at least one silane. Exemplary silanes described in the present disclosure for the surface treatment of the inorganic filler include silanes of Formula I and/or Formula II: (R)—(CRR)—(NH—C(O)—O—CH—CH)—N(R)—C(O)—NH—(CH—CH—O)—CRR—CH-(A) Formula I (R)—(CRR)—NH—C(O)—O—CRR-(L)-CH-(A) Formula II, wherein: Ris a silane-containing group of the formula —Si(Y)(R), wherein Y is a hydrolysable group, Ris a monovalent alkyl or aryl group, and p is 1, 2, or 3. Methods of making and using the surface treated inorganic dental fillers are also disclosed. 1. A surface-treated inorganic dental filler comprising an inorganic dental filler having a surface treated with at least one silane represented by Formula I:{'br': None, 'sup': Si', '1', '2', '5', '3', '4, 'sub': n', '2', '2', 'q', '2', '2', 't', '2, '(R)—(CRR)—(NH—C(O)—O—CH—CH)—N(R)—C(O)—NH—(CH—CH—O)—CRR—CH-(A) \u2003\u2003 Formula I,'}wherein:{'sup': Si', '6, 'sub': p', '3-p, 'Ris independently a silane-containing group of the formula —Si(Y)(R)'}Y is a hydrolysable group;{'sup': 1', '2', '3, 'each R, R, and Ris independently selected from H, an alkyl group, an aryl group, an alkaryl group, and an aralkyl group;'}{'sup': '4', 'sub': 2', 'm, 'each Ris independently selected from H, an alkyl group, an aryl group, an alkaryl group, an aralkyl group, and a group of the formula —(CH)-(A);'}{'sup': 1', '7, 'sub': '2', 'each A is independently a (meth)acryl group of the formula X—C(O)—C(R)═CH;'}{'sup': 1', '7, 'Xis —O, —S, or —NR;'}{'sup': 5', 'Si', '1', '2', 'Si', '1', '2', '8', '8', '3', '4', '8', '9, 'sub': n', '2', '2', 'q', 'n', '2', 'm', '2', 'm', '2', 'm', '2', '2', 't', '2', '2', 'm, 'Ris H, an alkyl group, a cycloalkyl group, an aryl group, an alkaryl group, an aralkyl group, a group of the formula (R)—(CRR)—(NH—C(O)—O—CH—CH)—, a group of the formula (R)—(CRR)—NH—C(O)—N(R)—(CH)—, a group of the formula —(CH)-(A), a group of the formula ( ...
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