02-01-2020 дата публикации
Номер: US20200002264A1
A method for producing a high-purity carboxylic acid ester, the method including bringing a crude carboxylic acid ester that contains anionic impurities and Ag, Al, Au, Ca, Cr, Cu, Fe, K, Mg, Na, Sn, and Zn metal impurities into contact with a cation-exchange resin, followed by bringing the crude carboxylic acid ester into contact with an anion-exchange resin to obtain to provide a high-purity carboxylic acid ester in which the Ag, Al, Au, Ca, Cr, Cu, Fe, K, Mg, Na, Sn, and Zn metal impurity content are each less than 1 ppb and the anionic impurity content is less than 1 ppm. 1. A method for producing a high-purity carboxylic acid ester , the method comprising:contacting a first carboxylic acid ester composition that contains anionic impurities and at least silver, aluminum, gold, calcium, copper, iron, potassium, magnesium, sodium, tin, and zinc as metal impurities with a first weakly basic anion-exchange resin to obtain a second carboxylic acid ester composition;contacting the second carboxylic acid ester composition with a strongly acidic cation-exchange resin to obtain a third carboxylic acid ester composition; andcontacting the third carboxylic acid ester composition with a second weakly basic anion-exchange resin to obtain the high-purity carboxylic acid ester,wherein:an amount of the silver, the aluminum, the gold, the calcium, the chromium, the copper, the iron, the potassium, the magnesium, the sodium, the tin, and the zinc metal impurities in the high-purity carboxylic acid ester is each less than 1 ppb, andan amount of the anionic impurities in the high-purity carboxylic acid ester is less than 1 ppm.2. The method according to claim 1 , wherein the carboxylic acid ester is at least one selected from the group consisting of propyl lactate claim 1 , methyl α-hydroxyisobutyrate claim 1 , ethyl α-hydroxyisobutyrate claim 1 , propyl α-hydroxyisobutyrate claim 1 , butyl α-hydroxyisobutyrate claim 1 , methyl β-hydroxyisobutyrate claim 1 , ethyl β- ...
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