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Небесная энциклопедия

Космические корабли и станции, автоматические КА и методы их проектирования, бортовые комплексы управления, системы и средства жизнеобеспечения, особенности технологии производства ракетно-космических систем

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Мониторинг СМИ

Мониторинг СМИ и социальных сетей. Сканирование интернета, новостных сайтов, специализированных контентных площадок на базе мессенджеров. Гибкие настройки фильтров и первоначальных источников.

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Поддерживает ввод нескольких поисковых фраз (по одной на строку). При поиске обеспечивает поддержку морфологии русского и английского языка
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Применить Всего найдено 15480. Отображено 100.
23-02-2012 дата публикации

Coated silver nanoparticles and manufacturing method therefor

Номер: US20120043510A1
Принадлежит: Yamagata University NUC

The present invention provides coated silver nanoparticles for use as an electrically conductive material capable of sintering at lower temperatures that is able to be used even with flexible printed substrates having low heat resistance, and a manufacturing method therefor. The coated silver nanoparticles of the present invention have a mean particle diameter of 30 nm or less and are coated with protective molecules amine, and are characterized in that the weight loss rate when heated to 160° C. in thermogravimetric measurement is 30% or more. The coated silver nanoparticles of the present invention are also characterized in that a silver-colored sintered film can be formed by sintering at a temperature of 100° C. or lower for 1 hour or less. These coated silver nanoparticles are manufactured by mixing a silver compound that forms metallic silver when decomposed by heating, an alkylamine and an alkyldiamine to prepare a complex compound, and by thermally decomposing the silver compound by heating the complex compound.

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05-04-2012 дата публикации

Process For Manufacturing Agglomerated Particles Of Tantalum, Mixed Tantalum Powder And Process For Manufacturing Same, Tantalum Pellet And Process For Manufacturing Same, And Capacitor

Номер: US20120081840A1
Принадлежит: Cabot Corp

A method for producing agglomerated tantalum particles, comprising: a step for grinding secondary tantalum particles, which are obtained by reducing a tantalum salt, and adding water thereto to give a water-containing mass; a step for drying said water-containing mass to give a dry mass; a step for sieving said dry mass to give spherical particles; and a step for heating said spherical particles. A mixed tantalum powder comprising a mixture of agglomerated tantalum particles (X) with agglomerated tantalum particles (Y), wherein said agglomerated tantalum particles (X) show a cumulative percentage of particles with particle size of 3 μm or less of 5 mass % or less after 25 W ultrasonic radiation for 10 min, while said agglomerated tantalum particles (Y) show a cumulative percentage of particles with particle size of 3 μm or less of 10 mass % or more after 25 W ultrasonic radiation for 10 min.

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19-04-2012 дата публикации

Conductive particle, and anisotropic conductive film, bonded structure, and bonding method

Номер: US20120090882A1

To provide a conductive particle, containing: a core particle; and a conductive layer formed on a surface of the core particle, wherein the core particle is a nickel particle, and wherein the conductive layer is a nickel plating layer a surface of which has a phosphorous concentration of 10% by mass or lower, and the conductive layer has an average thickness of 1 nm to 10 nm.

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26-04-2012 дата публикации

Discharge gap filling composition and electrostatic discharge protector

Номер: US20120099231A1
Принадлежит: Showa Denko KK

A discharge gap filling composition which includes metal powders (A) and a binder component (B), wherein surfaces of primary particles of the metal powders (A) are coated with a film composed of a metal oxide, and the primary particles of the metal powders (A) have a flake form. An electrostatic discharge protector is obtained using the composition.

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03-05-2012 дата публикации

Coated conductive particles and method for producing same

Номер: US20120104333A1
Принадлежит: Hitachi Chemical Co Ltd

[Problem to be Solved] To provide conductive particles which are capable of providing an anisotropically conductive adhesive that can maintain sufficient insulation characteristics and conduction characteristics even when used for the connection of a very small circuit, while having excellent moisture absorption resistance at a lower cost. [Solution] A coated conductive particle ( 5 ) comprises: a composite conductive particle ( 3 ) that has a resin particle ( 4 ) and a metal layer ( 6 ) that covers the resin particle ( 4 ); and insulating fine particles ( 1 ) that are provided on the outer side of the metal layer ( 6 ) so as to partially cover the surface of the metal layer ( 6 ). The metal layer ( 6 ) has a nickel-palladium alloy plating layer ( 6 a ).

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03-05-2012 дата публикации

Method for producing decorative metallic article with wood grain metal pattern, and decorative metallic article with wood grain metal pattern

Номер: US20120107561A1
Принадлежит: Aida Chemical Industries Co Ltd

Provided are a method for producing a decorative metallic article with a wood grain metal pattern and the decorative metallic article with the wood grain metal pattern; the decorative metallic article comprising a sintered copper part produced by sintering a plastic copper containing clay compound, and a sintered silver part produced by sintering a plastic silver containing clay compound. The method comprises: a plate forming step of forming a copper plate and a silver plate; a multi layering and adhesion step of mutually laminating the copper and silver plates one another by applying water to the surfaces of the plates, and elongating the laminated plates so that a thickness thereof decreases in 10% or more, thereby to adhesively paste together; a wood grain metal plate forming step of forming a wood grain pattern by carving the surface of the multi layered plate produced in the multi layering and adhesion step so as to expose at least a part of the plurality of plate layers, and elongating the surface of the multi layered plate to become flat; a decorative object forming step of forming a decorative object by using the prepared wood grain metal plate; a decorative object drying step of drying the decorative object; and a sinter producing step of sintering the decorative object produced in the decorative object drying step, thereby to obtain the decorative metallic article.

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10-05-2012 дата публикации

Rare earth magnet material and method for producing the same

Номер: US20120114515A1
Автор: Yuji Kaneko, Yukio Takada
Принадлежит: Toyota Central R&D Labs Inc

A method for producing a rare earth magnet material which allows efficient Dy or the like diffusion into an inside thereof. This method includes a preparation step of preparing a powder mixture of magnet powder including one or more rare earth elements including neodymium, boron, and the remainder being iron; and neodymium fluoride powder; a heating step of heating a compact of the powder mixture and causing oxygen around magnet powder particles to react with the fluoride powder, thereby obtaining a lump rare earth magnet material in which neodymium oxyfluoride is wholly distributed. The fluoride powder traps oxygen enclosed in the powder mixture and fixes the oxygen as stable NdOF. When Dy is diffused into this rare earth magnet material, Dy smoothly enters into its inside without being oxidized at grain boundaries. Consequently, coercivity of the entire rare earth magnet material can be efficiently increased without wasting scarce Dy.

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05-07-2012 дата публикации

Manufacturing and Applications of Metal Powders and Alloys

Номер: US20120167716A1
Автор: Andrew Matheson
Принадлежит: Boston Electronic Materials LLC

The present invention is directed to a method of manufacture of metal or alloy powders that uses liquid phase reduction of a metal halide, or a mixture of metal halides, to produce a metal particle coated in salts produced as a reaction byproduct. The reaction conditions can be chosen to select a range of metal particle sizes, and the salt coating prevents oxidation (or reaction with other atmospheric gases) and permits a range of applications hitherto difficult to achieve using metal powders.

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19-07-2012 дата публикации

Permanent magnet and manufacturing method thereof

Номер: US20120181476A1
Принадлежит: Nitto Denko Corp

There are provided a permanent magnet and a manufacturing method thereof capable of efficiently concentrating traces of Dy or Tb in grain boundaries of the magnet and sufficiently improving coercive force due to Dy or Tb while reducing amount of Dy or Tb to be used. To fine powder of milled neodymium magnet material is added an organometallic compound solution containing an organometallic compound expressed with a structural formula of M-(OR) x (M represents Dy or Tb, R represents a substituent group consisting of a straight-chain or branched-chain hydrocarbon, x represents an arbitrary integer) so as to uniformly adhere the organometallic compound to particle surfaces of the neodymium magnet powder. Thereafter, a compact body compacted through powder compaction is held for several hours in hydrogen atmosphere at 200 through 900 degrees Celsius for a hydrogen calcination process. Thereafter, through sintering process, the compact body is formed into a permanent magnet.

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08-11-2012 дата публикации

Radiation curable resin composition and rapid three dimensional imaging process using the same

Номер: US20120282439A1
Принадлежит: DSM IP ASSETS BV

The invention relates to a radiation curable resin composition comprising a cationically polymerizable component, a cationic photoinitiator, a hydroxy component, and an impact modifier. The resin composition can preferably be used in the preparation of three dimensional objects.

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03-01-2013 дата публикации

Method of making and using a reconfigurable downhole article

Номер: US20130004664A1
Принадлежит: Individual

A method of making a reconfigurable article is disclosed. The method includes providing a powder comprising a plurality of base material particles. The method also includes providing a powder comprising a plurality of removable material particles; and forming a base article from the base material comprising a plurality of removable material particles. A method of using a reconfigurable article is also disclosed. The method includes forming a base article, the base article comprising a base material and a removable material, wherein the base article comprises a downhole tool or component. The method also includes inserting the base article into a wellbore. The method further includes performing a first operation utilizing the base article; exposing the removable material of the base article to a wellbore condition that is configured to remove the removable material and form a modified article; and performing a second operation using the article.

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07-03-2013 дата публикации

Degradable high shock impedance material

Номер: US20130055852A1
Автор: Zhiyue Xu
Принадлежит: Baker Hughes Inc

A selectively corrodible powder compact that may be used to make the components of a selectively corrodible perforating system is disclosed. The selectively corrodible powder compact includes a cellular nanomatrix comprising a nanomatrix material. The selectively corrodible powder compact also includes a plurality of dispersed particles comprising a particle core material having a density of about 7.5 g/cm 3 or more, dispersed in the cellular nanomatrix. The selectively corrodible powder compact further includes a bond layer extending throughout the cellular nanomatrix between the dispersed particles.

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07-03-2013 дата публикации

Metal powder production method, metal powder produced thereby, conductive paste and multilayer ceramic electronic component

Номер: US20130059161A1
Принадлежит: Individual

Fine, highly-crystallized metal powder is produced at low cost and high efficiency by a method involving: ejecting raw material powder composed of one or more kinds of thermally decomposable metal compound powders into a reaction vessel through a nozzle together with a carrier gas and producing a metal powder by heating the raw material powder at a temperature T 2 which is higher than the decomposition temperature of the raw material powder and not lower than (Tm−200)° C. where Tm is the melting point (° C.) of the metal to be produced, while allowing the raw material powder to pass through the reaction vessel in a state where the raw material powder is dispersed in a gas phase at a concentration of 10 g/liter or less, wherein an ambient temperature T 1 of a nozzle opening part is set to a temperature of 400° C. or higher and lower than (Tm−200)° C.

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21-03-2013 дата публикации

Paste and method for connecting electronic component to substrate

Номер: US20130068373A1

A paste may be used to connect at least one electronic component to at least one substrate through contact regions, wherein at least one of the contact regions contains a non-noble metal. The paste contains (a) metal particles, (b) at least one activator that bears at least two carboxylic acid units in the molecule, and (c) a dispersion medium. A method for connecting at least one electronic component to at least one substrate through the contact regions includes steps of providing a substrate having a first contact region and an electronic component having a second contact region; providing the above paste; generating a structure, wherein the first contact region of the substrate contacts the second contact region of the electronic component through the paste; and sintering the structure while producing a module including at least the substrate and the electronic component connected to each other through the sintered paste.

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11-04-2013 дата публикации

MATERIAL FOR DECORATIVE PARTS

Номер: US20130087019A1
Принадлежит: Sumitomo Electric Industries, Ltd.

A lightweight material for decorative parts having a silver metallic color tone is provided. The material includes a sintered body including a main hard phase composed of a solid solution formed of titanium carbonitride and titanium carbide; a main binder phase composed of nickel; a first additive material composed of at least one selected from the group consisting of molybdenum carbide, niobium carbide, tungsten carbide, and tantalum carbide; a second additive material composed of at least one of chromium and chromium carbide; and the balance being incidental impurities. The N content in the sintered body is 2.0% to 6.0% by mass. The color tone of the sintered body satisfies L*=9 to 14, a*=−2 to 3, and b*=−6 to 0, which are values of the L*a*b* color system measured with a spectrophotometric colorimeter. 15.-. (canceled)6. A material for decorative parts comprising a sintered body that includes:a main hard phase composed of a solid solution formed of titanium carbonitride and titanium carbide;a main binder phase composed of nickel;a first additive material composed of at least one selected from the group consisting of molybdenum carbide, niobium carbide, tungsten carbide, and tantalum carbide;a second additive material composed of at least one of chromium and chromium carbide; andthe balance being incidental impurities,wherein a N content in the sintered body is 2.0% to 6.0% by mass, anda color tone of the sintered body satisfies the following values of an L*a*b* color system measured with a spectrophotometric colorimeterL*=9 to 14,a*=−2 to 3, andb*=−6 to 0.7. The material for decorative parts according to claim 6 , wherein a specific gravity of the sintered body is 5.5 to 7.5.8. The material for decorative parts according to claim 6 , wherein the sintered body is a nonmagnetic sintered body.9. The material for decorative parts according to claim 6 ,wherein a content of nickel serving as the main binder phase is 10% by mass or more and 15% by mass or less, anda ...

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16-05-2013 дата публикации

Surface-passivated lithium metal and method for the production thereof

Номер: US20130122318A1
Автор: Ulrich Wietelmann
Принадлежит: Chemetall GmbH

A surface-passivated lithium metal, which has a composite top layer containing or consisting of at least two poorly soluble components containing lithium. Production of the surface-passivated lithium metal such that lithium metal below 180° C., thus in the solid state, is transformed into an inert, aprotic solvent with a passivating agent of the general formula Li[P(C 2 O 4 ) −x/2 F x ] where x=0, 2, or 4 is also disclosed.

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06-06-2013 дата публикации

PROCESS FOR PRODUCTION OF (RARE EARTH)-MG-NI-BASED HYDROGEN STORAGE ALLOY

Номер: US20130142690A1
Принадлежит: SANTOKU CORPORATION

A safe and industrially advantageous production method is disclosed for producing a rare earth-Mg—Ni based hydrogen storage alloy which realizes production of a nickel-hydrogen rechargeable battery having excellent cycle characteristics and a large capacity. The method is for producing a rare earth-Mg—Ni based hydrogen storage alloy including element A, Mg, and element B, wherein element A is composed of at least one element R selected from rare earth elements including Sc and Y, and optionally at least one element selected from Zr, Hf, and Ca, and element B is composed of Ni and optionally at least one element selected from elements other than element A and Mg. The method includes first step of mixing an alloy consisting of elements A and B and Mg metal and/or a Mg-containing alloy having a melting point not higher than the melting point of Mg metal, and second step of heat-treating a mixture obtained from first step for 0.5 to 240 hours at a temperature 5 to 250° C. lower than a melting point of the rare earth-Mg—Ni based hydrogen storage alloy to be obtained. 1. A method for producing a rare earth-Mg—Ni based hydrogen storage alloy comprising element A , Mg , and element B , wherein said element A consists of at least one element R selected from rare earth elements including Sc and Y , and optionally at least one element selected from Zr , Hf , and Ca , and said element B consists of Ni and optionally at least one element selected from elements other than element A and Mg , said method comprising:first step of mixing an alloy consisting of elements A and B and Mg metal and/or a Mg-containing alloy having a melting point not higher than the melting point of Mg metal, andsecond step of heat-treating a mixture obtained from said first step for 0.5 to 240 hours at a temperature 5 to 250° C. lower than a melting point of said rare earth-Mg—Ni based hydrogen storage alloy to be obtained.250. The method according to claim 1 , wherein a mean particle diameter (D) of said ...

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20-06-2013 дата публикации

Iron-based mixture powder for sintering and iron-based sintered alloy

Номер: US20130152735A1
Принадлежит: Fine Sinter Co Ltd, Toyota Motor Corp

There is provided an iron-based mixture powder for sintering, as well as an iron-based sintered alloy using same, that are capable of reducing the cutting resistance of the iron-based sintered alloy and of mitigating the shortening of cutting tool life even when a metal fluoride powder is used. The iron-based mixture powder for sintering comprises an iron-based powder, a graphite powder, a hard powder that is harder than the iron-based powder, and a metalfluoride powder. With respect to particle asperity as expressed by the following equation, particle asperity=(perimeter of a section of a particle) 2 /(sectional area of the section×4Pi), the particle asperity of the metal fluoride powder is within the range of 2 to 5.

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22-08-2013 дата публикации

Starting material for a sintered bond and process for producing the sintered bond

Номер: US20130216847A1
Принадлежит: ROBERT BOSCH GMBH

The invention relates to a starter material for a sintering compound, said starter material comprising first particles of at least one metal having a first coating which is applied to the first particles and consists of an organic material, and second particles which contain an organic metal compound and/or a precious metal oxide, the organic metal compound and/or the precious metal oxide being converted during heat treatment of the starter material into the fundamental elemental metal and/or precious metal. The invention is characterized in that the second particles have a core of at least one metal and a second coating which is applied to the core and contains the organic metal compound and/or precious metal oxide. Furthermore, the first coating contains a reducing agent by means of which the organic metal compound and/or the precious metal oxide is/are reduced to the elemental metal and/or precious metal at a temperature below the sintering temperature of the elemental metal and/or precious metal.

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29-08-2013 дата публикации

Lubricant system for use in powder metallurgy

Номер: US20130224060A1
Принадлежит: Hoeganaes Corp

The present invention is directed to metallurgical powder compositions having improved lubricant properties. These compositions of the invention include at least 90 wt. % of an iron-based metallurgical powder; a Group 1 or Group 2 metal stearate; a first wax having a melting range of between about 80 and 100° C.; a second wax having a melting range of between about 80 and 90° C.; inc phosphate; boric acid; acetic acid; phosphoric acid; and polyvinylpyrrolidone. Methods of compacting the compositions, as well as compacted articles prepared using those methods, are also described.

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24-10-2013 дата публикации

Composite, soft-magnetic powder and its production method, and dust core formed thereby

Номер: US20130277601A1
Автор: Fumi Kurita, Hisato Tokoro
Принадлежит: Hitachi Metals Ltd

A composite, soft-magnetic powder comprising soft-magnetic, iron-based core particles having an average particle size of 2-100 μm, and boron nitride-based coating layers each covering at least part of each soft-magnetic, iron-based core particle, said coating layers being polycrystalline layers comprising fine boron nitride crystal grains having different crystal orientations and an average crystal grain size of 3-15 nm, the average thickness of said polycrystalline layers being 6.6% or less of the average particle size of said soft-magnetic, iron-based core particles, is produced by (1) mixing iron nitride powder having an average particle size of 2-100 μm with boron powder having an average particle size of 0.1-10 μm, (2) heat-treating the resultant mixed powder at a temperature of 600-850° C. in a nitrogen atmosphere, and (3) removing non-magnetic components.

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07-11-2013 дата публикации

Starting material for a sintered bond and process for producing the sintered bond

Номер: US20130292168A1
Принадлежит: ROBERT BOSCH GMBH

The invention relates to a starter material for a sintering compound, said starter material comprising particles which at least proportionally contain an organic metal compound and/or a precious metal oxide, the organic metal compound and/or the precious metal oxide being converted during heat treatment of the starter material into the elemental metal and/or precious metal. The invention is characterized in that the particles have a coating containing a reducing agent by means of which the organic metal compound and/or precious metal oxide is reduced to the elemental metal and/or precious metal at a temperature below the sintering temperature of the elemental metal and/or precious metal.

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21-11-2013 дата публикации

Composite material for the making of decorative items and procedure for the making of a decorative item

Номер: US20130307188A1
Принадлежит: ANTIGO PROPERTIES

Composite material for the making of decorative items which contains at least a polymeric component and at least a metallic powder dispersed in the polymeric component in an amount in weight between 2% and 95%. The metallic powder includes plate-like particles with a nanometric thickness of between 5 and 300 nm and a preferential growth in a two-dimensional surface with at least a dimension of between 0.6 and 100 μm. A procedure for the making of an ornamental article includes at least a phase for preparing at least a base component of a silicone resin; at least a phase for preparing the metallic powder; at least an initial phase for mixing the metallic powder with the silicone resin base component to obtain an even mixture; and at least an initial phase for reticulating the base component in the even mixture with the metallic powder distributed in a homogeneous way.

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26-12-2013 дата публикации

Method and system for preparing shaped particles

Номер: US20130340894A1
Автор: David Max Roundhill
Принадлежит: EMPIRE TECHNOLOGY DEVELOPMENT LLC

The present technology provides an illustrative method for preparing shaped nanoparticles. The method includes passing a metal vapor to a shaping apparatus and condensing the metal vapor within the shaping apparatus to form selectively-shaped metal nanoparticles. The method may also include forming the metal vapor by heating a bulk metal. In an embodiment, the shaping apparatus comprises a mesh separator that include a plurality of nano-sized, square-shaped pores or a plurality of shaping cups that includes a plurality of recesses.

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26-12-2013 дата публикации

Magnetic exchange coupled core-shell nanomagnets

Номер: US20130342297A1
Автор: Seok Bae, Yang-Ki Hong
Принадлежит: University of Alabama UA

A permanent magnet is fabricated such that it has a magnetically hard core surrounded by a thin magnetically soft shell. The magnetically hard core provides a relatively high intrinsic coercivity (H ci ), and the magnetically soft shell provides a relatively high magnetic flux density (B). Due to magnetic exchange coupling between the core and shell, a relatively high maximum energy product (BH) max is achievable over a wide temperature range, including temperatures above 150° C. Further, such effects can be achieved without using rare-earth metals or precious metals helping to keep the manufacturing costs of the magnet low. To allow sufficient exchange magnetic coupling between the core and shell, the width of the shell is less than about 40 nanometers, and the overall dimensions are controlled such that the width of the shell is less than two times the Bloch domain wall thickness of the core.

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02-01-2014 дата публикации

Composition of silver-conjugated compound composite

Номер: US20140001422A1
Принадлежит: Sumitomo Chemical Co Ltd

A composition of a silver-conjugated compound composite containing (1) a silver-conjugated compound composite containing a silver particle with a Feret diameter of 1,000 nm or less and a conjugated compound having a weight average molecular weight of 3.0×10 2 or more being adsorbed to the silver particles and (2) an ionic compound. The ionic compound may be a compound having a structure represented by the following Formula (hh-1): [Chem. 1] M m′ + a X′ n′− b   (hh-1) wherein M m′+ represents a metal cation, X′ n′− represents an anion, a and b each independently represent an integer of 1 or more, and when M m′+ and X′ n′− are each plurally present, they may be the same as or different from each other.

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16-01-2014 дата публикации

Disintegrable deformation tool

Номер: US20140014339A1
Принадлежит: Baker Hughes Inc

A deformation system, including a deformable member and a tool operatively arranged to deform the member due to actuation of the tool from a first set of dimensions at which the deformable member is positionable with respect to a structure to a second set of dimensions at which the deformable member engages with the structure. The tool at least partially comprises a disintegrable material responsive to a selected fluid. A method of operating a deformation system is also included.

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02-01-2020 дата публикации

Particles having a sinterable core and a polymeric coating, use thereof, and additive manufacturing method using the same

Номер: US20200001359A1
Принадлежит: HOGANAS AB

Particles each having a sinterable core and a polymeric coating on at least a part of the core, wherein the polymeric coating includes a polymer that can be removed via decomposition by heat, catalytically or by solvent treatment, and wherein the polymeric coating is present in an amount of 0.10 to 3.00% by weight, relative to the total weight of the particles, as well as the use of these particles in an additive manufacturing process such as a powder bed and inkjet head 3D printing process. The particles and the process are able to provide a green part having improved strength and are thus suitable for the production of delicate structures which require a high green strength in order to minimize the risk of structural damage during green part handling.

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02-01-2020 дата публикации

METHOD FOR PREPARING NEODYMIUM-IRON-BORON PERMANENT MAGNETIC MATERIAL

Номер: US20200001360A1
Принадлежит:

A method for preparing a NdFeB permanent magnetic material may include providing a covered NdFeB magnetic powder by depositing heavy rare earth particles or high-melting particles onto a NdFeB magnetic powder by physical vapor deposition; and performing orientation molding and sintering on the covered NdFeB magnetic powder to provide the NdFeB permanent magnetic material. 110.-. (canceled)11. A method for preparing a NdFeB permanent magnetic material , the method comprising:preparing a NdFeB magnetic material;depositing heavy rare earth particles or high-melting particles onto the NdFeB magnetic material by physical vapor deposition to provide a covered NdFeB magnetic material; andperforming orientation molding and sintering on the covered NdFeB magnetic material to provide the NdFeB permanent magnetic material.12. The method according to claim 11 , further comprising first preparing the NdFeB magnetic material as a coarse powder with a particle size of 10 μm-2 mm claim 11 , andsubsequently refining the coarse powder into a fine powder after the physical vapor deposition.13. The method according to claim 11 , wherein the NdFeB magnetic material is prepared from a NdFeB magnet.14. The method according to claim 11 , wherein the preparation of the NdFeB magnetic material comprises mixing ingredients claim 11 , and smelting and strip casting the resulting mixture to obtain NdFeB sheets claim 11 , and wherein the depositing step comprises depositing heavy rare earth particles or high-melting particles onto the NdFeB sheets in an inert atmosphere by the physical vapor deposition method to form a covered NdFeB sheet claim 11 , the method further comprising crushing and milling the covered NdFeB sheet into a powder.15. The method according to claim 11 , wherein the depositing step further comprises selecting a desired high-melting target material claim 11 , placing the NdFeB magnetic material and particles of the high-melting target material in a physical vapor deposition ...

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03-01-2019 дата публикации

Metal powder atomization manufacturing processes

Номер: US20190001416A1
Принадлежит: AP&C Advanced Powders and Coatings Inc

There are provided reactive metal powder atomization manufacturing processes. For example, such processes include providing a heated metal source and contact the heated metal source with at least one additive gas while carrying out the atomization process. Such processes provide raw reactive metal powder having improved flowability. The at least one additive gas can be mixed together with an atomization gas to obtain an atomization mixture, and the heated metal source can be contacted with the atomization mixture while carrying out the atomization process. Reactive metal powder spheroidization manufacturing processes are also provided.

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07-01-2016 дата публикации

Core-shell nanoparticles and method for manufacturing the same

Номер: US20160002438A1
Принадлежит: DIC Corp

Provided are core-shell nanoparticles including a metal nanoparticle core and a shell layer composed of an oxide hybridized with a polyamine containing primary amino groups and/or secondary amino groups, core-shell metal nanoparticles prepared by removing the organic component from the shell layer and including a metal nanoparticle core and a shell layer based on silica, and simple and efficient methods for manufacturing such nanoparticles. Provided are a method for manufacturing a core-shell nanoparticle including performing a sol-gel reaction of an oxide source (C′) in the presence of a metal nanoparticle (A) having thereon a layer of a compound (B) containing a polyamine segment (b1) containing primary amino groups and/or secondary amino groups, a method for manufacturing a core-shell metal nanoparticle further including performing a sol-gel reaction of an organosilane to form a shell layer containing a polysilsesquioxane (D), and nanoparticles prepared by such methods.

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04-01-2018 дата публикации

LIGHT WEIGHT CEMENTED CARBIDE FOR FLOW EROSION COMPONENTS

Номер: US20180002783A1
Принадлежит:

A cemented carbide for a flow component for controlling the pressure and flow of well products includes in wt %: about 7 to about 9 Co; about 5 to about 7 Ni; about 19 to about 24 Ti C; about 1.5 to about 2.5 CrC; about 0.1 to about 0.3 Mo and balance of WC. A cemented carbide for fluid handling components and seal ring a comprises in wt %: about 1 to about 30 Ti C; about 12 to about 20 Co+Ni; about 0.5 to about 2.5 Cr; about 0.1 to about 0.3 Mo and balance of WC. A cemented carbide for fluid handling components and seal ring a comprises in wt %: about 15 to about 30 Ti C; about 5 to about 20 Ni; about 0.5 to about 2. Cr; about 0.5 to about 2.5 Mo and balance of WC. 1. A cemented carbide for a flow component for controlling the pressure and flow of well products , the cemented carbide having a composition comprising in wt % (weight %) of:about 7 to about 9 Co;about 5 to about 7 Ni;about 19 to about 24 TiC;{'sub': 3', '2, 'about 1.5 to about 2.5 CrC;'}about 0.1 to about 0.3 Mo; andbalance WC.2. The cemented carbide for a flow component of claim 1 , wherein the composition comprises about 20 to about 22 wt % TiC.3. The cemented carbide for a flow component according to claim 1 , wherein the composition comprises from about 1.8 to about 2.2 wt % CrC.4. The cemented carbide for a flow component according to claim 1 , wherein the composition comprises from about 5.3 to about 6.0 wt % Ni.5. The cemented carbide for a flow component according to claim 1 , wherein the composition comprises from about 8.0 to about 8.6 wt % Co.6. The cemented carbide for a flow component according to claim 1 , wherein the composition comprises from about 0.15 to about 0.25 wt % Mo.7. The cemented carbide for a flow component according to claim 1 , wherein the composition comprises WC of from about 50 wt % to about 69 wt %.8. The cemented carbide for a flow component according to claim 1 , wherein the composition has a density of from about 9.6 to about 10.2 g/cm.9. A cemented carbide for ...

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14-01-2016 дата публикации

Aluminum material for sintering, method for producing aluminum material for sintering, and method for producing porous aluminum sintered compact

Номер: US20160008884A1
Принадлежит: Mitsubishi Materials Corp

This aluminum sintering material is an aluminum sintering material that is used for producing a porous aluminum sintered compact in which a plurality of aluminum base materials are sintered together, and the aluminum sintering material includes: the aluminum base materials; and a plurality of titanium powder particles fixed to outer surfaces of the aluminum base materials, wherein the titanium powder particles are composed of either one or both of metallic titanium powder particles and hydrogenated titanium powder particles.

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08-01-2015 дата публикации

R-T-B-Ga-BASED MAGNET MATERIAL ALLOY AND METHOD OF PRODUCING THE SAME

Номер: US20150010426A1
Принадлежит:

Disclosed is an R-T-B—Ga-based magnet material alloy where R is at least one element selected from rare earth metals including Y, and T is one or more transition metals with Fe being an essential element. The R-T-B—Ga-based magnet material alloy includes: an RTB phase 3 which is a principal phase, and an R-rich phase (1 and 2) which is a phase enriched with the R, wherein a non-crystalline phase 1 in the R-rich phase has a Ga content (mass %) that is higher than a Ga content (mass %) of a crystalline phase 2 in the R-rich phase. With this, it is possible to enhance the magnetic properties of rare earth magnets that are manufactured from the alloy and reduce variations in the magnetic properties thereof. 1. An R-T-B—Ga-based magnet material alloy (where R is at least one element selected from rare earth metals including Y , and T is one or more transition metals with Fe being an essential element) , the R-T-B—Ga-based magnet material alloy , comprising:{'sub': 2', '14, 'an RTB phase which is a principal phase; and'}an R-rich phase which is a phase enriched with the R, the R-rich phase including a non-crystalline phase and a crystalline phase, the non-crystalline phase having a Ga content (mass%) that is higher than a Ga content (mass %) of the crystalline phase.2. The R-T-B—Ga-based magnet material alloy according to claim 1 , wherein the R-T-B—Ga-based magnet material alloy has an average thickness in a range of 0.1 mm to 1.0 mm.3. A method of producing the R-T-B—Ga-based magnet material alloy according to claim 1 , the method comprising:a first step of casting a ribbon from a molten R-T-B—Ga-based alloy using a strip casting method and crushing the ribbon to produce alloy flakes; anda second step of thermally maintaining the alloy flakes by holding the alloy flakes at a predetermined temperature for a predetermined time and then cooling the alloy flakes;the first step and the second step being performed under reduced pressure or in an inert gas atmosphere;the ...

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12-01-2017 дата публикации

Block copolymer comprising catechol ,segment and inorganic nanoparticles coated by said block copolymer, as well as method for producing block copolymer comprising catechol, segment and method for producing inorganic nanoparticles coated by said block copolymer

Номер: US20170008993A1
Автор: Hiroshi Yabu, Yuta Saito
Принадлежит: JAPAN SCIENCE AND TECHNOLOGY AGENCY

Provided is a block copolymer that makes it possible to produce inorganic nanoparticles that can be dispersed in an organic solvent, the inorganic nanoparticles being of uniform size and a reducing agent not having to be used. A block copolymer including a catechol segment represented by formula (1).

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11-01-2018 дата публикации

Methods of synthesizing dendritic gold nanoparticles

Номер: US20180009036A1
Автор: Chuanbin Mao, Penghe Qiu
Принадлежит: University of Oklahoma

Methods of synthesizing gold nanodendrites (AuNDs) using amines, such as long chain amines, as a structural directing agent are disclosed. Degree of branching (DB) of the AuNDs can be tuned by adjusting certain synthetic parameters, such as solvent type, and the type and concentration of the long chain amines. DB control results in dramatic tunability of the optical properties of the AuNDs in the near infrared (NIR) range enabling improved performance, for example as a photothermal cancer therapeutic.

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27-01-2022 дата публикации

METHOD FOR TREATMENT OF ELEMENTS OBTAINED BY AN ADDITIVE MANUFACTURING PROCESS

Номер: US20220024125A1
Автор: Abstreiter Tobias
Принадлежит:

A method for treatment of polymer elements obtained by an additive manufacturing process comprises applying to the polymer element a treating liquid in liquid form. 1. A method for treatment of polymer elements obtained by an additive manufacturing process comprisinga) a heating step for heating a treating liquid to a temperature below an upper threshold temperature, wherein the upper threshold temperature is in a range of about 1° C. to about 80° C. below the melting temperature of the polymer from which the polymer elements are formed,b) a smoothing step, wherein the polymer elements are in contact with the treating liquid at a temperature above a lower threshold temperature and below the upper threshold temperature for a predetermined time period, under conditions where the treating liquid is in liquid form,c) a cooling step for cooling the polymer elements,wherein the treating liquid comprises water and at least one monovalent aliphatic alcohol, wherein the weight ratio of water to alcohol is in a range of about 98:2 to about 20:80.2. The method of claim 1 , wherein the upper threshold temperature is in a range of about 100° C. to about 190° C.3. The method of claim 1 , wherein the at least one monovalent aliphatic alcohol is selected from ethanol claim 1 , propanol claim 1 , isopropanol claim 1 , methanol or a mixture thereof.4. The method of claim 1 , wherein the treating liquid comprises water and ethanol in a weight ratio of about 95:5 to about 30:70 and/or wherein the treating liquid is applied at a temperature in the range of about 100° C. to about 180° C. under conditions where the treating liquid is in liquid form.5. The method of claim 1 , wherein the treating liquid comprises at least one additional solvent and/or at least one plasticizer claim 1 , wherein the total amount of additional solvent and/or plasticizer is up to about 20 weight-%.6. The method of claim 5 , wherein the at least one additional solvent is substituted or unsubstituted aromatic C- ...

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10-01-2019 дата публикации

CUTTING TOOL

Номер: US20190010583A1
Принадлежит:

The present disclosure relates to a cutting tool of a cemented carbide substrate including WC and a binder phase having one or more of Co, Fe and Ni, wherein the cemented carbide also includes a finely dispersed eta phase of Me12C and/or Me6C carbides, where Me is one or more metals selected from W, Mo and the binder phase metals, wherein the substoichiometric carbon content in the cemented carbide is between −0.30 to −0.16 wt %. The disclosed cutting tool will achieve an improved resistance against comb cracks. 1. A cutting tool comprising a cemented carbide substrate comprising WC and a binder phase including one or more of Co , Fe and Ni , wherein the cemented carbide also includes an eta phase comprising Me12C and/or Me6C carbides where Me is one or more metals selected from W , Mo and the binder phase metals and wherein a substoichiometric carbon content in the cemented carbide is between −0.30 to −0.16 wt %.2. The cutting tool according to claim 1 , wherein the substoichiometric carbon content in the cemented carbide is between −0.28 to −0.17 wt %.3. The cutting tool according to claim 1 , wherein the amount of eta phase in the cemented carbide is between 2 to 10 vol %.4. The cutting tool according to claim 1 , wherein the eta phase has a grain size of 0.1 to 10 μm.5. The cutting tool according to claim 1 , wherein the binder phase content is 2 to 20 wt %.6. The cutting tool according to claim 1 , wherein the binder phase is cobalt.7. The cutting tool according to claim 1 , wherein the eta phase distribution is the same throughout the whole cemented carbide substrate.8. The cutting tool according to claim 1 , wherein the cemented carbide substrate is provided with a wear resistant CVD coating.9. The cutting tool according to claim 1 , wherein the cemented carbide substrate is provided with a CVD coating comprising at least a Ti(C claim 1 ,N) layer and a Al2O3 layer.10. A method of making a cutting tool comprising cemented carbide substrate claim 1 , the method ...

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09-01-2020 дата публикации

MICROGEL PARTICLES FOR USE IN 3D PRINTING AND 3D CELL GROWTH MEDIUM AND RELATED COMPOSITIONS, SYSTEMS, AND METHODS

Номер: US20200010798A1
Принадлежит:

Microgel particles for use in a three-dimensional cell growth medium are described. The microgel particles may be swellable and may have properties conducive to improved function and health of cells distributed within the three-dimensional cell growth medium. Related compositions, systems, and methods are also described. Also provided is a plurality of microgel particles and a liquid cell culture medium, wherein the microgel particles are swelled with the liquid cell culture medium to form a granular gel. Also provided is a method of preparing a three-dimensional cell growth medium is disclosed. The method may comprise: mixing a plurality of microgel particles, such as those described above, in a liquid cell culture medium. Also provided is a method of placing cells in a three-dimensional cell growth medium is disclosed. Also provided is a method of synthesizing a protein is disclosed. 1. A composition for use in a three-dimensional cell growth medium , the composition comprising: low charge density polymer molecules; and', 'crosslinker., 'a plurality of microgel particles, each of the plurality of microgel particles comprising a crosslinked polymeric network, wherein the crosslinked polymeric network comprises2. The composition of claim 1 , wherein each of the low charge density polymer molecules comprises a plurality of charged groups claim 1 , wherein an average spacing between the charged groups is greater than ¼ claim 1 , ½ claim 1 , 1 times claim 1 , 1.5 times claim 1 , or 2 times the Bjerrum length.3. The composition of claim 2 , wherein the charged groups are negatively charged groups.4. The composition of claim 2 , wherein each of the low charge density polymer comprises a first set of monomer units and a second set of monomer units claim 2 , wherein the second set of monomer units is derived from acidic monomers claim 2 , and wherein the second set of monomer units comprise the charged groups.5. The composition of claim 4 , wherein less than 60% of the sum ...

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12-01-2017 дата публикации

Assembly comprising an element that is capable of transmitting heat, a film of a polymer that is a good thermal conductor and electrical insulator, a sintered joint and a radiator and manufacturing method

Номер: US20170011991A1
Автор: Rabih KHAZAKA

An assembly comprises: at least one element that is capable of transmitting heat; at least one electrically insulating substrate comprising at least one film of a polymer that is a good thermal conductor and electrical insulator; at least one sintered metal joint that is in contact with the polymer film; a main radiator; the radiator being in direct contact, or in contact via a sintered joint, with the substrate.

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10-01-2019 дата публикации

SOFT MAGNETIC ALLOY POWDER AND DUST CORE USING SAME

Номер: US20190013123A1
Принадлежит:

Provided herein is a soft magnetic alloy powder that can exhibit a high saturation flux density and desirable soft magnetic characteristics. A dust core using the soft magnetic alloy powder is also provided. The soft magnetic alloy powder is an Fe-based nanocrystalline soft magnetic alloy powder of a crystallized Fe-based amorphous soft magnetic alloy powder, and has a DSC curve with a first peak that is 15% or less of a first peak of the Fe-based amorphous soft magnetic alloy in terms of a maximum value. 1. An Fe-based nanocrystalline soft magnetic alloy powder of a crystallized Fe-based amorphous soft magnetic alloy ,the Fe-based nanocrystalline soft magnetic alloy powder having a differential scanning calorimetry (DSC) curve with a first peak that is 15% or less of a first peak of the Fe-based amorphous soft magnetic alloy in terms of a maximum value.2. The Fe-based nanocrystalline soft magnetic alloy powder according to claim 1 , wherein the DSC curve of the Fe-based nanocrystalline soft magnetic alloy powder has a second peak occurring on a higher temperature side of the first peak of the Fe-based nanocrystalline soft magnetic alloy powder and having a maximum value that is 50% or more and 100% or less of a maximum value of a second peak of the Fe-based amorphous soft magnetic alloy occurring on a higher temperature side of the first peak of the Fe-based amorphous soft magnetic alloy.3. The Fe-based nanocrystalline soft magnetic alloy powder according to claim 1 , wherein the second peak of the Fe-based nanocrystalline soft magnetic alloy powder has two or more peaks including a low-temperature-side second peak claim 1 , and a high-temperature-side second peak.4. The Fe-based nanocrystalline soft magnetic alloy powder according to claim 3 , wherein the low-temperature-side second peak is smaller than the high-temperature-side second peak in terms of a maximum value.5. The Fe-based nanocrystalline soft magnetic alloy according to claim 3 , wherein the two or ...

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03-02-2022 дата публикации

METHOD FOR THE MANUFACTURE OF MULTIMATERIAL ROLL AND THE MULTIMATERIAL ROLL

Номер: US20220032351A1
Автор: TALVITIE Mikko
Принадлежит:

In the present there is presented a method to manufacture multimaterial rolls, comprising method to produce base material containing part of the roll, joining of special material containing part for that, hot working at least part of the length of the roll ingot containing base material and special material, —so that at least requested roll ingot length and diameter are achieved as well as final treatment of the roll ingot—to manufacture finished roll. This method enables manufacture of large rolls, for example having length more than 3 meters as one integrated component without welding or mechanical joint—so, that in the working surfaces of the rolls is used steel with high amount of alloying elements and carbide forming alloying elements. 1. Method for the manufacture of multimaterial rolls comprising following steps:Base material containing part of the roll ingot is produced based on the selected method so, that the base material is such ferrous material which contains other alloying elements than iron maximum 15 weight-%,Special material containing part is joined to the base material containing parts of the roll ingot, which is produced using a suitable method so that special material density is at least 90% of its theoretical density and it forms 5-40 volume-% of the total volume of base material and special materials, The length of the roll is longer than roll ingot length before hot working, and/or', 'The diameter of the roll is smaller than roll ingot diameter before hot working, and/or', 'Roll shaft diameter is smaller than base material diameter before hot working, and', 'Multimaterial special material layer thickness is at least 5 mm,, 'The base material and special material containing part of the roll ingot is hot worked at least for the part of the length of the roll ingot so, that following is reached after hot working;'}wherein, before hot working at least the special materials containing parts of the roll ingot is encapsulated by capsule using at ...

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03-02-2022 дата публикации

COMPOSITION FOR USE IN 3D PRINTING

Номер: US20220033616A1
Принадлежит:

A photocurable polymer composition for use with a three dimensional printing process and a method of manufacture of such composition. The composition includes a photocurable resin and a filler and can be tunable to a desired dielectric constant. The filler comprises about 0 to about 30 weight percent of the composition. 1. A photocurable polymer composition for use in a three-dimensional printer comprising:a photocurable resin;a filler;{'b': 0', '30, 'wherein said filler ranges from About to about weight percent of the composition and said photocurable polymer composition has a desired dielectric constant.'}2. The composition as recited in claim 1 , whereOIN the photocurable resin is an acrylate.3. The composition as recited in claim 1 , wherein the photocurable resin is an olefin.4. The composition as recited in claim 1 , wherein the filler is chosen from the group consisting of inorganic or organic fillers.5. The composition as recited in claim 3 , wherein the inorganic fillers are chosen from the group comprising of mica claim 3 , titanium dioxide and magnesium oxide.6. The composition as recited in claim 4 , wherein the fillers comprise a mixture of mica and magnesium oxide.7. A method of preparing a photocurable composition having a desired dielectric constant for use in a three-dimensional printer comprising adding filler to a photocurable resin and dispersing uniformly the filler in such photocurable resin.8. A part manufactured using a three-dimensional printer using a photocurable composition comprising a photocurable resin with filler dispersed uniformly in such resin to achieve a desired dielectric constant.9. The composition of claim 1 , wherein the photocurable resin is an epoxy. The present invention relates to a photocurable polymer composition used for three-dimensional printing which is tunable to a desired dielectric constant or dissipation factor.Three-dimensional printing or additive manufacturing has become increasingly popular over the past ...

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16-01-2020 дата публикации

Samarium-iron-nitrogen alloy powder and method for producing same

Номер: US20200016663A1

A samarium-iron-nitrogen alloy powder according to one embodiment of the present invention is characterized in that a value obtained by dividing the hydrogen content of the samarium-iron-nitrogen alloy powder by the BET specific surface area of the samarium-iron-nitrogen alloy powder is less than or equal to 400 ppm/(m2/g), and a value obtained by dividing the oxygen content of the samarium-iron-nitrogen alloy powder by the BET specific surface area of the samarium-iron-nitrogen alloy powder is less than or equal to 11,000 ppm/(m2/g).

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17-04-2014 дата публикации

Composite soft magnetic powder, composite soft magnetic powder core, and preparation method therefor

Номер: US20140104023A1
Принадлежит: Toyota Motor Corp, TSINGHUA UNIVERSITY

The present invention discloses a composite soft magnetic powder core and a preparation method therefor, which belong to the technical fields of soft magnetic materials and preparation thereof. An Fe/Fe 3 O 4 shell layer is generated in situ on surfaces of iron powder particles through a controlled oxidation process, to prepare Fe/Fe 3 O 4 composite soft magnetic powder having a uniform structure. The Fe/Fe 3 O 4 composite soft magnetic powder is mixed with suitable amount of silicone resin, and prepared into a high-performance Fe/Fe 3 O 4 composite soft magnetic powder core by using a powder metallurgy compaction process. Such magnetic powder core has a high density, a high magnetic conductivity, a high magnetic flux density, a low loss, and a high breaking strength, and is useful in a large-power and low-loss application scenario. The present invention has the advantages of being rich in raw material resources, simple in process and environmentally friendly, and being suitable for industrial production.

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25-01-2018 дата публикации

METHOD OF MAKING A POLYMER COMPOSITE

Номер: US20180022042A1
Принадлежит:

A method of making a composite feed material for fused deposition modeling (FDM) is disclosed. The method comprises providing composite particles made by a process of emulsion aggregation, the composite particles comprising at least one thermoplastic polymer and at least one carbon particle material. A composite feed material is formed for fused deposition modeling from the composite particles. The composite feed material is in a form selected from a filament and a paste. 1. A method of making a composite feed material for fused deposition modeling (FDM) , the method comprising:providing composite particles made by a process of emulsion aggregation, the composite particles comprising at least one thermoplastic polymer and at least one carbon particle material; andforming a composite feed material for fused deposition modeling from the composite particles, the composite feed material being in a form selected from a filament and a paste.2. The method of claim 1 , wherein the at least one thermoplastic polymer has a Tg of less than 100° C.3. The method of claim 1 , wherein the at least one thermoplastic polymer has a viscosity of less than 50 claim 1 ,000 cP claim 1 , where viscosity is determined at shear of 6.28 rad/sec using a TA instruments model DHR2 rheometer with 2 parallel (25 mm) plates at a temperature of 100° C.4. The method of claim 1 , wherein the at least one thermoplastic polymer is a latex.5. The method of claim 1 , wherein the at least one thermoplastic polymer is selected from the group consisting of polyacrylates claim 1 , polybenzimidazoles claim 1 , polycarbonates claim 1 , polyether sulfones claim 1 , polyaryl ether ketones claim 1 , polyetherimide claim 1 , polyethylenes claim 1 , polyphenylene oxides claim 1 , polypropylenes claim 1 , polystyrenes claim 1 , styrene-butyl acrylate claim 1 , polyesters claim 1 , polyurethanes claim 1 , polyamides claim 1 , Poly(vinylidene fluoride) (PVDF) claim 1 , polyvinyl chlorides and combinations thereof.6. ...

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24-01-2019 дата публикации

MACHINING TOOL

Номер: US20190024221A1
Принадлежит:

A cutting machining tool for metal-containing materials has a base material composed of cemented hard material with hard material particles embedded in a ductile metallic binder. The metallic binder is a Co—Ru alloy and the hard material particles are formed at least predominantly by tungsten carbide, having an average grain size of the tungsten carbide of 0.1-1.2 μm. The cemented hard material has a Co+Ru content of 5-17% by weight of the cemented hard material, a Ru content of 6-16% by weight of the Co+Ru content, a Mo content in the range 0.1-3.0% by weight of the cemented hard material, a content of Ti, Ta and/or Nb of in each case <0.2% by weight of the cemented hard material, and a V content of <0.3% by weight of the cemented hard material. 113-. (canceled)14. A cutting machining tool for metal-containing materials , the machining tool comprising:a base material composed of cemented hard material formed of hard material particles embedded in a ductile metallic binder, said metallic binder being a Co—Ru alloy and said hard material particles being at least predominantly formed by tungsten carbide, and said tungsten carbide having an average grain size of 0.1-1.2 μm;a (Co+Ru) content of 5-17% by weight of said cemented hard material;a Ru content of 6-16% by weight of said (Co+Ru) content;a Mo content in a range of 0.1-3.0% by weight of said cemented hard material;a content of one or more elements selected from the group consisting of Ti, Ta and Nb, in each case <0.2% by weight of said cemented hard material; anda V content of <0.3% by weight of said cemented hard material.15. The cutting machining tool according to claim 14 , wherein said V content amounts to <0.2% by weight of said cemented hard material.16. The cutting machining tool according to claim 14 , wherein said cemented hard material has an Mo content in a range 0.15-2.5% by weight of said cemented hard material.17. The cutting machining tool according to claim 14 , wherein the average grain size of ...

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23-01-2020 дата публикации

Highly active silica magnetic nanoparticles for purifying biomaterial and preparation method thereof

Номер: US20200024592A1
Принадлежит: Bioneer Corp

The present invention relates to a method for preparing highly active silica magnetic nanoparticles, highly active silica magnetic nanoparticles prepared by the method, and a method of isolating nucleic acid using the highly active silica magnetic nanoparticles. The highly active silica magnetic nanoparticles prepared according to the present invention contain magnetic nanoparticles completely coated with silica, can be used as a reagent for isolating biomaterials, particularly, nucleic acids, and can isolate and purify nucleic acid in a high yield.

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28-01-2021 дата публикации

Independent Control of Both Index and Dispersion in Gradient Index Optics

Номер: US20210026043A1
Принадлежит:

Three or more base optical materials are selectively combined into a trans-gradient index (GRIN) optical element (e.g., a lens). A wavelength-dependent index of refraction for light propagating perpendicular to the three or more optical materials equals: a volume fraction of a first optical material multiplied by a refractive index of the first optical material, plus a volume fraction of a second optical material multiplied by a refractive index of the second optical material, plus one minus the volume fraction of the first optical material and the volume of the second optical material all multiplied by the refractive index of a third optical material. The wavelength-dependent index of refraction distribution and a refractive index dispersion through the GRIN optical element may be independently specified from one another. A local refractive index at any point in the optical element is a fixed function of a refractive index of each individual optical material. 1. A method comprising:providing three or more base optical materials comprising a first base optical material, a second base optical material, and a third base optical material;selectively combining the three or more base optical materials into a set of trans-gradient index (GRIN) materials; andusing the set of trans-GRIN materials to independently control both an index of refraction distribution and an optical dispersion distribution through a GRIN optical element.2. The method of claim 1 , wherein a wavelength-dependent index of refraction for light propagating perpendicular to the three or more base optical materials equals:a volume fraction of the first base optical material multiplied by a refractive index of the first base optical material, plusa volume fraction of the second base optical material multiplied by a refractive index of the second base optical material, plusone minus the volume fraction of the first base optical material and the volume of the second base optical material all multiplied by ...

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29-01-2015 дата публикации

Porous structures and methods of making same

Номер: US20150030493A1
Принадлежит: Smith and Nephew Inc

The present disclosure provides methods to improve the properties of a porous structure formed by a rapid manufacturing technique. Embodiments of the present disclosure increase the bonding between the micro-particles 5 on the surface of the porous structure and the porous structure itself without substantially reduce the surface area of the micro-particles. In one aspect, embodiments of the present disclosure improves the bonding while preserving or increasing the friction of the structure against adjacent materials.

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02-02-2017 дата публикации

Method for Manufacturing Metal Powder

Номер: US20170028477A1

A method for manufacturing metal powder comprising: providing a basic metal salt solution; contacting the basic metal salt solution with a reducing agent to precipitate metal powder therefrom; and recovering precipitated metal powder from the solvent.

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01-02-2018 дата публикации

Abradable Material Feedstock and Methods and Apparatus for Manufacture

Номер: US20180029120A1
Автор: Christopher W. STROCK
Принадлежит: United Technologies Corp

A method for manufacturing a powder comprises vaporizing a solvent; passing a metallic powder and a polymer powder through the solvent vapor to mix the metallic powder with the polymer powder; and removing the solvent.

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02-02-2017 дата публикации

THREE-DIMENSION FORMING MATERIAL, THREE-DIMENSION FORMING SUPPORT MATERIAL, AND THREE-DIMENSION FORMING COMPOSITION SET

Номер: US20170029613A1
Принадлежит: FUJI XEROX CO., LTD.

A three-dimension forming material includes a radiation curable compound and has a total concentration of a magnesium ion and a calcium ion of 50 ppm or less, a concentration of an alkali metal ion of 100 ppm or less, and a concentration of a fatty acid compound of 50 ppm or less. 1. A three-dimension forming material ,comprising a radiation curable compound, andhaving a total concentration of a magnesium ion and a calcium ion of 50 ppm or less, a concentration of an alkali metal ion of 100 ppm or less, and a concentration of a fatty acid compound of 50 ppm or less.2. A three-dimension forming support material ,comprising a radiation curable compound and a plasticizer, andhaving a total concentration of a magnesium ion and a calcium ion of 50 ppm or less, a concentration of an alkali metal ion of 100 ppm or less, and a concentration of a fatty acid compound of 50 ppm or less.3. A three-dimension forming composition set comprising:{'claim-ref': {'@idref': 'CLM-00001', 'claim 1'}, 'the three-dimension forming material according to ; and'}a three-dimension forming support material that contains a radiation curable compound and a plasticizer.4. The three-dimension forming composition set according to claim 3 ,wherein the three-dimension forming support material has a total concentration of a magnesium ion and a calcium ion of 50 ppm or less, a concentration of an alkali metal ion of 100 ppm or less, and a concentration of a fatty acid compound of 50 ppm or less. This application is based on and claims priority under 35 USC 119 from Japanese Patent Application No. 2015-152853 filed Jul. 31, 2015.1. Technical FieldThe present invention relates to a three-dimension forming material, a three-dimension forming support material, and a three-dimension forming composition set.2. Related ArtThe three-dimension forming apparatus, also called as a 3D printer, for example, is known as an apparatus for fabricating a three-dimensional structure (for example, parts of industrial ...

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31-01-2019 дата публикации

Composition of particulate materials and process for obtaining self-lubricating sintered products

Номер: US20190030607A1

The metallurgical composition comprises a main particulate metallic material, for example iron or nickel, and at least one alloy element for hardening the main metallic material, which form a structural matrix; a particulate solid lubricant, such as graphite, hexagonal boron nitride or mixture thereof; and a particulate alloy element which is capable of forming, during the sintering of the composition conformed by compaction or by injection molding, a liquid phase, agglomerating the solid lubricant in discrete particles. The composition may comprise an alloy component to stabilize the alpha-iron matrix phase, during the sintering, in order to prevent the graphite solid lubricant from being solubilized in the iron. The invention further refers to the process for obtaining a self-lubricating sintered product.

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05-02-2015 дата публикации

SYSTEM AND METHOD OF FORMING NANOSTRUCTURED FERRITIC ALLOY

Номер: US20150033912A1
Принадлежит: GENERAL ELECTRIC COMPANY

A system for mechanical milling and a method of mechanical milling are disclosed. The system includes a container, a feedstock, and milling media. The container encloses a processing volume. The feedstock and the milling media are disposed in the processing volume of the container. The feedstock includes metal or alloy powder and a ceramic compound. The feedstock is mechanically milled in the processing volume using metallic milling media that includes a surface portion that has a carbon content less than about 0.4 weight percent. 1. A system , comprising:a container enclosing a processing volume;a feedstock comprising metal or alloy powder and a ceramic compound in the processing volume; anda metallic milling media disposed in the processing volume,wherein the metallic milling media comprises a surface portion having a carbon content less than about 0.4 weight percent.2. The system of claim 1 , wherein the ceramic compound comprises an oxide claim 1 , carbide claim 1 , nitride claim 1 , boride claim 1 , or any combinations thereof.3. The system of claim 1 , wherein a concentration of the ceramic compound is less than about 8 wt % of the the feedstock.4. The system of claim 3 , wherein the concentration of the ceramic compound is in a range from about 0.05 wt % to about 4 wt %.5. The system of claim 1 , wherein the metallic milling media comprises a ferrous alloy.6. The system of claim 5 , wherein the metallic milling media comprises a martensitic matrix.7. The system of claim 5 , wherein the metallic milling media comprises a bainitic matrix.8. The system of claim 1 , wherein the surface portion of the metallic milling media has a toughness greater than about 10 MPa m.9. The system of claim 1 , wherein a carbon content of an interior portion of the milling media is substantially same as that of the carbon content of the surface portion.10. The system of claim 9 , wherein a Rockwell hardness of the milling media is greater than about 40 HRC.11. The system of claim 1 ...

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05-02-2015 дата публикации

Method and apparatus for the recovery and regeneration of metal powder in EBM applications

Номер: US20150034123A1
Принадлежит:

The present invention relates to a method and an associated apparatus () for the recovery and regeneration of metal powder in EBM (Electron Beam Melting) applications. The method is of the type which envisages a step for recovery of weakly sintered powders inside a cleaning chamber () incorporating at least one compressed-air nozzle with supply, where necessary, of powder for sandblasting three-dimensional objects obtained by means of EBM sintering of the metal powders; according to the invention it is envisaged supplying into the cleaning chamber () metal powders having a predetermined low oxygen content and there is also a powder recirculating system () comprising at least one first buffer tank () inside which the regenerated powders are deposited for renewed supply of the aforementioned chamber (). 1239. Method for the recovery and regeneration of metal powders in EBM (Electron Beam Melting) applications , which envisages a step for recovery of weakly sintered powders inside a cleaning chamber () including at least one compressed-air nozzle with supplying , where necessary , of powder for sandblasting three-dimensional objects obtained by means of EBM sintering of said metal powders , characterized in that it comprises a path () for recovery and regeneration of said powders , comprising at least a first buffer tank () inside which the regenerated powders are deposited and in that metal powders (ELI , ELI*) with a predetermined low oxygen content are supplied at an access point along said recovery and regeneration path.22. Method according to claim 1 , characterized in that the supply of said (ELI) metal powders with a predetermined low oxygen content is performed directly inside said cleaning chamber ().310915. Method according to claim 1 , characterized in that it envisages a second buffer tank () connected downstream of and supplied by the first buffer tank () for topping up one or more hoppers or tanks () of corresponding EBM sintering apparatus.410. Method ...

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04-02-2021 дата публикации

METHOD FOR MANUFACTURING MATERIAL POWDER FOR METAL LAMINATING MODELLING

Номер: US20210031270A1
Автор: MURANAKA Katsutaka
Принадлежит: SODICK CO., LTD.

Provided is a method for manufacturing material powder for metal laminating modelling, in which a virgin material is manufactured based on the particle size distribution of the virgin material being an unused material powder, and the fluidity of an unsintered reused material after the virgin material is reused a predetermined number of times by a metal laminating modelling device, so that the particle size distribution of the virgin material corresponds to the fluidity of the reused material that is equal to or greater than a predetermined standard value. Silica particles may be added to the virgin material. 1. A method for manufacturing material powder for metal laminating modelling , wherein the material powder for metal laminating modelling is manufactured based onthe particle size distribution of a virgin material being the material powder that is unused, andthe fluidity of a reused material being the material powder that is unsintered, wherein the fluidity of the reused material is obtained after implementing a durability test in which the virgin material is reused a predetermined number of times in a manner that the virgin material is supplied to a metal laminating modelling device and then the reused material discharged from the metal laminating modelling device is recovered, subsequently, the reused material is supplied to the metal laminating modelling device and the reused material discharged from the metal laminating modelling device is recovered,so that the particle size distribution corresponds to the fluidity of the reused material being equal to or greater than a predetermined standard value of the fluidity.2. The method for manufacturing material powder for metal laminating modelling according to claim 1 , whereinthe durability test is implemented without performing laminating modelling.3. The method for manufacturing material powder for metal laminating modelling according to claim 1 , whereinthe fluidity is obtained based on a discharge time from ...

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04-02-2021 дата публикации

Light-curable composition

Номер: US20210032441A1
Принадлежит: TECHNISCHE UNIVERSITAET WIEN

A light-curable composition is provided which may be used as a photopolymerizable material in an additive manufacturing process. The additive manufacturing process involves heating the light-curable composition which has a viscosity at 20° C. of at least 20 Pa·s. The light-curable composition includes a photopolymerizable matrix material, at least one thermoplastic polymer dissolved therein, and at least one photoinitiator. Polycaprolactone or a derivative thereof is used as the dissolved thermoplastic polymer.

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01-05-2014 дата публикации

Metal nano particle and method for surface treating the same

Номер: US20140119978A1
Принадлежит: Samsung Electro Mechanics Co Ltd

Disclosed herein is a method for surface treating metal nano particles, including: surface treating metal nano particles with an alkanol amine containing solution.

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11-02-2016 дата публикации

Silver-Bismuth Powder,Conductive Paste and Conductive Film

Номер: US20160040271A1
Принадлежит: Dowa Electronics Materials Co Ltd

To provide a silver-bismuth powder, which includes: silver; and bismuth, wherein a mass ratio (silver:bismuth) of the silver to the bismuth is 95:5 to 40:60, wherein a cumulative 50% point of particle diameter (D50) of the silver-bismuth powder in a volume-based particle size distribution thereof as measured by a laser diffraction particle size distribution analysis is 0.1 μm to 10 μm, and wherein an oxygen content of the silver-bismuth powder is 5.5% by mass or less.

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24-02-2022 дата публикации

Method of controlled conversion of thermosetting resins and additive manufacturing thereof by selective laser sintering

Номер: US20220056305A1
Принадлежит:

The invention is directed to a method of controlled conversion of thermosetting resins and additive manufacturing thereof by selective laser sintering. Partial curing of a thermosetting formulation can be used to increase the Tof the resin and minimize the additional cure needed to cross-link a printed object. After printing, the partially cured material is finally cured via a slow temperature ramp maintained just below the material's evolving T. 1. A method for printing a thermosetting polymer , comprisingproviding a partially cured resin material,producing a resin powder from the partially cured resin material,printing and sintering the resin powder on a print bed at a bed temperature near a glass transition temperature of the resin powder to provide a printed part, andcuring the printed part according to a post-print cure schedule to provide a cured printed part.2. The method of claim 1 , wherein the resin material comprises a stoichiometrically balanced formulation comprising a thermosetting resin and a curing agent.3. The method of claim 2 , wherein the thermosetting resin comprises an epoxy.4. The method of claim 3 , wherein the epoxy comprises difunctional bisphenol A/epichlorohydrine epoxy.5. The method of claim 2 , wherein the thermosetting resin comprises a bismaleimide claim 2 , cyanate ester claim 2 , alkyne claim 2 , alkene claim 2 , acrylate claim 2 , anhydride claim 2 , carboxylic acid claim 2 , isocyanate claim 2 , or halide.6. The method of claim 2 , wherein the curing agent comprises an amine.7. The method of claim 6 , wherein the amine comprises 4 claim 6 ,4′-diaminodiphenylsulphone.8. The method of claim 2 , wherein the curing agent comprises a thiol claim 2 , alkene claim 2 , anhydride claim 2 , azide claim 2 , carboxylic acid claim 2 , or hydroxyl.9. The method of claim 1 , wherein the step of providing a partially cured resin material comprisesmixing a thermosetting resin with a curing agent to provide a thermosetting resin formulation, ...

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07-02-2019 дата публикации

PLA Pellets Enhanced with Calcium Carbonate from Powdered Zebra Mussel Shells and Quagga Mussel Shells

Номер: US20190040217A1
Автор: James Lorena
Принадлежит:

Provided are materials for 3D printing. The materials have calcium carbonate and polylactic acid. The calcium carbonate is derived from natural sources, such as the shells of zebra mussels or quagga mussels. The calcium carbonate can coat a pellet of polylactic acid. Also disclosed are methods of making and using the same. 1. A material for 3D printing , comprising CaCOand polylactic acid , wherein the CaCOis derived from crushed zebra mussel shells and/or crushed quagga mussel shells.2. The material of claim 1 , wherein the CaCOand the polylactic acid are present in a ratio of 1:3 of CaCOto polylactic acid.3. The material of claim 1 , wherein the CaCOand the polylactic acid are present in a ratio of 1:4 of CaCOto polylactic acid.4. The material of claim 1 , wherein the CaCOand the polylactic acid are present in a ratio of 1:5 of CaCOto polylactic acid.5. The material of claim 1 , wherein the CaCOis primarily calcite.6. The material of claim 5 , wherein the CaCOis only calcite.7. The material of claim 1 , wherein a grain size of the CaCOis less than or equal to 125 microns.8. The material of claim 7 , wherein the grain size is less than or equal to 63 microns.9. A method of preparing a 3D printing material claim 7 , comprising:i) combining calcium carbonate and polylactic acid to form a mixture, wherein the calcium carbonate is derived from crushed zebra mussel shells and/or crushed quagga mussel shells; andii) heating the mixture.10. The method of claim 9 , wherein the polylactic acid is a plurality of polylactic acid pellets.11. The method of claim 9 , wherein the calcium carbonate is less than or equal to 125 microns in grain size.12. The method of claim 11 , wherein the calcium carbonate is less than or equal to 63 microns in grain size.13. The method of claim 9 , wherein the mixture is heated to a temperature of 155 to 165° C.14. The method of claim 9 , further comprising passing the heated mixture through an extruder.15. The method of claim 9 , wherein the ...

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18-02-2021 дата публикации

IRON BASED POWDER

Номер: US20210046543A1
Принадлежит: Höganas AB (publ)

Disclosed is a new diffusion-bonded powder consisting of an iron powder having 1-5%, preferably 1.5-4% and most preferabiy 1.5-3.5% by weight of copper particles diffusion bonded to the surfaces of the iron powder particles. The new diffusion bonded powder is suitable for producing components having high sintered density and minimum variation in copper content. 1. An iron based powder consisting of particles of reduced copper oxide diffusion bonded to the surface of an atomized iron powder , wherein the content of copper is 1-5%-by weight of the iron based powder.2. The iron based powder according to claim 1 , wherein the maximum particle size is 250 μm claim 1 , at least 75% is below 150 μm and at most 30% is below 45 μm claim 1 , the apparent density is at least 2.70 g/cm3 and the oxygen content is at most 0.16% by weight and other compounds at most 1% by weight.3. The iron based powder according to having a SSF-factor of at most 2.0 claim 2 , wherein the SSF-factor is defined as the quotation between the Cu content in weight % in the fraction of the iron based powder which passes a 45 μm sieve and the Cu content in weight % in the fraction of the iron based powder which does not pass a 45 μm sieve.4. The iron based powder according to claim 1 , wherein the maximum copper content in a cross section of a sintered component made from said iron based powder is at most 100% higher than the nominal copper content claim 1 , wherein the sintered component is produced by mixing said iron-based powder with 0.5% of graphite claim 1 , having a particle size claim 1 , ×90 claim 1 , of at most 15 μm measured with laser diffraction according to ISO 13320:1999 claim 1 , and 0.9% of lubricant and the obtained mixture is transferred into a compaction die for production of tensile strength samples (TS-bars) according to ISO 2740: 2009 and subjected to a compaction pressure of 600 MPa and the compacted sample is thereafter ejected from the compaction die and subjected to a sintering ...

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06-02-2020 дата публикации

POLYMERIZABLE MONOMERS AND METHOD OF POLYMERIZING THE SAME

Номер: US20200040113A1
Принадлежит:

Provided herein are photopolymerizable monomers, optionally for use as reactive diluents in a high temperature lithography-based photopolymerization process, a method of producing polymers using said photopolymerizable monomers, the polymers thus produced, and orthodontic appliances comprising the polymers. 2. The orthodontic appliance of claim 1 , wherein the orthodontic appliance is an aligner claim 1 , expander or spacer.3. The orthodontic appliance of claim 1 , wherein the orthodontic appliance comprises a plurality of tooth receiving cavities configured to reposition teeth from a first configuration toward a second configuration.4. The orthodontic appliance of claim 1 , wherein the orthodontic appliance is one of a plurality of orthodontic appliances configured to reposition the teeth from an initial configuration toward a target configuration.5. The orthodontic appliance of claim 1 , wherein the orthodontic appliance is one of a plurality of orthodontic appliances configured to reposition the teeth from an initial configuration toward a target configuration according to a treatment plan.6. The orthodontic appliance of claim 1 , wherein the polymer is a crosslinked polymer.7. The orthodontic appliance of claim 1 , wherein the polymer has viscoelastic behavior in the temperature range from 20° C. to 40° C.8. The orthodontic appliance of claim 1 , comprising a feature size of less than or equal to about 5 μm.9. The orthodontic appliance of claim 1 , comprising a feature size within a range from about 5 μm to about 50 μm.10. The orthodontic appliance of claim 1 , comprising a strength that varies by no more than about 25% along all directions.11. The orthodontic appliance of claim 1 , wherein the orthodontic appliance is fabricated using direct fabrication.12. The orthodontic appliance of claim 11 , wherein the direct fabrication produces the orthodontic appliance in a time interval less than or equal to about 1 hour.13. The orthodontic appliance of claim 1 , ...

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18-02-2016 дата публикации

Method for Production of Performance Enhanced Metallic Materials

Номер: US20160045949A1
Автор: Yousefiani Ali
Принадлежит: The Boeing Company

A method for production of a metallic material from a semifinished metallic billet, the semifinished metallic billet including a nanocrystalline microstructure and/or an ultrafine-grained microstructure, the method including the steps of (1) subjecting the semifinished metallic billet to a rotary incremental forming process to form an intermediate wrought metallic billet, and (2) subjecting the intermediate wrought metallic billet to a high rate forming process to form a metallic product. 1. A method for production of metallic material from a semifinished metallic billet , said semifinished metallic billet comprising at least one of a nanocrystalline microstructure and an ultrafine-grained microstructure , said method comprising:subjecting said semifinished metallic billet to a rotary incremental forming process to form an intermediate wrought metallic billet; andsubjecting said intermediate wrought metallic billet to a high rate forming process.2. The method of wherein said rotary incremental forming process comprises a rotary swaging process.3. The method of wherein said high rate forming process comprises an extrusion process.4. The method of wherein said rotary incremental forming process comprises a rotary incremental forming process temperature (in degrees Kelvin) claim 1 , said rotary incremental forming process temperature being at most about 90 percent of a melting temperature (in degrees Kelvin) of said semifinished metallic billet.5. The method of wherein said high rate forming process comprises a high rate forming process temperature (in degrees Kelvin) claim 4 , said high rate forming process temperature being at most about 90 percent of said melting temperature (in degrees Kelvin) of said semifinished metallic billet.6. The method of wherein said high rate forming process temperature is less than said rotary incremental forming process temperature.7. The method of wherein said rotary incremental forming process comprises a rotary incremental forming ...

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18-02-2016 дата публикации

Preparation of formed orthopedic articles

Номер: US20160045957A1
Принадлежит: Howmedica Osteonics Corp

In one embodiment, the present invention may be a method of forming a porous and/or dense article from metal powder, including adding to a mold a first feedstock comprising an agglomerated metal powder and an agglomeration agent; forming said first feedstock into a green state dense article; and removing said agglomeration agent. Furthermore, the present invention may include a second feedstock including an agglomerated metal powder, a space filling material and an agglomeration agent which may be formed into a green state porous article. The present invention also includes a dense and/or porous article manufactured by various methods, as well as methods for creating the dense and porous feedstocks. Moreover, the present invention may include an article which may be a medical implant.

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18-02-2021 дата публикации

Method For Preparing Magnetic Powder And Magnetic Material

Номер: US20210047711A1
Принадлежит: LG CHEM, LTD.

A method of producing a magnetic powder and a magnetic powder is provided. The method of producing a magnetic powder according to an exemplary embodiment of the present disclosure includes: producing an iron powder by a reduction reaction of iron oxide, producing a magnetic powder using a molded body obtained by press molding a mixture including the iron powder, a rare earth oxide, boron, and calcium at a pressure of 22 MPa or more, and coating a surface of the magnetic powder with ammonium fluoride. 1. A method of producing a magnetic powder comprising:producing an iron powder by a reduction reaction of iron oxide;producing a magnetic powder using a molded body obtained by press molding a mixture including the iron powder, a rare earth oxide, boron, and calcium at a pressure of 22 MPa or more; and coating a surface of the magnetic powder with ammonium fluoride.2. The method of claim 1 , further comprising:before the coating of the surface of the magnetic powder with ammonium fluoride,mixing the magnetic powder with ammonium nitrate, methanol, and zirconia balls; andpulverizing the mixture.3. The method of claim 1 , whereinthe producing of the iron powder further comprises:reducing a mixture of at least one of an alkali metal oxide or an alkaline earth metal oxide with iron oxide under an inert gas atmosphere, in the presence of a reducing agent.4. The method of claim 3 , whereinthe mixture including the iron powder, the rare earth oxide, the boron, and the calcium is produced by adding neodymium oxide, boron, and calcium to the iron powder.5. The method of claim 1 , whereinthe producing of the iron powder further comprises:reducing a mixture of neodymium oxide and iron oxide which has been wet-mixed under an organic solvent, in the presence of a reducing agent to produce an iron powder and neodymium oxide-containing mixture.6. The method of claim 5 , whereinthe mixture including the iron powder, neodymium oxide, boron and calcium is produced by adding boron and ...

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18-02-2021 дата публикации

Silicon oxide-coated iron powder, method for producing the same, molded body for inductor using the same, and inductor

Номер: US20210050132A1
Принадлежит: Dowa Electronics Materials Co Ltd

A silicon oxide-coated iron powder has a small particle diameter, can achieve high in a high frequency band, and has high insulating property. In a method for producing the powder, a silicon alkoxide is added to a slurry containing iron powder having an average particle diameter of 0.25 μm or more and 0.80 μm or less and an average axial ratio of 1.5 or less dispersed in a mixed solvent of water and an organic material containing water in an amount of 1% by mass or more and 40% by mass or less. Then, a hydrolysis catalyst for the silicon alkoxide is added to perform silicon oxide coating, the method resulting in a silicon oxide-coated iron powder having the high μ′ in a high frequency band and the high insulating property.

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18-02-2021 дата публикации

Metal particle aggregates, method for producing same, paste-like metal particle aggregate composition, and method for producing bonded body using said paste-like metal particle aggregate composition

Номер: US20210050319A1
Принадлежит: Mitsubishi Materials Corp

A metal particle aggregate includes metal particles and an organic substance. The metal particles include first particles that contain one or both of silver and copper in an amount of 70% by mass or more relative to 100% by mass of all metals and have a particle diameter of 100 nm or more and less than 500 nm at a ratio of 20 to 30% by number, and include second particles that have a particle diameter of 50 nm or more and less than 100 nm, and third particles that have a particle diameter of less than 50 nm at a ratio of 80 to 70% by number in total. Surfaces of the first to third particles are covered with the same protective film.

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03-03-2022 дата публикации

Porous silver powders and method for preparing the same

Номер: US20220062985A1
Автор: Jong Goo Kang
Принадлежит: Individual

Provided is a porous silver powder and a preparation method thereof. More specifically, the present invention relates to porous silver powder that is easy to prepare, improves a sterilization effect because an specific surface area and a porosity are easily adjustable, improves electrical conductivity when molded as sintered body, contributes to reducing use of expensive silver when applied in various industrial fields, thus achieving price competitiveness, and is harmless to the human body because a particle size is adjustable to prevent the porous silver powder from being absorbed into the body; and a preparation method thereof.

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03-03-2022 дата публикации

Method for interconnecting components of an electronic system by sintering

Номер: US20220062990A1

Method for interconnecting components of an electronic system, the method comprising the steps of: a) depositing a sintering solution onto a first component in order to form an interconnection layer, the sintering solution comprising a solvent, metal nanoparticles dispersed in the solvent, and a stabilizing agent adsorbed onto the metal nanoparticles. the metal nanoparticles comprising for more than 95.0%, preferably for more than 99.0% of their mass a metal selected from silver, gold, copper and alloys thereof and having a polyhedral shape with an aspect ratio of more than 0.8, b) eliminating, at least partially, the solvent from the interconnection layer such as to form at least one agglomerate in which the stabilizing agent binds them together and maintains at least a portion of the metal nanoparticles at a distance from each other, c) debinding and sintering the interconnection layer by bringing the agglomerate into contact with at least one destabilizing agent configured to desorb the stabilizing agent from the metal nanoparticles in order to aggregate and coalesce said metal nanoparticles between themselves, and d) depositing a second component in contact with the interconnection layer before or during debinding or sintering.

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03-03-2022 дата публикации

METHOD OF POST MANUFACTURE PROCESSING OF 3D PRINTED PARTS

Номер: US20220063152A1
Автор: THIESSEN Robert
Принадлежит:

A method of post manufacture processing of 3D printed parts involves a step of forming at least one treatment aperture through an exterior shell of a 3D printed part to provide access to a lattice of multiple layers of extruded thermo-plastic filaments within a hollow cavity of the part. The method involves a step of inserting a stabilizing substance that flows before it is set and then hardens when set through the at least one treatment aperture into the hollow cavity of the part. The method involves a step of coating the lattice with the stabilizing substance to fill spaces between the multiple layers and between individual thermo-plastic filaments, such that, when set, the stabilizing substance fixes the multiple layers of extruded thermo-plastic filaments of the lattice in position. The method reinforces and stabilizes the internal lattice structure of the part, without significantly adding material or increasing manufacturing cost. 1. A method of post manufacture processing of 3D printed parts , comprising:forming at least one treatment aperture through an exterior shell of a 3D printed part to provide access to an internal lattice of multiple layers of extruded thermo-plastic filaments within a hollow cavity of the part;inserting a stabilizing substance that flows before it is set and then hardens when set through the at least one treatment aperture into the hollow cavity of the part; andcoating the lattice with the stabilizing substance to fill spaces between the multiple layers and between individual thermos-plastic filaments, such that, when set, the stabilizing substance fixes the multiple layers of extruded thermo-plastic filaments of the lattice in position.2. The method of claim 1 , wherein the stabilizing substance is inserted through the at least one treatment aperture by connecting fluids lines to the at least one treatment aperture of the part.3. The method of claim 2 , wherein the coating of the lattice is accomplished by creating a pressure ...

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14-02-2019 дата публикации

GRADE POWDERS AND SINTERED CEMENTED CARBIDE COMPOSITIONS

Номер: US20190047051A1
Принадлежит:

In one aspect, grade powder compositions are described herein comprising electrochemically processed sintered carbide scrap. In some embodiments, a grade powder composition comprises a reclaimed powder component in an amount of at least 75 weight percent of the grade powder composition, wherein the reclaimed carbide component comprises electrochemically processed sintered carbide scrap. 1. A grade powder composition comprising:a reclaimed carbide powder component in an amount of at least 70 weight percent of the grade powder composition, the reclaimed carbide component comprising electrochemically processed sintered carbide scrap.2. The grade powder composition of claim 1 , wherein the electrochemically processed sintered carbide scrap comprises tungsten carbide.3. The grade powder composition of claim 2 , wherein the reclaimed carbide powder component further comprises at least one metal carbide selected from the group consisting of Group IVB metal carbides claim 2 , Group VB metal carbides and Group VIB metal carbides.4. The grade powder composition of claim 1 , wherein the electrochemically processed sintered carbide scrap has an average particle size of 0.5 μm to 30 μm.5. The grade powder composition of claim 1 , wherein the electrochemically processed sintered carbide scrap has an average particle size of 1 μm to 5 μm.6. The grade powder composition of claim 1 , wherein the reclaimed carbide powder component is present in an amount of 75-99 weight percent of the grade powder composition.7. The grade powder composition of claim 1 , wherein the reclaimed carbide powder component is present in an amount of 90-99 weight percent of the grade powder composition.8. The grade powder composition of claim 1 , wherein the reclaimed carbide powder component consists essentially of the electrochemically processed sintered carbide scrap.9. The grade powder composition of further comprising powder metallic binder.10. The grade powder composition of claim 9 , wherein the ...

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13-02-2020 дата публикации

BIOPRINTING PROCESS

Номер: US20200046520A1
Принадлежит:

A bio-printing process comprises a step of preparing a target digital model representative of the three-dimensional organization of the tissue to be produced, a step of controlling a bio-printing instrument for the deposition of a plurality of layers of living cells and of biomaterials, a step of calculation of a digital printing model as a function of the digital model of the product to be produced, and of a model predicting change, and also characteristics of the constituents to be printed. The step of controlling the bio-printing instrument is carried out according to the digital printing model calculated in this way. A system is also described for implementing this process. 1. A bio-printing method , comprising:a step of preparing a target digital model representative of a three-dimensional organization of tissue to be manufactured; anda step of calculating a digital printing model according to the digital model of a product to be manufactured, and a predictive development model a, as well as the characteristics of components to be printed; anda step of controlling a bio-printing equipment for the deposition of a plurality of layers of living cells and biomaterials carried out according to the digital printing model thus calculated.2. The method of claim 1 , further comprising a 2D characterization step of each of the layers during the bio-printing step.3. The method of claim 1 , further comprising a step of maturing the printed item.4. The method of claim 1 , further comprising a step of 3D characterization of the bio-printed product immediately after the bio-printing.5. The method of claim 1 , further comprising a step of 3D characterization of the bio-printed product during its maturation.6. The method of claim 1 , wherein the predictive development model is stored on a shared server claim 1 , the bio-printing equipment including means for communicating with the server to select from a digital library a recorded predictive development model adapted to a ...

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08-05-2014 дата публикации

Material comprising a semi-heusler alloy and process for producing such a material

Номер: US20140127070A1
Принадлежит: ROBERT BOSCH GMBH

A material includes at least two different alloy phases. At least two alloy phases are each formed by at least one thermodynamically stable semi-Heusler alloy. The semi-Heusler alloys of the at least two alloy phases are different from one another. At least two of the semi-Heusler alloys have at least partly sintered particles that have an average particle size D 50 in the range of less than or equal to 100 nm. Such a material has particularly good thermoelectric properties. A process is implemented to produce the material.

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13-02-2020 дата публикации

IMMISCIBLE-INTERFACE ASSISTED DIRECT METAL DRAWING

Номер: US20200047251A1
Автор: HE Li, Song Xuan
Принадлежит:

A method of three-dimensional printing of target material can include filling a receptacle with a matrix suspension comprising a powder matrix suspended in a first liquid. A second suspension can be extruded into the matrix suspension, where the second suspension can include a target powder suspended in a second liquid. 1. A method of three-dimensional printing of target material comprising:filling a receptacle with a matrix suspension comprising a powder matrix suspended in a first liquid;extruding a second suspension into the matrix suspension, the second suspension comprising a target powder suspended in a second liquid;evaporating at least one of the first and second liquids by heating to a temperature high enough to facilitate evaporation of the first and second liquids but not high enough to sinter or melt the target powder or powder matrix; andheating the matrix suspension and the second suspension to a temperature high enough to dry the matrix suspension and the second suspension and high enough to sinter the target powder, but not high enough to sinter or melt the matrix powder, to form a sintered final product.2. The method of claim 1 , further comprising:removing the sintered final product from the powder matrix.3. The method of claim 1 , wherein the melting temperature of the target powder is higher than the melting temperature of the powder matrix.4. The method of claim 1 , wherein the second suspension is immiscible with the matrix suspension.5. The method of claim 1 , wherein the matrix suspension maintains the second suspension substantially in place during extruding of the target powder.6. The method of claim 1 , wherein extruding the second suspension into the matrix suspension is performed by injecting the second suspension into the matrix suspension.7. The method of claim 6 , wherein extruding the second suspension into the matrix suspension is performed using a movable nozzle or a movable needle.8. A method of creating a metal object using ...

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26-02-2015 дата публикации

Composite nanometal paste containing copper filler and joining method

Номер: US20150053753A1

The present invention addresses the problem of providing a composite nanometal paste which is relatively low in price and is excellent in terms of bonding characteristics, thermal conductivity, and electrical property. The present invention is a copper-filler-containing composite nanometal paste that contains composite nanometal particles each comprising a metal core and an organic coating layer formed thereon. The metal paste contains a copper filler and contains, as binders, first composite nanometal particles and second composite nanometal particles which differ from the first composite nanometal particles in the thermal decomposition temperature of the organic coating layer, wherein the mass proportion W1 of the organic coating layer in the first composite nanometal particles is in the range of 2-13 mass %, the mass proportion W2 of the organic coating layer in the second composite nanometal particles is in the range of 5-25 mass %, and these particles satisfy the relationships W1.

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23-02-2017 дата публикации

Process for producing shaped refractory metal bodies

Номер: US20170050244A1
Принадлежит: Individual

The present invention relates to a process for producing shaped articles composed of refractory metals.

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22-02-2018 дата публикации

ADHESIVE COMPOSITION

Номер: US20180051193A1
Принадлежит:

Provided are an adhesive composition and an organic electronic device (OED) including the same, and particularly, an adhesive composition, which may form an encapsulation structure effectively blocking moisture or oxygen flowing into an OED from the outside, thereby ensuring the lifespan of the OED, realize a top-emission OED, and exhibit excellent adhesive durability and reliability, and an OED including the same. 1. An adhesive composition for encapsulating an organic electronic element , comprising:{'sup': '2', 'an olefin-based resin having a water vapor transmission rate (WVTR) of 50 g/m·day or less;'}a heat-curable resin; anda photocurable compound.2. The adhesive composition of claim 1 , wherein the olefin-based rein has a weight average molecular weight of 100 claim 1 ,000 or less.3. The adhesive composition of claim 1 , wherein the olefin-based resin has one or more reactive functional groups having reactivity with the heat-curable resin.4. The adhesive composition of claim 3 , wherein the functional group having reactivity with the heat-curable resin is an acid anhydride group claim 3 , a carboxyl group claim 3 , an epoxy group claim 3 , an amino group claim 3 , a hydroxyl group claim 3 , an isocyanate group claim 3 , an oxazoline group claim 3 , an oxetane group claim 3 , a cyanate group claim 3 , a phenol group claim 3 , a hydrazide group or an amide group.5. The adhesive composition of claim 1 , wherein heat-curable resin comprises at least one heat-curable functional group.6. The adhesive composition of claim 5 , wherein the heat-curable functional group comprises an epoxy group claim 5 , an isocyanate group claim 5 , a hydroxyl group claim 5 , a carboxyl group or an amide group.7. The adhesive composition of claim 1 , wherein the heat-curable resin is comprised at 10 to 70 parts by weight with respect to 100 parts by weight of the olefin-based resin.8. The adhesive composition of claim 1 , further comprising:a heat-curing agent.9. The adhesive ...

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03-03-2022 дата публикации

HARD-MAGNET L10-CoPt NANOPARTICLES ADVANCE FUEL CELL CATALYSIS

Номер: US20220069317A1
Автор: Junrui Li, Shouheng Sun
Принадлежит: BROWN UNIVERSITY

A method includes converting ˜9 nm soft-magnet Al—CoPt into a hard-magnet L10-CoPt, acid etching the hard-magnet L10-CoPt, and annealing the acid etched hard-magnet L10-CoPt to generate a L10-CoPt/Pt catalyst.

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15-05-2014 дата публикации

Magnetic material and coil component

Номер: US20140132383A1
Принадлежит: TAIYO YUDEN CO LTD

An object is to provide a magnetic material and coil component offering improved magnetic permeability and insulation resistance, while also offering improved high-temperature load, moisture resistance, water absorbency, and other reliability characteristics at the same time. A magnetic material that has multiple metal grains constituted by Fe—Si-M soft magnetic alloy (where M is a metal element that oxidizes more easily than Fe), as well as oxide film constituted by an oxide of the soft magnetic alloy and formed on the surface of the metal grains, wherein the magnetic material has bonding parts where adjacent metal grains are bonded together via the oxide film formed on their surface, as well as bonding parts where metal grains are directly bonded together in areas having no oxide film, and resin material is filled in at least some of the voids generating as a result of accumulation of the metal grains.

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04-03-2021 дата публикации

Preparation of long-lasting antibacterial core-shell agent and application for the solid media or surface coating

Номер: US20210059247A1
Автор: Chun An Lai, Huang Chih Lu
Принадлежит: Meganite Inc

A long-lasting antibacterial core-shell agent, a method for preparing a long-lasting antibacterial agent and method for preparing a solid media utilizing a long-lasting antibacterial core-shell agent. The long-lasting antibacterial core-shell agent comprises an antibacterial core composed of an antibacterial metal powder, a poorly soluble metal salt and a metal oxide; and an outer shell composed of a porous oxide. The solid media prepared utilizing the long-lasting antibacterial core-shell agent has the ability to resist ultraviolet damage, inhibits oxygen oxidation, slowly releases metal ions and thereby exhibits long-term release of antibacterial ions and longitudinal antibacterial uniformity.

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21-02-2019 дата публикации

Liquid composition

Номер: US20190054525A1
Принадлежит: Shenmao Technology Inc

A liquid composition includes copper particles, an organic acid, and a solvent. The copper particle has a particle size of 0.5 μm˜30 μm which falls in a micron scale. The liquid composition performs reaction sintering by redox reactions taken place between the copper particles and an organic acid solution at a low temperature of 150° C. in order to produce a dense copper layer and improve the conventional micron-scale copper particles that requires a protective atmosphere for the high-temperature sintering before achieving the required densification. This liquid composition also prevents an excessive oxidation of the nano copper particles during the low-temperature sintering process and a failure of the dense sintering. Due to the agglomeration of nano copper particles, some areas have to be sintered first, so that the sintered products have a good uniformity of tissue and a low resistance below 0.04 ohm per square (Ω/□).

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04-03-2021 дата публикации

TANTALUM POWDER AND PREPARATION METHOD THEREFOR

Номер: US20210060654A1

A tantalum powder, a tantalum powder compact, a tantalum powder sintered body, a tantalum anode, an electrolytic capacitor and a preparation method for tantalum powder. The tantalum powder contains boron element, and the tantalum powder has a specific surface area of greater than or equal to 4 m/g; the ratio of the boron content of the tantalum powder to the specific surface area of the tantalum powder is 2˜16; the boron content is measured in weight ppm, and the specific surface area is measured in m/g; Powder that can pass through a ρ-mesh screen in the tantalum powder accounts for over 85% of the total weight of the tantalum powder, where ρ=150˜170; and the tantalum powder with high CV has a low leakage current and dielectric loss, and good moldability. 136-. (canceled)37. A method for preparing tantalum powder , comprising:{'sup': '2', '1) reducing a tantalum fluoride salt with a reducing agent in a molten diluent to obtain a raw tantalum powder, wherein said raw tantalum powder contains boron in an amount of 30˜300 ppm and has a specific surface area of ˜13 m/g;'}{'sup': '3', '2) granulating said tantalum powder to obtain a pre-agglomerated powder, wherein the pre-agglomerated powder has a bulk density of 1˜1.5 g/cm;'}the granulating comprises: mixing raw tantalum powder with water to obtain a powder mixed with water; drying the powder mixed with water to obtain a dried powder; and crushing and sieving the dried powder, wherein the mesh number of the screen for sieving is 120˜170 mesh, and powder that passes through the screen is pre-agglomerated powder; and3) sequentially subjecting said pre-agglomerated powder to one or more of the following steps: heat treatment, sieving, oxygen reduction treatment, and nitrogen doping;4) sequentially subjecting the powder obtained in the previous step to one or more of the following steps: acid washing, water washing, drying and sieving, to obtain a tantalum powder product;wherein, the tantalum powder product has an oxygen ...

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01-03-2018 дата публикации

Cermet Materials and Method for Making Such Materials

Номер: US20180057914A1

The invention relates to a cermet material comprising a first phase MAX having the general formula Ti n+1 AlC n and a second intermetallic phase having the general formula Ti x Al y , where n equals 1 or 2, x is between 1 and 3, y is between 1 and 3, and x+y≦4. The proportion by volume of the first phase in the material is between 70% and 95%. The proportion by volume of the second phase in the material is between 30% and 5%. The void ratio is less than 5%.

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20-02-2020 дата публикации

A PREPARATION METHOD OF A WC CEMENTED CARBIDE WITH ADJUSTABLE ALIGNMENT OF PLATE-SHAPE GRAINS

Номер: US20200056266A1
Принадлежит: SOUTH CHINA UNIVERSITY OF TECHNOLOGY

The invention discloses a preparation method of a WC cemented carbide with adjustable alignment of plate-shape grains. According to the theoretical composition of the cemented carbide, the weighed W powder is composed of two raw W materials with significantly different particle sizes in a certain mass ratio. Also graphite powder and Co powder are weighed. W—C—Co powder is subjected to planetary ball milling with controlled process parameters; then, after plasma-assisted ball milling, W—C—Co composite powder composed of small-sized lamellar W sheets and large-sized lamellar W sheet is obtained; Finally dense cemented carbide containing plate-shape WC grains is obtained by press molding of the ball milled power and in-situ carbonization through sintering at a high temperature. The invention not only provides simple preparation process with low energy consumption, but also can regulate the degree of orientated alignment of the plate-shape WC in the sintered block. Besides, the mechanical properties of the WC—Co cemented carbide containing plate-shape WC grains are optimized, so that the cemented carbide has excellent overall mechanical properties. 1. A preparation method of a WC cemented carbide with adjustable alignment of plate-shape grains , comprising the steps of:(1) weighting graphite powder, Co powder and W powder according to the composition of WC—XCo; characterized in that, the W powder comprises fine W particles and coarse W particles, and 6≤X≤20;the fine W particles has a particle size of 0.3 μm-1 μm; the coarse W particles has a particle size of 5 μm-25 μm;the mass ratio of the fine W particles to the coarse W particles is 1:4-4:1;(2) adding the graphite powder, the Co powder and the W powder in step (1), and required extra amount of carbon in a planetary ball mill for planetary ball milling to obtain W—C—Co powder;(3) placing the W—C—Co powder obtained in step (2) in a plasma-assisted high-energy ball mill for plasma-assisted ball milling to obtain W—C—Co ...

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04-03-2021 дата публикации

VALVE SEATS AND VALVE ASSEMBLIES FOR FLUID END APPLICATIONS

Номер: US20210062805A1
Принадлежит:

In one aspect, valve seats are described herein having structure and design addressing degradative stresses encountered by the seats during installation and operation in fluid ends. In some embodiments, a valve seat for use in a fluid end comprises a first section for insertion into a fluid passageway of the fluid end and a second section extending longitudinally from the first section, the second section comprising a frusto-conical valve mating surface, wherein the second section is encased in a ring imparting a compressive stress condition to the second section. 1. A valve seat for use in a fluid end comprising:a body including a first section for insertion into a fluid passageway of the fluid end and a second section extending longitudinally from the first section, the second section comprising a recess in which a sintered cemented carbide inlay is positioned, wherein the sintered cemented carbide inlay comprises a valve mating surface and exhibits a compressive stress condition.2. The valve seat of claim 1 , wherein the valve mating surface of the sintered cemented carbide inlay has surface roughness (R) of 1-15 μm.3. The valve seat of claim 1 , wherein the valve mating surface of the sintered cemented carbide inlay is frusto-conical.4. The valve seat of claim 1 , wherein the second section imparts the compressive stress condition to the sintered cemented carbide inlay.5. The valve seat of claim 4 , wherein an inner annular surface of the second section comprises one or more protrusions for engaging the sintered cemented carbide inlay.6. The valve seat of claim 1 , wherein the body is formed of metal or alloy.7. The valve seat of claim 1 , wherein outer diameter of the first section is equal to outer diameter of the second section.8. The valve seat of claim 1 , wherein outer diameters of the first and second sections are not equal.9. The valve seat of claim 8 , wherein the outer diameter of the second section is greater than the outer diameter of the first ...

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28-02-2019 дата публикации

AGGLOMERATED PARTICLE POWDER FOR ADDITIVE MANUFACTURING

Номер: US20190060993A1
Принадлежит:

Devices, systems, and methods are directed at spreading sequential layers of powder across a powder bed and applying energy to each layer to form a three-dimensional object. The powder can include granules including agglomerations of metallic particles to facilitate spreading the metallic particles in each layer. The energy can be directed to the powder to reflow the granules in each layer to bind the metallic particles in the layer to one another and to one or more adjacent layers to form the three-dimensional object. Thus, in general, the agglomeration of the metallic particles in the granules can overcome constraints associated with metallic particles that are of a size ordinarily unsuitable for flowing and/or a size that presents safety risks. By overcoming these constraints, the granules can improve formation of dense finished parts from a powder and can result in formation of unique microstructures in finished parts. 1. A powder for additive manufacturing of a three-dimensional object , the powder comprising:first metallic particles; andat least one component of a binder system, the first metallic particles agglomerated in the at least one component of the binder system in the form of discrete granules flowable relative to one another to form a layer having a thickness greater than about 30 microns and less than about 70 microns.2. The powder of claim 1 , wherein the discrete granules are substantially spherical.3. The powder of claim 1 , wherein the first metallic particles include a plurality of materials alloyable with one another.4. The powder of claim 3 , wherein the plurality of materials includes two or more of tungsten claim 3 , copper claim 3 , nickel claim 3 , cobalt claim 3 , and iron.5. The powder of claim 1 , wherein the first metallic particles in respective granules are lightly sintered to one another.6. The powder of claim 1 , wherein the at least one component of the binder system is water soluble to reflow the at least one component of the ...

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28-02-2019 дата публикации

Three-dimensional metallic objects having microstructures

Номер: US20190060994A1
Принадлежит: Desktop Metal Inc

Devices, systems, and methods are directed at spreading sequential layers of powder across a powder bed and applying energy to each layer to form a three-dimensional object. The powder can include granules including agglomerations of metallic particles to facilitate spreading the metallic particles in each layer. The energy can be directed to the powder to reflow the granules in each layer to bind the metallic particles in the layer to one another and to one or more adjacent layers to form the three-dimensional object. Thus, in general, the agglomeration of the metallic particles in the granules can overcome constraints associated with metallic particles that are of a size ordinarily unsuitable for flowing and/or a size that presents safety risks. By overcoming these constraints, the granules can improve formation of dense finished parts from a powder and can result in formation of unique microstructures in finished parts.

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10-03-2016 дата публикации

EDIBLE 3D PRINTER FILAMENT

Номер: US20160066601A1
Принадлежит:

The present invention relates to an edible 3D printer filament that incorporates an active ingredient such as an oil extract for taste, odor or medicinal benefit, and which is capable of retaining this benefit, despite the repeated thermal extrusion involved in 3D printing. The filament is made by mixing the active ingredient extraction with polyvinylpyrrolidone (PVP), starch, and super disintegrant, and spray drying the result to a powderized form. The powderized water soluble polymer with active ingredient is mixed with excipient ingredients including a plasticizer, colored/dyed arabic gum, a gelling agent, fillers, flour, a binding or thickening agent (which also gives the benefit of being, a stabilizer), a lubricant, and a preservative, and is heated. The result is hot melt extruded into a filament with a diameter of 1.75 mm or 3 mm. When printed, the thermoplastic has good strength, stiffness, and physical properties, and can be 3D-printed in any shape. 1. A method for producing an edible filament for use in a conventional 3D printer , comprising the steps of: obtaining dried plant material,', 'performing an extraction on said plant material to produce an essential oil (active ingredient) therefrom;, 'producing an essential oil by the substeps of'} active ingredient,', 'polyvinylpyrrolidone (PVP),', 'starch, and', 'a super disintegrant;, 'preparing a water soluble polymer compound by mixing;'}spray drying said water soluble polymer compound;mixing and heating said powderized water soluble polymer compound with a plasticizer, colored arabic gum, a gelling agent, filler, flour, a binding or thickening agent, a lubricant, and a preservative, thereby forming an edible thermoplastic;hot-melt extruding said edible thermoplastic through a die to produce a filament; andwinding said filament on a spool.2. The method of claim 1 , wherein said step of hot-melt extruding said edible thermoplastic comprises extruding through a die having a 1.75 mm diameter.3. The method of ...

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27-02-2020 дата публикации

Method for manufacturing photo-sintering particle, method for manufacturing photo-sintering target, and photo-sintering method

Номер: US20200061704A1

Provided is a method for manufacturing photonic sintering particles. According to an embodiment, the method includes: preparing nano particles; and forming oxide films having different thicknesses with reference to the thermal conductivity of a substrate, on which the nano particles are to be formed, on surfaces of the nano particles.

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12-03-2015 дата публикации

METHOD FOR PREPARING NEODYMIUM-IRON-BORON (ND-FE-B)-BASED SINTERED MAGNET

Номер: US20150071810A1
Принадлежит:

A method for preparing a Nd—Fe—B-based sintered magnet. The method includes: 1) providing a master alloy and an auxiliary alloy, the master alloy being a Nd—Fe—B alloy ingot or cast strip, the auxiliary alloy being a heavy rare earth alloy; 2) breaking up the master alloy using a hydrogen decrepitation process to yield a crude powder, conducting hydrogen absorption treatment on the auxiliary alloy and breaking up the hydrogenated auxiliary alloy to yield hydride particles; 3) uniformly mixing and stirring the crude powder of the master alloy and the hydride particles of the auxiliary alloy to yield a mixture; 4) milling the mixture obtained in step 3) to yield powders; 5) uniformly stirring the powders obtained in step 4) and conducting orientation forming treatment on the powders, to yield a raw body of a Nd—Fe—B based magnet; and 6) sintering the raw body of the Nd—Fe—B based magnet. 1. A method for preparing a Neodymium-Iron-Boron (Nd—Fe—B) based sintered magnet , the method comprising:{'sub': a', 'b', '100−a−b, '1) providing a master alloy and an auxiliary alloy, the master alloy being a Nd—Fe—B alloy ingot or cast strip, the auxiliary alloy being a heavy rare earth alloy having a formula of RMFe, wherein R represents Gd, Tb, Dy, Ho, or a mixture thereof, M represents Co, Mn, Cu, Al, Ti, Ga, Zr, V, Hf, W, B, Nb, or a mixture thereof, a and b are both expressed in percentage by weight, 30≦a<100, 0≦b<70;'}2) breaking up the master alloy using a hydrogen decrepitation process to yield a crude powder, conducting hydrogen absorption treatment on the auxiliary alloy and breaking up the hydrogenated auxiliary alloy to yield hydride particles;3) uniformly mixing and stirring the crude powder of the master alloy and the hydride particles of the auxiliary alloy to yield a mixture, wherein a weight percentage of the crude powder of the master alloy is greater than or equal to 75% and less than 100% of a total weight of the mixture, and a weight percentage of the hydride ...

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24-03-2022 дата публикации

Method for producing silver nanowires, silver nanowires, dispersion, and transparent conductive film

Номер: US20220088678A1
Принадлежит: Microwave Chemical Co Ltd

In order to provide a method for producing silver nanowires in which a local maximum of optical absorption in the plasmon absorption band can be shifted toward the short wavelength side without making the wire diameter smaller, a method for producing silver nanowires includes a step of heating a mixed liquid of a dispersion of silver nanowires and metal ions of a transition metal that is different from silver, and reducing the metal ions, thereby intermittently precipitating clumps of the transition metal on a surface of the silver nanowires. The thus produced silver nanowires have metal clumps intermittently along the length direction, and a local maximum of optical absorption in the plasmon absorption band of the silver nanowires has been shifted toward the short wavelength side.

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15-03-2018 дата публикации

ROCK DRILL BUTTON

Номер: US20180073108A1
Принадлежит:

A rock drill button having a body of sintered cemented carbide that has hard constituents of tungsten carbide (WC) in a binder phase of Co, wherein the cemented carbide has 4-12 mass % Co and balance WC and unavoidable impurities. The cemented carbide also has Cr in such an amount that the Cr/Co ratio is within the range of 0.043-0.19, and that the WC grain size mean value is above 1.75 μm. 1. A rock drill button , comprising:a body made of sintered cemented carbide that comprises hard constituents of tungsten carbide (WC) in a binder phase comprising Co, wherein the cemented carbide comprises 4-12 mass % Co, and a balance of WC and unavoidable impurities, Wherein said cemented carbide also comprises Cr in such an amount that the Cr/Co ratio is within the range of 0.043-0.19, and wherein a WC grain size mean value is above 1.75 μm.2. The rock drill button according to claim 1 , wherein the WC grain size mean value is above 2.0 μm.3. The rock drill button according to claim 1 , wherein the Cr/Co ratio is equal to or above 0.075.4. The rock drill button according to claim 1 , wherein the Cr/Co ratio is equal to or above 0.085.5. The rock drill button according to claim 1 , wherein the Cr/Co ratio is equal to or less than 0.15.6. The rock drill button according to claim 1 , wherein the Cr/Co ratio is equal to or less than 0.12.7. The rock drill button according to claim 1 , wherein the content of Cr in said cemented carbide is equal to or above 0.17 mass %.8. The rock drill button according to claim 1 , wherein the content of Cr in said cemented carbide is equal to or lower than 2.3 mass %.9. The rock drill button according to claim 1 , wherein the Cr is present in the binder phase as dissolved in cobalt.10. The rock drill button according to claim 1 , wherein the binder phase is essentially free from chromium carbide.11. The rock drill button according to claim 1 , wherein said cemented carbide has a hardness of not higher than 1500 HV3.12. The rock drill button ...

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24-03-2022 дата публикации

Silver paste

Номер: US20220089894A1
Принадлежит: Shoei Chemical Inc

The present invention provides a silver paste containing at least a silver powder, a binder resin, and an organic solvent, wherein the silver powder contains a first silver powder having a D50 of 3.50 to 7.50 μm and a second silver powder having a D50 of 0.80 to 2.00 μm, where D50 represents a 50% value of a volume-based cumulative fraction obtained by laser diffraction particle size distribution measurement; a copper content of the whole silver powder is 10 to 5000 ppm by mass; a copper content of the second silver powder is 80 ppm by mass or more; and the first silver powder contains substantially no copper. The present invention provides a silver paste containing a powder in a high concentration and excellent in printability, and provides a silver conductor film that has a high filling factor, a high film density, high electrical conductivity, and excellent migration resistance.

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18-03-2021 дата публикации

PROCESS FOR PRODUCING SPHEROIDIZED POWDER FROM FEEDSTOCK MATERIALS

Номер: US20210078072A1
Принадлежит:

Disclosed herein are embodiments of methods, devices, and assemblies for processing feedstock materials using microwave plasma processing. Specifically, the feedstock materials disclosed herein pertains to scrap materials, dehydrogenated or non-hydrogenated feed material, and recycled used powder. Microwave plasma processing can be used to spheroidize and remove contaminants. Advantageously, microwave plasma processed feedstock can be used in various applications such as additive manufacturing or powdered metallurgy (PM) applications that require high powder flowability. 1. (canceled)2. A method for manufacturing a spheroidized copper or copper alloy powder , the method comprising:providing a feedstock comprising a material selected from the group consisting of copper and copper alloys;the feedstock comprising metallic particles within a range of particle volumes suitable for use as feedstock in a microwave plasma process; andapplying the microwave plasma process to the metallic particles within the range of particle volumes to form spheroidized copper or copper alloy powder,wherein the feedstock comprises a microstructure that is retained in the spheroidized copper or copper alloy powder after applying the microwave plasma process.3. The method of claim 2 , wherein the range of particle volumes is between 15 and 63 microns.4. The method of claim 2 , wherein applying the microwave plasma process comprises introducing the copper or copper alloy particles into an exhaust of a microwave plasma torch or into a plume of the microwave plasma torch.5. The method of claim 2 , wherein the spheroidized powder comprises particles with a median sphericity of at least 0.75.6. The method claim 2 , wherein the spheroidized powder has a particle size distribution of between 5 and 45 microns at a low end of the particle size distribution range and between 15 and 105 microns at a high end of the particle size distribution range.7. A method for manufacturing a spheroidized copper or ...

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31-03-2022 дата публикации

Additive Manufactured Powder Processing System

Номер: US20220097132A1
Принадлежит: Raytheon Technologies Corporation

A system for treatment of atomized powder including a fluidized bed operable to treat feedstock alloy powders. A method of treating atomized powder including communicating an inert gas into a fluidized bed; communicating an atomized powder into the fluidized bed; and heating the atomized powder in the fluidized bed, eject the treated powders out of the fluidized bed to quench the powders. 1. A system for treatment of atomized powder , comprising:a fluidized bed operable to heat treat feedstock alloy powders, the feedstock alloy powders heat treated for microstructure control to condition the feedstock alloy powders into a state to facilitate solid-state consolidation, the fluidized bed receiving an inert gas;a quenching reservoir in communication with the fluidized bed;a three-way valve in communication with the quenching reservoir;a fine powder collector in communication with the three-way valve; anda water bubbler in communication with the three-way valve, the inert gas exiting from the fluidized bed to the water bubbler.2. The system as recited in claim 1 , wherein the feedstock alloy powders are degassed.3. The system as recited in claim 1 , further comprising an inert gas in communication with the fluidized bed.4. (canceled)5. (canceled)6. The system as recited in claim 1 , further comprising a quenching powder collector in communication with the three-way valve.7. The system as recited in claim 1 , further comprising a vibrator in communication with the fluidized bed and the line to a quenched powder collector to facilitate to eject the atomized powder.815-. (canceled) This application is a divisional of U.S. patent application Ser. No. 15/144,992, filed May 3, 2016.This invention was made with Government support awarded by the United States. The Government has certain rights in this invention.The present disclosure relates to additive manufacturing and, more particularly, to processing additive manufacturing feedstock powder.Precision engineered parts such as ...

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31-03-2022 дата публикации

HIGH ENTROPY ALLOY POWDER FOR LASER CLADDING AND APPLICATION METHOD THEREOF

Номер: US20220097133A1

The present disclosure discloses a high-entropy alloy powder for laser cladding and a use method thereof. The alloy powder is CoCrFeMnNiC, and x has a value of 0.1-0.15. The specific method includes: subjecting a 45 steel substrate to surface pretreatment, mixing the weighed CoCrFeMnNi high-entropy alloy powder with different content of a nano-C powder uniformly and pre-placed on the pre-treated substrate surface to form a prefabricated layer, then placing the prefabricated layer at 80-90° C. for constant temperature treatment for 8-12 h, and under a protective atmosphere, subjecting the cladding powder to laser cladding on the surface of the 45 steel. The method of the present disclosure prepares a CoCrFeMnNiChigh-entropy alloy coating with performance superior to the CoCrFeMnNi high-entropy alloy coating. 1. A high-entropy alloy powder for laser cladding , wherein the alloy powder is CoCrFeMnNiC , and x has a value of 0.1 to 0.15.2. A method for preparing a laser cladding coating with the high-entropy alloy powder according to claim 1 , specifically comprising the following steps:(1) subjecting a 45 steel substrate to surface pretreatment: sanding, cleaning, and drying for use;(2) weighing a CoCrFeMnNi high-entropy alloy powder with an equal atomic ratio and a nano-C powder in proportion, and mixing mechanically after weighing;(3) blending the mixed powders with absolute ethanol to prepare a paste, using a mold to bond the paste to a predetermined position on the steel substrate to obtain a prefabricated coating followed by drying, and subjecting a cladding powder to laser cladding on the surface of the 45 steel in a protective atmosphere.3. The method according to claim 1 , wherein in step (2) claim 1 , the CoCrFeMnNi high-entropy alloy powder has an average particle size of less than 25 μm claim 1 , and a powder purity of no less than 99.9%; the nano-C powder has an average particle size of 30 nm to 50 nm claim 1 , and a purity of no less than 99.99%.4. The ...

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12-03-2020 дата публикации

Spherical Tantalum Powder, Products Containing The Same, And Methods Of Making The Same

Номер: US20200078861A1
Принадлежит: Global Advanced Metals USA, Inc.

Tantalum powder that is highly spherical is described. The tantalum powder can be useful in additive manufacturing and other uses. Methods to make the tantalum powder are further described as well as methods to utilize the tantalum powder in additive manufacturing processes. Resulting products and articles using the tantalum powder are further described. 1. Tantalum powder comprisinga. a spherical shape wherein the powder has an average aspect ratio of from 1.0 to 1.25;b. a purity of tantalum of at least 99.99 wt % Ta based on total weight of said tantalum powder, excluding gas impurities;c. an average particle size of from about 0.5 micron to about 250 microns;d. an apparent density from about 4 g/cc to about 12.3 g/cc;e. a true density of from 16 g/cc to 16.6 g/cc; andf. a Hall flow rate of 20 sec or less.2. The tantalum powder of claim 1 , wherein said tantalum powder is plasma heat-treated.3. The tantalum powder of claim 1 , wherein said tantalum powder has an oxygen level of less than 400 ppm.4. The tantalum powder of claim 1 , wherein said tantalum powder has an oxygen level of from 20 ppm to 250 ppm.5. The tantalum powder of claim 1 , wherein said tantalum powder wherein said average aspect ratio is from 1.0 to 1.1.6. The tantalum powder of claim 1 , wherein said tantalum powder wherein said average aspect ratio is from 1.0 to 1.05.7. The tantalum powder of claim 1 , wherein said purity is at least 99.995 wt % Ta.8. The tantalum powder of claim 1 , wherein said average particle size is from about 0.5 micron to about 10 microns.9. The tantalum powder of claim 1 , wherein said average particle size is from about 5 microns to about 25 microns.10. The tantalum powder of claim 1 , wherein said average particle size is from about 15 microns to about 45 microns.11. The tantalum powder of claim 1 , wherein said average particle size is from about 35 microns to about 75 microns.12. The tantalum powder of claim 1 , wherein said average particle size is from about 55 ...

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24-03-2016 дата публикации

Conductive material and connected structure

Номер: US20160086687A1
Принадлежит: Sekisui Chemical Co Ltd

There is provided a conductive material which has a rapid reaction rate and is high in fluxing effect. The conductive material according to the present invention includes a conductive particle having solder at at least an external surface, an anionically hardenable compound, an anionic hardener, and an organic acid having a carboxyl group and having a functional group that is an esterified carboxyl group.

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