Fireproof wave-absorbing plate

04-03-2015 дата публикации
Номер:
CN104385428A
Автор: ZHU KUI
Принадлежит: 朱奎
Контакты:
Номер заявки: 54-10-20140023
Дата заявки: 18-09-2014

[1]

Technical Field

[2]

The invention relates to the field of building materials, in particular to a fire-proof suction wave plate.

[3]

Background Art

[4]

The building material as the ecological corn production process does not exist in the problems of pollution to the environment. If the raw material to cure, the development of the ecological function has different use of a building product, will greatly reduce the consumption of wood. The resistivity of the silicon carbide is between metal and the semiconductor, has a small density, has good high-temperature resistant property, wide absorption band, multi-band wave-absorbing material is an important component. The invention utilizes silicon carbide filling corn stalk, not only can demonstrate the wave-absorbing performance, but also can effectively improves the wear resistance.

[5]

Content of the invention

[6]

In response to the deficiencies in the prior art, the purpose of this invention is to provide a fire-proof suction wave plate.

[7]

Production of this invention comprises the steps of:

[8]

(1) purification of corn

[9]

(2) grinding and sieving corn stalk powder

[10]

The particle size of corn stalk powder 30-40 mesh.

[11]

(3) carbonization corn stalk powder

[12]

corn stalk powder into the high-pressure processing of the pot, in subsequently from the tank is introduced into the high-pressure saturated steam, the pressure to rise to 0.25 MPa, preserving the temperature and the pressure for 4 hours, the final pressure-relief, pressure is taken out after the cutting.

[13]

(4) drying corn stalk powder

[14]

At the temperature has been already preheated to 100 the defibrater [...] in the dry.

[15]

(5) by adding flame retardant and cementing agent urea-formaldehyde resin, and hot grinding corn stalk powder

[16]

Flame retardant synthetic process adopts the following: dicy, phosphoric acid, triethanolamine and water, according to the 5 [...] the 3 [...] the 2 [...] 10 heating quality of the mixed proportion of dissolved, in 85-95 the insulation under the conditions of [...] 3-4 hours, cooling to 60-70 the after [...] , the added mass ratio the 6 [...] the 4 [...] 3 of boric acid, borax, ammonia, boric acid quality dicy quality 6%, thermal insulation after dissolving the discharge reserve. Flame retardant and cementing agent is urea-formaldehyde resin mass ratio the 3 [...] 10, flame retardant is the quality of corn stalk powder 8%.

[17]

The fire retardant and cementing agent urea-formaldehyde resin is added in the milling chamber defibrater, corn stalk powder together with mechanical action, by grinding, in the fiber are mixed and penetrate corn. Saturated steam pressure 0.8-0.9 MPa, milling chamber pressure is 0.7-0.8 MPa, cooking time is 3-5min, the static disk of the abrasive grinding side clearance is 0.2 mm, the degree of balance 0.04 mm.

[18]

(6) adding silicon carbide and titanate coupling agent

[19]

corn stalk powder quality of the silicon carbide to 12%, the quality of the titanate coupling agent corn stalk powder 1.2%. Silicon carbide particle size is 60-80 mesh.

[20]

The silicon carbide and titanate coupling agent in the high-speed stirrer mixing stirring 5 min, then adding in the ball mill, and mixed uniformly corn stalk powder , and by utilizing ultrasonic oscillation the meter causes silicon carbide are uniformly dispersed in the matrix of corn.

[21]

Because the silicon carbide is extremely vulnerable to electrostatic, in particular under the action of the friction shear, so it is easy to be exclusive. caking, is not easy to be dispersed. In a high speed stirrer, a titanate coupling agent coated silicon carbide can prevent static electricity, so that the silicon carbide is dispersed evenly. Furthermore, organic titanate to silicon carbide surface activation processing, to improve the compatibility of the silicon carbide and corn stalk powder.

[22]

Reasonable silicon carbide particle size can be fill the gap between the fiber from corn stalk, help to improve the binding performance of the board, the strength of the reinforcement and density, and fine silicon carbide particle size will lead to reduced strength, silicon carbide particle size is determined according to the test.

[23]

(7) suction wave spreading fire

[24]

(8) pressure fire-proof suction wave plate

[25]

Pressure is 3 MPa, temperature is 170 the [...] , the pressing time is 12 min.

[26]

(9) forming

[27]

According to product requirements for cutting fire suction wave plate.

[28]

The invention has a good fire resistance, wave-absorbing ability, the characteristics of high wear resistance.

[29]

Mode of execution

[30]

Making this embodiment comprises the steps of:

[31]

(1) purification of corn

[32]

(2) grinding and sieving corn stalk powder

[33]

The particle size of corn stalk powder 30-40 mesh.

[34]

(3) carbonization corn stalk powder

[35]

corn stalk powder into the high-pressure processing of the pot, in subsequently from the tank is introduced into the high-pressure saturated steam, the pressure to rise to 0.25 MPa, preserving the temperature and the pressure for 4 hours, the final pressure-relief, pressure is taken out after the cutting.

[36]

(4) drying corn stalk powder

[37]

At the temperature has been already preheated to 100 the defibrater [...] in the dry.

[38]

(5) by adding flame retardant and cementing agent urea-formaldehyde resin, and hot grinding corn stalk powder

[39]

Flame retardant synthetic process adopts the following: dicy, phosphoric acid, triethanolamine and water, according to the 5 [...] the 3 [...] the 2 [...] 10 heating quality of the mixed proportion of dissolved, in 85-95 the insulation under the conditions of [...] 3-4h, cooling to 60-70 the after [...] , the added mass ratio the 6 [...] the 4 [...] 3 of boric acid, borax, ammonia, boric acid quality dicy quality 6%, thermal insulation after dissolving the discharge reserve. Flame retardant and cementing agent is urea-formaldehyde resin mass ratio the 3 [...] 10, flame retardant is the quality of corn stalk powder 8%.

[40]

The fire retardant and cementing agent urea-formaldehyde resin is added in the milling chamber defibrater, corn stalk powder together with mechanical action, by grinding, in the fiber are mixed and penetrate corn. Saturated steam pressure 0.8-0.9 MPa, milling chamber pressure is 0.7-0.8 MPa, cooking time is 3-5min, the static disk of the abrasive grinding side clearance is 0.2 mm, the degree of balance 0.04 mm.

[41]

(6) adding silicon carbide and titanate coupling agent

[42]

corn stalk powder quality of the silicon carbide to 12%, the quality of the titanate coupling agent corn stalk powder 1.2%. Silicon carbide particle size is 60-80 mesh.

[43]

The silicon carbide and titanate coupling agent in the high-speed stirrer mixing stirring 5 min, then adding in the ball mill, and mixed uniformly corn stalk powder , and by utilizing ultrasonic oscillation the meter causes silicon carbide are uniformly dispersed in the matrix of corn.

[44]

(7) suction wave spreading fire

[45]

(8) pressure fire-proof suction wave plate

[46]

Pressure is 3 MPa, temperature is 170 the [...] , the pressing time is 12 min.

[47]

(9) forming

[48]

According to product requirements for cutting fire suction wave plate.



[1]

The invention discloses a fireproof wave-absorbing plate which is characterized by being manufactured according to the following steps: (1) purifying corn stalks; (2) crushing and screening corn stalk powder; (3) carbonizing the corn stalk powder; (4) drying the corn stalk powder; (5) feeding fire retardant and cementing agent urea resin into the corn stalk powder, and carrying out hot grinding on the corn stalk powder; (6) feeding silicon carbide and titanate coupling agent; blending and mixing the silicon carbide and the titanate coupling agent for 5 minutes in a high-speed mixer, then feeding the mixture into a ball mill, evenly mixing the product with the corn stalk powder, and using an ultrasonic oscillator to enable the silicon carbide to be evenly dispersed in a corn stalk matrix; (7) laying the fireproof wave-absorbing plate; (8) pressing the fireproof wave-absorbing plate; (9) molding. The fireproof wave-absorbing plate has the characteristics of being good in fire resistance, high in wave absorption capacity and high in wear resistance.



1. A fireproof suction wave plate, is characterized in that the preparation step comprises:

(1) purification of corn

(2) grinding and sieving corn stalk powder

The particle size of corn stalk powder 30-40 mesh;

(3) carbonization corn stalk powder

corn stalk powder into the high-pressure processing of the pot, in subsequently from the tank is introduced into the high-pressure saturated steam, the pressure to rise to 0.25 MPa, preserving the temperature and the pressure for 4 hours, the final pressure-relief, of pressure taken out after cutting;

(4) drying corn stalk powder

At the temperature has been already preheated to 100 the drying defibrater [...] ;

(5) by adding flame retardant and cementing agent urea-formaldehyde resin, and hot grinding corn stalk powder

The fire retardant and cementing agent urea-formaldehyde resin is added in the milling chamber defibrater, corn stalk powder together with mechanical action, by grinding, in the fiber are mixed and penetrate corn; saturated steam pressure 0.8-0.9 MPa, milling chamber pressure is 0.7-0.8 MPa, cooking time is 3-5min, the static disk of the abrasive grinding side clearance is 0.2 mm, the degree of balance 0.04 mm;

(6) adding silicon carbide and titanate coupling agent

The silicon carbide and titanate coupling agent in the high-speed stirrer mixing stirring 5 min, then adding in the ball mill, and mixed uniformly corn stalk powder , and by utilizing ultrasonic oscillation the meter causes silicon carbide are uniformly dispersed in the matrix of corn;

(7) suction wave spreading fire

(8) pressure fire-proof suction wave plate

Pressure is 3 MPa, temperature is 170 the [...] , the pressing time is 12 min;

(9) forming

According to product requirements for cutting fire suction wave plate.

2. Fireproof suction wave plate according to Claim 1, characterized in that flame retardant synthetic process adopts the following: dicy, phosphoric acid, triethanolamine and water, according to the 5 [...] the 3 [...] the 2 [...] 10 heating quality of the mixed proportion of dissolved, in 85-95 the insulation under the conditions of [...] 3-4 hours, cooling to 60-70 the after [...] , the added mass ratio the 6 [...] the 4 [...] 3 of boric acid, borax, ammonia, boric acid quality dicy quality 6%, thermal insulation after dissolving the discharge reserve.

3. Fireproof suction wave plate according to Claim 1, which is characterized in that a fire retardant and a binder is urea-formaldehyde resin mass ratio the 3 [...] 10.

4. Fireproof suction wave plate according to Claim 1, is characterized in that the flame retardant is the quality of corn stalk powder 8%.

5. Fireproof suction wave plate according to Claim 1, which is characterized in that the quality of the silicon carbide as corn stalk powder 12%.

6. Fireproof suction wave plate according to Claim 1, which is characterized in that the quality of the titanate coupling agent as corn stalk powder 1.2%.

7. Fireproof suction wave plate according to Claim 1, is characterized in that the silicon carbide particle size is 60-80 mesh.