18-04-2023 дата публикации
Номер: CN115974658A
Принадлежит:
The invention relates to a method for synthesizing diether fluorene from ethylene carbonate, and belongs to the technical field of high polymer material processing. The method for synthesizing bis-ether fluorene from ethylene carbonate comprises the following steps: a, synthesizing a crude product bis-ether fluorene: under the protection of an inert atmosphere, mixing bisphenol fluorene and ethylene carbonate, stirring for 10-15 minutes until the solution is in a homogeneous phase, adding a basic catalyst, heating to 120-180 DEG C, and reacting for 7-10 hours to obtain a crude product solution containing bis-ether fluorene; and b, purifying the crude product solution to obtain diether fluorene. According to the method for synthesizing diether fluorene from ethylene carbonate, provided by the invention, the raw materials are convenient to transport, the synthesis process and the post-treatment process are simple, the product conversion rate is relatively high, the solvent recycling rate ...
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