09-06-2023 дата публикации
Номер: CN116239459A
Принадлежит:
The invention discloses a laboratory preparation method of 2, 4-dichlorphenoxyacetic acid, and relates to the technical field of preparation methods of pesticide products, and the laboratory preparation method comprises the following steps: step 1, adding 2, 4-dichlorophenol into a certain amount of polar solvent, stirring and dissolving, adding solid alkali, dropwise adding methyl chloroacetate at a certain temperature, reacting for a certain time, and filtering to obtain 2, 4-dichlorophenoxyacetic acid; after the reaction is finished, distilling off the solvent under reduced pressure to obtain methyl 2, 4-dichlorophenoxyacetate; and 2, slowly dropwise adding water into a reaction flask filled with methyl 2, 4-dichlorophenoxyacetate, carrying out reflux hydrolysis, cooling to 70 DEG C, maintaining the temperature, slowly dropwise adding concentrated hydrochloric acid into the reaction, stirring for 1.5 hours after dropwise adding, cooling to room temperature, filtering, washing with water ...
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