01-08-2023 дата публикации
Номер: CN116515128A
Автор:
ZHANG SEN,
QU JIANHONG,
WANG XIAODONG,
LI QIANSHAN,
WANG LEILEI,
HAN JUNCHANG,
ZHANG XIAOFEI,
WANG CHUNPENG,
CHANG LEI,
QIANG HAILIANG,
WANG SHUMAO,
GUO YE,
CAO CHAO,
JU QINGWEI,
YANG HAO
Принадлежит:
The invention provides an environment-friendly shale inhibitor and a preparation method thereof. The preparation method specifically comprises the following steps: S1, preparing cotton straw powder, adding an alkaline solution, heating in a water bath, filtering, adjusting the pH value of slurry to 4-5, adding ethanol for reaction, filtering again, and collecting filtrate; s2, under a protective atmosphere and a vacuum condition, mixing [EM < iM >] CH3COO ionic liquid with the filtrate, stirring, heating, and carrying out suction filtration to obtain filter residues which are crude lignin; s3, extracting by taking tetrahydrofuran as a solvent to obtain refined lignin; and S4, dissolving the refined lignin in water, adding a p-benzenesulfonic acid solution, heating in a water bath, dropwise adding a 2, 3-epoxypropyltrimethylammonium chloride solution, carrying out a heat preservation reaction, after the reaction is finished, carrying out centrifugal separation, taking supernate, and carrying ...
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