16-08-2018 дата публикации
Номер: US20180230012A1
Принадлежит:
A method of producing a spherical boron nitride fine particle includes reacting ammonia with an alkoxide borate at an ammonia/alkoxide borate molar ratio of 1 to 10 in an inert gas stream at 750° C. or higher within 30 seconds, then applying heat treatment to a reaction product in an atmosphere of ammonia gas or a mixed gas of ammonia gas and an inert gas at 1,000 to 1,600° C. for at least 1 hour, and further firing the reaction product in an inert gas atmosphere at 1,800 to 2,200° C. for at least 0.5 hour. 1. A method of producing a spherical boron nitride fine particle, characterized by reacting ammonia with an alkoxide borate at an ammonia/alkoxide borate molar ratio of 1 to 10 in an inert gas stream at 750° C. or higher within 30 seconds, then applying heat treatment to a reaction product in an atmosphere of ammonia gas or a mixed gas of ammonia gas and an inert gas at 1,000 to 1,600° C. for at least 1 hour, and further firing the reaction product in an inert gas atmosphere at 1,800 to 2,200° C. for at least 0.5 hour. This is a divisional application Ser. No. 15/117,853 filed Aug. 10, 2016, which is a National Phase of International Application No. PCT/JP2015/053489 filed Feb. 9, 2015, and claims priority from Japanese Patent Application No. 2014-024009 filed Feb. 12, 2014, the disclosure of which is hereby incorporated by reference herein in its entirety.The present invention relates to a spherical boron nitride fine particle well suited for use as a highly thermoconductive filler or the like, and a production method thereof.Hexagonal boron nitride (hereinafter called “boron nitride”), because of having lubrication capability, high thermal conductivity and insulation capability, is now widely used as releasing agents for solid lubricants, molten glasses and aluminum or the like as well as fillers for thermal radiation materials.To be compatible with higher performances of recent computers and electronic hardware in particular, measures against thermal radiation ...
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