18-07-2012 дата публикации
Номер: CN102585135A
Принадлежит:
The invention discloses a reactive intumescent flame retardant for polyurethane and a synthesis method of the reactive intumescent flame retardant, relates to a flame retardant technology, in particular to a novel intumescent flame retardant which contains an acid source, a carbon source and a gas source simultaneously and contains a hydroxyl group serving as an active group. The chemical name of the reactive intumescent flame retardant for polyurethane is 3,9-di{N,N-di(2-ethoxyl)-amino}-2,4,8,10-4-oxo-3,9-diphosphate spiro-3,9-dioxo-[5,5]-undecane. The structure of the reactive intumescent flame retardant is shown as a formula (I). The synthesis method comprises the following steps of: adding 3,9-di{N,N-di(2-ethoxyl)-amino}-2,4,8,10-4-oxo-3,9-diphosphate spiro-3,9-dioxo-[5,5]-undecane into water; dropwise adding diethanolameine and triethylamine at the temperature of 0-5 DEG C; reacting at the temperature of 50-60 DEG C for 4-6 hours; concentrating under reduced pressure; purifying; and ...
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