15-09-2016 дата публикации
Номер: US20160264470A1
Принадлежит:
A low temperature co-fired ceramic powder has a chemical composition of xRO-yR′O-zMO-wM′O, wherein R is Li, Na and/or K, R′ is Mg, Ca, Sr, Ba, Zn and/or Cu, M is B, Al, Ga, In, Bi, Nd, Sm, and/or La, M′ is Si, Ge, Sn, Ti, and/or Zr, x≧0, y≧0, z≧20%, w≧15%, and x+y+z+w=1. The preparation method comprises: weighing constituent powders according to the composition of the ceramic powder, and uniformly mixing these powders as a raw material powder; and presintering the raw material powder in a muffle furnace followed by grinding, the presintering comprising gradiently heating the raw material powder to a maximum temperature of 950° C. by first rising to 350-450° C. and staying thereat for a period, then staying at intervals of 50-100° C. for a period. 1. A preparation method for a low temperature co-fired ceramic powder which has a chemical composition of xRO-yR′O-zMO-wM′O , wherein R is selected from at least one of Li , Na , and K , R′ is selected from at least one of Mg , Ca , Sr , Ba , Zn , and Cu , M is selected from at least one of B , Al , Ga , In , Bi , Nd , Sm , and La , M′ is selected from at least one of Si , Ge , Sn , Ti , and Zr , x , y , z , and w represent weight percentages , x≧0 , y≧0 , z≧20% , w≧15% , and x+y+z+w=1 , the preparation method comprising the steps of:{'sub': 2', '2', '3', '2, '1) weighing RO powder, r′O powder, MOpowder, and M′Opowder according to the composition of the low temperature co-fired ceramic powder, and uniformly mixing these powders as a raw material powder; and'}2) presintering the raw material powder in a muffle furnace followed by grinding to give the low temperature co-fired ceramic powder, the presintering comprising gradiently heating the raw material powder to a maximum temperature of not higher than 950° C., during which a furnace temperature first rises to 350-450° C. and stays thereat for a period, then, as the temperature rises, stays at each interval of 50-100° C. thereabove for a period.2. The preparation method ...
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