02-06-2023 дата публикации
Номер: CN116202906A
Принадлежит:
The invention discloses a pretreatment method of a molten salt chlorination bed layer sample, which comprises the following steps: S1, adding a proper amount of sample into a three-neck flask, then pouring hydrochloric acid with a certain concentration into the three-neck flask, stirring, heating the three-neck flask, and connecting a condensation reflux device; s2, rapidly pouring the dissolved sample into a filtering device, and separating insoluble solids from soluble liquids; s3, transferring the insoluble solid separated in the step S2 into the three-necked flask used in the step S1, then adding deionized water into the three-necked flask, stirring, heating the three-necked flask, and connecting a condensation reflux device; s4, quickly pouring the sample dissolved in the step S3 into a filtering device, separating insoluble solids from soluble liquid, and washing the insoluble solids by using deionized water; the content of oxides of titanium and impurities in the titanium raw material ...
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