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Небесная энциклопедия

Космические корабли и станции, автоматические КА и методы их проектирования, бортовые комплексы управления, системы и средства жизнеобеспечения, особенности технологии производства ракетно-космических систем

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Мониторинг СМИ

Мониторинг СМИ и социальных сетей. Сканирование интернета, новостных сайтов, специализированных контентных площадок на базе мессенджеров. Гибкие настройки фильтров и первоначальных источников.

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Поддерживает ввод нескольких поисковых фраз (по одной на строку). При поиске обеспечивает поддержку морфологии русского и английского языка
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Применить Всего найдено 68. Отображено 66.
22-08-2017 дата публикации

Method and system for starting up a distillation tower

Номер: US0009739528B2

The present disclosure provides method for clean methane startup of a distillation tower. The method includes maintaining a rectifier section and a lower section in the distillation tower, feeding stream to the lower section, directly feeding methane to at least one of the rectifier section and a rectifier section outlet line of the rectifier section when a contaminant concentration of the contaminant exiting as a vapor in an upper portion of the lower section is outside of a predetermined concentration and introducing the vapor from the lower section to the rectifier section when the contaminant concentration exiting the upper portion of the lower section is within the predetermined concentration.

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16-01-2018 дата публикации

Method and device for separating hydrocarbons and contaminants with a spray assembly

Номер: US0009869511B2

A method for separating a feed stream in a distillation tower comprising maintaining a controlled freeze zone (CFZ) section in the distillation tower, receiving a freezing zone liquid stream in a spray nozzle assembly in the CFZ section, wherein the spray nozzle assembly comprises a plurality of outer spray nozzles on an outer periphery of the spray nozzle assembly and at least one inner spray nozzle interior to the outer spray nozzles, wherein each outer spray nozzle is configured to spray the freezing zone liquid stream along a central spray axis, and wherein the central spray axis of at least one of the outer spray nozzles is not parallel to a CFZ wall, and spraying the freezing zone liquid stream through the spray nozzle assembly into the CFZ section to keep a temperature and pressure at which the solid and the hydrocarbon-enriched vapor stream form.

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30-03-2017 дата публикации

Aromatization of Non-Aromatic Hydrocarbon

Номер: US20170088484A1
Принадлежит:

The invention relates to producing aromatic hydrocarbon by aromatization of non-aromatic hydrocarbon, including feed pretreatment, aromatization of the aromatization feed's Chydrocarbon and C non-aromatic hydrocarbon, and recovery of an aromatic product. The invention also relates to modules for carrying out the pretreatment, aromatization, and recovery, and also modules for auxiliary function such as power generation. 1. A system for producing aromatic hydrocarbon , comprising:{'sup': '3', 'sub': 2', '3+', '2+', '3+', '2, "(a) a an aromatizer configured for (i) receiving a preselected amount ≧1 million standard cubic feet per day [MSCFD] (29,000 NMD) of an aromatization feed, the aromatization feed comprising Chydrocarbon and C non-aromatic hydrocarbon and having a preselected C non-aromatic hydrocarbon concentration in the range of from 15 mole % to 90 mole % per mole of aromatization feed, and (ii) aromatization of (A) at least a portion of the aromatization feed's C non-aromatic hydrocarbon and (B) at least a portion of the aromatization feed's Chydrocarbon to produce a reaction effluent comprising molecular hydrogen, non-aromatic hydrocarbon, and aromatic hydrocarbon; and"}(b) a product recoverer in fluidic communication with the aromatizer, the product recoverer being configured for recovering at least first and second products from the reaction effluent, wherein the first product comprises at least a portion of the reaction effluent's aromatic hydrocarbon and the second product comprises a tail gas containing (i) at least a portion of the reaction effluent's molecular hydrogen and (ii) at least a portion of the reaction effluent's non-aromatic hydrocarbon.2. The system of claim 1 , wherein the system further comprises a feed pretreater configured for (A) receiving ≧2 MSCFD (57 claim 1 ,000 NMD) of a gaseous feed and (B) producing the aromatization feed from the gaseous feed claim 1 , the gaseous feed comprising 0 mole % to 98 mole % methane claim 1 , 1 mole % ...

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07-02-2017 дата публикации

Method of removing solids by modifying a liquid level in a distillation tower

Номер: US0009562719B2

The present disclosure provides a method of separating a feed stream in a distillation tower. The method includes maintaining a controlled freeze zone section in a distillation tower; maintaining a melt tray assembly within the controlled freeze zone section that operates at a temperature and pressure at which solid melts; forming solids in a controlled freeze zone section; raising a liquid level of a liquid in the melt tray assembly when the solids accumulate on a mechanical component in the controlled freeze zone section; raising a liquid temperature of the liquid while raising the liquid level; and lowering the liquid level after at least one of (a) a predetermined time period has passed and (b) an alternative temperature of the mechanical component is within an expected temperature range of a baseline temperature of the mechanical component.

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31-10-2017 дата публикации

Method and system of dehydrating a feed stream processed in a distillation tower

Номер: US0009803918B2

The present disclosure provides a method of dehydrating a feed stream processed in a distillation tower. The method may include (a) introducing a feed stream comprising a first contaminant stream into a distillation tower; (b) forming a solid from the feed stream in a controlled freeze zone section of the distillation tower; (c) feeding a second contaminant stream into the feed stream outside the distillation tower; and (d) removing water from the feed stream with a second contaminant stream by feeding the second contaminant stream.

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05-09-2017 дата публикации

Method and system of maintaining a liquid level in a distillation tower

Номер: US0009752827B2

The present disclosure provides a distillation tower that may include a stripper section constructed and arranged to separate a feed stream at a temperature and pressure at which the feed stream forms no solid; a controlled freeze zone section constructed and arranged to separate the feed stream at a temperature and pressure at which the feed stream forms a solid; a melt tray assembly in the controlled freeze zone section that includes a liquid; an underflow weir in the controlled freeze zone section that alters a flow of the liquid in the melt tray assembly; an overflow weir in the controlled freeze zone section that works with the underflow weir to alter the flow of the liquid in the melt tray assembly and is adjacent to the underflow weir; and a covering element in the controlled freeze zone section that is connected to and extends from the underflow weir.

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24-10-2017 дата публикации

Hydrocarbon dehydrocyclization in the presence of carbon dioxide

Номер: US0009796643B2

The invention relates to converting non-aromatic hydrocarbon in the presence of CO 2 to produce aromatic hydrocarbon. CO 2 methanation using molecular hydrogen produced during the aromatization increases aromatic hydrocarbon yield. The invention also relates to equipment and materials useful in such upgrading, to processes for carrying out such upgrading, and to the use of such processes for, e.g., natural gas upgrading.

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30-03-2017 дата публикации

Hydrocarbon Dehydrocyclization in the Presence of Carbon Dioxide

Номер: US20170088486A1
Принадлежит: ExxonMobil Chemical Patents Inc

The invention relates to converting non-aromatic hydrocarbon in the presence of CO 2 to produce aromatic hydrocarbon. CO 2 methanation using molecular hydrogen produced during the aromatization increases aromatic hydrocarbon yield. The invention also relates to equipment and materials useful in such upgrading, to processes for carrying out such upgrading, and to the use of such processes for, e.g., natural gas upgrading.

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28-11-2017 дата публикации

Method and device for separating a feed stream using radiation detectors

Номер: US0009829247B2

The present disclosure provides a method for separating a feed stream in a distillation tower. The method may include forming solids in a controlled freeze zone section of the distillation tower; emitting radiation from a first radiation source in the controlled freeze zone section while the controlled freeze zone section forms no solids; detecting radiation emitted by the first radiation source as a first radiation level; detecting radiation emitted by the first radiation source as a second radiation level after detecting the first radiation level; and determining whether the solids adhered to at least one of on and around a first mechanical component included in the controlled freeze zone section based on the first radiation level and the second radiation level.

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23-01-2018 дата публикации

Method and device for separating hydrocarbons and contaminants with a heating mechanism to destabilize and/or prevent adhesion of solids

Номер: US0009874396B2

The present disclosure provides a method for separating a feed stream in a distillation tower which includes separating a feed stream in a stripper section into an enriched contaminant bottom liquid stream and a freezing zone vapor stream; contacting the freezing zone vapor stream in the controlled freeze zone section with a freezing zone liquid stream at a temperature and pressure at which a solid and a hydrocarbon-enriched vapor stream form; directly applying heat to a controlled freeze zone wall of the controlled freeze zone section with a heating mechanism coupled to at least one of a controlled freeze zone internal surface of the controlled freeze zone wall and a controlled freeze zone external surface of the controlled freeze zone wall; and at least one of destabilizing and preventing adhesion of the solid to the controlled freeze zone wall with the heating mechanism.

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22-08-2017 дата публикации

Method and system for separating fluids in a distillation tower

Номер: US0009739529B2

A method and system for separating fluids in a distillation tower. The method may include feeding a stream to the distillation tower, wherein the stream includes carbon dioxide, reducing a carbon dioxide concentration of the stream received by the rectifier section by feeding a first cryogenic fluid to the controlled freeze zone section and accumulating rectifier section stream in at least one of a holding vessel and a sump of the rectifier section, and terminating reducing the carbon dioxide concentration when the carbon dioxide concentration of the stream travelling from the controlled freeze zone section to the rectifier section is less than or equal to a maximum carbon dioxide concentration. The first cryogenic fluid may comprise a substantially carbon-dioxide-free fluid.

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23-01-2018 дата публикации

Method and system for preventing accumulation of solids in a distillation tower

Номер: US0009874395B2

The present disclosure provides a method for preventing accumulation of solids in a distillation tower. The method includes introducing a feed stream into a controlled freeze zone section of a distillation tower; forming solids in the controlled freeze zone section from the feed stream; discontinuously injecting a first freeze-inhibitor solution into the controlled freeze zone section toward a location in the controlled freeze zone section that accumulates the solids; and destabilizing accumulation of the solids from the location with the first freeze-inhibitor solution.

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23-03-2017 дата публикации

Heating Component to Reduce Solidification in a Cryogenic Distillation System

Номер: US20170082357A1
Принадлежит:

A method and a system for feeding a feed gas including methane (CH) and carbon dioxide (CO) to a cryogenic distillation column are provided herein. The method includes flowing a freeze zone COvapor stream into a freezing section of the column to produce an overhead stream that exits the column. The method includes heating the overhead stream via a heating component to reduce or prevent solidification of the COin the overhead stream. 1. A method comprising:{'sub': 4', '2, 'feeding a feed gas comprising methane (CH) and carbon dioxide (CO) to a cryogenic distillation column during start-up of the cryogenic distillation column;'}producing an acid gas rich bottom stream and a freeze zone vapor stream;flowing the freeze zone vapor stream into a freezing section of the cryogenic distillation column, wherein the freeze zone vapor stream exits the cryogenic distillation column as an overhead stream;{'sub': '2', 'heating the overhead stream via a heating component to form a heated overhead stream to reduce or prevent solidification of the COin the overhead stream;'}flowing the heated overhead stream into a heat exchanger to substantially reduce or prevent solidification in the heat exchanger;compressing the heated overhead stream via an overhead compressor to produce a high-pressure vapor; andreducing pressure of the high-pressure vapor to produce a liquid-vapor stream at an inlet of the cryogenic distillation column, wherein the liquid-vapor stream is introduced into the cryogenic distillation column as a refluxing spray.2. The method of claim 1 , wherein the heating of the overhead stream comprises raising a temperature of the overhead stream by about 0.5° F. to about 10° F.3. The method of claim 1 , comprising measuring a temperature of the heated overhead stream at an inlet of the heat exchanger.4. The method of claim 1 , comprising regulating an amount of heat emitted by the heating component via a control system claim 1 , wherein the control system maintains a ...

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21-11-2017 дата публикации

Method and system of modifying a liquid level during start-up operations

Номер: US0009823016B2

The present disclosure provides a method for separating a feed stream in a distillation tower. The method includes operating a controlled freeze zone section in a distillation tower that separates a feed stream at a temperature and pressure at which the feed stream forms a solid in the controlled freeze zone section, wherein the feed stream includes a first contaminant; maintaining a melt tray assembly in the controlled freeze zone section; introducing the feed stream to the controlled freeze zone section; and accumulating a liquid in the melt tray assembly until the liquid is at a predetermined liquid level in the controlled freeze zone section, by: feeding a second contaminant to the controlled freeze zone section; and adding the second contaminant to the melt tray assembly, wherein the liquid comprises the second contaminant.

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02-01-2020 дата публикации

Hybrid Tray for Introducing a Low CO2 Feed Stream into a Distillation Tower

Номер: US20200002634A1
Принадлежит:

A method of separating a feed stream in a distillation tower. Vapor is permitted to rise upwardly from a distillation section of the distillation tower. A feed stream is introduced into a controlled freeze zone section of the distillation tower, the controlled freeze zone section being situated above the distillation section. The feed stream is released above a level of a liquid retained by a melt tray assembly in the controlled freeze zone section. Vapor from the distillation section is directed into the liquid retained by the melt tray assembly. A solid is formed from the feed stream in the controlled freeze zone section. 1. A distillation tower for separating a feed stream , the distillation tower comprising:a distillation section permitting vapor to rise upwardly therefrom; a spray assembly in the controlled freeze zone upper section, and', 'a melt tray assembly in the controlled freeze zone lower section;, 'a controlled freeze zone section situated above the distillation section, the controlled freeze zone constructed and arranged to form a solid from a feed stream, the controlled freeze zone section including'} a feed stream manifold that directs the feed stream into the distillation tower,', 'at least one vapor stream riser that directs the vapor from the distillation section into liquid retained by the melt tray assembly, and', 'at least one feed stream riser having a lower end operationally connected to the feed stream manifold and an upper end positioned above a level of the liquid retained by the melt tray assembly, wherein the feed stream is released above the level of the liquid retained by the melt tray assembly., 'wherein the melt tray assembly includes'}2. The distillation tower of claim 1 , wherein the at least one vapor stream riser passes through the feed stream manifold without mixing the feed stream with the vapor stream from the distillation section.3. The distillation tower of claim 1 , further comprising:a distribution cap disposed on an ...

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02-01-2020 дата публикации

Mixing and Heat Integration of Melt Tray Liquids in a Cryogenic Distillation Tower

Номер: US20200003490A1
Принадлежит:

A cryogenic distillation tower for separating a feed stream. The tower includes a distillation section. A controlled freeze zone section is situated above the distillation section and forms a solid from the feed stream. The controlled freeze zone section includes a spray assembly in an upper section and a melt tray assembly in a lower section. The melt tray assembly includes at least one vapor stream riser that directs the vapor from the distillation section into liquid retained by the melt tray assembly, and one or more draw-off openings positioned to permit a portion of the liquid to exit the controlled freeze zone section. The portion of the liquid indirectly exchanges heat with a heating fluid. One or more return inlets return the portion of the liquid to the melt tray assembly after it has been heated in the heat exchanger. 1. A cryogenic distillation tower for separating a feed stream , the distillation tower comprising:a distillation section permitting vapor to rise upwardly therefrom;one or more lines for directing the feed stream into the distillation tower; a spray assembly in an upper section of the controlled freeze zone, and', at least one vapor stream riser that directs the vapor from the distillation section into liquid retained by the melt tray assembly, and', 'one or more draw-off openings positioned to permit a portion of the liquid retained by the melt tray assembly to exit the controlled freeze zone section;, 'a melt tray assembly in a lower section of the controlled freeze zone, wherein the melt tray assembly includes'}], 'a controlled freeze zone section situated above the distillation section, the controlled freeze zone constructed and arranged to form a solid from the feed stream, the controlled freeze zone section including'}a heat exchanger arranged to heat the portion of the liquid through indirect heat exchange with a heating fluid; andone or more return inlets that return the portion of the liquid to the melt tray assembly after the ...

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14-01-2016 дата публикации

Method and System For Separating Fluids In A Distillation Tower

Номер: US20160010917A1
Принадлежит: Individual

A method and system for separating fluids in a distillation tower. The method may include feeding a stream to the distillation tower, wherein the stream includes carbon dioxide, reducing a carbon dioxide concentration of the stream received by the rectifier section by feeding a first cryogenic fluid to the controlled freeze zone section and accumulating rectifier section stream in at least one of a holding vessel and a sump of the rectifier section, and terminating reducing the carbon dioxide concentration when the carbon dioxide concentration of the stream travelling from the controlled freeze zone section to the rectifier section is less than or equal to a maximum carbon dioxide concentration. The first cryogenic fluid may comprise a substantially carbon-dioxide-free fluid.

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25-01-2018 дата публикации

Hydrocarbon Dehydrocyclization in the Presence of Carbon Dioxide

Номер: US20180022667A1
Принадлежит: ExxonMobil Chemical Patents Inc

The invention relates to converting non-aromatic hydrocarbon in the presence of CO 2 to produce aromatic hydrocarbon. CO 2 methanation using molecular hydrogen produced during the aromatization increases aromatic hydrocarbon yield. The invention also relates to equipment and materials useful in such upgrading, to processes for carrying out such upgrading, and to the use of such processes for, e.g., natural gas upgrading.

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30-03-2017 дата публикации

Treatment Plant for Hydrocarbon Gas Having Variable Contaminant Levels

Номер: US20170089638A1
Принадлежит:

A method of designing, constructing, and operating a hydrocarbon gas treatment plant is disclosed. A target hydrocarbon production range for a hydrocarbon gas meeting a required product specification is established. A cryogenic distillation column is designed and constructed with a vapor capacity to meet the target hydrocarbon production range. A variable feed refrigeration system is incorporated to cool an inlet feed of the hydrocarbon gas. The variable feed refrigeration system is designed to handle the target hydrocarbon production range and a wide range of contaminant concentrations in the inlet feed. A variable bottoms heating system is incorporated to handle heating duties associated with the wide range of contaminant concentrations in the inlet feed. A variable bottoms pumping system is incorporated to handle liquid flows associated with the wide range of contaminant concentrations in the inlet feed. 1. A method of treating , in a gas treatment plant , a feed gas stream comprising hydrocarbon gas and acid gas , the method comprising:(a) measuring the acid gas concentration in the feed gas stream at a first time to determine a first acid gas fraction;(b) cooling and liquefying at least a first portion of the feed gas stream in a first feed refrigeration unit;(c) separating the liquefied acid gas from the first portion of the feed gas stream to create a first vapor stream having a first composition;(d) separating, primarily by freezing, from the first vapor stream substantially all of the acid gas remaining in the first vapor stream to create a hydrocarbon gas stream;(e) melting the frozen acid gas;(f) removing the melted acid gas and the liquefied acid gas, which together form a bottoms stream;(g) removing the hydrocarbon gas stream; cooling and liquefying at least a first portion of the feed gas stream using the first feed refrigeration unit and cooling and liquefying at least a second portion of the acid gas stream using at least one additional feed ...

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11-04-2019 дата публикации

FIXED BED RADIAL FLOW REACTOR FOR LIGHT PARAFFIN CONVERSION

Номер: US20190105626A1
Принадлежит:

Systems and methods are provided for conversion of light paraffinic gases to form liquid products in a process performed in a fixed bed radial-flow reactor. The light paraffins can correspond to C paraffins. Examples of liquid products that can be formed include C-Caromatics, such as benzene, toluene, and xylene. The fixed bed radial-flow reactor can allow for improved control over the reaction conditions for paraffin conversion in spite of the fixed bed nature of the reactor. This can allow the process to operate with improved efficiency while reducing or minimizing the complexity of operation relative to non-fixed bed reactor systems. 112.-. (canceled)13. A method for processing a paraffin-containing feed , comprising:{'sub': 3+', '6', '12, 'exposing a feed comprising about 30 vol % to about 70 vol % of C paraffins to one or more fixed beds of a conversion catalyst to form a conversion effluent comprising C-Caromatics, the one or more fixed beds of the conversion catalyst comprising fixed beds in one or more radial flow reactors, a combined pressure drop across the one or more fixed beds being less than about 100 kPag, the one or more radial flow reactors comprising{'b': '1', 'an outer annular volume defined by an interior of a reactor wall and an exterior of a gas-permeable wall, the interior of the reactor wall defining an outer annular radius R;'}{'b': '3', 'a central volume defined by the interior of a central column and a column cap, the interior of the central column defining a column radius R; and'}{'b': '2', 'an inner annular volume defined by an interior of the gas-permeable wall, an exterior of the central column, an inner annular top, and an inner annular bottom, the interior of the gas-permeable wall defining an inner annular radius R, the inner annular volume comprising a catalyst bed, the inner annular volume being in direct fluid communication with the outer annular volume through the gas-permeable wall, the inner annular volume being in direct ...

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11-06-2015 дата публикации

METHOD AND SYSTEM FOR SEPARATING A FEED STREAM WITH A FEED STREAM DISTRIBUTION MECHANISM

Номер: US20150158796A1
Автор: Valencia Jaime A.
Принадлежит:

The present disclosure provides a distillation tower for separating a feed stream. The distillation tower includes a controlled freeze zone section having a controlled freeze zone upper section and a controlled freeze zone lower section below the controlled freeze zone upper section. The controlled freeze zone section includes: (a) a spray assembly in the controlled freeze zone upper section; (b) a melt tray assembly in the controlled freeze zone lower section; (c) a feed stream distribution mechanism between the spray assembly and the melt tray assembly. The feed stream distribution mechanism is constructed and arranged to uniformly distribute the feed stream in the controlled freeze zone section. 1. A distillation tower for separating a feed stream , the distillation tower comprising: (a) a spray assembly in the controlled freeze zone upper section;', '(b) a melt tray assembly in the controlled freeze zone lower section;', '(c) a feed stream distribution mechanism between the spray assembly and the melt tray assembly,, 'a controlled freeze zone section having a controlled freeze zone upper section and a controlled freeze zone lower section below the controlled freeze zone upper section, wherein the controlled freeze zone section is constructed and arranged to form a solid from a feed stream and the controlled freeze zone section compriseswherein the feed stream distribution mechanism is constructed and arranged to uniformly distribute at least a portion of the feed stream in the controlled freeze zone section.2. The distillation tower of claim 1 , wherein the feed stream distribution mechanism is separate and distinct from the spray assembly and the melt tray assembly.3. The distillation tower of claim 1 , wherein the feed stream distribution mechanism comprises a pipe header having orifices that are closer to the melt tray assembly than the spray assembly.4. The distillation tower of claim 3 , wherein the orifices are oriented towards a controlled freeze zone ...

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11-06-2015 дата публикации

METHOD AND SYSTEM OF MAINTAINING A LIQUID LEVEL IN A DISTILLATION TOWER

Номер: US20150159939A1
Автор: Valencia Jaime A.
Принадлежит:

The present disclosure provides a distillation tower that may include a stripper section constructed and arranged to separate a feed stream at a temperature and pressure at which the feed stream forms no solid; a controlled freeze zone section constructed and arranged to separate the feed stream at a temperature and pressure at which the feed stream forms a solid; a melt tray assembly in the controlled freeze zone section that includes a liquid; an underflow weir in the controlled freeze zone section that alters a flow of the liquid in the melt tray assembly; an overflow weir in the controlled freeze zone section that works with the underflow weir to alter the flow of the liquid in the melt tray assembly and is adjacent to the underflow weir; and a covering element in the controlled freeze zone section that is connected to and extends from the underflow weir. 1. A distillation tower comprising:a stripper section constructed and arranged to separate a feed stream at a temperature and pressure at which the feed stream forms no solid;a controlled freeze zone section constructed and arranged to separate the feed stream at a temperature and pressure at which the feed stream forms a solid;a melt tray assembly in the controlled freeze zone section that includes a liquid;an underflow weir in the controlled freeze zone section that alters a flow of the liquid in the melt tray assembly;an overflow weir in the controlled freeze zone section that works with the underflow weir to alter the flow of the liquid in the melt tray assembly and is adjacent to the underflow weir; anda covering element in the controlled freeze zone section that is connected to and extends from the underflow weir.2. The distillation tower of claim 1 , wherein the controlled freeze zone section includes a controlled freeze zone wall and wherein the overflow weir is directly adjacent to the controlled freeze zone wall.3. The distillation tower of claim 1 , wherein the controlled freeze zone section includes ...

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11-06-2015 дата публикации

Method and system of dehydrating a feed stream processed in a distillation tower

Номер: US20150159940A1
Принадлежит: Individual

The present disclosure provides a method of dehydrating a feed stream processed in a distillation tower. The method may include (a) introducing a feed stream comprising a first contaminant stream into a distillation tower; (b) forming a solid from the feed stream in a controlled freeze zone section of the distillation tower; (c) feeding a second contaminant stream into the feed stream outside the distillation tower; and (d) removing water from the feed stream with a second contaminant stream by feeding the second contaminant stream.

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11-06-2015 дата публикации

METHOD AND SYSTEM FOR PREVENTING ACCUMULATION OF SOLIDS IN A DISTILLATION TOWER

Номер: US20150159941A1
Принадлежит:

The present disclosure provides a method for preventing accumulation of solids in a distillation tower. The method includes introducing a feed stream into a controlled freeze zone section of a distillation tower; forming solids in the controlled freeze zone section from the feed stream; discontinuously injecting a first freeze-inhibitor solution into the controlled freeze zone section toward a location in the controlled freeze zone section that accumulates the solids; and destabilizing accumulation of the solids from the location with the first freeze-inhibitor solution. 1. A method for preventing accumulation of solids in a distillation tower , the method comprising:introducing a feed stream into a controlled freeze zone section of a distillation tower;forming solids in the controlled freeze zone section from the feed stream;discontinuously injecting a first freeze-inhibitor solution into the controlled freeze zone section toward a location in the controlled freeze zone section that accumulates the solids; anddestabilizing accumulation of the solids from the location with the first freeze-inhibitor solution.2. The method of claim 1 , wherein the first freeze-inhibitor solution comprises any carbon dioxide solubilizing solvent that remains unfrozen in the controlled freeze zone section.3. The method of claim 1 , wherein the first freeze-inhibitor solution comprises at least one of light hydrocarbons and light alcohols.4. The method of claim 1 , wherein the first freeze-inhibitor solution comprises at least one of ethane claim 1 , methanol claim 1 , propane and butane.5. The method of claim 1 , wherein discontinuously injecting the first freeze-inhibitor solution comprises releasing the first freeze-inhibitor solution from the location.6. The method of claim 1 , wherein the location comprises at least one of a spray assembly of the controlled freeze zone section and a first freeze-inhibitor injection piping arrangement adjacent to a controlled freeze zone wall of the ...

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11-06-2015 дата публикации

METHOD AND DEVICE FOR SEPARATING HYDROCARBONS AND CONTAMINANTS WITH A SURFACE TREATMENT MECHANISM

Номер: US20150159942A1
Принадлежит:

The disclosure includes a method for separating a feed stream in a distillation tower may comprise maintaining a controlled freeze zone section in the distillation tower that forms solids from a feed stream, wherein the controlled freeze zone section includes one or more internally disposed elements and a controlled freeze zone wall having an internal wall surface inside of the distillation tower, modifying at least one of the internally disposed elements, the internal wall surface, or both with a treatment mechanism that includes at least one of (a) removing portions of the internal wall surface and (b) applying a coating surface, introducing the feed stream into the controlled freeze zone section, forming the solids from the feed stream in the controlled freeze zone section, and at least one of preventing and destabilizing adhesion of the solids to the internal wall surface with the treatment mechanism. 1. A method for separating a feed stream in a distillation tower comprising:maintaining a controlled freeze zone section in the distillation tower that forms solids from a feed stream, wherein the controlled freeze zone section includes one or more internally disposed elements and a controlled freeze zone wall having an internal wall surface inside of the distillation tower;modifying at least one of the internally disposed elements, the internal wall surface, or both with a treatment mechanism that includes at least one of (a) removing portions of the internal wall surface and (b) applying a coating surface;introducing the feed stream into the controlled freeze zone section;forming the solids from the feed stream in the controlled freeze zone section; andat least one of preventing and destabilizing adhesion of the solids to the internal wall surface with the treatment mechanism.2. The method of claim 1 , wherein removing portions of the internal wall surface comprises one of mechanically and electrochemically removing material from the internal wall surface.3. The ...

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11-06-2015 дата публикации

METHOD AND DEVICE FOR SEPARATING HYDROCARBONS AND CONTAMINANTS WITH A SPRAY ASSEMBLY

Номер: US20150159943A1
Принадлежит:

A method for separating a feed stream in a distillation tower comprising maintaining a controlled freeze zone (CFZ) section in the distillation tower, receiving a freezing zone liquid stream in a spray nozzle assembly in the CFZ section, wherein the spray nozzle assembly comprises a plurality of outer spray nozzles on an outer periphery of the spray nozzle assembly and at least one inner spray nozzle interior to the outer spray nozzles, wherein each outer spray nozzle is configured to spray the freezing zone liquid stream along a central spray axis, and wherein the central spray axis of at least one of the outer spray nozzles is not parallel to a CFZ wall, and spraying the freezing zone liquid stream through the spray nozzle assembly into the CFZ section to keep a temperature and pressure at which the solid and the hydrocarbon-enriched vapor stream form. 1. A method for separating a feed stream in a distillation tower comprising:maintaining a controlled freeze zone section in the distillation tower;receiving a freezing zone liquid stream in a spray nozzle assembly in the controlled freeze zone section, wherein the spray nozzle assembly comprises a plurality of outer spray nozzles on an outer periphery of the spray nozzle assembly and at least one inner spray nozzle interior to the plurality of outer spray nozzles, wherein each outer spray nozzle is configured to spray the freezing zone liquid stream along a central spray axis, and wherein the central spray axis of at least one of the plurality of outer spray nozzles is not parallel to a controlled freeze zone wall; andspraying the freezing zone liquid stream through the spray nozzle assembly into the controlled freeze zone section to keep the controlled freeze zone section at a temperature and pressure at which the solid and the hydrocarbon-enriched vapor stream form.2. The method of claim 1 , wherein an angle of the central spray axis of at least one of the plurality of outer spray nozzles is achieved by angling ...

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11-06-2015 дата публикации

METHOD AND DEVICE FOR SEPARATING A FEED STREAM USING RADIATION DETECTORS

Номер: US20150159944A1
Принадлежит:

The present disclosure provides a method for separating a feed stream in a distillation tower. The method may include forming solids in a controlled freeze zone section of the distillation tower; emitting radiation from a first radiation source in the controlled freeze zone section while the controlled freeze zone section forms no solids; detecting radiation emitted by the first radiation source as a first radiation level; detecting radiation emitted by the first radiation source as a second radiation level after detecting the first radiation level; and determining whether the solids adhered to at least one of on and around a first mechanical component included in the controlled freeze zone section based on the first radiation level and the second radiation level. 1. A method for separating a feed stream in a distillation tower comprising:forming solids in a controlled freeze zone section of the distillation tower;emitting radiation from a first radiation source in the controlled freeze zone section while the controlled freeze zone section forms no solids;detecting radiation emitted by the first radiation source as a first radiation level;detecting radiation emitted by the first radiation source as a second radiation level after detecting the first radiation level; anddetermining whether the solids adhered to at least one of on and around a first mechanical component included in the controlled freeze zone section based on the first radiation level and the second radiation level.2. The method of claim 1 , wherein the first mechanical component comprises one of: (a) a wall of the controlled freeze zone section and (b) a channel of the controlled freeze zone section.3. The method of claim 1 , wherein determining whether the solids adhered comprises:using the first radiation level to generate a baseline radiation level in the controlled freeze zone section and comparing the second radiation level to a radiation deviation range, the radiation deviation range dependent on ...

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11-06-2015 дата публикации

METHOD OF REMOVING SOLIDS BY MODIFYING A LIQUID LEVEL IN A DISTILLATION TOWER

Номер: US20150159945A1
Принадлежит:

The present disclosure provides a method of separating a feed stream in a distillation tower. The method includes maintaining a controlled freeze zone section in a distillation tower; maintaining a melt tray assembly within the controlled freeze zone section that operates at a temperature and pressure at which solid melts; forming solids in a controlled freeze zone section; raising a liquid level of a liquid in the melt tray assembly when the solids accumulate on a mechanical component in the controlled freeze zone section; raising a liquid temperature of the liquid while raising the liquid level; and lowering the liquid level after at least one of (a) a predetermined time period has passed and (b) an alternative temperature of the mechanical component is within an expected temperature range of a baseline temperature of the mechanical component. 1. A method of separating a feed stream in a distillation tower comprising:maintaining a controlled freeze zone section in a distillation tower that operates at a temperature and pressure at which a solid forms;maintaining a melt tray assembly within the controlled freeze zone section that operates at a temperature and pressure at which the solid melts;forming solids in the controlled freeze zone section;raising a liquid level of a liquid in the melt tray assembly when the solids accumulate on a mechanical component in the controlled freeze zone section;raising a liquid temperature of the liquid while raising the liquid level; andlowering the liquid level after at least one of (a) a predetermined time period has passed and (b) an alternative temperature of the mechanical component is within an expected temperature range of a baseline temperature of the mechanical component.2. The method of claim 1 , wherein raising the liquid level comprises determining whether the solids have accumulated on the mechanical component.3. The method of claim 1 , wherein the mechanical component comprises a controlled freeze zone wall.4. The ...

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11-06-2015 дата публикации

METHOD AND SYSTEM OF MODIFYING A LIQUID LEVEL DURING START-UP OPERATIONS

Номер: US20150159946A1
Автор: Valencia Jaime A.
Принадлежит:

The present disclosure provides a method for separating a feed stream in a distillation tower. The method includes operating a controlled freeze zone section in a distillation tower that separates a feed stream at a temperature and pressure at which the feed stream forms a solid in the controlled freeze zone section, wherein the feed stream includes a first contaminant; maintaining a melt tray assembly in the controlled freeze zone section; introducing the feed stream to the controlled freeze zone section; and accumulating a liquid in the melt tray assembly until the liquid is at a predetermined liquid level in the controlled freeze zone section, by: feeding a second contaminant to the controlled freeze zone section; and adding the second contaminant to the melt tray assembly, wherein the liquid comprises the second contaminant. 1. A method for separating a feed stream in a distillation tower , the method comprising:operating a controlled freeze zone section in a distillation tower that separates a feed stream at a temperature and pressure at which the feed stream forms a solid in the controlled freeze zone section, wherein the feed stream includes a first contaminant;maintaining a melt tray assembly in the controlled freeze zone section;introducing the feed stream to the controlled freeze zone section; and feeding a second contaminant to the controlled freeze zone section; and', 'adding the second contaminant to the melt tray assembly, wherein the liquid comprises the second contaminant., 'accumulating a liquid in the melt tray assembly until the liquid is at a predetermined liquid level in the controlled freeze zone section, by2. The method of claim 1 , wherein feeding the second contaminant occurs at least one of before and after introducing the feed stream.3. The method of claim 1 , wherein feeding the second contaminant comprises at least one of directly feeding the second contaminant to the controlled freeze zone section and indirectly feeding the second ...

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11-06-2015 дата публикации

METHOD AND DEVICE FOR SEPARATING HYDROCARBONS AND CONTAMINANTS WITH A HEATING MECHANISM TO DESTABILIZE AND/OR PREVENT ADHESION OF SOLIDS

Номер: US20150159947A1
Принадлежит:

The present disclosure provides a method for separating a feed stream in a distillation tower which includes separating a feed stream in a stripper section into an enriched contaminant bottom liquid stream and a freezing zone vapor stream; contacting the freezing zone vapor stream in the controlled freeze zone section with a freezing zone liquid stream at a temperature and pressure at which a solid and a hydrocarbon-enriched vapor stream form; directly applying heat to a controlled freeze zone wall of the controlled freeze zone section with a heating mechanism coupled to at least one of a controlled freeze zone internal surface of the controlled freeze zone wall and a controlled freeze zone external surface of the controlled freeze zone wall; and at least one of destabilizing and preventing adhesion of the solid to the controlled freeze zone wall with the heating mechanism. 1. A method for separating a feed stream in a distillation tower comprising:introducing a feed stream into one of a stripper section and a controlled freeze zone section of a distillation tower, the feed stream comprising a hydrocarbon and a contaminant;separating the feed stream in the stripper section into an enriched contaminant bottom liquid stream, comprising the contaminant, and a freezing zone vapor stream, comprising the hydrocarbon, at a temperature and pressure at which no solid forms;contacting the freezing zone vapor stream in the controlled freeze zone section with a freezing zone liquid stream, comprising the hydrocarbon, at a temperature and pressure at which a solid, comprising the contaminant, and a hydrocarbon-enriched vapor stream, comprising the hydrocarbon, form;directly applying heat to a controlled freeze zone wall of the controlled freeze zone section with a heating mechanism coupled to at least one of a controlled freeze zone internal surface of the controlled freeze zone wall and a controlled freeze zone external surface of the controlled freeze zone wall; andat least ...

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16-08-2018 дата публикации

FIXED BED RADIAL FLOW REACTOR FOR LIGHT PARAFFIN CONVERSION

Номер: US20180229198A1
Принадлежит:

Systems and methods are provided for conversion of light paraffinic gases to form liquid products in a process performed in a fixed bed radial-flow reactor. The light paraffins can correspond to C paraffins. Examples of liquid products that can be formed include C-Caromatics, such as benzene, toluene, and xylene. The fixed bed radial-flow reactor can allow for improved control over the reaction conditions for paraffin conversion in spite of the fixed bed nature of the reactor. This can allow the process to operate with improved efficiency while reducing or minimizing the complexity of operation relative to non-fixed bed reactor systems. 1. A fixed bed radial flow reactor , comprising:an outer annular volume defined by an interior of a reactor wall and an exterior of a gas-permeable catalyst bed wall, the interior of the reactor wall defining an outer annular radius R1;a central volume defined by the interior of a gas-permeable central column wall and a column cap, the interior of the central column wall defining a column radius R3;an inner annular volume defined by an interior of the catalyst bed wall, an exterior of the central column wall, an inner annular top, and an inner annular bottom, the interior of the catalyst bed wall defining an inner annular radius R2, the inner annular volume comprising a catalyst bed, the inner annular volume being in direct fluid communication with the outer annular volume through the catalyst bed wall, the inner annular volume being in direct fluid communication with the central volume through the central column;{'sub': 'P,e', 'a plurality of catalyst particles in the catalyst bed, the catalyst particles comprising an equivalent particle diameter d; and'}a first reactor opening and a second reactor opening, the first reactor opening being in fluid communication with the outer annular volume, the second reactor opening being in fluid communication with the central volume,{'sub': 'P,e', 'claim-text': {'br': None, 'i': C*d', '≤R', 'R', ...

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05-10-2017 дата публикации

Self-Sourced Reservoir Fluid For Enhanced Oil Recovery

Номер: US20170283688A1
Принадлежит:

Disclosed techniques include a method of obtaining an enhanced oil recovery fluid from a hydrocarbon reservoir, comprising producing a hydrocarbon stream from the hydrocarbon reservoir, separating an associated gas stream from the hydrocarbon stream, and condensing at least a portion of the associated gas stream to obtain an enriched hydrocarbon fluid suitable for injecting into a liquid layer of the hydrocarbon reservoir to enhance recovery of hydrocarbons from the hydrocarbon reservoir. 1. A method of obtaining an enhanced oil recovery fluid from a hydrocarbon reservoir , comprising:producing a hydrocarbon stream from the hydrocarbon reservoir;separating an associated gas stream from the hydrocarbon stream; andcondensing at least a portion of the associated gas stream to obtain an enriched hydrocarbon fluid suitable for injecting into a liquid layer of the hydrocarbon reservoir to enhance recovery of hydrocarbons from the hydrocarbon reservoir.2. The method of claim 1 , further comprising:separating a methane-rich stream from the associated gas stream, wherein the methane-rich stream comprises substantially methane.3. The method of claim 2 , wherein the methane stream is in a gas phase.4. The method of claim 1 , wherein condensing at least a portion of the associated gas stream comprises reducing the temperature of the associated gas stream by between 1° Celsius and 130° Celsius.5. The method of claim 1 , wherein the condensing at least a portion of the associated gas stream comprises reducing the temperature of the associated gas stream to a temperature between +50° Celsius and −70° Celsius.6. The method of claim 1 , wherein separating the associated gas stream from the hydrocarbon stream claim 1 , condensing at least a portion of the associated gas stream claim 1 , or both occur at a facility located proximate to the hydrocarbon reservoir.7. The method of claim 1 , wherein the condensing step and the separating step occur at substantially the same time.8. A ...

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22-10-2015 дата публикации

Method and System For Starting Up A Distillation Tower

Номер: US20150300735A1
Автор: Valencia Jaime A.
Принадлежит:

The present disclosure provides method for clean methane startup of a distillation tower. The method includes maintaining a rectifier section and a lower section in the distillation tower, feeding stream to the lower section, directly feeding methane to at least one of the rectifier section and a rectifier section outlet line of the rectifier section when a contaminant concentration of the contaminant exiting as a vapor in an upper portion of the lower section is outside of a predetermined concentration and introducing the vapor from the lower section to the rectifier section when the contaminant concentration exiting the upper portion of the lower section is within the predetermined concentration. 1. A method for startup of a distillation tower , the method comprising:maintaining a rectifier section in the distillation tower;maintaining a lower section in the distillation tower that is configured to form solids from a contaminant within a stream that enters the distillation tower;feeding the stream to the lower section;directly feeding methane to at least one of the rectifier section and a rectifier section outlet line of the rectifier section when a contaminant concentration of the contaminant exiting as a vapor in an upper portion of the lower section is outside of a predetermined concentration;introducing the vapor from the lower section to the rectifier section when the contaminant concentration exiting the upper portion of the lower section is within the predetermined concentration.2. The method of claim 1 , further comprising:producing hydrocarbons from the distillation tower.3. The method of claim 1 , wherein the predetermined concentration is between 2 and 7 percent.4. The method of claim 1 , wherein the predetermined concentration is between 3 and 6 percent.5. The method of claim 1 , further comprising discontinuing directly feeding methane to the rectifier section when the contaminant concentration exiting the upper portion of the lower section is within ...

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22-12-2016 дата публикации

Purge To Intermediate Pressure In Cryogenic Distillation

Номер: US20160370110A1
Принадлежит:

A system and method for an intermediate pressure vessel to receive a purge in a cryogenic distillation column system. The vessel operates at an intermediate pressure to reduce solidification of the purge. The cryogenic distillation column receives a natural gas having methane and acid gas. The column discharges an overhead stream rich in the methane, and a bottoms stream rich in the acid gas. An overhead system receives the overhead stream, and discharges a vapor methane product, and a cooled liquid for reflux to the cryogenic distillation column. 1. A cryogenic distillation column system comprising: an overhead stream rich in the methane; and', 'a bottoms stream rich in the acid gas;, 'a cryogenic distillation column configured to receive a natural gas comprising methane and acid gas, and to discharge a vapor methane product;', 'a cooled liquid for reflux to the cryogenic distillation column; and, 'an overhead system configured to receive the overhead stream, and to dischargean intermediate pressure vessel configured to receive a purge and operate at an intermediate pressure to reduce solidification of the purge.2. The system of claim 1 , wherein the overhead system is configured to discharge a cooled vapor through a Joule-Thompson (JT) valve to the cryogenic distillation column during startup claim 1 , and wherein the intermediate pressure vessel is configured to receive the purge during startup of the cryogenic distillation column system.3. The system of claim 1 , comprising a purge valve to provide the purge to the intermediate pressure vessel claim 1 , and wherein the intermediate pressure vessel comprises a heater.4. The system of claim 1 , wherein the purge is from the overhead system.5. The system of claim 1 , wherein the cryogenic distillation column comprises two columns claim 1 , and wherein the purge comprises a plurality of purges.6. The system of claim 1 , wherein the cryogenic distillation column has a freezing section claim 1 , and wherein the ...

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28-12-2017 дата публикации

Reducing Refrigeration and Dehydration Load for a Feed Stream Entering a Cryogenic Distillation Process

Номер: US20170370640A1
Принадлежит:

A system for conditioning a sour gas feed stream for a cryogenic distillation tower, comprising a dehydration unit configured to separate the sour gas feed stream into a first stream comprising water and a feed stream, and a sequential cooling assembly coupled to both the dehydration unit and the cryogenic distillation tower, wherein the sequential cooling assembly comprises a first stage configured to separate the feed stream into a partially cooled feed stream and a second stream comprising acid gas, a second stage configured to cool the partially cooled feed stream into a cooled feed stream and a third stream comprising acid gas, and a cooled feed stream header coupled to a cryogenic distillation tower feed inlet, wherein the first stage, the second stage, or both are configured to send at least one of the second and third streams to a bottom section of the cryogenic distillation tower. 1. A system for conditioning a sour gas feed stream for a cryogenic distillation tower , comprising:a dehydration unit configured to separate the sour gas feed stream into a first stream comprising water and a feed stream; and a first stage configured to separate the feed stream into a partially cooled feed stream and a second stream comprising acid gas;', 'a second stage configured to cool the partially cooled feed stream into a cooled feed stream and a third stream comprising acid gas; and', 'a cooled feed stream header coupled to a cryogenic distillation tower feed inlet,', 'wherein the first stage, the second stage, or both are configured to send at least one of the second and third streams to a bottom section of the cryogenic distillation tower., 'a sequential cooling assembly coupled to both the dehydration unit and the cryogenic distillation tower, wherein the sequential cooling assembly comprises2. The system of claim 1 , wherein the first stage comprises a first separator coupled to a first cryogenic distillation tower bottom section inlet.3. The system of claim 1 , ...

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27-11-2018 дата публикации

Method and system for separating a feed stream with a feed stream distribution mechanism

Номер: US10139158B2
Автор: Jaime A. Valencia
Принадлежит: ExxonMobil Upstream Research Co

The present disclosure provides a distillation tower for separating a feed stream. The distillation tower includes a controlled freeze zone section having a controlled freeze zone upper section and a controlled freeze zone lower section below the controlled freeze zone upper section. The controlled freeze zone section includes: (a) a spray assembly in the controlled freeze zone upper section; (b) a melt tray assembly in the controlled freeze zone lower section; (c) a feed stream distribution mechanism between the spray assembly and the melt tray assembly. The feed stream distribution mechanism is constructed and arranged to uniformly distribute the feed stream in the controlled freeze zone section.

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18-06-2019 дата публикации

Self-sourced reservoir fluid for enhanced oil recovery

Номер: US10323495B2
Принадлежит: ExxonMobil Upstream Research Co

Disclosed techniques include a method of obtaining an enhanced oil recovery fluid from a hydrocarbon reservoir, comprising producing a hydrocarbon stream from the hydrocarbon reservoir, separating an associated gas stream from the hydrocarbon stream, and condensing at least a portion of the associated gas stream to obtain an enriched hydrocarbon fluid suitable for injecting into a liquid layer of the hydrocarbon reservoir to enhance recovery of hydrocarbons from the hydrocarbon reservoir.

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30-07-2019 дата публикации

Heating component to reduce solidification in a cryogenic distillation system

Номер: US10365037B2
Принадлежит: ExxonMobil Upstream Research Co

A method and a system for feeding a feed gas including methane (CH 4 ) and carbon dioxide (CO 2 ) to a cryogenic distillation column are provided herein. The method includes flowing a freeze zone CO 2 vapor stream into a freezing section of the column to produce an overhead stream that exits the column. The method includes heating the overhead stream via a heating component to reduce or prevent solidification of the CO 2 in the overhead stream.

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22-02-2022 дата публикации

Treatment plant for hydrocarbon gas having variable contaminant levels

Номер: US11255603B2
Принадлежит: ExxonMobil Upstream Research Co

A method of designing, constructing, and operating a hydrocarbon gas treatment plant is disclosed. A target hydrocarbon production range for a hydrocarbon gas meeting a required product specification is established. A cryogenic distillation column is designed and constructed with a vapor capacity to meet the target hydrocarbon production range. A variable feed refrigeration system is incorporated to cool an inlet feed of the hydrocarbon gas. The variable feed refrigeration system is designed to handle the target hydrocarbon production range and a wide range of contaminant concentrations in the inlet feed. A variable bottoms heating system is incorporated to handle heating duties associated with the wide range of contaminant concentrations in the inlet feed. A variable bottoms pumping system is incorporated to handle liquid flows associated with the wide range of contaminant concentrations in the inlet feed.

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19-04-2022 дата публикации

Hybrid tray for introducing a low CO2 feed stream into a distillation tower

Номер: US11306267B2
Принадлежит: ExxonMobil Upstream Research Co

A method of separating a feed stream in a distillation tower. Vapor is permitted to rise upwardly from a distillation section of the distillation tower. A feed stream is introduced into a controlled freeze zone section of the distillation tower, the controlled freeze zone section being situated above the distillation section. The feed stream is released above a level of a liquid retained by a melt tray assembly in the controlled freeze zone section. Vapor from the distillation section is directed into the liquid retained by the melt tray assembly. A solid is formed from the feed stream in the controlled freeze zone section.

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05-07-2022 дата публикации

Mixing and heat integration of melt tray liquids in a cryogenic distillation tower

Номер: US11378332B2
Принадлежит: ExxonMobil Upstream Research Co

A cryogenic distillation tower for separating a feed stream. The tower includes a distillation section. A controlled freeze zone section is situated above the distillation section and forms a solid from the feed stream. The controlled freeze zone section includes a spray assembly in an upper section and a melt tray assembly in a lower section. The melt tray assembly includes at least one vapor stream riser that directs the vapor from the distillation section into liquid retained by the melt tray assembly, and one or more draw-off openings positioned to permit a portion of the liquid to exit the controlled freeze zone section. The portion of the liquid indirectly exchanges heat with a heating fluid. One or more return inlets return the portion of the liquid to the melt tray assembly after it has been heated in the heat exchanger.

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06-02-2018 дата публикации

Method and system of dehydrating a feed stream processed in a distillation tower

Номер: CA2925404C
Принадлежит: ExxonMobil Upstream Research Co

The present disclosure provides a method of dehydrating a feed stream processed in a distillation tower. The method may include (a) introducing a feed stream comprising a first contaminant stream into a distillation tower; (b) forming a solid from the feed stream in a controlled freeze zone section of the distillation tower; (c) feeding a second contaminant stream into the feed stream outside the distillation tower; and (d) removing water from the feed stream with a second contaminant stream by feeding the second contaminant stream.

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25-08-2020 дата публикации

Self-sourced reservoir fluid for enhanced oil recovery

Номер: CA3024545C
Принадлежит: ExxonMobil Upstream Research Co

Disclosed techniques include a method of obtaining an enhanced oil recovery fluid from a hydrocarbon reservoir, comprising producing a hydrocarbon stream (102) from the hydrocarbon reservoir (104), separating an associated gas stream (118) from the hydrocarbon stream (102), and condensing at least a portion of the associated gas stream (118) to obtain an enriched hydrocarbon fluid (124) suitable for injecting into a liquid layer (108) of the hydrocarbon reservoir (104) to enhance recovery of hydrocarbons from the hydrocarbon reservoir.

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06-02-2018 дата публикации

Method and device for separating hydrocarbons and contaminants with a surface treatment mechanism

Номер: CA2925410C
Принадлежит: ExxonMobil Upstream Research Co

The disclosure includes a method for separating a feed stream in a distillation tower may comprise maintaining a controlled freeze zone section in the distillation tower that forms solids from a feed stream, wherein the controlled freeze zone section includes one or more internally disposed elements and a controlled freeze zone wall having an internal wall surface inside of the distillation tower, modifying at least one of the internally disposed elements, the internal wall surface, or both with a treatment mechanism that includes at least one of (a) removing portions of the internal wall surface and (b) applying a coating surface, introducing the feed stream into the controlled freeze zone section, forming the solids from the feed stream in the controlled freeze zone section, and at least one of preventing and destabilizing adhesion of the solids to the internal wall surface with the treatment mechanism.

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09-02-2021 дата публикации

Fixed bed radial flow reactor for light paraffin conversion

Номер: US10913042B2
Принадлежит: ExxonMobil Research and Engineering Co

Systems and methods are provided for conversion of light paraffinic gases to form liquid products in a process performed in a fixed bed radial-flow reactor. The light paraffins can correspond to C 3+ paraffins. Examples of liquid products that can be formed include C 6 -C 12 aromatics, such as benzene, toluene, and xylene. The fixed bed radial-flow reactor can allow for improved control over the reaction conditions for paraffin conversion in spite of the fixed bed nature of the reactor. This can allow the process to operate with improved efficiency while reducing or minimizing the complexity of operation relative to non-fixed bed reactor systems.

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11-06-2015 дата публикации

Method and system of dehydrating a feed stream processed in a distillation tower

Номер: CA2925404A1
Принадлежит: ExxonMobil Upstream Research Co

The present disclosure provides a method of dehydrating a feed stream processed in a distillation tower. The method may include (a) introducing a feed stream comprising a first contaminant stream into a distillation tower; (b) forming a solid from the feed stream in a controlled freeze zone section of the distillation tower; (c) feeding a second contaminant stream into the feed stream outside the distillation tower; and (d) removing water from the feed stream with a second contaminant stream by feeding the second contaminant stream.

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11-06-2015 дата публикации

Method and device for separating hydrocarbons and contaminants with a spray assembly

Номер: CA2931409A1
Принадлежит: ExxonMobil Upstream Research Co

A method for separating a feed stream in a distillation tower comprising maintaining a controlled freeze zone (CFZ) section in the distillation tower, receiving a freezing zone liquid stream in a spray nozzle assembly in the CFZ section, wherein the spray nozzle assembly comprises a plurality of outer spray nozzles on an outer periphery of the spray nozzle assembly and at least one inner spray nozzle interior to the outer spray nozzles, wherein each outer spray nozzle is configured to spray the freezing zone liquid stream along a central spray axis, and wherein the central spray axis of at least one of the outer spray nozzles is not parallel to a CFZ wall, and spraying the freezing zone liquid stream through the spray nozzle assembly into the CFZ section to keep a temperature and pressure at which the solid and the hydrocarbon-enriched vapor stream form.

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31-07-1992 дата публикации

Method and apparatus for separating carbon dioxide and other acid gases from methane by the use of distillation and a controlled freezing zone

Номер: MY102554A
Принадлежит: Exxon Production Research Co

THE INVENTION RELATES TO METHOD AND APPARATUS FOR SEPARATING CARBON DIOXIDE AND OTHER ACID GASES FROM METHANE BY TREATING THE FEEDSTREAM IN AT LEAST ONE DISTILLATION ZONE AND A CONTROLLED FREEZING ZONE. THE FREEZING ZONE PRODUCES A CARBON DIOXIDE SLUSH WHICH IS MELTED AND FED INTO A DISTILLATION SECTION. THE APPARATUS USED TO PRACTICE THE PROCESS IS PREFERABLY IN A SINGLE VESSEL.@@(FIG. 2)

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04-04-2019 дата публикации

Method and system for starting up a distillation tower.

Номер: MX363831B
Автор: A Valencia Jaime
Принадлежит: Exxonmobil Upstream Res Co

La presente descripción proporciona un método para el arranque con metano limpio de una torre de destilación. El método incluye mantener una sección rectificadora y una sección inferior en la torre de destilación, alimentar la corriente a la sección inferior, alimentar directamente metano a por lo menos una de la sección rectificadora y una línea de salida de sección rectificadora de la sección rectificadora cuando una concentración de contaminante que sale como un vapor en una porción superior de la sección inferior está fuera de una concentración predeterminada e introducir el vapor desde la sección inferior a la sección rectificadora cuando la concentración de contaminante que sale de la porción superior de la sección inferior está dentro de la concentración predeterminada.

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06-04-1992 дата публикации

Bubble cap tray for melting solids and method for using same

Номер: CA2050106A1
Принадлежит: Exxon Production Research Co

An elongated bubble cap tray allows three phases: solid, vapor and liquid, to come in contact at the bottom of a controlled freezing zone and transfer heat and mass amongst themselves. Complete melting of the solid phase may be achieved in this tray, significantly reducing or totally eliminating the need for an external source of energy as well as its associated heat transfer equipment:

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10-01-2019 дата публикации

Self-sourced reservoir fluid for enhanced oil recovery.

Номер: MX2018011641A
Принадлежит: Exxonmobil Upstream Res Co

Las técnicas descritas incluyen un método para obtener un fluido de recuperación de petróleo mejorada a partir de un yacimiento de hidrocarburo, que comprende producir una corriente de hidrocarburo (102) del yacimiento de hidrocarburo (104), separar una corriente de gas asociada (118) de la corriente de hidrocarburo (102) y condensar por lo menos una porción de la corriente de gas asociada (118) para obtener un fluido de hidrocarburo enriquecido (124) adecuado para la inyección en una capa de líquido (108) del yacimiento de hidrocarburo (104) para mejorar la recuperación de hidrocarburos del yacimiento de hidrocarburo.

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02-10-2018 дата публикации

Method and system for separating a feed stream with a feed stream distribution mechanism

Номер: CA2924695C
Автор: Jaime A. Valencia
Принадлежит: ExxonMobil Upstream Research Co

The present disclosure provides a distillation tower for separating a feed stream. The distillation tower includes a controlled freeze zone section having a controlled freeze zone upper section and a controlled freeze zone lower section below the controlled freeze zone upper section. The controlled freeze zone section includes: (a) a spray assembly in the controlled freeze zone upper section; (b) a melt tray assembly in the controlled freeze zone lower section; (c) a feed stream distribution mechanism between the spray assembly and the melt tray assembly. The feed stream distribution mechanism is constructed and arranged to uniformly distribute the feed stream in the controlled freeze zone section.

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17-03-2016 дата публикации

Method and system of maintaining a liquid level in a distillation tower

Номер: WO2015084495A3
Автор: Jaime A. Valencia
Принадлежит: EXXONMOBIL UPSTREAM RESEARCH COMPANY

The present disclosure provides a distillation tower that may include a stripper section constructed and arranged to separate a feed stream at a temperature and pressure at which the feed stream forms no solid; a controlled freeze zone section constructed and arranged to separate the feed stream at a temperature and pressure at which the feed stream forms a solid; a melt tray assembly in the controlled freeze zone section that includes a liquid; an underflow weir in the controlled freeze zone section that alters a flow of the liquid in the melt tray assembly; an overflow weir in the controlled freeze zone section that works with the underflow weir to alter the flow of the liquid in the melt tray assembly and is adjacent to the underflow weir; and a covering element in the controlled freeze zone section that is connected to and extends from the underflow weir.

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19-04-1988 дата публикации

Method and apparatus for separating carbon dioxide and other acid gases from methane by the use of distillation and a controlled freezing zone

Номер: CA1235368A
Принадлежит: Exxon Production Research Co

ABSTRACT The invention relates to method and apparatus for separating carbon dioxide and other acid gases from methane by treating the feedstream in at least one distillation zone and a controlled freezing zone. The freezing zone produces a carbon dioxide slush which is melted and fed into a distillation section. The apparatus used to practice the process is prefer-ably in a single vessel.

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22-02-2018 дата публикации

Treatment plant for hydrocarbon gas having variable contaminant levels

Номер: AU2016327820A1
Принадлежит: ExxonMobil Upstream Research Co

A method of designing, constructing, and operating a hydrocarbon gas treatment plant is disclosed. A target hydrocarbon production range for a hydrocarbon gas meeting a required product specification is established. A cryogenic distillation column is designed and constructed with a vapor capacity to meet the target hydrocarbon production range. A variable feed refrigeration system is incorporated to cool an inlet feed of the hydrocarbon gas. The variable feed refrigeration system is designed to handle the target hydrocarbon production range and a wide range of contaminant concentrations in the inlet feed. A variable bottoms heating system is incorporated to handle heating duties associated with the wide range of contaminant concentrations in the inlet feed. A variable bottoms pumping system is incorporated to handle liquid flows associated with the wide range of contaminant concentrations in the inlet feed.

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29-06-2021 дата публикации

Treatment plant for hydrocarbon gas having variable contaminant levels

Номер: CA2998466C
Принадлежит: ExxonMobil Upstream Research Co

A method of designing, constructing, and operating a hydrocarbon gas treatment plant is disclosed. A target hydrocarbon production range for a hydrocarbon gas meeting a required product specification is established. A cryogenic distillation column is designed and constructed with a vapor capacity to meet the target hydrocarbon production range. A variable feed refrigeration system is incorporated to cool an inlet feed of the hydrocarbon gas. The variable feed refrigeration system is designed to handle the target hydrocarbon production range and a wide range of contaminant concentrations in the inlet feed. A variable bottoms heating system is incorporated to handle heating duties associated with the wide range of contaminant concentrations in the inlet feed. A variable bottoms pumping system is incorporated to handle liquid flows associated with the wide range of contaminant concentrations in the inlet feed.

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21-11-2017 дата публикации

Method and device for separating a feed stream using radiation detectors

Номер: CA2924402C
Принадлежит: ExxonMobil Upstream Research Co

The present disclosure provides a method for separating a feed stream in a distillation tower. The method may include forming solids in a controlled freeze zone section of the distillation tower; emitting radiation from a first radiation source in the controlled freeze zone section while the controlled freeze zone section forms no solids; detecting radiation emitted by the first radiation source as a first radiation level; detecting radiation emitted by the first radiation source as a second radiation level after detecting the first radiation level; and determining whether the solids adhered to at least one of on and around a first mechanical component included in the controlled freeze zone section based on the first radiation level and the second radiation level.

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11-06-2015 дата публикации

Method and system of modifying a liquid level during start-up operations

Номер: WO2015084499A2
Автор: Jaime A. Valencia
Принадлежит: EXXONMOBIL UPSTREAM RESEARCH COMPANY

The present disclosure provides a method for separating a feed stream in a distillation tower. The method includes operating a controlled freeze zone section in a distillation tower that separates a feed stream at a temperature and pressure at which the feed stream forms a solid in the controlled freeze zone section, wherein the feed stream includes a first contaminant; maintaining a melt tray assembly in the controlled freeze zone section; introducing the feed stream to the controlled freeze zone section; and accumulating a liquid in the melt tray assembly until the liquid is at a predetermined liquid level in the controlled freeze zone section, by: feeding a second contaminant to the controlled freeze zone section; and adding the second contaminant to the melt tray assembly, wherein the liquid comprises the second contaminant.

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01-09-2016 дата публикации

Reducing refrigeration and dehydration load for a feed stream entering a cryogenic distillation process

Номер: CA2972796A1
Принадлежит: ExxonMobil Upstream Research Co

A system for conditioning a sour gas feed stream for a cryogenic distillation tower, comprising a dehydration unit configured to separate the sour gas feed stream into a first stream comprising water and a feed stream, and a sequential cooling assembly coupled to both the dehydration unit and the cryogenic distillation tower, wherein the sequential cooling assembly comprises a first stage configured to separate the feed stream into a partially cooled feed stream and a second stream comprising acid gas, a second stage configured to cool the partially cooled feed stream into a cooled feed stream and a third stream comprising acid gas, and a cooled feed stream header coupled to a cryogenic distillation tower feed inlet, wherein the first stage, the second stage, or both are configured to send at least one of the second and third streams to a bottom section of the cryogenic distillation tower.

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24-06-2016 дата публикации

Method and device for separating hydrocarbons and contaminants with a spray assembly.

Номер: MX2016004189A
Принадлежит: Exxonmobil Upstream Res Co

Un método para separar una corriente de alimentación en una torre de destilación que comprende mantener una sección de zona de congelación controlada (CFZ) en la torre de destilación, recibir una corriente de líquido de zona de congelación en un ensamblaje de boquilla de rocío en la sección CFZ, en donde el ensamblaje de boquillas de rocío comprende una pluralidad de boquillas de rocío exteriores en una periferia exterior del ensamblaje de boquilla de rocío y por lo menos una boquilla de rocío interior interna a las boquillas de rocío exteriores, en donde la boquilla de rocío exterior se configura para rociar la corriente de líquido de zona de congelación a lo largo de un eje de rocío central, y en donde el eje de rocío central de por lo menos una de las boquillas de rocío exteriores no está paralelo a la pared CFZ, y rociar la corriente de líquido de zona de congelación a través del ensamblaje de boquilla de rocío en la sección CFZ para mantener una temperatura y presión en la cual se forman el sólido y la corriente de vapor enriquecida en hidrocarburo.

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09-11-2017 дата публикации

Purge to intermediate pressure in cryogenic distillation

Номер: AU2016281501A1
Принадлежит: ExxonMobil Upstream Research Co

A system and method for an intermediate pressure vessel to receive a purge in a cryogenic distillation column system. The vessel operates at an intermediate pressure to reduce solidification of the purge. The cryogenic distillation column receives a natural gas having methane and acid gas. The column discharges an overhead stream rich in the methane, and a bottoms stream rich in the acid gas. An overhead system receives the overhead stream, and discharges a vapor methane product, and a cooled liquid for reflux to the cryogenic distillation column.

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25-05-2017 дата публикации

Method and system of modifying a liquid level during start-up operations

Номер: AU2014357668B2
Автор: Jaime A. Valencia
Принадлежит: ExxonMobil Upstream Research Co

The present disclosure provides a method for separating a feed stream in a distillation tower. The method includes operating a controlled freeze zone section in a distillation tower that separates a feed stream at a temperature and pressure at which the feed stream forms a solid in the controlled freeze zone section, wherein the feed stream includes a first contaminant; maintaining a melt tray assembly in the controlled freeze zone section; introducing the feed stream to the controlled freeze zone section; and accumulating a liquid in the melt tray assembly until the liquid is at a predetermined liquid level in the controlled freeze zone section, by: feeding a second contaminant to the controlled freeze zone section; and adding the second contaminant to the melt tray assembly, wherein the liquid comprises the second contaminant.

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27-02-2018 дата публикации

Method and device for separating hydrocarbons and contaminants with a heating mechanism to destabilize and/or prevent adhesion of solids

Номер: CA2925955C
Принадлежит: ExxonMobil Upstream Research Co

The present disclosure provides a method for separating a feed stream in a distillation tower which includes separating a feed stream in a stripper section into an enriched contaminant bottom liquid stream and a freezing zone vapor stream; contacting the freezing zone vapor stream in the controlled freeze zone section with a freezing zone liquid stream at a temperature and pressure at which a solid and a hydrocarbon-enriched vapor stream form; directly applying heat to a controlled freeze zone wall of the controlled freeze zone section with a heating mechanism coupled to at least one of a controlled freeze zone internal surface of the controlled freeze zone wall and a controlled freeze zone external surface of the controlled freeze zone wall; and at least one of destabilizing and preventing adhesion of the solid to the controlled freeze zone wall with the heating mechanism.

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21-07-2020 дата публикации

self-produced reservoir fluid for improved oil recovery

Номер: BR112018068799B1
Принадлежит: EXXONMOBIL UPSTREAM RESEARCH COMPANY

São reveladas técnicas que incluem um método de obtenção de um fluido de recuperação de óleo melhorado a partir de um reservatório de hidrocarboneto que compreende produzir uma corrente de hidrocarboneto a partir do reservatório de hidrocarboneto, separar uma corrente de gás associada da corrente de hidrocarboneto, e condensar pelo menos uma porção da corrente de gás associada para obter um fluido de hidrocarboneto enriquecido adequado para injeção em uma camada de líquido do reservatório de hidrocarboneto para melhorar a recuperação de hidrocarbonetos a partir do reservatório de hidrocarboneto. Techniques are disclosed which include a method of obtaining an improved oil recovery fluid from a hydrocarbon reservoir which comprises producing a hydrocarbon stream from the hydrocarbon reservoir, separating an associated gas stream from the hydrocarbon stream, and condensing at least a portion of the associated gas stream to obtain an enriched hydrocarbon fluid suitable for injection into a liquid layer of the hydrocarbon reservoir to improve the recovery of hydrocarbons from the hydrocarbon reservoir.

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23-09-2020 дата публикации

Method and device for separating hydrocarbons and contaminants with a heating mechanism to destabilize and/or prevent adhesion of solids

Номер: MY177768A
Принадлежит: Exxonmobil Upstream Res Co

The present disclosure provides a method for separating a feed stream (10) in a distillation tower (104; 204) which includes separating a feed stream (10) in a stripper section into an enriched contaminant bottom liquid stream and a freezing zone vapor stream; contacting the freezing zone vapor stream in the controlled freeze zone section with a freezing zone liquid stream at a temperature and pressure at which a solid and a hydrocarbon-enriched vapor stream form; directly applying heat to a controlled freeze zone wall (46) of the controlled freeze zone section with a heating mechanism (36; 136) coupled to at least one of a controlled freeze zone internal surface (31) of the controlled freeze zone wall (46) and a controlled freeze zone external surface (47) of the controlled freeze zone wall (46); and at least one of destabilizing and preventing adhesion of the solid to the controlled freeze zone wall (46) with the heating mechanism (36; 136).

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23-09-2020 дата публикации

Method and system for separating fluids in a distillation tower

Номер: MY177735A
Принадлежит: Exxonmobil Upstream Res Co

A method and system for separating fluids in a distillation tower (104, 204). The method may include feeding a stream to the distillation tower, wherein the stream includes carbon dioxide, reducing a carbon dioxide concentration of the stream received by the rectifier section (110) by feeding a first cryogenic fluid to the controlled freeze zone section (108) and accumulating rectifier section stream in at least one of a holding vessel (126) and a sump of the rectifier section (110), and terminating reducing the carbon dioxide concentration when the carbon dioxide concentration of the stream travelling from the controlled freeze zone section (108) to the rectifier section (110) is less than or equal to a maximum carbon dioxide concentration. The first cryogenic fluid may comprise a substantially carbon� dioxide-free fluid.

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