Method and apparatus for temperature calibration in microwave assisted chemistry
Опубликовано: 05-04-1999
Автор(ы): Edward Earl King, Todd Mark Hochrad, William Edward Jennings
Принадлежит: CEM Corp
Реферат: A method and apparatus are disclosed for externally and noninvasively determining the temperatures of chemical reactions inside a plurality of separate closed vessels that are made of materials that substantially transparent to microwave radiation but that are poor conductors of heat. The method comprises exposing a plurality of substantially microwave-transparent of vessels containing chemical reagents therein to microwave radiation, concurrently measuring the temperature of the reagents inside a first vessel using a first temperature sensor inside the first vessel and while measuring the temperature of the exterior of the first vessel using a second temperature sensor positioned externally to the first vessel, and immediately thereafter successively measuring the temperature of the exterior of the remainder of the vessels using the second sensor.
Method of and apparatus for extracting chemicals
Номер патента: WO2009068977A1. Автор: Ewa Cukrowska. Владелец: UNIVERSITY OF WITWATERSRAND, JOHANNESBURG. Дата публикации: 2009-06-04.